CN104906147A - Method for extracting terpene powder from Antrodia camphorata - Google Patents
Method for extracting terpene powder from Antrodia camphorata Download PDFInfo
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- CN104906147A CN104906147A CN201510238303.1A CN201510238303A CN104906147A CN 104906147 A CN104906147 A CN 104906147A CN 201510238303 A CN201510238303 A CN 201510238303A CN 104906147 A CN104906147 A CN 104906147A
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Abstract
A method for extracting terpene powder from Antrodia camphorate comprises the following steps: grinding Antrodia camphorate by using a wood block to form powder with the granularity of 100-200 meshes, blending the Antrodia camphorate powder with alcohol according to a part ratio of 1:15-25, pouring the Antrodia camphorate powder along the center of an alcohol container little by little for 2min or less in the blending process, closing the alcohol container, preserving in a shady place, opening the closed container, and airing after complete evaporation of the alcohol to form the terpene powder, wherein the concentration of the alcohol is 50-70%. The method for extracting the terpene powder from Antrodia camphorate reserves most of terpene components in the Antrodia camphorate by adopting specific alcohol degree and specific preservation conditions.
Description
Technical field
The present invention relates to a kind of method extracting terpenoid powder from Antrodia Camphorata, belong to Antrodia Camphorata material abstraction technique field.
Background technology
Antrodia Camphorata has higher medical value, and triterpenoid compound is that current Antrodia camphorata sporophore finds maximum terpenoid chemical compositions, is generally considered to the main source of bitterness composition in Antrodia camphorata extract.Wherein nearly more than 10 kind of new discovery triterpenes by Antrodia camphorata exclusive, experiment confirms: these triterpenoid compound can suppress the propagation of hepatoma carcinoma cell, poisoning mouse leukemia (P-388 murine leukemia) cytoactive, anti-parasympathetic nervous effect, serotonin antagonist active, activate the functions such as nerve growth ability; Play prior anti-tumor activity than polysaccharides and regulate role.Hyperpietic is often because hypertension, and cause rupture of blood vessel in brain and apoplexy, triterpenoid compound effectively can suppress Angiotensin Converting Enzyme(ACE) activity, and then to reduce blood pressure.
From foregoing, the terpenoid in Antrodia Camphorata has boundless market application background, so the present invention devises a kind of method extracting terpenoid powder from Antrodia Camphorata.
Summary of the invention
The present invention proposes a kind of method extracting terpenoid powder from Antrodia Camphorata, adopt the mode of grinding and alcoholic extract, the extraction efficiency of terpenoid is greatly improved.
Object of the present invention carrys out specific implementation by the following technical programs:
A kind of method extracting terpenoid powder from Antrodia Camphorata, first the grinding of Antrodia Camphorata wooden unit being formed granularity is 100-200 object powder, then described Antrodia Camphorata powder and ethanol are allocated according to the number that proportioning is 1:15-25, in the process of allotment, topple over piecemeal along the center of alcohol container for described Antrodia Camphorata powder, this process duration is no more than 2 minutes, then alcohol container closed and keep in Dark Place, the concentration of described ethanol is between 50-70%, then hermetic container is opened, Deng vaporized alcohol completely after, dry and form terpenoid powder.
Preferably, described Antrodia Camphorata powder and ethanol are allocated according to the number that proportioning is 1:20.
Preferred further, described alcohol concentration is 60%.
A kind of method extracting terpenoid powder from Antrodia Camphorata of the present invention, adopts alcoholic strength and the preservation condition of particular requirement, the ter penoids major part of Antrodia Camphorata can be remained.
Detailed description of the invention
First it may be noted that embodiments of the invention only disclose preferred embodiment several, not should be appreciated that paired restriction of the invention process, protection scope of the present invention is still as the criterion with the content disclosed in claims.
embodiment one
From Antrodia Camphorata, extract a method for terpenoid powder, first the grinding of Antrodia Camphorata wooden unit being formed granularity is 100 object powder, then described Antrodia Camphorata powder and ethanol is allocated according to the number that proportioning is 1:15.
In the process of allotment, topple over piecemeal along the center of alcohol container for described Antrodia Camphorata powder, this process duration 1 minute.
Then closed by alcohol container and keep in Dark Place, the concentration of described ethanol is 50, then opens hermetic container, after waiting vaporized alcohol completely, dries and forms terpenoid powder.
embodiment two
From Antrodia Camphorata, extract a method for terpenoid powder, first the grinding of Antrodia Camphorata wooden unit being formed granularity is 200 object powder, then described Antrodia Camphorata powder and ethanol is allocated according to the number that proportioning is 1:125.
In the process of allotment, topple over piecemeal along the center of alcohol container for described Antrodia Camphorata powder, this process duration 1 minute.
Then closed by alcohol container and keep in Dark Place, the concentration of described ethanol is 70, then opens hermetic container, after waiting vaporized alcohol completely, dries and forms terpenoid powder.
embodiment three
From Antrodia Camphorata, extract a method for terpenoid powder, first the grinding of Antrodia Camphorata wooden unit being formed granularity is 100 object powder, then described Antrodia Camphorata powder and ethanol is allocated according to the number that proportioning is 1:25.
In the process of allotment, topple over piecemeal along the center of alcohol container for described Antrodia Camphorata powder, this process duration 1 minute.
Then closed by alcohol container and keep in Dark Place, the concentration of described ethanol is 60, then opens hermetic container, after waiting vaporized alcohol completely, dries and forms terpenoid powder.
embodiment four
From Antrodia Camphorata, extract a method for terpenoid powder, first the grinding of Antrodia Camphorata wooden unit being formed granularity is 100 object powder, then described Antrodia Camphorata powder and ethanol is allocated according to the number that proportioning is 1:21.
In the process of allotment, topple over piecemeal along the center of alcohol container for described Antrodia Camphorata powder, this process duration 1.5 minutes.
Then closed by alcohol container and keep in Dark Place, the concentration of described ethanol is 55, then opens hermetic container, after waiting vaporized alcohol completely, dries and forms terpenoid powder.
embodiment five
From Antrodia Camphorata, extract a method for terpenoid powder, first the grinding of Antrodia Camphorata wooden unit being formed granularity is 150 object powder, then described Antrodia Camphorata powder and ethanol is allocated according to the number that proportioning is 1:25.
In the process of allotment, topple over piecemeal along the center of alcohol container for described Antrodia Camphorata powder, this process duration 1 minute.
Then closed by alcohol container and keep in Dark Place, the concentration of described ethanol is 59, then opens hermetic container, after waiting vaporized alcohol completely, dries and forms terpenoid powder.
embodiment six
From Antrodia Camphorata, extract a method for terpenoid powder, first the grinding of Antrodia Camphorata wooden unit being formed granularity is 200 object powder, then described Antrodia Camphorata powder and ethanol is allocated according to the number that proportioning is 1:21.
In the process of allotment, topple over piecemeal along the center of alcohol container for described Antrodia Camphorata powder, this process duration 1 minute.
Then closed by alcohol container and keep in Dark Place, the concentration of described ethanol is 51, then opens hermetic container, after waiting vaporized alcohol completely, dries and forms terpenoid powder.
embodiment seven
From Antrodia Camphorata, extract a method for terpenoid powder, first the grinding of Antrodia Camphorata wooden unit being formed granularity is 200 object powder, then described Antrodia Camphorata powder and ethanol is allocated according to the number that proportioning is 1:15.
In the process of allotment, topple over piecemeal along the center of alcohol container for described Antrodia Camphorata powder, this process duration 1 minute.
Then closed by alcohol container and keep in Dark Place, the concentration of described ethanol is 53, then opens hermetic container, after waiting vaporized alcohol completely, dries and forms terpenoid powder.
embodiment eight
From Antrodia Camphorata, extract a method for terpenoid powder, first the grinding of Antrodia Camphorata wooden unit being formed granularity is 180 object powder, then described Antrodia Camphorata powder and ethanol is allocated according to the number that proportioning is 1:25.
In the process of allotment, topple over piecemeal along the center of alcohol container for described Antrodia Camphorata powder, this process duration 1 minute.
Then closed by alcohol container and keep in Dark Place, the concentration of described ethanol is 58, then opens hermetic container, after waiting vaporized alcohol completely, dries and forms terpenoid powder.
embodiment nine
From Antrodia Camphorata, extract a method for terpenoid powder, first the grinding of Antrodia Camphorata wooden unit being formed granularity is 190 object powder, then described Antrodia Camphorata powder and ethanol is allocated according to the number that proportioning is 1:25.
In the process of allotment, topple over piecemeal along the center of alcohol container for described Antrodia Camphorata powder, this process duration 1 minute.
Then closed by alcohol container and keep in Dark Place, the concentration of described ethanol is 56, then opens hermetic container, after waiting vaporized alcohol completely, dries and forms terpenoid powder.
Finally being also pointed out that any entity or individual use or implement technical scheme of the present invention is all to infringement of the present invention, and any entity or individual, without the permission of the applicant, can not implement this patent separately.And any entity or individual are subject to inspiration of the present invention or implement through simple adjustment, also should think the protection domain of this patent.
Claims (3)
1. one kind extracts the method for terpenoid powder from Antrodia Camphorata, first the grinding of Antrodia Camphorata wooden unit being formed granularity is 100-200 object powder, then described Antrodia Camphorata powder and ethanol are allocated according to the number that proportioning is 1:15-25, in the process of allotment, topple over piecemeal along the center of alcohol container for described Antrodia Camphorata powder, this process duration is no more than 2 minutes, then alcohol container closed and keep in Dark Place, the concentration of described ethanol is between 50-70%, then hermetic container is opened, Deng vaporized alcohol completely after, dry and form terpenoid powder.
2. a kind of method extracting terpenoid powder from Antrodia Camphorata as claimed in claim 1, it is characterized in that, described Antrodia Camphorata powder and ethanol are allocated according to the number that proportioning is 1:20.
3. a kind of method extracting terpenoid powder from Antrodia Camphorata as claimed in claim 1, it is characterized in that, described alcohol concentration is 60%.
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Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20080119565A1 (en) * | 2004-10-19 | 2008-05-22 | Golden Biotechnology Corporation | Novel compounds from antrodia camphorata |
CN103159732A (en) * | 2011-12-15 | 2013-06-19 | 台湾利得生物科技股份有限公司 | Polyacetylene compound, extract containing same and application of polyacetylene compound |
-
2015
- 2015-05-12 CN CN201510238303.1A patent/CN104906147A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20080119565A1 (en) * | 2004-10-19 | 2008-05-22 | Golden Biotechnology Corporation | Novel compounds from antrodia camphorata |
TWI335314B (en) * | 2007-10-19 | 2011-01-01 | Golden Biotechnology Corp | |
CN103159732A (en) * | 2011-12-15 | 2013-06-19 | 台湾利得生物科技股份有限公司 | Polyacetylene compound, extract containing same and application of polyacetylene compound |
Non-Patent Citations (3)
Title |
---|
陆震鸣: "樟芝深层液态发酵及其三萜类化合物的研究", 《万方数据》 * |
陆震鸣: "樟芝菌粉抗氧化和预防大鼠急性酒精性肝损伤的研究", 《万方数据》 * |
陆震鸣等: "樟芝菌粉三萜类化合物含量的测定", 《中成药》 * |
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Application publication date: 20150916 |