CN104856034A - Ginseng and lily composite health buccal tablet and preparation method thereof - Google Patents
Ginseng and lily composite health buccal tablet and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a ginseng and lily composite health buccal tablet and a preparation method thereof, in particular to a ginseng and lily composite health buccal tablet prepared by taking ginseng as a raw material and taking lyophilized ginseng powder with a health effect obtained by freezing, drying and crushing, added lyophilized lily freeze-dried powder with a health effect and the like as main raw materials and a preparation method thereof. A ginseng and lily processing process does not damage the original nutrition characteristics, the taste and the effective functions of the raw materials, so that the natural characteristics of the buccal tablet are ensured.
Description
Technical field
The present invention relates to field of health care food, i.e. a kind of ginseng, lily compound health lozenge and preparation method thereof, refer in particular to a kind of with the preparation method of ginseng freeze-dried powder, the lily freeze-dried powder ginseng that is raw material, lily compound health lozenge.
Background technology
The dry root of araliaceae ginseng plant's ginseng, as rare traditional Chinese medicine tonic, has very long applicating history in China, just it is classified as top grade in Shennong's Herbal.Just start to apply ginseng as tonic as far back as the people Tang Dynasty, have and reinforce vital energy, for the deficiency of vital energy for de-heavily card, have invigorating the lung and benefiting vital QI, for insufficiency of lung-QI,deficiency of lung-QI, dyspnea with shortness of breath, weak breath is weak, has a delicate constitution.
One of medicinal and edible plants that lily or the Ministry of Public Health of China promulgate in the first batch, lily is perennial root plant, and take bulb as food, meat plumpness, multi-disc, color and luster is pure white, taste is sweet, delicate fragrance, slightly bitter taste.One of medicinal and edible plants that lily or the Ministry of Public Health of China promulgate in the first batch, its bulb contains starch, protein, fat and calcium, phosphorus, iron and the nutritional labeling such as vitamin B1, B2, C.Have relieving cough and reducing sputum, hypnosis is calmed the nerves, and antifatigue and resist oxygen lack, to be flatly slightly cold, and has clearing away the heart fire and tranquillizing to moisten the lung and relieve the cough, diuresis, raises peripheral leukocytes, protection gastric mucosa and suppress the effects such as delayed hypersensitivity reaction.The exploitation of ginseng, lily product health products very lacks, and far can not meet the needs in health care market, is that ginseng, the exploitation of lily compound health lozenge that main additive is produced has great importance, has unique market orientation and active demand with lily.
Summary of the invention
The present invention relates to a kind of ginseng, lily compound health lozenge and preparation method thereof.Refer in particular to and a kind of obtain lozenge, this freeze-dried powder technology of preparing with ginseng freeze-dried powder, lily freeze-dried powder for raw material, anti-oxidation, not easily bonds, and reduces the loss of active ingredient, instant, farthest plays the beneficial functional of furrow lozenge.
Technical solution of the present invention is: a kind of ginseng, lily compound health lozenge, is made up of the raw material of following weight:
(1) ginseng freeze-dried powder 10-15 part, lily freeze-dried powder 15-20 part.
(2) sucrose 20-25 part, dextrin 15-20 part, sweet mellow wine 15-20 part, Mint Essence 1-3 part.
Preferably ginseng, lily compound health lozenge, make 2000 lozenges by the raw material of following weight, the heavy 0.5g of every sheet:
(1) ginseng freeze-dried powder 0.15kg, lily freeze-dried powder 0.18kg.
(2) sucrose 0.23kg, dextrin 0.20 kg, sweet mellow wine 0.20kg, Mint Essence 0.01kg.
Ginseng freeze-dried powder, preparation method thereof step is as follows:
(1) sorting cleaning: put into clear water after selecting fresh ginseng, soaks, and repeatedly cleans surperficial earth dirt with clear water.
(2) cut into slices: clean fresh ginseng, slice thickness is 0.2cm ~ 0.4cm, the pure water that limit trimming puts into 1 ~ 2 times soaks.
(3) heat is boiled, is softened: ginseng sheet is together put into jacketed pan together with immersion water, at 98 ~ 102 DEG C, boils 4 ~ 6h, constantly supply the moisture content of evaporation simultaneously when boiling, until ginseng sheet is well-done.
(4) broken, making beating: well-done ginseng sheet is poured in the lump in high speed bruisher be broken into slurries together with being boiled liquid.
(5) defibrination, homogeneous: the slurries of making beating are iterated through colloid mill and refines 3 times, make granular size control at 10 ~ 30 μm, obtains screened stock.
(6) pre-freeze: ginseng screened stock is put into pallet, thickness is 0.5 ~ 0.8cm, puts into freeze dryer pre-freeze, and pre-freezing temperature-25 DEG C ~-30 DEG C, freeze-off time is 3 ~ 5h.
(7) freeze drying.
1. lyophilization, freeze dryer starts vacuum system, pressure in storehouse is evacuated to 30 ~ 50pa, takes slow intensification, with the heating rate of 1 DEG C per hour, be slowly warmed up to-15 ~-20 DEG C, insulation 8 ~ 10h, again with the heating rate of 2 DEG C per hour, be slowly warmed up to-8 DEG C ~-10 DEG C, insulation 5 ~ 6h.Slow intensification can make temperature in whole sublimation process not exceed eutectic point, and ice crystal can not be caused to melt and affect the quality of freeze-dried powder.
2. parsing-desiccation, after lyophilization, with the heating rate of 3 DEG C per hour, is slowly warmed up to 40 ~ 50 DEG C, and insulation 6 ~ 8h, final pressure is 10 ~ 20Pa.
(8) pulverize: in environment temperature≤25 DEG C, relative humidity controls to pulverize below 30%, obtains the ginseng freeze-dried powder of 100 ~ 200 object.
Lily method for preparing freeze-dried powder step is as follows:
(1) select materials.
(2) burst cleaning: with cutter by near for lily bulb portion crosscut, clear water rinses, and pulls the rear pure water putting into rapidly 1 ~ 2 times out and soaks.
(3) heat is boiled, is softened: together poured in jacketed pan together with immersion water by lily slice, boil 0.5 ~ 1h, until lily is well-done at 95 DEG C ~ 100 DEG C.
(3) broken, making beating: lily slice is put into high speed bruisher in the lump pull an oar together with being boiled liquid, is broken into slurries.
(5) defibrination, homogeneous: the slurries of making beating are iterated through colloid mill and refines 3 times, make granular size control at 10 ~ 30 μm, obtains screened stock.
(5) pre-freeze: lily screened stock is put into pallet, thickness is 0.5 ~ 0.8cm, is placed in pre-freeze in freeze dryer, pre-freezing temperature-25 DEG C ~-30 DEG C, and freeze-off time is 8 ~ 10h.
(6) freeze drying: 1. lyophilization, freeze dryer starts vacuum system, pressure in storehouse is evacuated to 10 ~ 12pa, take slow intensification, with the heating rate of 1 DEG C per hour, be slowly warmed up to-20 DEG C ~-25 DEG C, insulation 5 ~ 6h, again with the heating rate of 2 DEG C per hour, be slowly warmed up to-8 DEG C ~-10 DEG C, insulation 6 ~ 8h.
2. parsing-desiccation, after lyophilization, with the heating rate of 3 DEG C per hour, is slowly warmed up to 20 ~ 30 DEG C, and be incubated 6 ~ 10 hours, final pressure is 8 ~ 15Pa.
(7) pulverize: in environment temperature≤25 DEG C, relative humidity controls to carry out below 30%, with airslide disintegrating mill, dried material is ground into 100 ~ 200 object lily freeze-dried powders.
The preparation method of ginseng, lily compound health lozenge, its step is as follows:
(1) raw material preparation: get ginseng freeze-dried powder 0.15kg, lily freeze-dried powder 0.18kg.
(2) additive preparation: get sucrose 0.23kg, dextrin 0.20 kg, sweet mellow wine 0.20kg, Mint Essence 0.01kg mix, mistake 80 ~ 100 mesh sieves are for subsequent use.
(3) mix: fully mix preparing the tablet raw material that contains sieved with filler.
(4) soft material preparation: be that 75% ethanol slowly adds and constantly stirs by the volume fraction prepared, makes neither too hard, nor too soft soft material.
(5) granulate: the softwood made is dropped in granulator, granulates with 18 mesh sieves.
(6) dry: to make wet granular and load in drip pan, be placed in 60 DEG C of air dry ovens dry, time 120min; 1 time is stirred every 30min time dry.
(7) compressing tablet: by adding the magnesium of its quality 0.3% in the particle after oven dry, mix, sends in tablet press machine, being pressed into is heavily circle or the triangle tablet of 0.3 gram ~ 0.5 gram, after polishing, the lozenge of obtained hardness >=13kg, preferred 13kg≤hardness≤32 kg.
(8) sterilization packaging: the lozenge pressed is sent into ultraviolet sterilization room, and sterilizing 30min under uviol lamp, then carries out blister package, and sealing is preserved.
Compared with prior art, major advantage of the present invention is:
(1) this product is extremely welcome a kind of product form on market, and technique is simple, and cost is low, substantially increases the added value of product, has great potentiality to be exploited.
(2) raw material sources are convenient, and production equipment is simple, production cost is lower.
(3) dry under vacuo, oxygen is few, and readily oxidizable substance obtains protection.Adopt the Physical Processing of the original nutriment not destroying raw material in process, maintain the taste of raw material and the natural sex of nutritive peculiarity.
(4) freeze drying can solve that look in process becomes, local flavor is lost, nutritive loss and the problem such as local flavor is not good.The maximum beneficial functional playing health care; Mouthfeel is good, production process consumes energy less, cost is low, is applicable to large-scale production, has significant economic benefit and social benefit.
Detailed description of the invention
Embodiment 1
Detailed description of the invention prepared by ginseng freeze-dried powder
(1) sorting cleaning: choosing ginseng root white or yellow-white, without taking out ditch, gas is fragrant, mildly bitter flavor is sweet, free from insect pests, go mouldy, the fresh ginseng of sick scar, putting into clear water after removing impurity refuse, slightly through soaking, repeatedly cleaning surperficial earth dirt with clear water.
(2) cut into slices: clean fresh ginseng, adopt craft or slicer to cut into slices, slice thickness is 0.2cm ~ 0.4cm.。While cut, the pure water putting into 1 ~ 2 times soaks, in order to avoid open-assembly time longly causes brown stain in atmosphere.
(3) heat is boiled, is softened: ginseng sheet is together put into jacketed pan together with immersion water, at 98 ~ 102 DEG C, boils 4 ~ 6h, constantly supply the moisture content of evaporation simultaneously when boiling, until ginseng sheet is well-done.
(4) broken, making beating: well-done ginseng sheet is poured in the lump in high speed bruisher be broken into slurries together with being boiled liquid.
(5) defibrination, homogeneous: the slurries of making beating are iterated through colloid mill and refines 3 times, make granular size control at 10 ~ 30 μm, obtains screened stock.
(6) pre-freeze: ginseng screened stock is put into pallet, thickness is 0.5 ~ 0.8cm, pallet is placed on the dividing plate in drying box of freeze dryer, Feng Canghou carries out prefreezing, pre-freezing temperature-25 DEG C ~-30 DEG C, freeze-off time is 3 ~ 5h, moisture in Chinese yam screened stock is fully freezed, guarantees that no liquid exists.
(7) freeze drying
1. lyophilization
Freeze dryer starts vacuum system, and pressure in storehouse is evacuated to 30 ~ 50pa, then starts heating schedule and heats.Take slow intensification, with the heating rate of 1 DEG C per hour, be slowly warmed up to-15 ~-20 DEG C, insulation 8 ~ 10h, then with the heating rate of 2 DEG C per hour, be slowly warmed up to-8 DEG C ~-10 DEG C, insulation 5 ~ 6h, the lyophilization stage terminates.
2. parsing-desiccation
After lyophilization, with the heating rate of 3 DEG C per hour, be slowly warmed up to 40 ~ 50 DEG C, insulation 6 ~ 8h, final pressure is 10 ~ 20Pa, and small part colloid Bound moisture removing in starching, when material temperature is consistent with plate temperature, drying terminates rear outlet.
(8) pulverize: for preventing the ginseng freeze-dried powder crushing operation process moisture absorption from going bad, require in environment temperature≤25 DEG C, relative humidity controls to carry out below 30%.With airslide disintegrating mill, dried material was ground into the ginseng freeze-dried powder of 100 ~ 200 object.
Embodiment 2
Detailed description of the invention prepared by lily freeze-dried powder
(1) select materials: choose that color and luster is good, strong flavor, rotten of removing, stem tabernaemontanus bulrush and other impurity fresh lily bulb of fine quality.
(2) burst cleaning: after selecting, with cutter by near for lily bulb portion crosscut, make scale naturally separately after with clear water flushing to epidermis without dirt, pull out after washing.And the pure water putting into rapidly 1 ~ 2 times soaks, in order to avoid open-assembly time longly causes brown stain in atmosphere.
(3) heat is boiled, is softened: together poured in jacketed pan together with immersion water by lily slice, boil 0.5 ~ 1h, constantly supply the moisture content of evaporation simultaneously when boiling, until lily is well-done at 95 DEG C ~ 100 DEG C.
(3) broken, making beating: lily slice is put into high speed bruisher in the lump pull an oar together with being boiled liquid, is broken into slurries.
(5) defibrination, homogeneous: the slurries of making beating are iterated through colloid mill and refines 3 times, make granular size control at 10 ~ 30 μm, obtains screened stock.
(5) pre-freeze: lily screened stock is put into pallet, thickness is 0.5 ~ 0.8cm, pallet is placed on the dividing plate in drying box of freeze dryer, Feng Canghou carries out prefreezing, pre-freezing temperature-25 DEG C ~-30 DEG C, freeze-off time is 8 ~ 10h, moisture in lily screened stock is fully freezed, guarantees that no liquid exists.
(6) freeze drying
1. lyophilization, freeze dryer starts vacuum system, and pressure in storehouse is evacuated to 10 ~ 12pa, then starts heating schedule and heats.Take slow intensification, with the heating rate of 1 DEG C per hour, be slowly warmed up to-20 DEG C ~-25 DEG C, insulation 5 ~ 6h, then with the heating rate of 2 DEG C per hour, be slowly warmed up to-8 DEG C ~-10 DEG C, insulation 6 ~ 8h, the lyophilization stage terminates.
2. parsing-desiccation, after lyophilization, with the heating rate of 3 DEG C per hour, is slowly warmed up to 20 ~ 30 DEG C, and be incubated 6 ~ 10 hours, final pressure is 8 ~ 15Pa, and small part colloid Bound moisture removing in starching, when material temperature is consistent with plate temperature, drying terminates rear outlet.
(7) pulverize: for preventing the lily freeze-dried powder crushing operation process moisture absorption from going bad, require in environment temperature≤25 DEG C, relative humidity controls to carry out below 30%.With airslide disintegrating mill, dried material was ground into 100 ~ 200 object lily freeze-dried powders.
Embodiment 3
Ginseng, lily compound health lozenge, make 2000 lozenges by the raw material of following weight, the heavy 0.5g of every sheet:
(1) ginseng freeze-dried powder 0.15kg, lily freeze-dried powder 0.18kg.
(2) sucrose 0.23kg, dextrin 0.20 kg, sweet mellow wine 0.20kg, Mint Essence 0.01kg.
Embodiment 4
Ginseng, lily compound health lozenge prepare example
(1) raw material preparation: prepare 2000 lozenges, the heavy 0.5g of every sheet, takes ginseng pulverate 0.15kg, lily root flour 0.18kg
(2) additive preparation: prepare 2000 lozenges, the heavy 0.5g of every sheet, take sucrose 0.23kg, dextrin 0.20 kg, sweet mellow wine 0.20kg, that Mint Essence 0.01kg puts into multifunctional mixer mixing is full and uniform, mistake 80 ~ 100 mesh sieves are for subsequent use.
(3) mix: fully mix preparing the tablet raw material that contains sieved with filler
(4) soft material preparation: be that 75% ethanol slowly adds and constantly stirs by the volume fraction prepared, makes neither too hard, nor too soft soft material.
(5) granulate: the softwood made is dropped in oscillating granulator, granulates with 18 mesh sieves.
(6) dry: make wet granular and load in drip pan, be placed in 60 DEG C of air dry ovens dry, the time is about 120min.1 time is stirred every 30min, to accelerate rate of drying time dry.When dry terminal pinches dry granular with hand, feel is clear-cut, tack-free, firmly one pinches to crumb reluctantly and is advisable,
(7) compressing tablet: add the magnesium of its quality 0.3% by the particle after drying, mix, send in tablet press machine, being pressed into is heavily circle or the triangle tablet of 0.5 gram, after polishing, the lozenge of obtained hardness >=13kg.
(8) sterilization packaging: the lozenge pressed is sent into ultraviolet sterilization room, sterilizing 30min under uviol lamp.Then carry out blister package, make it lucifuge, sealing is preserved.
Claims (5)
1. ginseng, a lily compound health lozenge, is characterized in that being made up of the raw material of following weight:
(1) 10 ~ 15 parts, ginseng freeze-dried powder, lily freeze-dried powder 15 ~ 20 parts;
(2) sucrose 20 ~ 25 parts, 15 ~ 20 parts, dextrin, 15 ~ 20 parts, sweet mellow wine, Mint Essence 1 ~ 3 part.
2. according to ginseng according to claim 1, lily compound health lozenge, it is characterized in that making 2000 lozenges by the raw material of following weight, the heavy 0.5g of every sheet:
(1) ginseng freeze-dried powder 0.15kg, lily freeze-dried powder 0.18kg;
(2) sucrose 0.23kg, dextrin 0.20 kg, sweet mellow wine 0.20kg, Mint Essence 0.01kg.
3., according to the ginseng described in claim 1 or 2, lily compound health lozenge, it is characterized in that ginseng freeze-dried powder, preparation method thereof step is as follows:
(1) sorting cleaning: put into clear water after selecting fresh ginseng, soaks, and repeatedly cleans surperficial earth dirt with clear water;
(2) cut into slices: clean fresh ginseng, slice thickness is 0.2cm ~ 0.4cm, the pure water that limit trimming puts into 1 ~ 2 times soaks;
(3) heat is boiled, is softened: ginseng sheet is together put into jacketed pan together with immersion water, at 98 ~ 102 DEG C, boils 4 ~ 6h, constantly supply the moisture content of evaporation simultaneously when boiling, until ginseng sheet is well-done;
(4) broken, making beating: well-done ginseng sheet is poured in the lump in high speed bruisher be broken into slurries together with being boiled liquid;
(5) defibrination, homogeneous: the slurries of making beating are iterated through colloid mill and refines 3 times, make granular size control at 10 ~ 30 μm, obtains screened stock;
(6) pre-freeze: ginseng screened stock is put into pallet, thickness is 0.5 ~ 0.8cm, puts into freeze dryer pre-freeze, pre-freezing temperature-25 DEG C ~-30 DEG C, and freeze-off time is 3 ~ 5h;
(7) freeze drying:
1. lyophilization, freeze dryer starts vacuum system, pressure in storehouse is evacuated to 30 ~ 50pa, takes slow intensification, with the heating rate of 1 DEG C per hour, be slowly warmed up to-15 ~-20 DEG C, insulation 8 ~ 10h, again with the heating rate of 2 DEG C per hour, be slowly warmed up to-8 DEG C ~-10 DEG C, insulation 5 ~ 6h;
2. parsing-desiccation, after lyophilization, with the heating rate of 3 DEG C per hour, is slowly warmed up to 40 ~ 50 DEG C, insulation 6 ~ 8h, and final pressure is 10 ~ 20Pa;
(8) pulverize: in environment temperature≤25 DEG C, relative humidity controls to pulverize below 30%, obtains the ginseng freeze-dried powder of 100 ~ 200 object.
4., according to the ginseng described in claim 1 or 2, lily compound health lozenge, it is characterized in that lily method for preparing freeze-dried powder step is as follows:
(1) select materials;
(2) burst cleaning: with cutter by near for lily bulb portion crosscut, clear water rinses, and pulls the rear pure water putting into rapidly 1 ~ 2 times out and soaks;
(3) heat is boiled, is softened: together poured in jacketed pan together with immersion water by lily slice, boil 0.5 ~ 1h, until lily is well-done at 95 DEG C ~ 100 DEG C;
(3) broken, making beating: lily slice is put into high speed bruisher in the lump pull an oar together with being boiled liquid, is broken into slurries;
(5) defibrination, homogeneous: the slurries of making beating are iterated through colloid mill and refines 3 times, make granular size control at 10 ~ 30 μm, obtains screened stock;
(5) pre-freeze: lily screened stock is put into pallet, thickness is 0.5 ~ 0.8cm, is placed in pre-freeze in freeze dryer, pre-freezing temperature-25 DEG C ~-30 DEG C, and freeze-off time is 8 ~ 10h;
(6) freeze drying: 1. lyophilization, freeze dryer starts vacuum system, pressure in storehouse is evacuated to 10 ~ 12pa, take slow intensification, with the heating rate of 1 DEG C per hour, be slowly warmed up to-20 DEG C ~-25 DEG C, insulation 5 ~ 6h, again with the heating rate of 2 DEG C per hour, be slowly warmed up to-8 DEG C ~-10 DEG C, insulation 6 ~ 8h;
2. parsing-desiccation, after lyophilization, with the heating rate of 3 DEG C per hour, is slowly warmed up to 20 ~ 30 DEG C, and be incubated 6 ~ 10 hours, final pressure is 8 ~ 15Pa;
(7) pulverize: in environment temperature≤25 DEG C, relative humidity controls to carry out below 30%, with airslide disintegrating mill, dried material is ground into 100 ~ 200 object lily freeze-dried powders.
5. a preparation method for ginseng as claimed in claim 2, lily compound health lozenge, is characterized in that step is as follows:
(1) raw material preparation: get ginseng freeze-dried powder 0.15kg, lily freeze-dried powder 0.18kg;
(2) additive preparation: get sucrose 0.23kg, dextrin 0.20 kg, sweet mellow wine 0.20kg, Mint Essence 0.01kg mix, mistake 80 ~ 100 mesh sieves are for subsequent use;
(3) mix: fully mix preparing the tablet raw material that contains sieved with filler;
(4) soft material preparation: be that 75% ethanol slowly adds and constantly stirs by the volume fraction prepared, makes neither too hard, nor too soft soft material;
(5) granulate: the softwood made is dropped in granulator, granulates with 18 mesh sieves;
(6) dry: to make wet granular and load in drip pan, be placed in 60 DEG C of air dry ovens dry, time 120min; 1 time is stirred every 30min time dry;
(7) compressing tablet: add the magnesium of its quality 0.3% by the particle after drying, mix, send in tablet press machine, being pressed into is heavily circle or the triangle tablet of 0.3 gram ~ 0.5 gram, after polishing, the lozenge of obtained hardness >=13kg;
(8) sterilization packaging: the lozenge pressed is sent into ultraviolet sterilization room, and sterilizing 30min under uviol lamp, then carries out blister package, and sealing is preserved.
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CN111184210A (en) * | 2018-11-15 | 2020-05-22 | 卢中奇 | Ginseng and lily compound health-care buccal tablet and preparation method thereof |
CN111248437A (en) * | 2020-03-21 | 2020-06-09 | 柳州昕霖科技有限公司 | Preparation method of lily lyophilized powder |
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WO2020052004A1 (en) * | 2018-09-11 | 2020-03-19 | 朱秀青 | Medicinal material mashing apparatus for producing healthcare ointment |
WO2020052005A1 (en) * | 2018-09-11 | 2020-03-19 | 朱秀青 | Medicinal material mashing apparatus |
CN111184210A (en) * | 2018-11-15 | 2020-05-22 | 卢中奇 | Ginseng and lily compound health-care buccal tablet and preparation method thereof |
CN111248437A (en) * | 2020-03-21 | 2020-06-09 | 柳州昕霖科技有限公司 | Preparation method of lily lyophilized powder |
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