CN104752118A - Plasma processing chamber and manufacturing method of electrostatic chuck of plasma processing chamber - Google Patents

Plasma processing chamber and manufacturing method of electrostatic chuck of plasma processing chamber Download PDF

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Publication number
CN104752118A
CN104752118A CN201310726396.3A CN201310726396A CN104752118A CN 104752118 A CN104752118 A CN 104752118A CN 201310726396 A CN201310726396 A CN 201310726396A CN 104752118 A CN104752118 A CN 104752118A
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China
Prior art keywords
manufacture method
metal contact
contact wires
electrostatic chuck
ceramic bases
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CN201310726396.3A
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Chinese (zh)
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CN104752118B (en
Inventor
贺小明
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Medium and Micro Semiconductor Equipment (Shanghai) Co., Ltd.
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Advanced Micro Fabrication Equipment Inc Shanghai
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Priority to CN201310726396.3A priority Critical patent/CN104752118B/en
Priority to TW103145166A priority patent/TWI574294B/en
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J9/00Apparatus or processes specially adapted for the manufacture, installation, removal, maintenance of electric discharge tubes, discharge lamps, or parts thereof; Recovery of material from discharge tubes or lamps
    • H01J9/24Manufacture or joining of vessels, leading-in conductors or bases
    • H01J9/245Manufacture or joining of vessels, leading-in conductors or bases specially adapted for gas discharge tubes or lamps

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  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Container, Conveyance, Adherence, Positioning, Of Wafer (AREA)
  • Drying Of Semiconductors (AREA)

Abstract

The invention provides a plasma processing chamber and a manufacturing method of an electrostatic chuck of the plasma processing chamber. The manufacturing method comprises the following steps of providing a ceramic substrate, forming a plurality of through holes which are used for containing a plurality of metal connecting lines in the ceramic substrate, providing the metal connecting lines, cooling the metal connecting lines to be below a room temperature, embedding the cooled metal connecting lines into the through holes of the ceramic substrate, placing the ceramic substrate embedded with the metal connecting lines in the room temperature, placing a direct current electrode layer on the ceramic substrate, and coating an anticorrosive layer on the ceramic substrate placed with the direct current electrode layer. The metal connecting lines manufactured by the method cannot damage the direct current electrode layer, and continuous coating of an anticorrosive layer on the direct current electrode layer is very stable.

Description

The manufacture method of plasma process chamber and electrostatic chuck thereof
Technical field
The present invention relates to field of semiconductor manufacture, particularly relate to the manufacture method of a kind of plasma process chamber and electrostatic chuck thereof.
Background technology
Plasma treatment appts utilizes the operation principle of vacuum reaction chamber to carry out the processing of the substrate of semiconductor chip and plasma flat-plate.The operation principle of vacuum reaction chamber is in vacuum reaction chamber, pass into the reacting gas containing suitable etchant source gas, and then radio-frequency (RF) energy input is carried out to this vacuum reaction chamber, with activated reactive gas, excite and maintain plasma, so that the material layer etched respectively on substrate surface or over the substrate surface depositing layer of material, and then semiconductor chip and plasma flat-plate are processed.
Plasma process chamber comprises a base station, is placed pending substrate above base station.Be provided with an electrostatic chuck above base station, electrostatic chuck is used for clamping substrate.An embedded DC electrode in the insulating barrier on electrostatic chuck upper strata, DC electrode is connected with a DC power supply.Before substrate processing procedure starts, DC power supply puts on DC electrode, makes DC electrode produce an absorption affinity, is held on base station by substrate.And after processing procedure terminates, close the DC power supply put in DC electrode, thus remove the absorption affinity between substrate and electrostatic chuck, manipulator stretches in chamber from exterior thereto, and substrate is removed chamber smoothly.
DC electrode is generally be embedded in the insulating barrier of electrostatic chuck, and DC electrode layer is general very thin.And metal between DC electrode and DC power supply, must be had to connect, be generally that metal wire is set as connecting line in electrostatic chuck inside.But the DC electrode of very thin thickness is easy to produce in the process arranging metal wire break.
The present invention proposes based on this just.
Summary of the invention
For the problems referred to above in background technology, the present invention proposes the manufacture method of a kind of plasma process chamber and electrostatic chuck thereof.
First aspect present invention provides a kind of manufacture method of electrostatic chuck of plasma process chamber, and wherein, described manufacture method comprises the steps:
One ceramic bases is provided;
Described ceramic bases beats some through holes, and described through hole is for holding metal contact wires;
There is provided some metal contact wires, below described some metal contact wires cool to room temperature, and among the described some through holes cooled some metal contact wires being inlaid into respectively described ceramic bases;
By above-mentioned ceramic bases of inlaying metal contact wires as among normal temperature;
DC electrode is placed on described ceramic bases;
Etch resistant layer is deposited on the ceramic bases that placed DC electrode layer.
Further, the diameter of described through hole is greater than the diameter of cooled metal contact wires.
Further, the coefficient of thermal expansion of described metal contact wires oil is much larger than ceramic bases and DC electrode layer.
Further, the material of described metal contact wires comprises: copper, silver, aluminium, gold.
Further, the material of described ceramic bases comprises aluminium oxide.
Further, the material of described DC electrode comprises tungsten.
Further, described manufacture method also comprises the steps: to provide some copper metal contact wires, described some copper metal contact wires are cooled to less than-100 DEG C, and among the described some through holes cooled some metal contact wires being inlaid into respectively described ceramic bases.
Further, described manufacture method also comprises the steps: to utilize the method for vacuum moulding machine or printing DC electrode to be placed on described ceramic bases.
Further, the material of described etch resistant layer comprises yittrium oxide or yttrium nitride.
Further, described etch resistant layer is applied by physical vapour deposition (PVD) or plasma spray coating.
Further, described manufacture method also comprises the steps: to connect soft metal connecting line below metal contact wires.
Second aspect present invention provide a kind of plasma process chamber manufacture method, it is characterized in that, described manufacture method comprises the manufacture method of the electrostatic chuck described in first aspect present invention.
The manufacture method of plasma process chamber provided by the invention and electrostatic chuck thereof, metal contact wires can be set in electrostatic chuck region successfully below DC electrode layer, can not damage DC electrode layer, so that the follow-up top layer at electrostatic chuck coating etch resistant layer.
Accompanying drawing explanation
Fig. 1 is the structural representation of plasma process chamber and lifting device;
Fig. 2 (a) ~ 2 (d) is the process chart manufactured according to the electrostatic chuck of the plasma process chamber of the present invention's specific embodiment;
Fig. 3 is the structural representation of the base station of plasma process chamber according to a specific embodiment of the present invention.
Embodiment
Below in conjunction with accompanying drawing, the specific embodiment of the present invention is described.
It is to be noted; " semiconductor arts piece ", " wafer " and " substrate " these words often will be exchanged use in explanation subsequently; in the present invention; they all refer to that, in the processed process conditions of process chamber, process conditions is not limited to wafer, substrate, substrate, large-area flat-plate substrate etc.For convenience of description, mainly exemplary illustration will be made for " substrate " herein in execution mode illustrates and illustrates.
Fig. 1 shows the structural representation of plasma process chamber and lifting device.Plasma process chamber 100 has a process chambers (not shown), and process chambers is essentially cylindricality, and process chambers sidewall 102 perpendicular, there is in process chambers top electrode arranged in parallel and bottom electrode.Usually, the region between top electrode and bottom electrode is processing region P, this region P by formation high-frequency energy to light and maintain plasma.Above base station 106, place substrate W to be processed, this substrate W can be the semiconductor chip treating to etch or to process or the glass plate treating to be processed into flat-panel monitor.Wherein, described base station 106 is for clamping substrate W.Reacting gas is input to the gas spray 109 in process chambers from gas source 103, one or more radio-frequency power supply 104 can be applied individually on the bottom electrode or is applied on top electrode and bottom electrode respectively simultaneously, in order to be transported on bottom electrode by radio-frequency power or on top electrode and bottom electrode, thus produce large electric field in process chambers inside.In the involved processing region P between the upper and lower electrodes of most of electric field line, this electric field accelerates the electronics being present in process chambers inside on a small quantity, makes it the gas molecule collision with the reacting gas inputted.These collisions cause exciting of the ionization of reacting gas and plasma, thus produce plasma in process chambers.The neutral gas molecule of reacting gas loses electronics when standing these highfields, leaves the ion of positively charged.The ion of positively charged accelerates towards bottom electrode direction, and the neutral substance in processed substrate is combined, and excites substrate to process, i.e. etching, deposit etc.Certain suitable position of plasma process chamber 100 is provided with exhaust gas region, and exhaust gas region is connected with external exhaust apparatus (such as vacuum pump 105), in order to extract chamber out by by the reacting gas crossed and bi-product gas in processing procedure.Wherein, plasma confinement ring 107 for by plasma confinement in processing region P.Chamber sidewall 102 is connected with earth terminal, is wherein provided with a resistance 108.
As everyone knows, electrostatic chuck (ESC, electrostatic chuck) is the core component in plasma process chamber.Due to the carrier that electrostatic chuck is as bottom electrode and substrate, it is necessarily rigid and constitutionally stable, to prevent plasma bombardment and substrate wearing and tearing in product processing procedure process.But the electrostatic chuck of prior art is mostly formed at and binds solid ceramic disk in anodized aluminium substrate.The ceramic disk of electrostatic chuck is usually by Al 2o 3or AlN makes, and comprise some metals and the mixture based on silicon, such as TiO 2, SiO 2deng.When electrostatic chuck operates under the environment comprising halogen (such as F, Cl etc.) plasma, the ceramic base (Al of electrostatic chuck 2o 3or AlN) and other compositions of comprising all will be subject to the bombardment of plasma, but other compositions wherein comprised will be etched under relatively higher corrosion rate.Therefore, plasma etching can change the characteristic (surface roughness, resistance coefficient etc.) of the form on electrostatic chuck surface, composition and ceramic base, and cause the change of the function of electrostatic chuck further, such as leakage current, helium leakage rate, de-clamping time etc.
In order to composition, the structure and characteristics of stable electrostatic chuck, prior art usually electrostatic chuck surface-coated or encapsulation resisting plasma corrosion material, to prevent electrostatic chuck by plasma etching.But, with plasma spray coating (plasma spray on electrostatic chuck, PS) mode applies etch resistant layer and inadvisable, this is because the etch resistant layer of plasma spray coating such as yittrium oxide has pore and frangible in structure, and the etch resistant layer of yittrium oxide is softer than silicon wafer, can cause like this producing particle contamination in processing procedure.Also can utilize physical vapour deposition (PVD) (plasma enhanced physical vapour deposition in the ceramic disk of electrostatic chuck in prior art, PEPVD) the plasma etch resistant layer that deposition compact is hard, such as yittrium oxide or yittrium oxide/aluminium oxide mixing.But, directly restricted technically at electrostatic chuck deposited on silicon because depositing temperature be usually easy to reach 100 DEG C and more than, this is because in physical vapour deposition (PVD) processing procedure, electrostatic chuck can be heated in plasma or coating deposition source.But because the binder fusing point between ceramic matrix and aluminum substrate is lower, the temperature of electrostatic chuck can not higher than 100 DEG C and above.
The disclosed method improving electrostatic chuck performance of prior art comprises (1) and first in the ceramic bases of electrostatic chuck, applies improvement etch resistant layer further, and (2) are then coated with etch resistant layer ceramic bases by bonding and aluminium substrate forms electrostatic chuck.Prior art makes it have a lot of particular characteristics by applying etch resistant layer on electrostatic chuck, and such as high rigidity, good thermal conductivity, durable structure are with the corrosion of anti-multiple plasma chemistries.In fact, electrostatic chuck production procedure conventionally, forms electric connecting point (electrical joint) and also has a lot of technical problem among the alumina substrate under DC electrode.Particularly, mention that the DC electrode in electrostatic chuck is also connected with a DC power supply above, therefore technique has needed at the critical metal of using immediately below DC electrode of the alumina substrate of electrostatic chuck as connecting line.And the thinner thickness of DC electrode, only only have the tungsten of 10 ~ 20um, and the quality of the etch resistant layer of top is comparatively soft, therefore after DC electrode layer is formed, does metal contact wires again, metal contact wires has and greatly may damage DC electrode layer.
The invention provides the manufacture method of a kind of plasma process chamber and electrostatic chuck thereof.As shown in Figure 1, electrostatic chuck 101 is positioned at the top of base station 106, it is for clamping substrate W thereon, a direct current electrode layer 110 is provided with in material layer above electrostatic chuck, DC electrode layer 110 directly must connect a DC power supply 111, produces one by substrate W clamping chucking power thereon to make DC electrode layer 110 under the effect being applied with DC power supply 111.Therefore, the connecting line for being electrically connected must be there is between DC electrode layer 110 and DC power supply 111, and also must need to arrange metal connecting line in electrostatic chuck 101.Goal of the invention of the present invention is just that the electrostatic chuck 101 associated materials layer field between DC electrode layer 110 and the connecting line that is connected with DC power supply 111 thereof is formed and is electrically connected (electrode joint).
First aspect present invention provides a kind of manufacture method of electrostatic chuck of plasma process chamber.Fig. 2 is the process chart manufactured according to the electrostatic chuck of the plasma process chamber of the present invention's specific embodiment.According to a preferred specific embodiment of the present invention, it makes use of principle of expanding with heat and contracting with cold (cooling and expansion) and formed in the electrostatic chuck 101 associated materials layer field between DC electrode layer 110 and the connecting line that is connected with DC power supply 111 thereof and be electrically connected (electrode joint).In the present embodiment, the manufacture method of described electrostatic chuck 101 comprises the steps:
As shown in Fig. 2 (a), first provide a ceramic bases 1012.
Then, described ceramic bases 1012 beats some through holes 1014, described through hole 1014 is for holding metal contact wires.For simplicity's sake, illustrate only a through hole 1014 at Fig. 2 (a).
Then, as shown in Fig. 2 (b), some metal contact wires 1016 are provided, below described some metal contact wires 1016 cool to room temperature, therefore will reduce according to the volume of this metal contact wires 1016 of principle expanded with heat and contract with cold, among the described some through holes 1014 now cooled some metal contact wires 1016 being inlaid into respectively described ceramic bases 1012.
Then, by above-mentioned ceramic bases 1012 of having inlayed metal contact wires 1016 as among normal temperature.Now, owing to increasing compared to temperature before, metal contact wires 1016 is all again be made up of the metal that coefficient of thermal expansion is very high, and therefore, metal contact wires 1016 will expand to fill up through hole 1014.
Then, as shown in Fig. 2 (b), DC electrode layer 110 is placed on described ceramic bases.Because DC electrode layer 110 just manufactures after metal contact wires 1016 is formed, therefore do not deposit in the prior art that DC electrode layer 110 is due to thinner and defect that is that destroyed by the metal contact wires 1016 of rear formation, this has absolutely proved superiority of the present invention.Wherein, the thickness of DC electrode layer 110 is approximately 0.2mm or less.
Finally, as shown in Fig. 2 (d), deposit etch resistant layer 1018 placed on the ceramic bases 1012 of DC electrode layer 110, electrostatic chuck 101 has manufactured.Now, successfully electrical connection is defined among the ceramic bases 1012 under the DC electrode layer 110 of electrostatic chuck 101.
Especially, the diameter of described through hole 1014 is greater than the diameter of cooled metal contact wires 1016, to make metal contact wires 1016 can be inlaid into smoothly among through hole 1014 under the state of cooling, and is expanded to and almost fills up through hole 1014 after recovery room temperature.Exemplarily, the diameter of described through hole 1014 is 1mm.
Especially, the coefficient of thermal expansion of described metal contact wires 1016 is much larger than ceramic bases 1012 and DC electrode layer 110.Following table has used the coefficient of thermal expansion of the metal material of ceramic bases 1012, DC electrode layer 110 and metal contact wires 1016.
Further, the material of described metal contact wires 1016 comprises: copper, silver, aluminium, gold, and the material of described ceramic bases 1012 comprises aluminium oxide, and the material of described DC electrode layer 110 comprises tungsten.As shown above, as the thermal coefficient of expansion of the metallic material of aluminum of metal contact wires 1016, copper, silver, gold, brass much larger than as the material oxidation aluminium of ceramic bases 1012 and aluminium nitride and the tungsten as DC electrode layer 110.Therefore, under same room temperature condition, metal contact wires 1016 expands more severe, therefore metal contact wires 1016 also just embedded among the ceramic bases 1012 of electrostatic chuck 101 smoothly, and this is the difference of the coefficient of thermal expansion due to the ceramic bases 2012 and metal contact wires 1016 that present invention utilizes electrostatic chuck 101.
Further, described manufacture method also comprises the steps: to provide some copper metal contact wires, described some copper metal contact wires are cooled to less than-100 DEG C, and among the described some through holes cooled some metal contact wires being inlaid into respectively described ceramic bases.
It should be noted that, in the above-described embodiments, the diameter of metal contact wires 1016 meticulously selects and calculates, and narrows down to the through hole that can be applicable in the ceramic bases 1012 of electrostatic chuck 101 to make it under cooling effect.
Further, described manufacture method also comprises the steps: to utilize the method for vacuum moulding machine or printing (printing) to be placed on described ceramic bases 1012 by DC electrode layer 110.
Further, the material of described etch resistant layer 1018 comprises yittrium oxide or yttrium nitride.Particularly, the etch resistant layer 1018 on electrostatic chuck 101 top layer is applied by physical vapour deposition (PVD) or plasma spray coating, and it has structure that is fine and close and high porosity, and has plasma corrosion resistance.
Fig. 3 is the structural representation of the base station of plasma process chamber according to a specific embodiment of the present invention.Further, the manufacture method of the electrostatic chuck of plasma process chamber provided by the invention also comprises the steps: to connect soft metal connecting line 1017 at metal contact wires less than 1016, thus completes whole connecting lines of DC electrode 110 and DC power supply.Wherein, in soft metal connecting line 1017 lower end, namely below base station 106, manufacture a joint 1017a at soft metal connecting line 1017, extend the DC power supply 111 connected into shown in Fig. 1.
As shown in Figure 3, according to a variation of the present invention, can also on electrostatic chuck 101 applied in two coats etch resistant layer, namely on original etch resistant layer 1018, apply one deck etch resistant layer 1019 again, with the function making electrostatic chuck 101 have reinforcement.The manufacture method of electrostatic chuck 101 provided by the invention can to realize on electrostatic chuck 101 continuously coated with multiple layer etch resistant layer, even if the quality of etch resistant layer is soft again again, also can not cause the breakage of DC electrode layer 110.
Second aspect present invention provides a kind of manufacture method of plasma process chamber, and wherein, described manufacture method comprises the manufacture method of the electrostatic chuck described in first aspect present invention.
Although content of the present invention has done detailed introduction by above preferred embodiment, will be appreciated that above-mentioned description should not be considered to limitation of the present invention.After those skilled in the art have read foregoing, for multiple amendment of the present invention and substitute will be all apparent.Therefore, protection scope of the present invention should be limited to the appended claims.In addition, any Reference numeral in claim should be considered as the claim involved by restriction; " comprise " word and do not get rid of device unlisted in other claim or specification or step; The word such as " first ", " second " is only used for representing title, and does not represent any specific order.

Claims (12)

1. a manufacture method for the electrostatic chuck of plasma process chamber, wherein, described manufacture method comprises the steps:
One ceramic bases is provided;
Described ceramic bases beats some through holes, and described through hole is for holding metal contact wires;
There is provided some metal contact wires, below described some metal contact wires cool to room temperature, and among the described some through holes cooled some metal contact wires being inlaid into respectively described ceramic bases;
By above-mentioned ceramic bases of inlaying metal contact wires as among normal temperature;
DC electrode is placed on described ceramic bases;
Etch resistant layer is applied on the ceramic bases that placed DC electrode layer.
2. manufacture method according to claim 1, is characterized in that, the diameter of described through hole is greater than the diameter of cooled metal contact wires.
3. manufacture method according to claim 2, is characterized in that, the coefficient of thermal expansion of described metal contact wires is much larger than ceramic bases and DC electrode layer.
4. manufacture method according to claim 3, is characterized in that, the material of described metal contact wires comprises: copper, silver, aluminium, gold.
5. manufacture method according to claim 3, is characterized in that, the material of described ceramic bases comprises aluminium oxide.
6. manufacture method according to claim 3, is characterized in that, the material of described DC electrode layer comprises tungsten.
7. manufacture method according to claim 1, it is characterized in that, described manufacture method also comprises the steps: to provide some copper metal contact wires, described some copper metal contact wires are cooled to less than-100 DEG C, and among the described some through holes cooled some metal contact wires being inlaid into respectively described ceramic bases.
8. manufacture method according to claim 1, is characterized in that, described manufacture method also comprises the steps: to utilize the method for vacuum moulding machine or printing DC electrode to be placed on described ceramic bases.
9. manufacture method according to claim 1, is characterized in that, the material of described etch resistant layer comprises yittrium oxide, yttrium nitride.
10. manufacture method according to claim 1, is characterized in that, described etch resistant layer is applied by physical vapour deposition (PVD) or plasma spray coating.
11. manufacture methods according to claim 1, is characterized in that, described manufacture method also comprises the steps: to connect soft metal connecting line below metal contact wires.
The manufacture method of 12. 1 kinds of plasma process chamber, is characterized in that, described manufacture method comprises the manufacture method of the electrostatic chuck described in any one of claim 1 to 11.
CN201310726396.3A 2013-12-25 2013-12-25 Plasma processing chamber and manufacturing method of electrostatic chuck of plasma processing chamber Active CN104752118B (en)

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CN201310726396.3A CN104752118B (en) 2013-12-25 2013-12-25 Plasma processing chamber and manufacturing method of electrostatic chuck of plasma processing chamber
TW103145166A TWI574294B (en) 2013-12-25 2014-12-24 A method of manufacturing a plasma processing chamber and an electrostatic chuck thereof

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CN201310726396.3A CN104752118B (en) 2013-12-25 2013-12-25 Plasma processing chamber and manufacturing method of electrostatic chuck of plasma processing chamber

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Cited By (1)

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CN116246992A (en) * 2021-12-08 2023-06-09 美科陶瓷科技有限公司 Electrostatic chuck

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CN1868051A (en) * 2003-08-18 2006-11-22 艾克塞利斯技术公司 MEMS based multi-polar electrostatic chuck
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CN104752118B (en) 2017-02-15
TWI574294B (en) 2017-03-11
TW201535457A (en) 2015-09-16

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Address after: 201201 No. 188 Taihua Road, Jinqiao Export Processing Zone, Pudong New Area, Shanghai

Patentee after: Medium and Micro Semiconductor Equipment (Shanghai) Co., Ltd.

Address before: 201201 No. 188 Taihua Road, Jinqiao Export Processing Zone, Pudong New Area, Shanghai

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