CN103710241B - A kind of preparation method of Cordyceps militaris assembled alcoholic drinks - Google Patents
A kind of preparation method of Cordyceps militaris assembled alcoholic drinks Download PDFInfo
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- CN103710241B CN103710241B CN201310733646.6A CN201310733646A CN103710241B CN 103710241 B CN103710241 B CN 103710241B CN 201310733646 A CN201310733646 A CN 201310733646A CN 103710241 B CN103710241 B CN 103710241B
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Abstract
The preparation method who the invention provides a kind of Cordyceps militaris assembled alcoholic drinks, it comprises the following steps: choose high-quality fruiting bodies of cordyceps militaris and dry, adopt low temperature superfine communication technique to obtain Cordyceps militaris Ultramicro-powder; Cordyceps militaris Ultramicro-powder and high-quality high spirit are fully mixed, be then placed in ceramic wine jar and soak, ceramic wine jar place room temperature is controlled at 15-20 DEG C, regularly stirs, and crosses leaching supernatant, obtains the former wine of Cordyceps militaris; Former Cordyceps militaris wine is blent to the alcoholic drink that is deployed into suitable alcoholic strength with blending liquid. This preparation method's step is simple, low for equipment requirements, quality controllable, and cost is low, and in the Cordyceps militaris assembled alcoholic drinks wine body preparing by the method, active component is abundant can survey.
Description
Technical field
The present invention relates to health liquor preparing technical field, be specifically related to a kind of Cordyceps militaris preparation taking Cordyceps militaris as primary raw materialThe preparation method of wine.
Background technology
Cordyceps militaris (Cordycepsmilitaris), has another name called northern Chinese caterpillar fungus, is under the jurisdiction of Ascomycotina, the ergot of mycotaSection, Cordyceps. Cordyceps militaris is a kind of fungi taking silkworm chrysalis as host, belongs to together with Cordyceps sinensis is equal, and chemical composition is basicUnanimously, its antineoplastic component cordycepin content is higher than Cordyceps sinensis, and is the new resource food of Ministry of Public Health's approval, has anti-Tumour, antiviral, antibacterial, anti-inflammatory, delay senility, improve the multiple efficacies such as immunity, be suitable for crowd extensive. OrderThe front existing brewed health liquor forming that carries out taking Cordyceps militaris as primary raw material.
As the notification number Chinese invention patent that is CN100352907C disclose a kind of ferment cordyceps sinensis, health lycium chinense andPreparation method, it uses matrimony vine premenstrual ferment, rear ferment to be refined into Lycium chinense wine, then with cordyceps mycelia through high-grade wine lixiviate essenceSystem, mixes in proportion, with the bent wine of a small amount of delicate fragrance type, first two wine is blent into the series wine of different components different taste, itsContent >=the 0.2mg/L of middle cordycepin. And according to a large amount of relevant reports, the contained cordycepin amount of mycelium is low, preparation after soakingHealth liquor in contained cordycepin lower, so the cordycepin content in this wine is only in the level of 0.2mg/L.
Notification number is that the Chinese invention patent of CN101341985B discloses a kind of Chinese caterpillar fungus health wine and preparation method thereof, shouldIn health liquor, cordycepin component content is that 20-100mg/L, Chinese caterpillar fungus adenosine component content are 20-150mg/L. But this health careThe preparation method of wine is the extract that first obtains each component, then according to predefined each component content carrying each componentGet liquid and white spirit mixed obtains, and the extract preparation process complexity of each component: first by raw material drying to water content 13% withUnder, pulverize, obtain powder material after crossing 60-80 mesh sieve, then add and be equivalent to doubly pure of powder material volume 8-20Water forms mixed liquor, by mixed liquor multiple tank Continuous Countercurrent Extraction 4-6 hour under normal pressure, 75-95 DEG C condition, collectTo extract. The leaching process complexity of this extract, high to equipment requirement, energy waste is serious, and raw material is at 75-95Continuous flow upstream under DEG C high temperature conditions like this, can the destruction of its active ingredient be serious, extract desired concn each groupDivide content to remain suspicious.
Summary of the invention
Technical problem to be solved by this invention is for above the deficiencies in the prior art, and a kind of Cordyceps militaris assembled alcoholic drinks is providedPreparation method, this preparation method's step is simple, low for equipment requirements, quality controllable, and cost is low. Prepare by the methodThe Cordyceps militaris assembled alcoholic drinks obtaining, abundant can the survey of active component in wine body.
The technical solution adopted in the present invention is:
A preparation method for Cordyceps militaris assembled alcoholic drinks, the method comprises the following steps:
(1) the preparation processing of raw material: choose high-quality fruiting bodies of cordyceps militaris and dry, adopt low temperature superfine communication technique to obtainCordyceps militaris Ultramicro-powder;
(2) acquisition of the former wine of Cordyceps militaris: Cordyceps militaris Ultramicro-powder and high-quality high spirit are fully mixed, be then placed onIn pottery wine jar, soak, ceramic wine jar place room temperature is controlled at 15-20 DEG C, regularly stirs, and crosses leaching supernatant, obtains pupaThe former wine of Chinese caterpillar fungus;
(3) allotment of cordyceps militaris liquor: former Cordyceps militaris wine is blent to the alcoholic drink that is deployed into suitable alcoholic strength with blending liquid.
In described step (1), high-quality fruiting bodies of cordyceps militaris refers to a golden yellow megaspore fruiting bodies of cordyceps militaris.
In described step (1), oven dry is preferably high-quality fruiting bodies of cordyceps militaris is evenly spread out, and is placed under 37 DEG C of hot air circulationDry, its moisture is controlled at below 10%.
In described step (1), low temperature superfine communication technique is preferably high-quality fruiting bodies of cordyceps militaris is placed in to micronized pulverization machineCarry out ultramicro grinding, pulverize simultaneously and in overall process, use the water of 4-10 DEG C as micronized pulverization machine internal coolant.
To be preferably alcoholic strength be the aromatic Chinese spirit of 60-65 ° to high-quality high spirit in described step (2).
In described step (2), the mixed proportion of Cordyceps militaris Ultramicro-powder and high-quality high spirit is preferably 8g: 100ml or 16g:100ml。
In described step (2) Cordyceps militaris Ultramicro-powder and high-quality high spirit after mixing, be placed in ceramic wine jar, soak timeBetween be preferably 9 days.
In described step (2), regularly stir and be preferably stirring in every 1-2 days once.
In described step (3), blending liquid is preferably high-quality low alcohol white spirit and brewing water, and wherein high-quality low alcohol white spirit is preferablyAlcoholic strength is the aromatic Chinese spirit of 14-55 °.
In described step (3), suitably alcoholic strength refers to that alcoholic strength is 30-55 °.
Compared with prior art, the present invention has following remarkable advantage and beneficial effect:
(1) the present invention is taking fruiting bodies of cordyceps militaris as primary raw material, after oven dry, ultramicro grinding are processed, by necessarily joiningThan mixing with high quality liquor, be prepared through immersion, lixiviate, filtration, allotment, filling mode. By to techniqueThe research of process and control, particularly by controlling fruiting bodies of cordyceps militaris and the mixed proportion of white wine and the time of lixiviate,Make to prepare that in the former wine of Cordyceps militaris of gained, cordycepin content reaches as high as 670mg/L, adenosine content reaches as high as 260Mg/L, so the bioactive substance content such as cordycepin, adenosine in the Cordyceps militaris assembled alcoholic drinks being deployed into the former wine of this Cordyceps militarisHeight, content of material is stablized controlled, and product quality is good, and health care is strong.
(2) the present invention uses micronizer, carries out low temperature ultramicro grinding, to abolish hard thin of fruiting bodies of cordyceps militarisCell wall, is conducive to the stripping of content, improves the recovery rate of active principle in Cordyceps militaris.
(3) whole process of the present invention is carried out handle control to temperature, and when wherein fruiting bodies of cordyceps militaris is dried, temperature is controlled at 37 DEG C, superWhen Crushing of Ultrafine, temperature is controlled at 4-10 DEG C, and when lixiviate, temperature control 15-20 DEG C, supervises in real time by the temperature to these processesSurvey and control, effectively ensured the activity of extract in Cordyceps militaris, ensure its medical value.
(4) the whole preparation process of the present invention is simple to operate, low for equipment requirements, workable, is applicable to extensiveSuitability for industrialized production, is easy to promote.
(5) the Cordyceps militaris assembled alcoholic drinks of preparing by the method, abundant can the survey of active component in wine body, product quality canControl, material damages few, and cost is low, and product is easy to preserve; Wine body does not contain any synthetic dyestuff and synthetic non-natural compound, mouthfulTaste is pure, has higher medicinal and nutritive value.
Brief description of the drawings
Shown in Fig. 1 be in Cordyceps militaris assembled alcoholic drinks of the present invention cordycepin at the content of different soak time sections;
Shown in Fig. 2 be in Cordyceps militaris assembled alcoholic drinks of the present invention adenosine at the content of different soak time sections.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further described in detail. Be noted that following illustrating is all exemplary, be intended to the invention provides further instruction. Except as otherwise noted, all Science and Technology arts that the present invention usesLanguage has the identical meanings of conventionally understanding with the technical field of the invention personnel.
Embodiment 1: the preparation of raw material
1, dry
Choose a golden yellow megaspore fruiting bodies of cordyceps militaris as raw material, be placed in the stainless steel disc that is lined with gauze, allEven spreading out, 37 DEG C of hot air circulation are dried, and its moisture is controlled at below 10%.
2, pulverize
Take the fruiting bodies of cordyceps militaris that 200g is dried at every turn, put into micronized pulverization machine and carry out ultramicro grinding, simultaneously brokenOverall process as micronized pulverization machine internal coolant, is guaranteed the release of active ingredient and bioactive steady with the water of 4～10 DEG CFixed, ultramicro grinding is 5-15min, gropes 6-10min be advisable through practice, and 6min is for the most suitable.
Embodiment 2: the acquisition of the former wine of Cordyceps militaris
1, mix and soak
By Cordyceps militaris Ultramicro-powder and high-quality high spirit, (selecting alcoholic strength is here the aromatic Chinese spirit of 65 degree, is purchased from weighing apparatusShui Ganling spring Wine Co., Ltd) press respectively 2g: 100ml, 4g: 100ml, 8g: 100ml, 16g: 100ml'sRatio fully mixes, and is placed on respectively in ceramic wine jar and soaks, and ceramic wine jar place room temperature is controlled at 15-20 DEG C.
2, lixiviate
Within every two days, stir once, the active ingredient in lixiviate Cordyceps militaris leaves standstill 3 days, while altogether immersion after stirring 3 timesBetween be 9 days. Sampling respectively in the 1st, 3,4,5,6,7,8,9 days after immersion, detect immersion by HPLCCordycepin and adenosine content in liquid, result as depicted in figs. 1 and 2. Drawn by Fig. 1 and the comprehensive comparison of Fig. 2 and analysis,Soaking after 9 days in leaching liquor, cordycepin and adenosine content are the highest.
The mixed proportion that is Cordyceps militaris Ultramicro-powder and white wine when fruiting bodies of cordyceps militaris dry powder is 16g: when 100ml, by thisThe preparation method of invention, in the time that soak time is 9 days, in wine body, the content of adenosine can reach 260 μ g/ml,260mg/L. And taking adenosine content in fruiting bodies of cordyceps militaris dry powder as 2/1000ths, the theoretical peak of adenosine content is320mg/L, thus, this preparation method's material damages few, and in raw material, utilization rate of active components reaches 81.25%, utilization rateHigh.
3, filter
Draw the supernatant of leaching liquor, further filter out the solids of suspension with filter plant, obtain the former wine of Cordyceps militaris.
Embodiment 3: the allotment of cordyceps militaris liquor
1, allotment
By former Cordyceps militaris for wine low high quality liquor (selecting alcoholic strength is here the aromatic Chinese spirit of 55 degree, is purchased from HengshuiGan Ling spring Wine Co., Ltd) and brewing water is blent, and to be deployed into alcoholic strength be that (concrete alcoholic strength content is according to visitor for 30-55 degreeFamily need or during as concrete health care suitable alcohol drink content and determine) alcoholic drink.
2, filling
By deployed alcoholic drink quantitative separating, sealing.
3, detect
The Cordyceps militaris assembled alcoholic drinks obtaining is carried out to organoleptic indicator's detection and physical and chemical index detection, and result is respectively as table 1 and table 2Shown in.
After testing, its cordycepin of Cordyceps militaris assembled alcoholic drinks that this preparation method obtains and adenosine content are all higher than general commercially available Chinese caterpillar fungusHealth liquor, so the Cordyceps militaris assembled alcoholic drinks that this preparation method obtains has good using value aspect health liquor.
4, preserve
Lucifuge, dry, room temperature preservation.
The above, be only the preferred embodiments of the present invention, it should be pointed out that for those skilled in the art, not departing under the prerequisite of core technology of the present invention, can also make improvements and modifications, these improvements and modificationsAlso should belong to scope of patent protection of the present invention. Any changing in implication and the scope suitable with claims of the present inventionBecome, all should think to be included in the scope of claims.
Table 1: organoleptic indicator
| Project | Index |
| Outward appearance | Be golden yellow or brown color, clarification, has allowed a small amount of precipitation after being long placed in |
| Fragrance | There is the peculiar smell of Cordyceps militaris and aroma, free from extraneous odour |
| Flavour | There is the distinctive flavour of this product |
| Style | There is the typical style of this product |
Table 2: physical and chemical index
Claims (7)
1. a preparation method for Cordyceps militaris assembled alcoholic drinks, is characterized in that comprising the following steps:
(1) the preparation processing of raw material: choose high-quality fruiting bodies of cordyceps militaris and dry, adopt low temperature superfine communication technique to obtainCordyceps militaris Ultramicro-powder;
(2) acquisition of the former wine of Cordyceps militaris: Cordyceps militaris Ultramicro-powder and high-quality high spirit are fully mixed, and high-quality height is whiteWine is that alcoholic strength is the aromatic Chinese spirit of 65 °, and the mixed proportion of Cordyceps militaris Ultramicro-powder and high-quality high spirit is 16g:100ml, is then placed in ceramic wine jar and soaks, and after Cordyceps militaris Ultramicro-powder and high-quality high spirit mix, is placed on potteryThe time of soaking in wine jar is 9 days, and ceramic wine jar place room temperature is controlled at 15-20 DEG C, regularly stirs, and crosses leaching supernatant,Obtain the former wine of Cordyceps militaris;
(3) allotment of cordyceps militaris liquor: former Cordyceps militaris wine is blent to the alcoholic drink that is deployed into suitable alcoholic strength with blending liquid.
2. the preparation method of a kind of Cordyceps militaris assembled alcoholic drinks according to claim 1, is characterized in that: described step (1)Middle high-quality fruiting bodies of cordyceps militaris refers to golden yellow megaspore head, is not stained with the fruiting bodies of cordyceps militaris of culture medium.
3. the preparation method of a kind of Cordyceps militaris assembled alcoholic drinks according to claim 1, is characterized in that: described step (1)Middle oven dry refers to high-quality fruiting bodies of cordyceps militaris is evenly spread out, and is placed under 37 DEG C of hot air circulation and dries, and makes its moisture controlBuilt in below 10%.
4. the preparation method of a kind of Cordyceps militaris assembled alcoholic drinks according to claim 1, is characterized in that: described step (1)Middle low temperature superfine communication technique refers to that high-quality fruiting bodies of cordyceps militaris is placed in to micronized pulverization machine carries out ultramicro grinding, simultaneously powderIn broken overall process, use the water of 4-10 DEG C as micronized pulverization machine internal coolant.
5. the preparation method of a kind of Cordyceps militaris assembled alcoholic drinks according to claim 1, is characterized in that: described step (2)In regularly stir and refer to every 1-2 days and stir once.
6. the preparation method of a kind of Cordyceps militaris assembled alcoholic drinks according to claim 1, is characterized in that: described step (3)Middle blending liquid is high-quality low alcohol white spirit and brewing water, and wherein high-quality low alcohol white spirit is that alcoholic strength is that the Luzhou-flavor of 14-55 ° is whiteWine.
7. the preparation method of a kind of Cordyceps militaris assembled alcoholic drinks according to claim 1, is characterized in that: described step (3)In suitably alcoholic strength refer to that alcoholic strength is 30-55 °.
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| CN103981069A (en) * | 2014-04-16 | 2014-08-13 | 田润生 | Chinese caterpillar fungus wine preparation method |
| CN105368652A (en) * | 2014-08-29 | 2016-03-02 | 宿迁楚霸菌业有限公司 | Method for preparing wine through selenium-rich cordyceps militaris trophoplasm waste |
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| CN105154297A (en) * | 2015-09-23 | 2015-12-16 | 安徽阳光药业有限公司 | New method for preparing health-preserving health-care cordyceps sinensis wine |
| CN107095886A (en) * | 2016-02-20 | 2017-08-29 | 王弘 | A kind of Cordyceps militaris medicinal liquor and preparation method thereof |
| CN106609234A (en) * | 2016-10-24 | 2017-05-03 | 安徽华艾堂医药有限公司 | Cordyceps militaris wine capable of preserving health, and preparation method thereof |
| CN109536353A (en) * | 2017-09-22 | 2019-03-29 | 邓维国 | A kind of preparation method and products obtained therefrom of integration of drinking and medicinal herbs Cordyceps militaris health preserving wine |
| CN108728314A (en) * | 2018-06-12 | 2018-11-02 | 深圳市鑫木森实业发展有限公司 | A kind of SOD white wine preparation methods for supporting kidney function effect with protect liver |
| CN109666569A (en) * | 2018-12-27 | 2019-04-23 | 薛文 | A kind of Cordyceps militaris barley wine and preparation method thereof |
| CN111500400A (en) * | 2019-06-12 | 2020-08-07 | 钟秀义 | A wine containing selenium-rich Cordyceps |
| CN110964618A (en) * | 2019-12-30 | 2020-04-07 | 珠海市祖龙酒业有限公司 | Anti-fatigue health wine and preparation method thereof |
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Effective date of registration: 20170414 Address after: 550025 Guizhou Province in the New District of Guizhou security comprehensive security zone Patentee after: Guizhou Institute of precision medicine Limited by Share Ltd Address before: 300457 Tianjin international economic and Technological Development Zone, Binhai New Area, Tianjin Dongting Road, No. 220, Tianjin international joint Academy of biological medicine experimental building N511 Patentee before: Is the source of Tang (Tianjin) Biotechnology Co. Ltd. |
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Address after: 550025 Guizhou Province in the New District of Guizhou security comprehensive security zone Patentee after: Guizhou Gui'an precision Medicine Co.,Ltd. Address before: 550025 Guizhou Province in the New District of Guizhou security comprehensive security zone Patentee before: ACADEMY OF PRECISION MEDICINE, GUIAN, GUIZHOU Co.,Ltd. |