CN104839726A - Ginseng and radix polygonati officinalis compound health-care buccal tablet and preparation method thereof - Google Patents
Ginseng and radix polygonati officinalis compound health-care buccal tablet and preparation method thereof Download PDFInfo
- Publication number
- CN104839726A CN104839726A CN201510295091.0A CN201510295091A CN104839726A CN 104839726 A CN104839726 A CN 104839726A CN 201510295091 A CN201510295091 A CN 201510295091A CN 104839726 A CN104839726 A CN 104839726A
- Authority
- CN
- China
- Prior art keywords
- ginseng
- freeze
- polygonati officinalis
- radix polygonati
- dried powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 241000208340 Araliaceae Species 0.000 title claims abstract description 60
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 title claims abstract description 59
- 235000003140 Panax quinquefolius Nutrition 0.000 title claims abstract description 59
- 235000008434 ginseng Nutrition 0.000 title claims abstract description 59
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 150000001875 compounds Chemical class 0.000 title claims abstract description 19
- 229940046011 buccal tablet Drugs 0.000 title abstract 4
- 239000006189 buccal tablet Substances 0.000 title abstract 4
- 239000000843 powder Substances 0.000 claims abstract description 32
- 239000002994 raw material Substances 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 8
- 239000007937 lozenge Substances 0.000 claims description 28
- 238000004108 freeze drying Methods 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- 238000010438 heat treatment Methods 0.000 claims description 20
- 238000009413 insulation Methods 0.000 claims description 18
- 238000010009 beating Methods 0.000 claims description 12
- 239000002002 slurry Substances 0.000 claims description 12
- 239000003826 tablet Substances 0.000 claims description 12
- 235000009508 confectionery Nutrition 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- 230000001954 sterilising effect Effects 0.000 claims description 9
- 239000004375 Dextrin Substances 0.000 claims description 8
- 229920001353 Dextrin Polymers 0.000 claims description 8
- 235000006679 Mentha X verticillata Nutrition 0.000 claims description 8
- 235000002899 Mentha suaveolens Nutrition 0.000 claims description 8
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims description 8
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 8
- 229930006000 Sucrose Natural products 0.000 claims description 8
- 239000000084 colloidal system Substances 0.000 claims description 8
- 235000019425 dextrin Nutrition 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 8
- 239000005720 sucrose Substances 0.000 claims description 8
- 238000004140 cleaning Methods 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 230000008020 evaporation Effects 0.000 claims description 6
- 238000001704 evaporation Methods 0.000 claims description 6
- 238000007710 freezing Methods 0.000 claims description 6
- 230000008014 freezing Effects 0.000 claims description 6
- 239000008187 granular material Substances 0.000 claims description 6
- 238000007654 immersion Methods 0.000 claims description 6
- 239000007779 soft material Substances 0.000 claims description 6
- 238000004659 sterilization and disinfection Methods 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 5
- 238000009966 trimming Methods 0.000 claims description 4
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 3
- 240000002948 Ophiopogon intermedius Species 0.000 claims description 3
- 239000000654 additive Substances 0.000 claims description 3
- 230000000996 additive effect Effects 0.000 claims description 3
- 239000000945 filler Substances 0.000 claims description 3
- 238000013467 fragmentation Methods 0.000 claims description 3
- 238000006062 fragmentation reaction Methods 0.000 claims description 3
- 229910052749 magnesium Inorganic materials 0.000 claims description 3
- 239000011777 magnesium Substances 0.000 claims description 3
- 235000012054 meals Nutrition 0.000 claims description 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 238000005498 polishing Methods 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
- 239000011122 softwood Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 238000009777 vacuum freeze-drying Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- 235000013305 food Nutrition 0.000 abstract description 3
- 235000015097 nutrients Nutrition 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 208000000059 Dyspnea Diseases 0.000 description 2
- 206010013975 Dyspnoeas Diseases 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 230000000050 nutritive effect Effects 0.000 description 2
- 238000002791 soaking Methods 0.000 description 2
- 238000009955 starching Methods 0.000 description 2
- 230000001256 tonic effect Effects 0.000 description 2
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 1
- 241000251468 Actinopterygii Species 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 235000002722 Dioscorea batatas Nutrition 0.000 description 1
- 235000006536 Dioscorea esculenta Nutrition 0.000 description 1
- 240000001811 Dioscorea oppositifolia Species 0.000 description 1
- 235000003416 Dioscorea oppositifolia Nutrition 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 206010037660 Pyrexia Diseases 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 235000019636 bitter flavor Nutrition 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005496 eutectics Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229940107131 ginseng root Drugs 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 208000019622 heart disease Diseases 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 208000032839 leukemia Diseases 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000012476 oxidizable substance Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- 231100000241 scar Toxicity 0.000 description 1
- 208000013220 shortness of breath Diseases 0.000 description 1
- 238000005092 sublimation method Methods 0.000 description 1
- 230000005760 tumorsuppression Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention relates to the field of health care food, relates to a ginseng and radix polygonati officinalis compound health-care buccal tablet and a preparation method thereof, and particularly relates to a preparation method of a ginseng and radix polygonati officinalis compound health-care buccal tablet which is prepared from raw materials of ginseng freezing-dried powder and radix polygonati officinalis freezing-dried powder. According to the preparation method, by adopting a ginseng and radix polygonati officinalis processing process, original nutrient characteristics, the taste and the effective function of the raw materials cannot be damaged, and the naturality of ginseng and radix polygonati officinalis compound health-care buccal tablet is ensured.
Description
Technical field
The present invention relates to field of health care food, i.e. a kind of ginseng, radix polygonati officinalis compound health lozenge and preparation method thereof, refer in particular to a kind of with the preparation method of ginseng freeze-dried powder, the radix polygonati officinalis freeze-dried powder ginseng that is raw material, radix polygonati officinalis compound health lozenge.
Background technology
The dry root of araliaceae ginseng plant's ginseng, as rare traditional Chinese medicine tonic, has very long applicating history in China, just it is classified as top grade in Shennong's Herbal.Just start to apply ginseng as tonic as far back as the people Tang Dynasty, have and reinforce vital energy, for the deficiency of vital energy for de-heavily card, have invigorating the lung and benefiting vital QI, for insufficiency of lung-QI,deficiency of lung-QI, dyspnea with shortness of breath, weak breath is weak, has a delicate constitution.
Radix polygonati officinalis belongs to radix polygonati officinalis section herbaceos perennial, and rhizome is medicine-food two-purpose, and radix polygonati officinalis belongs to medicine-food two-purpose herbaceous plant, has unique Nutrition and health function, by people's extensive concern.Radix polygonati officinalis belongs to radix polygonati officinalis section herbaceos perennial, and rhizome is medicine-food two-purpose, the relevant radix polygonati officinalis of kind, eastern radix polygonati officinalis, southern radix polygonati officinalis point, wherein close radix polygonati officinalis be northeast product.Polygonati rhizoma has nourishing yin to moisten dryness, to promote the production of body fluid cough-relieving, control pyreticosis the moon wound, deficient fever, Tumor suppression, delay senility, strengthen immunologic function etc., have certain curative effect to diabetes, heart disease, leukaemia, health food, beverage, electuary can be done, can eat raw, also can stir-fry and eat or boiled dinner with the food such as meat, egg, fish, be deeply by the health care ticbit of consumers.The exploitation of ginseng, radix polygonati officinalis product health products very lacks, and far can not meet the needs in health care market, and exploitation ginseng, radix polygonati officinalis compound lozenge have unique market orientation and active demand.
Summary of the invention
The present invention relates to a kind of ginseng, radix polygonati officinalis compound health lozenge and preparation method thereof.Refer in particular to and a kind of obtain lozenge, this freeze-dried powder technology of preparing with ginseng freeze-dried powder, radix polygonati officinalis freeze-dried powder for raw material, anti-oxidation, not easily bonds, and reduces the loss of active ingredient, instant, farthest plays the beneficial functional of furrow lozenge.
Technical solution of the present invention is: ginseng, radix polygonati officinalis compound health lozenge, it is characterized in that being made up of the raw material of following weight:
(1) 10 ~ 15 parts, ginseng freeze-dried powder, radix polygonati officinalis freeze-dried powder 15 ~ 20 parts.
(2) sucrose 20 ~ 25 parts, 15 ~ 20 parts, dextrin, 15 ~ 20 parts, sweet mellow wine, Mint Essence 1 ~ 3 part.
Preferably, ginseng, radix polygonati officinalis compound health lozenge, it makes 2000 lozenges by the raw material of following weight, the heavy 0.5g of every sheet:
(1) ginseng freeze-dried powder 0.15kg, radix polygonati officinalis freeze-dried powder 0.18kg.
(2) sucrose 0.25kg, dextrin 0.20 kg, sweet mellow wine 0.20kg, Mint Essence 0.01kg.
Ginseng freeze-dried powder, preparation method thereof step is as follows:
(1) sorting cleaning: put into clear water after selecting fresh ginseng, soaks, and repeatedly cleans surperficial earth dirt with clear water.
(2) cut into slices: clean fresh ginseng, slice thickness is 0.2cm ~ 0.4cm, the pure water that limit trimming puts into 1 ~ 2 times soaks.
(3) heat is boiled, is softened: ginseng sheet is together put into jacketed pan together with immersion water, at 98 ~ 102 DEG C, boils 4 ~ 6h, constantly supply the moisture content of evaporation simultaneously when boiling, until ginseng sheet is well-done.
(4) broken, making beating: well-done ginseng sheet is poured in the lump in high speed bruisher be broken into slurries together with being boiled liquid.
(5) defibrination, homogeneous: the slurries of making beating are iterated through colloid mill and refines 3 times, make granular size control at 10 ~ 30 μm, obtains screened stock.
(6) pre-freeze: ginseng screened stock is put into pallet, thickness is 0.5 ~ 0.8cm, puts into freeze dryer pre-freeze, and pre-freezing temperature-25 DEG C ~-30 DEG C, freeze-off time is 3 ~ 5h.
(7) freeze drying:
1. lyophilization, freeze dryer starts vacuum system, pressure in storehouse is evacuated to 30 ~ 50pa, takes slow intensification, with the heating rate of 1 DEG C per hour, be slowly warmed up to-15 ~-20 DEG C, insulation 8 ~ 10h, again with the heating rate of 2 DEG C per hour, be slowly warmed up to-8 DEG C ~-10 DEG C, insulation 5 ~ 6h.Slow intensification can make temperature in whole sublimation process not exceed eutectic point, and ice crystal can not be caused to melt and affect the quality of freeze-dried powder.
2. parsing-desiccation, after lyophilization, with the heating rate of 3 DEG C per hour, is slowly warmed up to 40 ~ 50 DEG C, and insulation 6 ~ 8h, final pressure is 10 ~ 20Pa.
(8) pulverize: in environment temperature≤25 DEG C, relative humidity controls to pulverize below 30%, obtains the ginseng freeze-dried powder of 100 ~ 200 object.
Radix polygonati officinalis method for preparing freeze-dried powder step is as follows:
(1) sorting cleaning: select materials and repeatedly clean surperficial earth dirt with clear water.
(2) stripping and slicing: be cut into the sheet that 0.2cm ~ 0.4cm is thick, the pure water that limit trimming puts into 1 ~ 2 times soaks.
(3) heat is boiled, is softened: together poured in jacketed pan together with immersion water by radix polygonati officinalis sheet, boil 2 ~ 5h, constantly supply the moisture content of evaporation simultaneously when boiling, until the tuber of dwarf lilyturf is well-done at 95 DEG C ~ 100 DEG C.
(4) making beating, fragmentation: well-done radix polygonati officinalis sheet is put into high speed bruisher in the lump together with soak and pulls an oar, be broken into slurries.
(5) defibrination, homogeneous: the slurries of making beating are iterated through colloid mill and refines 3 times, make granular size control at 10 ~ 30 μm, obtains screened stock.
(6) pre-freeze: radix polygonati officinalis screened stock is put into charging tray, thickness is 0.5 ~ 0.8cm, puts into vacuum freeze-drying machine, and pre-freezing temperature-30 DEG C ~-35 DEG C also keeps 3 ~ 6h.
(7) freeze drying
1. lyophilization, freeze dryer starts vacuum system, pressure in storehouse is evacuated to 30 ~ 50pa, takes slow intensification, with the heating rate of 1 DEG C per hour, be slowly warmed up to-20 ~-25 DEG C, insulation 6 ~ 8h, again with the heating rate of 2 DEG C per hour, be slowly warmed up to-10 DEG C ~-12 DEG C, insulation 3 ~ 6h.
2. parsing-desiccation, after lyophilization, with the heating rate of 3 DEG C per hour, is slowly warmed up to 40 ~ 50 DEG C, and insulation 6 ~ 8h, final pressure is 10 ~ 20Pa.
(8) pulverize: in environment temperature≤25 DEG C, relative humidity controls to carry out below 30%.With airslide disintegrating mill, dried material was ground into 100 ~ 200 object radix polygonati officinalis freeze-dried powders.
The preparation method of ginseng, radix polygonati officinalis compound health lozenge, its step is as follows:
(1) raw material preparation: take raw meal ginseng 0.15kg, radix polygonati officinalis 0.16kg.
(2) additive preparation: take sucrose 0.25kg, dextrin 0.20kg, sweet mellow wine 20kg, Mint Essence 0.01kg, mixing, crosses 80 ~ 100 mesh sieves for subsequent use.
(3) mix: fully mix preparing the tablet raw material that contains sieved with filler.
(4) soft material preparation: be that 75% ethanol slowly adds and constantly stirs by the volume fraction prepared, makes neither too hard, nor too soft soft material.
(5) granulate: the softwood made is dropped in oscillating granulator, granulates with 18 mesh sieves.
(6) dry: to make wet granular and load in drip pan, be placed in 60 DEG C of air dry ovens dry, time 120min.1 time is stirred every 30min time dry.
(7) compressing tablet: by adding the magnesium of its quality 0.3% in the particle after oven dry, mix, sends in tablet press machine, being pressed into is heavily circle or the triangle tablet of 0.3 gram ~ 0.5 gram, after polishing, the lozenge of obtained hardness >=13kg, preferred 13kg≤hardness≤32 kg.
(8) sterilization packaging: the lozenge pressed is sent into ultraviolet sterilization room, sterilizing 30min under uviol lamp; Then carry out blister package, sealing is preserved.
Compared with prior art, major advantage of the present invention is:
(1) this product is extremely welcome a kind of product form on market, and technique is simple, and cost is low, substantially increases the added value of product, has great potentiality to be exploited.
(2) raw material sources are convenient, and production equipment is simple, production cost is lower.
(3) dry under vacuo, oxygen is few, and readily oxidizable substance obtains protection.Adopt the Physical Processing of the original nutriment not destroying raw material in process, maintain the taste of raw material and the natural sex of nutritive peculiarity.
(4) freeze drying can solve that look in process becomes, local flavor is lost, nutritive loss and the problem such as local flavor is not good.The maximum beneficial functional playing health care; Mouthfeel is good, production process consumes energy less, cost is low, is applicable to large-scale production, has significant economic benefit and social benefit.
Detailed description of the invention
Embodiment 1
Detailed description of the invention prepared by ginseng freeze-dried powder
(1) sorting cleaning: choosing ginseng root white or yellow-white, without taking out ditch, gas is fragrant, mildly bitter flavor is sweet, free from insect pests, go mouldy, the fresh ginseng of sick scar, putting into clear water after removing impurity refuse, slightly through soaking, repeatedly cleaning surperficial earth dirt with clear water.
(2) cut into slices: clean fresh ginseng, adopt craft or slicer to cut into slices, slice thickness is 0.2cm ~ 0.4cm.While cut, the pure water putting into 1 ~ 2 times soaks, in order to avoid open-assembly time longly causes brown stain in atmosphere.
(3) heat is boiled, is softened: ginseng sheet is together put into jacketed pan together with immersion water, at 98 ~ 102 DEG C, boils 4 ~ 6h, constantly supply the moisture content of evaporation simultaneously when boiling, until ginseng sheet is well-done.
(4) broken, making beating: well-done ginseng sheet is poured in the lump in high speed bruisher be broken into slurries together with being boiled liquid.
(5) defibrination, homogeneous: the slurries of making beating are iterated through colloid mill and refines 3 times, make granular size control at 10 ~ 30 μm, obtains screened stock.
(6) pre-freeze: ginseng screened stock is put into pallet, thickness is 0.5 ~ 0.8cm, pallet is placed on the dividing plate in drying box of freeze dryer, Feng Canghou carries out prefreezing, pre-freezing temperature-25 DEG C ~-30 DEG C, freeze-off time is 3 ~ 5h, moisture in Chinese yam screened stock is fully freezed, guarantees that no liquid exists.
(7) freeze drying
1. lyophilization, freeze dryer starts vacuum system, and pressure in storehouse is evacuated to 30 ~ 50pa, then starts heating schedule and heats.Take slow intensification, with the heating rate of 1 DEG C per hour, be slowly warmed up to-15 ~-20 DEG C, insulation 8 ~ 10h, then with the heating rate of 2 DEG C per hour, be slowly warmed up to-8 DEG C ~-10 DEG C, insulation 5 ~ 6h, the lyophilization stage terminates.
2. parsing-desiccation, after lyophilization, with the heating rate of 3 DEG C per hour, is slowly warmed up to 40 ~ 50 DEG C, insulation 6 ~ 8h, and final pressure is 10 ~ 20Pa, and small part colloid Bound moisture removing in starching, when material temperature is consistent with plate temperature, drying terminates rear outlet.
(8) pulverize: for preventing the ginseng freeze-dried powder crushing operation process moisture absorption from going bad, require in environment temperature≤25 DEG C, relative humidity controls to carry out below 30%.With airslide disintegrating mill, dried material was ground into the ginseng freeze-dried powder of 100 ~ 200 object.
Embodiment 2
Detailed description of the invention prepared by radix polygonati officinalis freeze-dried powder
(1) sorting cleaning: select golden yellow color, the fresh radix polygonati officinalis that the shape that is translucent is of fine quality.Reject disease stem, worm stem, black stem.Slightly through soaking, repeatedly clean surperficial earth dirt with clear water.
(2) stripping and slicing: adopt artificial or slicer to cut into slices, be cut into the sheet that 0.2cm ~ 0.4cm is thick.While cut, the pure water putting into 1 ~ 2 times soaks, in order to avoid open-assembly time longly causes brown stain in atmosphere.
(3) heat is boiled, is softened: together poured in jacketed pan together with immersion water by radix polygonati officinalis sheet, boil 2 ~ 5h, constantly supply the moisture content of evaporation simultaneously when boiling, until the tuber of dwarf lilyturf is well-done at 95 DEG C ~ 100 DEG C.
(4) making beating, fragmentation: well-done radix polygonati officinalis sheet is put into high speed bruisher in the lump together with soak and pulls an oar, be broken into slurries.
(5) defibrination, homogeneous: the slurries of making beating are iterated through colloid mill and refines 3 times, make granular size control at 10 ~ 30 μm, obtains screened stock.
(6) pre-freeze: radix polygonati officinalis screened stock is put into charging tray, thickness is 0.5 ~ 0.8cm, puts into vacuum freeze-drying machine, Feng Canghou first opens refrigeration, pre-freezing temperature-30 DEG C ~-35 DEG C also keeps 3 ~ 6h, moisture in radix polygonati officinalis screened stock is fully freezed, guarantees that no liquid exists.
(7) freeze drying
1. lyophilization, freeze dryer starts vacuum system, and pressure in storehouse is evacuated to 30 ~ 50pa, then starts heating schedule and heats.Take slow intensification, with the heating rate of 1 DEG C per hour, be slowly warmed up to-20 ~-25 DEG C, insulation 6 ~ 8h, then with the heating rate of 2 DEG C per hour, be slowly warmed up to-10 DEG C ~-12 DEG C, insulation 3 ~ 6h, the lyophilization stage terminates.
2. parsing-desiccation, after lyophilization, with the heating rate of 3 DEG C per hour, is slowly warmed up to 40 ~ 50 DEG C, insulation 6 ~ 8h, and final pressure is 10 ~ 20Pa, and small part colloid Bound moisture removing in starching, when material temperature is consistent with plate temperature, drying terminates rear outlet.
(8) pulverize: for preventing the radix polygonati officinalis freeze-dried powder crushing operation process moisture absorption from going bad, require in environment temperature≤25 DEG C, relative humidity controls to carry out below 30%.With airslide disintegrating mill, dried material was ground into 100 ~ 200 object radix polygonati officinalis freeze-dried powders.
Embodiment 3
Ginseng, radix polygonati officinalis compound health lozenge, it makes 2000 lozenges by the raw material of following weight, the heavy 0.5g of every sheet:
(1) ginseng freeze-dried powder 0.15kg, radix polygonati officinalis freeze-dried powder 0.18kg.
(2) sucrose 0.25kg, dextrin 0.20 kg, sweet mellow wine 0.20kg, Mint Essence 0.01kg.
Embodiment 4
Ginseng, radix polygonati officinalis compound health lozenge prepare example
(1) raw material preparation: prepare 2000 lozenges, the heavy 0.5g of every sheet, takes raw meal ginseng 0.15kg, radix polygonati officinalis 0.16kg.
(2) additive preparation: prepare 2000 lozenges, the heavy 0.5g of every sheet, takes sucrose 0.25kg, dextrin 0.20kg, sweet mellow wine 20kg, Mint Essence 0.01kg, puts into multifunctional mixer and mixes full and uniform, cross 80 ~ 100 mesh sieves for subsequent use.
(3) mix: fully mix preparing the tablet raw material that contains sieved with filler.
(4) soft material preparation: be that 75% ethanol slowly adds and constantly stirs by the volume fraction prepared, makes neither too hard, nor too soft soft material.
(5) granulate: the softwood made is dropped in oscillating granulator, granulates with 18 mesh sieves.
(6) dry: make wet granular and load in drip pan, be placed in 60 DEG C of air dry ovens dry, the time is about 120min.1 time is stirred every 30min, to accelerate rate of drying time dry.When dry terminal pinches dry granular with hand, feel is clear-cut, tack-free, firmly one pinches to crumb reluctantly and is advisable.
(7) compressing tablet: add the magnesium of its quality 0.3% by the particle after drying, mix, send in tablet press machine, being pressed into is heavily circle or the triangle tablet of 1 gram, after polishing, the lozenge of obtained hardness >=13kg.
(8) sterilization packaging: the lozenge pressed is sent into ultraviolet sterilization room, sterilizing 30min under uviol lamp.Then carry out blister package, make it lucifuge, sealing is preserved.
Claims (5)
1. ginseng, a radix polygonati officinalis compound health lozenge, is characterized in that being made up of the raw material of following weight:
(1) 10 ~ 15 parts, ginseng freeze-dried powder, radix polygonati officinalis freeze-dried powder 15 ~ 20 parts;
(2) sucrose 20 ~ 25 parts, 15 ~ 20 parts, dextrin, 15 ~ 20 parts, sweet mellow wine, Mint Essence 1 ~ 3 part.
2. according to ginseng according to claim 1, radix polygonati officinalis compound health lozenge, it is characterized in that making 2000 lozenges by the raw material of following weight, the heavy 0.5g of every sheet:
(1) ginseng freeze-dried powder 0.15kg, radix polygonati officinalis freeze-dried powder 0.18kg;
(2) sucrose 0.25kg, dextrin 0.20 kg, sweet mellow wine 0.20kg, Mint Essence 0.01kg.
3., according to the ginseng described in claim 1 or 2, radix polygonati officinalis compound health lozenge, it is characterized in that ginseng freeze-dried powder, preparation method thereof step is as follows:
(1) sorting cleaning: put into clear water after selecting fresh ginseng, soaks, and repeatedly cleans surperficial earth dirt with clear water;
(2) cut into slices: clean fresh ginseng, slice thickness is 0.2cm ~ 0.4cm, the pure water that limit trimming puts into 1 ~ 2 times soaks;
(3) heat is boiled, is softened: ginseng sheet is together put into jacketed pan together with immersion water, at 98 ~ 102 DEG C, boils 4 ~ 6h, constantly supply the moisture content of evaporation simultaneously when boiling, until ginseng sheet is well-done;
(4) broken, making beating: well-done ginseng sheet is poured in the lump in high speed bruisher be broken into slurries together with being boiled liquid;
(5) defibrination, homogeneous: the slurries of making beating are iterated through colloid mill and refines 3 times, make granular size control at 10 ~ 30 μm, obtains screened stock;
(6) pre-freeze: ginseng screened stock is put into pallet, thickness is 0.5 ~ 0.8cm, puts into freeze dryer pre-freeze, pre-freezing temperature-25 DEG C ~-30 DEG C, and freeze-off time is 3 ~ 5h;
(7) freeze drying:
1. lyophilization, freeze dryer starts vacuum system, pressure in storehouse is evacuated to 30 ~ 50pa, takes slow intensification, with the heating rate of 1 DEG C per hour, be slowly warmed up to-15 ~-20 DEG C, insulation 8 ~ 10h, again with the heating rate of 2 DEG C per hour, be slowly warmed up to-8 DEG C ~-10 DEG C, insulation 5 ~ 6h;
2. parsing-desiccation, after lyophilization, with the heating rate of 3 DEG C per hour, is slowly warmed up to 40 ~ 50 DEG C, insulation 6 ~ 8h, and final pressure is 10 ~ 20Pa;
(8) pulverize: in environment temperature≤25 DEG C, relative humidity controls to pulverize below 30%, obtains the ginseng freeze-dried powder of 100 ~ 200 object.
4., according to the ginseng described in claim 1 or 2, radix polygonati officinalis compound health lozenge, it is characterized in that radix polygonati officinalis method for preparing freeze-dried powder step is as follows:
(1) sorting cleaning: select materials and repeatedly clean surperficial earth dirt with clear water;
(2) stripping and slicing: be cut into the sheet that 0.2cm ~ 0.4cm is thick, the pure water that limit trimming puts into 1 ~ 2 times soaks;
(3) heat is boiled, is softened: together poured in jacketed pan together with immersion water by radix polygonati officinalis sheet, boil 2 ~ 5h, constantly supply the moisture content of evaporation simultaneously when boiling, until the tuber of dwarf lilyturf is well-done at 95 DEG C ~ 100 DEG C;
(4) making beating, fragmentation: well-done radix polygonati officinalis sheet is put into high speed bruisher in the lump together with soak and pulls an oar, be broken into slurries;
(5) defibrination, homogeneous: the slurries of making beating are iterated through colloid mill and refines 3 times, make granular size control at 10 ~ 30 μm, obtains screened stock;
(6) pre-freeze: radix polygonati officinalis screened stock is put into charging tray, thickness is 0.5 ~ 0.8cm, puts into vacuum freeze-drying machine, and pre-freezing temperature-30 DEG C ~-35 DEG C also keeps 3 ~ 6h;
(7) freeze drying
1. lyophilization, freeze dryer starts vacuum system, pressure in storehouse is evacuated to 30 ~ 50pa, takes slow intensification, with the heating rate of 1 DEG C per hour, be slowly warmed up to-20 ~-25 DEG C, insulation 6 ~ 8h, again with the heating rate of 2 DEG C per hour, be slowly warmed up to-10 DEG C ~-12 DEG C, insulation 3 ~ 6h;
2. parsing-desiccation, after lyophilization, with the heating rate of 3 DEG C per hour, is slowly warmed up to 40 ~ 50 DEG C, insulation 6 ~ 8h, and final pressure is 10 ~ 20Pa;
(8) pulverize: in environment temperature≤25 DEG C, relative humidity controls to carry out below 30%, with airslide disintegrating mill, dried material is ground into 100 ~ 200 object radix polygonati officinalis freeze-dried powders.
5. a preparation method for ginseng as claimed in claim 2, radix polygonati officinalis compound health lozenge, is characterized in that step is as follows:
(1) raw material preparation: take raw meal ginseng 0.15kg, radix polygonati officinalis 0.16kg;
(2) additive preparation: take sucrose 0.25kg, dextrin 0.20kg, sweet mellow wine 20kg, Mint Essence 0.01kg, mixing, crosses 80 ~ 100 mesh sieves for subsequent use;
(3) mix: fully mix preparing the tablet raw material that contains sieved with filler;
(4) soft material preparation: be that 75% ethanol slowly adds and constantly stirs by the volume fraction prepared, makes neither too hard, nor too soft soft material;
(5) granulate: the softwood made is dropped in oscillating granulator, granulates with 18 mesh sieves;
It is (6) dry: to make wet granular and load in drip pan, be placed in 60 DEG C of air dry ovens dry, time 120min,
1 time is stirred every 30min time dry;
(7) compressing tablet: add the magnesium of its quality 0.3% by the particle after drying, mix, send in tablet press machine, being pressed into is heavily circle or the triangle tablet of 0.3 gram ~ 0.5 gram, after polishing, the lozenge of obtained hardness >=13kg;
(8) sterilization packaging: the lozenge pressed is sent into ultraviolet sterilization room, sterilizing 30min under uviol lamp; Then carry out blister package, sealing is preserved.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510295091.0A CN104839726A (en) | 2015-06-03 | 2015-06-03 | Ginseng and radix polygonati officinalis compound health-care buccal tablet and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510295091.0A CN104839726A (en) | 2015-06-03 | 2015-06-03 | Ginseng and radix polygonati officinalis compound health-care buccal tablet and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104839726A true CN104839726A (en) | 2015-08-19 |
Family
ID=53840021
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510295091.0A Pending CN104839726A (en) | 2015-06-03 | 2015-06-03 | Ginseng and radix polygonati officinalis compound health-care buccal tablet and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104839726A (en) |
-
2015
- 2015-06-03 CN CN201510295091.0A patent/CN104839726A/en active Pending
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102613500B (en) | Solid ginger beverage | |
| CN103989141A (en) | Healthy chilli sauce and preparation method thereof | |
| CN104856034A (en) | Ginseng and lily composite health buccal tablet and preparation method thereof | |
| CN103610203A (en) | Method for preparing instant actinidia arguta powder through vacuum freeze drying | |
| CN104605119A (en) | Lotus-leaf-scented high-calcium soft candy and preparation method thereof | |
| CN104621324A (en) | Corn-flavor high-calcium soft sweet and preparation method thereof | |
| CN106473110A (en) | A kind of freeze-drying instant tremella | |
| CN104839807B (en) | A kind of processing technology of the compound soup stock of instant edible mushroom | |
| CN105394277A (en) | Ginger-jujube tea | |
| CN109303301A (en) | A kind of instant jujube tremella lotus seeds cake and preparation method thereof | |
| CN104286757A (en) | Heat-clearing pear powder and preparation method thereof | |
| CN104839723A (en) | Ginseng and radix ophiopogonis composite health buccal tablet and preparation method thereof | |
| CN104839722A (en) | Ginseng and Chinese yam compound healthcare buccal tablet and preparation method thereof | |
| CN104055022A (en) | Teenager brain strengthening flour and preparation method thereof | |
| CN104839724A (en) | Ginseng and red date compound health-care buccal tablet and preparation method thereof | |
| CN107396962A (en) | A kind of drying means of Chinese yam slices | |
| CN110447877A (en) | A kind of functional edible mushroom toppings and preparation method thereof | |
| CN106072542A (en) | A kind of Millettia Speciosa decoction pieces and preparation method thereof | |
| CN101611860A (en) | The method that the utilization Freeze Drying Technique is produced edible fungi instant soup blend | |
| CN105029150B (en) | One kind is puffing to bake peony pollen and preparation method thereof | |
| CN104957605A (en) | Ginseng and Chinese wolfberry fruit compound health-care buccal tablet and preparation method thereof | |
| CN104839726A (en) | Ginseng and radix polygonati officinalis compound health-care buccal tablet and preparation method thereof | |
| CN104106647A (en) | Sauced donkey meat tea flavor bean curd and preparation method thereof | |
| CN107080027A (en) | The processing method of Moringa Pueravia flower tea | |
| CN106376700A (en) | Preparation method of mussel-polygonatum odoratum compound pressed candy |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| EXSB | Decision made by sipo to initiate substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150819 |
|
| RJ01 | Rejection of invention patent application after publication |