CN103710241A - Preparation method of cordyceps militaris compound wine - Google Patents
Preparation method of cordyceps militaris compound wine Download PDFInfo
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- CN103710241A CN103710241A CN201310733646.6A CN201310733646A CN103710241A CN 103710241 A CN103710241 A CN 103710241A CN 201310733646 A CN201310733646 A CN 201310733646A CN 103710241 A CN103710241 A CN 103710241A
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Abstract
The invention provides a preparation method of cordyceps militaris compound wine. The preparation method comprises the following steps: selecting and drying high-quality cordyceps militaris fruit bodies and obtaining cordyceps militaris superfine powder by adopting the low temperature superfine grinding technology; fully and uniformly mixing the cordyceps militaris superfine powder with high-quality spirit with high alcohol content, then putting the mixture in a ceramic wine jar to be soaked, controlling the room temperature of the ceramic wine jar to be 15-20 DEG C, stirring the mixture periodically, filtering the solution and taking the supernatant, thus obtaining the cordyceps militaris wine base; blending the cordyceps militaris wine base with a blending liquid to prepare the drink wine with an appropriate alcohol content. The preparation method is simple in steps, has low equipment requirements and is controllable in quality and low in cost and the active ingredients in the body of the cordyceps militaris compound wine prepared by the method are abundant and measurable.
Description
Technical field
The present invention relates to health promoting wine preparing technical field, be specifically related to a kind of preparation method of take the Cordyceps militaris (L.) Link. assembled alcoholic drinks that Cordyceps militaris (L.) Link. is main raw material.
Background technology
Cordyceps militaris (L.) Link. (Cordyceps militaris), has another name called Cordyceps militaris, is under the jurisdiction of Ascomycotina, Clavicipitaceae, the Cordyceps of mycota.Cordyceps militaris (L.) Link. is a kind of fungi that silkworm chrysalis is host of take, belong to together with Cordyceps sinensis is equal, chemical composition is basically identical, its antineoplastic component cordycepin content is higher than Cordyceps sinensis, the new resource food of Qie Shi Ministry of Health approval, have antitumor, antiviral, antibacterial, anti-inflammatory, delay senility, improve the multiple efficacies such as immunizing power, applicable crowd is extensive.At present existingly take Cordyceps militaris (L.) Link. and carry out the brewed health promoting wine forming as main raw material.
The Chinese invention patent that is CN100352907C as notification number discloses a kind of ferment cordyceps sinensis, health lycium chinense and preparation method thereof, it uses the premenstrual ferment of matrimony vine, rear ferment to be refined into Lycium chinense wine, then refining through high-grade wine lixiviate with Cordyceps mycelium, be mixed in proportion, with the bent wine of a small amount of scent type, first two wine is blent into the series wine of different components different taste, the wherein content >=0.2mg/L of cordycepin.And according to a large amount of relevant reports, the contained cordycepin amount of mycelium is low, after soaking, in the health promoting wine of preparation, contained cordycepin is lower, so the cordycepin content in this wine is only in the level of 0.2mg/L.
Notification number is that the Chinese invention patent of CN101341985B discloses a kind of Chinese caterpillar fungus health wine and preparation method thereof, and in this health promoting wine, cordycepin component content is that 20-100mg/L, Chinese caterpillar fungus adenosine component content are 20-150mg/L.But the preparation method of this health promoting wine is the extracting solution that first obtains each component, then according to predefined each component content, the extracting solution of each component and white spirit mixed are obtained, and the extracting solution preparation process of each component is complicated: first by raw material drying to water content below 13%, pulverize, excessively after 60-80 mesh sieve, obtain powder raw material, then add and be equivalent to powder raw material volume 8-20 pure water formation mixed solution doubly, by mixed solution multiple tank Continuous Countercurrent Extraction 4-6 hour under normal pressure, 75-95 ℃ condition, collect and obtain extracting solution.The leaching process of this extracting solution is complicated, and high to equipment requirements, energy dissipation is serious, and raw material continuous countercurrent under 75-95 ℃ of high temperature condition like this, and the destruction of its effective constituent is serious, and can each component concentration that extract desired concn remain suspicious.
Summary of the invention
Technical problem to be solved by this invention is for above the deficiencies in the prior art, and a kind of preparation method of Cordyceps militaris (L.) Link. assembled alcoholic drinks is provided, and this preparation method's step is simple, low for equipment requirements, quality controllable, and cost is low.The Cordyceps militaris (L.) Link. assembled alcoholic drinks preparing by the method, abundant can the survey of activeconstituents in wine body.
The technical solution adopted in the present invention is:
A preparation method for Cordyceps militaris (L.) Link. assembled alcoholic drinks, the method comprises the following steps:
(1) preparation of raw material is processed: choose high-quality Cordyccps-militaris-(L.)-link. Sporophore and dry, adopt superfine comminution at low temperature technology to obtain Cordyceps militaris (L.) Link. super-fine powder;
(2) acquisition of the former wine of Cordyceps militaris (L.) Link.: Cordyceps militaris (L.) Link. super-fine powder and high-quality high spirit are fully mixed, be then placed in ceramic wine jar and soak, ceramic wine jar place room temperature is controlled at 15-20 ℃, regularly stirs, and crosses leaching supernatant, obtains the former wine of Cordyceps militaris (L.) Link.;
(3) allotment of cordyceps militaris liquor: the former wine of Cordyceps militaris (L.) Link. is blent to the alcoholic drink that is deployed into suitable alcoholic strength with blending liquid.
In described step (1), high-quality Cordyccps-militaris-(L.)-link. Sporophore refers to a golden yellow megaspore Cordyccps-militaris-(L.)-link. Sporophore.
In described step (1), oven dry is preferably high-quality Cordyccps-militaris-(L.)-link. Sporophore is evenly spread out, and is placed under 37 ℃ of hot air circulation and dries, and its moisture content is controlled at below 10%.
Superfine comminution at low temperature technological selection carries out micronizing for high-quality Cordyccps-militaris-(L.)-link. Sporophore is placed in to micronized pulverization machine in described step (1), pulverizes simultaneously and in whole process, uses the water of 4-10 ℃ as micronized pulverization machine internal coolant.
To be preferably alcoholic strength be the aromatic Chinese spirit of 60-65 ° to high-quality high spirit in described step (2).
In described step (2), the blending ratio of Cordyceps militaris (L.) Link. super-fine powder and high-quality high spirit is preferably 8g: 100ml or 16g: 100ml.
Cordyceps militaris (L.) Link. super-fine powder and high-quality high spirit are placed on the time of soaking in ceramic wine jar and are preferably 9 days after mixing in described step (2).
In described step (2), regularly stir and be preferably stirring in every 1-2 days once.
Blending liquid is preferably high-quality low alcohol white spirit and brewing water in described step (3), and to be wherein preferably alcoholic strength be the aromatic Chinese spirit of 14-55 ° to high-quality low alcohol white spirit.
In described step (3), suitably alcoholic strength refers to that alcoholic strength is 30-55 °.
Compared with prior art, the present invention has following remarkable advantage and beneficial effect:
(1) the present invention be take Cordyccps-militaris-(L.)-link. Sporophore as main raw material, after oven dry, micronizing are processed, mixes according to a certain ratio with high quality liquor, through immersion, lixiviate, filtration, allotment, filling mode, is prepared.By to the research of technological process and control, particularly by controlling Cordyccps-militaris-(L.)-link. Sporophore and the blending ratio of white wine and the time of lixiviate, make to prepare that in the former wine of Cordyceps militaris (L.) Link. of gained, cordycepin content reaches as high as 670mg/L, adenosine content reaches as high as 260mg/L, so the bioactive substance content such as cordycepin, adenosine is high in the Cordyceps militaris (L.) Link. assembled alcoholic drinks being deployed into the former wine of this Cordyceps militaris (L.) Link., substances content is stablized controlled, quality product is good, and nourishing function is strong.
(2) the present invention uses supper micron mill, carries out superfine comminution at low temperature, to abolish the hard cell walls of Cordyccps-militaris-(L.)-link. Sporophore, is conducive to the stripping of content, improves the extraction yield of active principle in Cordyceps militaris (L.) Link..
(3) whole process of the present invention is carried out handle control to temperature, when wherein Cordyccps-militaris-(L.)-link. Sporophore is dried, temperature is controlled at 37 ℃, during micronizing, temperature is controlled at 4-10 ℃, during lixiviate, temperature is controlled 15-20 ℃, by temperature Real-Time Monitoring and control to these processes, effectively guarantee the activity of extract in Cordyceps militaris (L.) Link., guaranteed its pharmaceutical use.
(4) the whole preparation process of the present invention is simple to operate, low for equipment requirements, workable, is applicable to large-scale industrial production, is easy to promote.
(5) the Cordyceps militaris (L.) Link. assembled alcoholic drinks of preparing by the method, abundant can the survey of activeconstituents in wine body, quality product is controlled, and material damages few, and cost is low, and product is easy to preserve; Wine body is not containing any synthetic colour and synthetic non-natural compound, and pure taste, has higher medicinal and nutritive value.
Accompanying drawing explanation
Shown in Fig. 1 be in Cordyceps militaris (L.) Link. assembled alcoholic drinks of the present invention cordycepin at the content of different soak time sections;
Shown in Fig. 2 be in Cordyceps militaris (L.) Link. assembled alcoholic drinks of the present invention adenosine at the content of different soak time sections.
Embodiment
Below in conjunction with embodiment, the present invention is further described in detail.Be noted that following illustrating is all exemplary, be intended to the invention provides further instruction.Except as otherwise noted, all Science and Technology terms that the present invention uses have the identical meanings of conventionally understanding with the technical field of the invention personnel.
Embodiment 1: the preparation of raw material
1, dry
Choose a golden yellow megaspore Cordyccps-militaris-(L.)-link. Sporophore as raw material, be placed in the Stainless Steel Disc that is lined with gauze, evenly spread out, 37 ℃ of hot air circulation are dried, and its moisture content is controlled at below 10%.
2, pulverize
Take the Cordyccps-militaris-(L.)-link. Sporophore that 200g is dried at every turn, put into micronized pulverization machine and carry out micronizing, simultaneously broken whole process with the water of 4～10 ℃ as micronized pulverization machine internal coolant, guarantee release and bioactive the stablizing of effective constituent, micronizing is 5-15min, through practice, grope 6-10min and be advisable, 6min is for the most suitable.
Embodiment 2: the acquisition of the former wine of Cordyceps militaris (L.) Link.
1, mix and soak
By Cordyceps militaris (L.) Link. super-fine powder and high-quality high spirit, (selecting alcoholic strength is here the aromatic Chinese spirit of 65 degree, be purchased from Hengshui Gan Ling spring Wine Co., Ltd) respectively in 2g: the ratio of 100ml, 4g: 100ml, 8g: 100ml, 16g: 100ml fully mixes, be placed on respectively in ceramic wine jar and soak, ceramic wine jar place room temperature is controlled at 15-20 ℃.
2, lixiviate
Within every two days, stir once, the effective constituent in lixiviate Cordyceps militaris (L.) Link., after stirring 3 times standing 3 days, soak time was 9 days altogether.Sampling respectively in the 1st, 3,4,5,6,7,8,9 days after immersion, detect cordycepin and adenosine content in soak solution by HPLC, and result as depicted in figs. 1 and 2.By Fig. 1 and the comprehensive comparison of Fig. 2 and analysis, drawn, after soaking 9 days in vat liquor cordycepin and adenosine content the highest.
The blending ratio that is Cordyceps militaris (L.) Link. super-fine powder and white wine when Cordyccps-militaris-(L.)-link. Sporophore dry powder is 16g: during 100ml, by preparation method of the present invention, when soak time is 9 days, in wine body, the content of adenosine can reach 260 μ g/ml, i.e. 260mg/L.And take adenosine content in Cordyccps-militaris-(L.)-link. Sporophore dry powder, be 2/1000ths, the theoretical maximum of adenosine content is 320mg/L, and thus, it is few that this preparation method's material damages, and in raw material, utilization rate of active components reaches 81.25%, and utilization ratio is high.
3, filter
Draw the supernatant liquor of vat liquor, with filter plant, further filter out the solids of suspension, obtain the former wine of Cordyceps militaris (L.) Link..
Embodiment 3: the allotment of cordyceps militaris liquor
1, allotment
By Cordyceps militaris (L.) Link. for former wine low high quality liquor (selecting alcoholic strength is here the aromatic Chinese spirit of 55 degree, is purchased from Hengshui Gan Ling spring Wine Co., Ltd) and brewing water blend be deployed into alcoholic strength be 30-55 degree (concrete alcoholic strength content according to client, need or during as concrete nourishing function suitable alcohol drink content and determine) alcoholic drink.
2, filling
By deployed alcoholic drink quantitative separating, sealing.
3, detect
The Cordyceps militaris (L.) Link. assembled alcoholic drinks obtaining is carried out to Oranoleptic indicator's detection and physical and chemical index detection, and result respectively as shown in Table 1 and Table 2.
After testing, its cordycepin of Cordyceps militaris (L.) Link. assembled alcoholic drinks that this preparation method obtains and adenosine content are all higher than general commercially available Chinese caterpillar fungus health wine, so the Cordyceps militaris (L.) Link. assembled alcoholic drinks that this preparation method obtains has good using value aspect health promoting wine.
4, preserve
Lucifuge, dry, room temperature preservation.
The above, be only the preferred embodiments of the present invention, should be understood that; for those skilled in the art; not departing under the prerequisite of core technology of the present invention, can also make improvements and modifications, these improvements and modifications also should belong to scope of patent protection of the present invention.The implication suitable with claims of the present invention and any change in scope, all should think to be included in the scope of claims.
Table 1: Oranoleptic indicator
| Project | Index |
| Outward appearance | Be golden yellow or brown color, clarification, has allowed a small amount of precipitation after being long placed in |
| Fragrance | There is the peculiar smell of Cordyceps militaris (L.) Link. and aroma, free from extraneous odour |
| Flavour | There is the distinctive flavour of this product |
| Style | There is the typical style of this product |
Table 2: physical and chemical index
Claims (10)
1. a preparation method for Cordyceps militaris (L.) Link. assembled alcoholic drinks, is characterized in that comprising the following steps:
(1) preparation of raw material is processed: choose high-quality Cordyccps-militaris-(L.)-link. Sporophore and dry, adopt superfine comminution at low temperature technology to obtain Cordyceps militaris (L.) Link. super-fine powder;
(2) acquisition of the former wine of Cordyceps militaris (L.) Link.: Cordyceps militaris (L.) Link. super-fine powder and high-quality high spirit are fully mixed, be then placed in ceramic wine jar and soak, ceramic wine jar place room temperature is controlled at 15-20 ℃, regularly stirs, and crosses leaching supernatant, obtains the former wine of Cordyceps militaris (L.) Link.;
(3) allotment of cordyceps militaris liquor: the former wine of Cordyceps militaris (L.) Link. is blent to the alcoholic drink that is deployed into suitable alcoholic strength with blending liquid.
2. the preparation method of a kind of Cordyceps militaris (L.) Link. assembled alcoholic drinks according to claim 1, is characterized in that: the middle high-quality Cordyccps-militaris-(L.)-link. Sporophore of described step (1) refers to golden yellow megaspore head, is not stained with the Cordyccps-militaris-(L.)-link. Sporophore of substratum.
3. the preparation method of a kind of Cordyceps militaris (L.) Link. assembled alcoholic drinks according to claim 1, it is characterized in that: in described step (1), oven dry refers to high-quality Cordyccps-militaris-(L.)-link. Sporophore is evenly spread out, be placed under 37 ℃ of hot air circulation and dry, its moisture content is controlled at below 10%.
4. the preparation method of a kind of Cordyceps militaris (L.) Link. assembled alcoholic drinks according to claim 1, it is characterized in that: superfine comminution at low temperature technology refers to that high-quality Cordyccps-militaris-(L.)-link. Sporophore is placed in to micronized pulverization machine carries out micronizing in described step (1), pulverize simultaneously and in whole process, use the water of 4-10 ℃ as micronized pulverization machine internal coolant.
5. the preparation method of a kind of Cordyceps militaris (L.) Link. assembled alcoholic drinks according to claim 1, is characterized in that: in described step (2), high-quality high spirit is that alcoholic strength is the aromatic Chinese spirit of 60-65 °.
6. the preparation method of a kind of Cordyceps militaris (L.) Link. assembled alcoholic drinks according to claim 1, is characterized in that: in described step (2), the blending ratio of Cordyceps militaris (L.) Link. super-fine powder and high-quality high spirit is 8g: 100ml or 16g: 100ml.
7. the preparation method of a kind of Cordyceps militaris (L.) Link. assembled alcoholic drinks according to claim 1, is characterized in that: after the middle Cordyceps militaris (L.) Link. super-fine powder of described step (2) and high-quality high spirit mix, being placed on the time of soaking in ceramic wine jar is 9 days.
8. the preparation method of a kind of Cordyceps militaris (L.) Link. assembled alcoholic drinks according to claim 1, is characterized in that: in described step (2), regularly stir and refer to stirring in every 1-2 days once.
9. the preparation method of a kind of Cordyceps militaris (L.) Link. assembled alcoholic drinks according to claim 1, is characterized in that: in described step (3), blending liquid is high-quality low alcohol white spirit and brewing water, and wherein high-quality low alcohol white spirit is that alcoholic strength is the aromatic Chinese spirit of 14-55 °.
10. the preparation method of a kind of Cordyceps militaris (L.) Link. assembled alcoholic drinks according to claim 1, is characterized in that: in described step (3), suitably alcoholic strength refers to that alcoholic strength is 30-55 °.
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103981069A (en) * | 2014-04-16 | 2014-08-13 | 田润生 | Chinese caterpillar fungus wine preparation method |
| CN104371896A (en) * | 2014-11-28 | 2015-02-25 | 河南省新境界酒业有限公司 | Healthcare aloe wine |
| CN105154297A (en) * | 2015-09-23 | 2015-12-16 | 安徽阳光药业有限公司 | New method for preparing health-preserving health-care cordyceps sinensis wine |
| CN105368652A (en) * | 2014-08-29 | 2016-03-02 | 宿迁楚霸菌业有限公司 | Method for preparing wine through selenium-rich cordyceps militaris trophoplasm waste |
| CN106609234A (en) * | 2016-10-24 | 2017-05-03 | 安徽华艾堂医药有限公司 | Cordyceps militaris wine capable of preserving health, and preparation method thereof |
| CN107095886A (en) * | 2016-02-20 | 2017-08-29 | 王弘 | A kind of Cordyceps militaris medicinal liquor and preparation method thereof |
| CN108728314A (en) * | 2018-06-12 | 2018-11-02 | 深圳市鑫木森实业发展有限公司 | A kind of SOD white wine preparation methods for supporting kidney function effect with protect liver |
| CN109536353A (en) * | 2017-09-22 | 2019-03-29 | 邓维国 | A kind of preparation method and products obtained therefrom of integration of drinking and medicinal herbs Cordyceps militaris health preserving wine |
| CN109666569A (en) * | 2018-12-27 | 2019-04-23 | 薛文 | A kind of Cordyceps militaris barley wine and preparation method thereof |
| CN110964618A (en) * | 2019-12-30 | 2020-04-07 | 珠海市祖龙酒业有限公司 | Anti-fatigue health wine and preparation method thereof |
| CN111500400A (en) * | 2019-06-12 | 2020-08-07 | 钟秀义 | A wine containing selenium-rich Cordyceps |
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| CN106609234A (en) * | 2016-10-24 | 2017-05-03 | 安徽华艾堂医药有限公司 | Cordyceps militaris wine capable of preserving health, and preparation method thereof |
| CN109536353A (en) * | 2017-09-22 | 2019-03-29 | 邓维国 | A kind of preparation method and products obtained therefrom of integration of drinking and medicinal herbs Cordyceps militaris health preserving wine |
| CN108728314A (en) * | 2018-06-12 | 2018-11-02 | 深圳市鑫木森实业发展有限公司 | A kind of SOD white wine preparation methods for supporting kidney function effect with protect liver |
| CN109666569A (en) * | 2018-12-27 | 2019-04-23 | 薛文 | A kind of Cordyceps militaris barley wine and preparation method thereof |
| CN111500400A (en) * | 2019-06-12 | 2020-08-07 | 钟秀义 | A wine containing selenium-rich Cordyceps |
| CN110964618A (en) * | 2019-12-30 | 2020-04-07 | 珠海市祖龙酒业有限公司 | Anti-fatigue health wine and preparation method thereof |
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Effective date of registration: 20170414 Address after: 550025 Guizhou Province in the New District of Guizhou security comprehensive security zone Patentee after: Guizhou Institute of precision medicine Limited by Share Ltd Address before: 300457 Tianjin international economic and Technological Development Zone, Binhai New Area, Tianjin Dongting Road, No. 220, Tianjin international joint Academy of biological medicine experimental building N511 Patentee before: Is the source of Tang (Tianjin) Biotechnology Co. Ltd. |
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Address after: 550025 Guizhou Province in the New District of Guizhou security comprehensive security zone Patentee after: Guizhou Gui'an precision Medicine Co.,Ltd. Address before: 550025 Guizhou Province in the New District of Guizhou security comprehensive security zone Patentee before: ACADEMY OF PRECISION MEDICINE, GUIAN, GUIZHOU Co.,Ltd. |
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