CN107927156A - A kind of crude antistaling agent for strawberry preservation and preparation method thereof and preservation method - Google Patents
A kind of crude antistaling agent for strawberry preservation and preparation method thereof and preservation method Download PDFInfo
- Publication number
- CN107927156A CN107927156A CN201711214788.6A CN201711214788A CN107927156A CN 107927156 A CN107927156 A CN 107927156A CN 201711214788 A CN201711214788 A CN 201711214788A CN 107927156 A CN107927156 A CN 107927156A
- Authority
- CN
- China
- Prior art keywords
- extracting solution
- pomelo peel
- strawberry
- apple skin
- antistaling agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000016623 Fragaria vesca Nutrition 0.000 title claims abstract description 69
- 235000011363 Fragaria x ananassa Nutrition 0.000 title claims abstract description 69
- 238000004321 preservation Methods 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 238000000034 method Methods 0.000 title claims abstract description 13
- 240000009088 Fragaria x ananassa Species 0.000 title 1
- 241000220223 Fragaria Species 0.000 claims abstract description 72
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 60
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 29
- 240000000560 Citrus x paradisi Species 0.000 claims abstract 15
- 244000276331 Citrus maxima Species 0.000 claims description 77
- 239000000706 filtrate Substances 0.000 claims description 54
- 238000000605 extraction Methods 0.000 claims description 39
- 238000010992 reflux Methods 0.000 claims description 39
- 239000000843 powder Substances 0.000 claims description 34
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 28
- 230000006837 decompression Effects 0.000 claims description 26
- 238000001914 filtration Methods 0.000 claims description 25
- 239000008367 deionised water Substances 0.000 claims description 20
- 229910021641 deionized water Inorganic materials 0.000 claims description 20
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 20
- 235000010987 pectin Nutrition 0.000 claims description 16
- 229920001277 pectin Polymers 0.000 claims description 16
- 239000001814 pectin Substances 0.000 claims description 16
- 238000004064 recycling Methods 0.000 claims description 14
- 201000010099 disease Diseases 0.000 claims description 8
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 claims description 8
- 229930003944 flavone Natural products 0.000 claims description 8
- 235000011949 flavones Nutrition 0.000 claims description 8
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 8
- 235000013824 polyphenols Nutrition 0.000 claims description 8
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 claims description 7
- 241000607479 Yersinia pestis Species 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 7
- 150000002212 flavone derivatives Chemical class 0.000 claims description 7
- 150000003839 salts Chemical class 0.000 claims description 7
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 claims description 7
- 235000013399 edible fruits Nutrition 0.000 abstract description 12
- 230000000694 effects Effects 0.000 abstract description 6
- 239000002994 raw material Substances 0.000 abstract description 3
- 230000002195 synergetic effect Effects 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000004575 stone Substances 0.000 abstract description 2
- 239000002699 waste material Substances 0.000 abstract description 2
- 241000220225 Malus Species 0.000 description 58
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 20
- 238000004140 cleaning Methods 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 10
- 238000001035 drying Methods 0.000 description 10
- 238000002156 mixing Methods 0.000 description 10
- 235000021028 berry Nutrition 0.000 description 8
- 244000025254 Cannabis sativa Species 0.000 description 7
- 235000001759 Citrus maxima Nutrition 0.000 description 6
- 235000021012 strawberries Nutrition 0.000 description 6
- 239000007788 liquid Substances 0.000 description 5
- 239000000284 extract Substances 0.000 description 4
- 239000003755 preservative agent Substances 0.000 description 3
- 230000002335 preservative effect Effects 0.000 description 3
- 244000307700 Fragaria vesca Species 0.000 description 2
- 235000013717 Houttuynia Nutrition 0.000 description 2
- 240000000691 Houttuynia cordata Species 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 239000000469 ethanolic extract Substances 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- WCGUUGGRBIKTOS-GPOJBZKASA-N (3beta)-3-hydroxyurs-12-en-28-oic acid Chemical compound C1C[C@H](O)C(C)(C)[C@@H]2CC[C@@]3(C)[C@]4(C)CC[C@@]5(C(O)=O)CC[C@@H](C)[C@H](C)[C@H]5C4=CC[C@@H]3[C@]21C WCGUUGGRBIKTOS-GPOJBZKASA-N 0.000 description 1
- JDLKFOPOAOFWQN-VIFPVBQESA-N Allicin Natural products C=CCS[S@](=O)CC=C JDLKFOPOAOFWQN-VIFPVBQESA-N 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- 240000003152 Rhus chinensis Species 0.000 description 1
- 235000014220 Rhus chinensis Nutrition 0.000 description 1
- 241000220222 Rosaceae Species 0.000 description 1
- JDLKFOPOAOFWQN-UHFFFAOYSA-N allicin Chemical compound C=CCSS(=O)CC=C JDLKFOPOAOFWQN-UHFFFAOYSA-N 0.000 description 1
- 235000010081 allicin Nutrition 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000001143 conditioned effect Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000012055 fruits and vegetables Nutrition 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 230000029058 respiratory gaseous exchange Effects 0.000 description 1
- 230000014860 sensory perception of taste Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229940096998 ursolic acid Drugs 0.000 description 1
- PLSAJKYPRJGMHO-UHFFFAOYSA-N ursolic acid Natural products CC1CCC2(CCC3(C)C(C=CC4C5(C)CCC(O)C(C)(C)C5CCC34C)C2C1C)C(=O)O PLSAJKYPRJGMHO-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B7/00—Preservation or chemical ripening of fruit or vegetables
- A23B7/16—Coating with a protective layer; Compositions or apparatus therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a kind of crude antistaling agent for strawberry preservation and preparation method thereof and preservation method, the crude antistaling agent is made of pomelo peel extracting solution and apple skin extracting solution, wherein pomelo peel extracting solution volume fraction shared in crude antistaling agent is 40% 55%, and apple skin extracting solution volume fraction shared in antistaling agent is 45% 60%.It is synergistic at the same time using pomelo peel and the extracting solution of apple skin in the crude antistaling agent of the present invention, it is of good preservation effect；Preservation method using the present invention can cause healthy fruit of the strawberry when fresh keeping time is 20 days to be more than 90%, and percentage of water loss is less than 2%, and does not have peculiar smell.The preparation method of the present invention is simple and convenient, and pomelo peel and apple skin are industrial processes discarded object, using pomelo peel and apple skin as raw material, prepares the crude antistaling agent for strawberry, not only turns waste into wealth, but also also reduces pollution of the discarded object to environment, kills two birds with one stone.
Description
Technical field
The invention belongs to preserving fruit and vegetable utilizing field, and in particular to a kind of crude antistaling agent and its preparation side for strawberry preservation
Method and preservation method.
Background technology
Strawberry is perennial herb, is rose family pseudocarp reality, and the lovely luster of strawberry, fragrance is tempting, possesses the mouth of uniqueness
Sense, it is also very high containing abundant nutriment, edible value.In addition, strawberry also has medical value, such as heat-clearing and fire-reducing, anticancer
Disease and anti-aging.The water content of strawberry is very high, but without hard outer tissue, thus strawberry be very easy in transportational process by
To mechanical damage, the ethylene contents that strawberry discharges after adopting rise violently rapidly, and its own microorganism carried also allows its preservation
Phase is very short, causes to rot and lose commodity value, can only preserve 1~2d at normal temperatures.There is substantial amounts of strawberry also not every year
Sell away and just rot, cause serious economic loss and the wasting of resources, therefore, finding suitable strawberry preservation technology is
The task of top priority.
At present, for Storage of Strawberry based on deepfreeze, this method can reduce strawberry softening rate to a certain extent, but
It is that fruit dehydration is very fast, air conditioned storage, reduced pressure treatment, radiation treatment can extend the shelf life of strawberry, but cost is higher.
Fresh-keeping using chemical substance, its residual has hidden danger to health.In recent years, crude antistaling agent was got over for the research of strawberry preservation
Come more.Crude antistaling agent mainly includes stomata of the Antibacterial Constituents with sterilization and anticorrosion with blocking moisture loss, reduces
Water loss, can prevent gas exchanges inside and outside fruit, suppress respiration, and can prevent the film infected of microorganism into
Point.But many crude antistaling agents extract from natural drug, such as allicin (application number 201410572415.6, Yi Zhongcao more
Certain kind of berries fresh-keeping liquid and preparation method thereof), Chinese gall (application number 201510180807.2, a kind of Chinese herb residues leaching liquor-gelatin strawberry
The preparation method of preservative film), radix glycyrrhizae, cordate houttuynia (application number 201510533552.3, a kind of composite preservative of strawberry) etc., this
Although a little natural components have preferable sterilization and anticorrosion activity, can have strawberry and make us not pleasant peculiar smell, so that shadow
Ring the sale of strawberry.Therefore, for current strawberry preservation technology there are the drawbacks of, develop a kind of compound guarantor of green safe strawberry
Fresh dose is necessary.
The content of the invention
Goal of the invention：For problem present on current strawberry preservation technology, the present invention provides one kind and is used for strawberry preservation
Crude antistaling agent, which prepares the crude antistaling agent for strawberry using pomelo peel and apple skin as raw material, can be to grass
The certain kind of berries carries out effectively fresh-keeping.
The present invention also provides the preparation method and preservation method of the crude antistaling agent for strawberry preservation.
Technical solution：To achieve these goals, a kind of crude antistaling agent for strawberry preservation as described herein, institute
State crude antistaling agent to be made of pomelo peel extracting solution and apple skin extracting solution, wherein pomelo peel extracting solution institute in crude antistaling agent
The volume fraction accounted for is 40%-55%v/v, and apple skin extracting solution volume fraction shared in antistaling agent is 45%-60%v/
v。
The preparation method of crude antistaling agent of the present invention, comprises the following steps：
(1) pomelo peel is cleaned, dried, pulverized and sieved, obtain pomelo peel coarse powder；Pomelo peel coarse powder is placed in ethanol water
In, refluxing extraction, extracting solution filtering, obtains filtrate and filter residue；Decompression filtrate recycling ethanol is simultaneously concentrated into pomelo peel general flavone content
It is pomelo peel extracting solution A in 30-35mg/mL；
Filter residue is placed in deionized water, with salt acid for adjusting pH, refluxing extraction, filtrate is filtered, and filter residue discards, and filtrate subtracts
Pressure is concentrated into pomelo peel pectin content in 10-15mg/mL, is pomelo peel extracting solution B；Pomelo peel extracting solution A and B are mixed in equal volume
Close, obtain pomelo peel extracting solution；
(2) apple skin is cleaned, dried, pulverized and sieved, obtain apple skin coarse powder；Ethanol water is placed in by apple skin coarse powder
In, refluxing extraction, extracting solution filtering, obtains filtrate and filter residue；Decompression filtrate recycling ethanol is simultaneously concentrated into Determination of Polyphenols in 20-
25mg/mL, is apple skin extracting solution A；
Filter residue is placed in deionized water, with salt acid for adjusting pH, refluxing extraction, filtrate is filtered, and filter residue discards, and filtrate subtracts
Pressure is concentrated into apple skin pectin content in 10-15mg/mL, is apple skin extracting solution B；Apple skin extracting solution A and B are mixed in equal volume
Close, obtain apple skin extracting solution；
(3) the apple skin extracting solution that the pomelo peel extracting solution and step (2) obtained step (1) obtains mixes in proportion
To the crude antistaling agent for strawberry preservation.
Wherein, step (1) the pomelo peel coarse powder is 1 by mass volume ratio:It is 70- that 8-12mg/mL, which adds volume fraction,
Refluxing extraction in 80% ethanol water.It is preferred that pomelo peel coarse powder is 1 by mass volume ratio:10mg/mL adds volume fraction
For in the ethanol water of 75%v/v.
Wherein, the step (1) filter residue is 1 by mass volume ratio:6-10mg/mL is added in deionized water.It is preferred that
Filter residue is 1 by mass volume ratio:8mg/mL adds refluxing extraction in deionized water.
Wherein, step (2) the apple skin coarse powder is 1 by mass volume ratio:It is 80- that 8-12mg/mL, which adds volume fraction,
Refluxing extraction in 90% ethanol water.Preferably apple skin coarse powder is 1 by mass volume ratio:10mg/mL adds volume fraction
For in the ethanol water of 90%v/v.
Wherein, the step (2) filter residue is 1 by mass volume ratio:6-10mg/mL is added in deionized water.It is preferred that
Filter residue is 1 by mass volume ratio:8mg/mL adds refluxing extraction in deionized water.
Wherein, step (1) and step (2) described refluxing extraction are 2-3 times, each 1-1.5h.Preferably, refluxing extraction 2
Secondary, each 1.5h, extracting solution merges filtering.
Wherein, step (1) and step (2) the salt acid for adjusting pH are 2-3.Preferably, with the salt acid for adjusting pH of 1mol/L
For 2.
Crude antistaling agent of the present invention is used for the preservation method of strawberry preservation, includes the following steps：
1) eight to ninety percent ripe strawberries are harvested, no disease and pests harm is selected, has no mechanical damage, uniform fresh strawberry；
2) strawberry is placed in crude antistaling agent and soaks 20min, taken out strawberry, dry；The strawberry dried is deposited in cold
Storehouse is fresh-keeping.
Wherein, the temperature of step (2) described freezer be 2-10 DEG C, relative humidity 85-90%.
Beneficial effect：Compared with prior art, the present invention has following conspicuousness beneficial effect：
1st, in crude antistaling agent of the invention pomelo peel, apple skin ethanol extract be mainly flavones and Polyphenols activity into
Point, and containing certain ursolic acid, these compounds not only have higher antibacterial and antioxidation activity in vitro, are taken the photograph by human body
Enter, also have and remove free radical and reducing blood lipid isoreactivity.
2nd, pomelo peel, apple skin ethanol extract can extract partial pericarp fruit wax, and water extract is mainly pectin, fruit wax
Layer protecting film can be formed in strawberry surface with pectin, and fruit wax has certain waterproof action, can preferably prevent strawberry water
The loss divided.
3rd, pomelo peel and apple bark extract all have delicate fragrance fruity in crude antistaling agent, even if remaining on strawberry,
Consumer will not be allowed to produce the not pleasant sense of taste.
4th, preparation method of the invention is simple and convenient, and pomelo peel and apple skin are industrial processes discarded object, with pomelo peel
It is raw material with apple skin, prepares the crude antistaling agent for strawberry, not only turn waste into wealth, but also also reduce discarded object to environment
Pollution, kill two birds with one stone.
5th, at the same time using pomelo peel and the extracting solution of apple skin in crude antistaling agent of the invention, synergistic, fresh-keeping effect
Fruit is good；Preservation method using the present invention can cause healthy fruit of the strawberry when fresh keeping time is 20 days to be more than 90%, dehydration
Rate is less than 2%.
Embodiment
The present invention will be further described with reference to embodiments.
Embodiment 1
(1) pomelo peel cleaning, drying, crushed 60 mesh sieves, obtain pomelo peel coarse powder.By mass volume ratio 1:10g/mL is by shaddock
Sub- skin coarse powder is placed in the ethanol water of 75%v/v concentration, refluxing extraction 2 times, each 1.5h, and extracting solution merges, and filtering, obtains
Filtrate and filter residue.Decompression filtrate recycling ethanol is simultaneously concentrated into pomelo peel general flavone content in 30mg/mL, is pomelo peel extracting solution A.
It is 1 by mass volume ratio:Filter residue is placed in deionized water by 8g/mL, and pH2 is adjusted with the hydrochloric acid of 1mol/L, refluxing extraction 2 times,
Each 1.5h, merging filtrate, filtering, filter residue discards, and filtrate decompression is concentrated into pomelo peel pectin content in 10mg/mL, is shaddock
Skin extracting solution B.By pomelo peel extracting solution A and B by volume 1:1 mixing, obtains pomelo peel extracting solution.
(2) apple skin cleaning, drying, crushed 80 mesh sieves, obtain apple skin coarse powder.By mass volume ratio 1:10g/mL is by apple
Pericarp coarse powder is placed in the ethanol water of 90%v/v concentration, refluxing extraction 2 times, each 1.5h, and extracting solution merges, and filtering, obtains
Filtrate and filter residue.Decompression filtrate recycling ethanol is simultaneously concentrated into Determination of Polyphenols in 25mg/mL, is apple skin extracting solution A.By quality
Volume ratio 1:Filter residue is placed in deionized water by 8g/mL, and pH2 is adjusted with the hydrochloric acid of 1mol/L, refluxing extraction 2 times, each 1.5h,
Merging filtrate, filtering, filter residue discards, and filtrate decompression is concentrated into apple skin pectin content in 15mg/mL, is apple skin extracting solution B.
By apple skin extracting solution A and B by volume 1:1 mixing, obtains apple skin extracting solution.
(3) it is 40% by pomelo peel extracting solution volume fraction v/v shared in crude antistaling agent, apple skin extracting solution exists
Shared volume fraction v/v is 60% in antistaling agent, is mixed to get crude antistaling agent.
(4) eight to ninety percent ripe strawberries are harvested, no disease and pests harm is selected, has no mechanical damage, uniform fresh strawberry.By grass
The certain kind of berries, which is placed in crude antistaling agent, soaks 20min, takes out strawberry, dries.The strawberry dried is deposited in into 2-10 DEG C of environment temperature, phase
It is fresh-keeping to the freezer that humidity is 85-90%.
Embodiment 2
(1) pomelo peel cleaning, drying, crushed 60 mesh sieves, obtain pomelo peel coarse powder.By mass volume ratio 1:10g/mL is by shaddock
Sub- skin coarse powder is placed in the ethanol water of 75%v/v concentration, refluxing extraction 2 times, each 1.5h, and extracting solution merges, and filtering, obtains
Filtrate and filter residue.Decompression filtrate recycling ethanol is simultaneously concentrated into pomelo peel general flavone content in 35mg/mL, is pomelo peel extracting solution A.
By mass volume ratio 1:Filter residue is placed in deionized water by 8g/mL, and pH2 is adjusted with the hydrochloric acid of 1mol/L, refluxing extraction 2 times, often
Secondary 1.5h, merging filtrate, filtering, filter residue discards, and filtrate decompression is concentrated into pomelo peel pectin content in 15mg/mL, is pomelo peel
Extracting solution B.By pomelo peel extracting solution A and B by volume 1:1 mixing, obtains pomelo peel extracting solution.
(2) apple skin cleaning, drying, crushed 80 mesh sieves, obtain apple skin coarse powder.By mass volume ratio 1:10g/mL is by apple
Pericarp coarse powder is placed in the ethanol water of 90%v/v concentration, refluxing extraction 2 times, each 1.5h, and extracting solution merges, and filtering, obtains
Filtrate and filter residue.Decompression filtrate recycling ethanol is simultaneously concentrated into Determination of Polyphenols in 20mg/mL, is apple skin extracting solution A.By quality
Volume ratio 1:Filter residue is placed in deionized water by 8g/mL, and pH2 is adjusted with the hydrochloric acid of 1mol/L, refluxing extraction 2 times, each 1.5h,
Merging filtrate, filtering, filter residue discards, and filtrate decompression is concentrated into apple skin pectin content in 10mg/mL, is apple skin extracting solution B.
By apple skin extracting solution A and B by volume 1:1 mixing, obtains apple skin extracting solution.
(3) it is 55% by pomelo peel extracting solution volume fraction v/v shared in crude antistaling agent, apple skin extracting solution exists
Shared volume fraction v/v is 45% in antistaling agent, is mixed to get crude antistaling agent.
(4) eight to ninety percent ripe strawberries are harvested, no disease and pests harm is selected, has no mechanical damage, uniform fresh strawberry.By grass
The certain kind of berries, which is placed in crude antistaling agent, soaks 20min, takes out strawberry, dries.The strawberry dried is deposited in into 2-10 DEG C of environment temperature, phase
It is fresh-keeping to the freezer that humidity is 85-90%.
Embodiment 3
(1) pomelo peel cleaning, drying, crushed 60 mesh sieves, obtain pomelo peel coarse powder.By mass volume ratio 1:10g/mL is by shaddock
Sub- skin coarse powder is placed in the ethanol water of 75%v/v concentration, refluxing extraction 2 times, each 1.5h, and extracting solution merges, and filtering, obtains
Filtrate and filter residue.Decompression filtrate recycling ethanol is simultaneously concentrated into pomelo peel general flavone content in 33mg/mL, is pomelo peel extracting solution A.
By mass volume ratio 1:Filter residue is placed in deionized water by 8g/mL, and pH2 is adjusted with the hydrochloric acid of 1mol/L, refluxing extraction 2 times, often
Secondary 1.5h, merging filtrate, filtering, filter residue discards, and filtrate decompression is concentrated into pomelo peel pectin content in 13mg/mL, is pomelo peel
Extracting solution B.By pomelo peel extracting solution A and B by volume 1:1 mixing, obtains pomelo peel extracting solution.
(2) apple skin cleaning, drying, crushed 80 mesh sieves, obtain apple skin coarse powder.By mass volume ratio 1:10g/mL is by apple
Pericarp coarse powder is placed in the ethanol water of 90%v/v concentration, refluxing extraction 2 times, each 1.5h, and extracting solution merges, and filtering, obtains
Filtrate and filter residue.Decompression filtrate recycling ethanol is simultaneously concentrated into Determination of Polyphenols in 22mg/mL, is apple skin extracting solution A.By quality
Volume ratio 1:Filter residue is placed in deionized water by 8g/mL, and pH2 is adjusted with the hydrochloric acid of 1mol/L, refluxing extraction 2 times, each 1.5h,
Merging filtrate, filtering, filter residue discards, and filtrate decompression is concentrated into apple skin pectin content in 12mg/mL, is apple skin extracting solution B.
By apple skin extracting solution A and B by volume 1:1 mixing, obtains apple skin extracting solution.
(3) it is 50% by pomelo peel extracting solution volume fraction v/v shared in crude antistaling agent, apple skin extracting solution exists
Shared volume fraction v/v is 50% in antistaling agent, is mixed to get crude antistaling agent.
(4) eight to ninety percent ripe strawberries are harvested, no disease and pests harm is selected, has no mechanical damage, uniform fresh strawberry.By grass
The certain kind of berries, which is placed in crude antistaling agent, soaks 20min, takes out strawberry, dries.The strawberry dried is deposited in into 2-10 DEG C of environment temperature, phase
It is fresh-keeping to the freezer that humidity is 85-90%.
Embodiment 4
(1) pomelo peel cleaning, drying, crushed 60 mesh sieves, obtain pomelo peel coarse powder.By mass volume ratio 1:8g/mL is by shaddock
Sub- skin coarse powder is placed in the ethanol water of 70%v/v concentration, refluxing extraction 3 times, each 1h, and extracting solution merges, and filtering, must filter
Liquid and filter residue.Decompression filtrate recycling ethanol is simultaneously concentrated into pomelo peel general flavone content in 32mg/mL, is pomelo peel extracting solution A.Press
Mass volume ratio 1:Filter residue is placed in deionized water by 6g/mL, and pH3 is adjusted with the hydrochloric acid of 1mol/L, refluxing extraction 2 times, every time
1.5h, merging filtrate, filtering, filter residue discards, and filtrate decompression is concentrated into pomelo peel pectin content in 12mg/mL, is carried for pomelo peel
Take liquid B.By pomelo peel extracting solution A and B by volume 1:1 mixing, obtains pomelo peel extracting solution.
(2) apple skin cleaning, drying, crushed 80 mesh sieves, obtain apple skin coarse powder.By mass volume ratio 1:12g/mL is by apple
Pericarp coarse powder is placed in the ethanol water of 80%v/v concentration, refluxing extraction 2 times, each 1.5h, and extracting solution merges, and filtering, obtains
Filtrate and filter residue.Decompression filtrate recycling ethanol is simultaneously concentrated into Determination of Polyphenols in 23mg/mL, is apple skin extracting solution A.By quality
Volume ratio 1:Filter residue is placed in deionized water by 10g/mL, and pH3 is adjusted with the hydrochloric acid of 1mol/L, refluxing extraction 2 times, every time
1.5h, merging filtrate, filtering, filter residue discards, and filtrate decompression is concentrated into apple skin pectin content in 13mg/mL, is carried for apple skin
Take liquid B.By apple skin extracting solution A and B by volume 1:1 mixing, obtains apple skin extracting solution.
(3) it is 48% by pomelo peel extracting solution volume fraction v/v shared in crude antistaling agent, apple skin extracting solution exists
Shared volume fraction v/v is 52% in antistaling agent, is mixed to get crude antistaling agent.
(4) eight to ninety percent ripe strawberries are harvested, no disease and pests harm is selected, has no mechanical damage, uniform fresh strawberry.By grass
The certain kind of berries, which is placed in crude antistaling agent, soaks 20min, takes out strawberry, dries.The strawberry dried is deposited in into 2-10 DEG C of environment temperature, phase
It is fresh-keeping to the freezer that humidity is 85-90%.
Embodiment 5
(1) pomelo peel cleaning, drying, crushed 60 mesh sieves, obtain pomelo peel coarse powder.By mass volume ratio 1:12g/mL is by shaddock
Sub- skin coarse powder is placed in the ethanol water of 80%v/v concentration, refluxing extraction 2 times, each 1.5h, and extracting solution merges, and filtering, obtains
Filtrate and filter residue.Decompression filtrate recycling ethanol is simultaneously concentrated into pomelo peel general flavone content in 32mg/mL, is pomelo peel extracting solution A.
By mass volume ratio 1:Filter residue is placed in deionized water by 10g/mL, and pH2 is adjusted with the hydrochloric acid of 1mol/L, refluxing extraction 2 times, often
Secondary 1.5h, merging filtrate, filtering, filter residue discards, and filtrate decompression is concentrated into pomelo peel pectin content in 12mg/mL, is pomelo peel
Extracting solution B.By pomelo peel extracting solution A and B by volume 1:1 mixing, obtains pomelo peel extracting solution.
(2) apple skin cleaning, drying, crushed 80 mesh sieves, obtain apple skin coarse powder.By mass volume ratio 1:8g/mL is by apple
Pericarp coarse powder is placed in the ethanol water of 80%v/v concentration, refluxing extraction 3 times, each 1h, and extracting solution merges, and filtering, must filter
Liquid and filter residue.Decompression filtrate recycling ethanol is simultaneously concentrated into Determination of Polyphenols in 22mg/mL, is apple skin extracting solution A.By mass body
Product ratio 1:Filter residue is placed in deionized water by 6g/mL, adjusts pH3 with the hydrochloric acid of 1mol/L, refluxing extraction 2 times, each 1.5h, is closed
And filtrate, filtering, filter residue discards, and filtrate decompression is concentrated into apple skin pectin content in 12mg/mL, is apple skin extracting solution B.Will
Apple skin extracting solution A and B by volume 1:1 mixing, obtains apple skin extracting solution.
(3) it is 47% by pomelo peel extracting solution volume fraction v/v shared in crude antistaling agent, apple skin extracting solution exists
Shared volume fraction v/v is 53% in antistaling agent, is mixed to get crude antistaling agent.
(4) eight to ninety percent ripe strawberries are harvested, no disease and pests harm is selected, has no mechanical damage, uniform fresh strawberry.By grass
The certain kind of berries, which is placed in crude antistaling agent, soaks 20min, takes out strawberry, dries.The strawberry dried is deposited in into 2-10 DEG C of environment temperature, phase
It is fresh-keeping to the freezer that humidity is 85-90%.
Test example
The crude antistaling agent prepared using 1-3 of the embodiment of the present invention handles strawberry, investigate shelf-life of strawberry, healthy fruit and
Percentage of water loss (20 days) and whether there is peculiar smell, the results are shown in Table 1.
Wherein comparative example 1, under 1 step of embodiment (4) equal conditions, crude antistaling agent processing grass is prepared without the present invention
The certain kind of berries；
Comparative example 2 is under equal conditions, using a kind of composite preservative of strawberry of the prior art
(201510533552.3) step (4) in embodiment 1 is pressed to handle；
Comparative example 3 is the pure pomelo peel extracting solution prepared using the embodiment of the present invention 1, and by step (4) place in embodiment 1
Reason；
Comparative example 4 is the pure apple skin extracting solution prepared using the embodiment of the present invention 1, and by step (4) in embodiment 1
Processing.
Table 1
| Shelf-life (my god) | Healthy fruit (%) | Peculiar smell | Percentage of water loss (%) | |
| Embodiment 1 | 21 | More than 90% | Nothing | Less than 2% |
| Embodiment 2 | 22 | More than 90% | Nothing | Less than 2% |
| Embodiment 3 | 22 | More than 90% | Nothing | Less than 2% |
| Comparative example 1 | 7 | 0 | Nothing | ———— |
| Comparative example 2 | 20 | Less than 80% (20 days) | Have | More than 10% (20 days) |
| Comparative example 3 | 14 | Less than 75% (14 days) | Nothing | More than 10% (14 days) |
| Comparative example 4 | 15 | Less than 75% (15 days) | Nothing | More than 10% (15 days) |
As seen from the results in Table 1,1-3 of the embodiment of the present invention prepare crude antistaling agent processing strawberry after, 2-10 DEG C of temperature,
Relative humidity can reach more than 21 days for the 85-90% shelf-lifves, wherein healthy fruit at 20 days can reach more than 90%, and
And percentage of water loss is less than 2%, completely without peculiar smell.Unprocessed strawberry compared to comparative example 1 extends 14-15 days；And contrast
Although the shelf-life, also the present invention was close after the antistaling agent processing of example 2, not as of the invention, percentage of water loss adds the healthy fruit of 20 days
Height, and due to containing the exhausted cordate houttuynia of radix glycyrrhizae in antistaling agent so that strawberry has obvious peculiar smell；Comparative example 3 and 4 uses single
Pomelo peel extracting solution or single apple skin extracting solution, indices are substantially not as the crude antistaling agent of the present invention；Illustrate this
Invention is synergistic at the same time using pomelo peel and the extracting solution of apple skin, of good preservation effect.
Claims (10)
- A kind of 1. crude antistaling agent for strawberry preservation, it is characterised in that the crude antistaling agent by pomelo peel extracting solution and Apple skin extracting solution forms, and wherein pomelo peel extracting solution volume fraction shared in crude antistaling agent is 40%-55%, apple Skin extracting solution volume fraction shared in antistaling agent is 45%-60%.
- 2. the preparation method of the crude antistaling agent described in a kind of claim 1, it is characterised in that comprise the following steps：(1) pomelo peel is cleaned, dried, pulverized and sieved, obtain pomelo peel coarse powder；Pomelo peel coarse powder is placed in ethanol water, Refluxing extraction, extracting solution filtering, obtains filtrate and filter residue；Decompression filtrate recycling ethanol is simultaneously concentrated into pomelo peel general flavone content and exists 30-35mg/mL, is pomelo peel extracting solution A；Filter residue is placed in deionized water, with salt acid for adjusting pH, refluxing extraction, filtrate is filtered, and filter residue discards, and filtrate decompression is dense Pomelo peel pectin content is reduced in 10-15mg/mL, is pomelo peel extracting solution B；Pomelo peel extracting solution A and B are mixed in equal volume, Obtain pomelo peel extracting solution；(2) apple skin is cleaned, dried, pulverized and sieved, obtain apple skin coarse powder；It is placed in by apple skin coarse powder in ethanol water, Refluxing extraction, extracting solution filtering, obtains filtrate and filter residue；Decompression filtrate recycling ethanol is simultaneously concentrated into Determination of Polyphenols in 20-25mg/ ML, is apple skin extracting solution A；Filter residue is placed in deionized water, with salt acid for adjusting pH, refluxing extraction, filtrate is filtered, and filter residue discards, and filtrate decompression is dense Apple skin pectin content is reduced in 10-15mg/mL, is apple skin extracting solution B；Apple skin extracting solution A and B are mixed in equal volume, Obtain apple skin extracting solution；(3) the apple skin extracting solution that the pomelo peel extracting solution and step (2) obtained step (1) obtains is mixed to get use in proportion In the crude antistaling agent of strawberry preservation.
- 3. preparation method according to claim 2, it is characterised in that step (1) the pomelo peel coarse powder presses quality volume Than for 1:8-12g/mL adds refluxing extraction in the ethanol water that volume fraction is 70-80%.
- 4. preparation method according to claim 2, it is characterised in that the step (1) filter residue presses mass volume ratio For 1:6-10g/mL adds refluxing extraction in deionized water.
- 5. preparation method according to claim 2, it is characterised in that step (2) the apple skin coarse powder presses quality volume Than for 1:8-12g/mL adds refluxing extraction in the ethanol water that volume fraction is 80-90%.
- 6. preparation method according to claim 2, it is characterised in that the step (2) filter residue presses mass volume ratio For 1:6-10g/mL adds refluxing extraction in deionized water.
- 7. preparation method according to claim 2, it is characterised in that step (1) and step (2) described refluxing extraction are 2- 3 times, each 1-1.5h.
- 8. preparation method according to claim 2, it is characterised in that step (1) and step (2) the salt acid for adjusting pH are 2-3。
- 9. the crude antistaling agent described in a kind of claim 1 is used for the preservation method of strawberry preservation, it is characterised in that including as follows Step：1) strawberry is harvested, no disease and pests harm is selected, has no mechanical damage, uniform fresh strawberry；2) strawberry is completely disposed in crude antistaling agent and soaked, taken out strawberry, dry；The strawberry dried is deposited in freezer to protect It is fresh.
- 10. preservation method according to claim 9, it is characterised in that the temperature of step (2) described freezer is 2-10 DEG C, relatively Humidity is 85-90%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711214788.6A CN107927156B (en) | 2017-11-28 | 2017-11-28 | Natural preservative for strawberry preservation and preparation method and preservation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711214788.6A CN107927156B (en) | 2017-11-28 | 2017-11-28 | Natural preservative for strawberry preservation and preparation method and preservation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107927156A true CN107927156A (en) | 2018-04-20 |
| CN107927156B CN107927156B (en) | 2021-03-19 |
Family
ID=61950396
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711214788.6A Active CN107927156B (en) | 2017-11-28 | 2017-11-28 | Natural preservative for strawberry preservation and preparation method and preservation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107927156B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110122557A (en) * | 2019-06-14 | 2019-08-16 | 新疆京洲和合生物科技开发有限公司 | A kind of preservation method of Kuerle delicious pear |
| CN110692898A (en) * | 2019-11-25 | 2020-01-17 | 衡阳市君玲传统食品科技发展有限责任公司 | Rice dumpling preservative and preparation method and preservation method thereof |
| CN110692921A (en) * | 2019-11-25 | 2020-01-17 | 衡阳市君玲传统食品科技发展有限责任公司 | Preserved meat and Chinese chestnut rice dumpling and making method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102766280A (en) * | 2011-09-01 | 2012-11-07 | 上海宇飞金属制品有限公司 | Pectin preservative film, its raw material composition and preparation method thereof |
| CN106889179A (en) * | 2017-02-16 | 2017-06-27 | 佛山市恒南医药科技有限公司 | One Plant Extracts antistaling agent, its preparation method and its application |
-
2017
- 2017-11-28 CN CN201711214788.6A patent/CN107927156B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102766280A (en) * | 2011-09-01 | 2012-11-07 | 上海宇飞金属制品有限公司 | Pectin preservative film, its raw material composition and preparation method thereof |
| CN106889179A (en) * | 2017-02-16 | 2017-06-27 | 佛山市恒南医药科技有限公司 | One Plant Extracts antistaling agent, its preparation method and its application |
Non-Patent Citations (2)
| Title |
|---|
| 张怡，曾绍校，郑宝东: "柚子皮总黄酮提取工艺的而研究", 《中国农学通报》 * |
| 李琪，等人: "微波提取苹果皮中多酚物质的工艺研究", 《中国果菜》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110122557A (en) * | 2019-06-14 | 2019-08-16 | 新疆京洲和合生物科技开发有限公司 | A kind of preservation method of Kuerle delicious pear |
| CN110692898A (en) * | 2019-11-25 | 2020-01-17 | 衡阳市君玲传统食品科技发展有限责任公司 | Rice dumpling preservative and preparation method and preservation method thereof |
| CN110692921A (en) * | 2019-11-25 | 2020-01-17 | 衡阳市君玲传统食品科技发展有限责任公司 | Preserved meat and Chinese chestnut rice dumpling and making method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107927156B (en) | 2021-03-19 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Sharifi-Rad et al. | Plants of the genus Allium as antibacterial agents: From tradition to pharmacy | |
| Bhat et al. | Coriander (Coriandrum sativum L.): Processing, nutritional and functional aspects | |
| KR101234744B1 (en) | Method for Production of Functional Soybean Paste and Functional Soybean Paste Produced by The Same Method | |
| CN104286158B (en) | A kind of honey peach gather before preservative specially | |
| CN104286159A (en) | Fresh keeping method for honey peach | |
| CN101933533A (en) | Plant source preservative and preparation method and application thereof | |
| CN107927156A (en) | A kind of crude antistaling agent for strawberry preservation and preparation method thereof and preservation method | |
| KR101703420B1 (en) | Food additives compositions comprising Cudrania tricuspidata extrat and preparation method thereof | |
| CN102885133A (en) | Dried lily flower preservative as well as preparation method and application thereof | |
| CN109105481A (en) | A kind of preservation method of citrus | |
| KR101478784B1 (en) | Manufacturing method of functional salt using chamaecyparis obtusa | |
| CN108522648A (en) | A kind of fresh-keeping and preserving method of navel orange | |
| KR101349101B1 (en) | Natural germicide composition and methods for manufacturing a natural germicide | |
| CN104430636A (en) | Composition for preventing and treating diseases and insect pests of asparagus | |
| KR101226459B1 (en) | Manufacturing Method of Dried Citrus Unshiu Peel Tea And Citrus Unshiu Peel Tea Using The Same | |
| KR102402908B1 (en) | Grape tea composition and manufacturing method | |
| CN109418388A (en) | A kind of fruit antistaling agent and its application method | |
| CN108617761A (en) | A kind of fresh-keeping and preserving method of Ponkan | |
| CN105284963B (en) | Cock skin fruit tree special plant fungicide and its production method | |
| KR20190073126A (en) | Natural Preservatives and method for extending the shelf life | |
| CN107343532A (en) | A kind of antistaling agent of Han Jia Betel extracts and Prochloraz | |
| CN106436476A (en) | Environment-friendly fruit and vegetable preservative paper | |
| KR101654633B1 (en) | Manufacturing method of Red Allium hookeri using Allium hookeri root and Red Allium hookeri using Allium hookeri root manufactured by the same | |
| CN102823637A (en) | Meat product fresh-keeping agent and meat product fresh-keeping method | |
| KR100872582B1 (en) | Functional fresh-cut yam containing natural spice and method for manufacturing thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20180420 Assignee: Jiangsu Mingjia Construction Engineering Co.,Ltd. Assignor: HUAIYIN INSTITUTE OF TECHNOLOGY Contract record no.: X2021980010817 Denomination of invention: The invention relates to a natural preservative for strawberry preservation, a preparation method and a preservation method thereof Granted publication date: 20210319 License type: Common License Record date: 20211018 |
|
| EE01 | Entry into force of recordation of patent licensing contract |