CN104706703A - Elaeagnus mollis diels-lepidium meyenii walp compound tablet and preparation method thereof - Google Patents
Elaeagnus mollis diels-lepidium meyenii walp compound tablet and preparation method thereof Download PDFInfo
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Abstract
The invention provides an elaeagnus mollis diels oil-lepidium meyenii walp compound tablet and a preparation method thereof; with utilization of a modern nutrition essence extraction process, the health care effects of elaeagnus mollis diels and lepidium meyenii walp are fully played, and synergistic effect of the elaeagnus mollis diels and the lepidium meyenii walp is achieved. In the preparation process, a supercritical carbon dioxide method is adopted for extracting extracts of the elaeagnus mollis diels oil and the lepidium meyenii walp, microcrystalline cellulose, functional oligosaccharide and magnesium stearate are selected as auxiliary materials, sieving and tabletting are carried out to prepare the elaeagnus mollis diels oil-lepidium meyenii walp compound tablet. Rich proteins in the elaeagnus mollis diels seed kernels make up the shortcoming of less lepidium meyenii walp protein content, and lepidium meyenii walp specific active components of macamides and macaenes make up the deficiency of elaeagnus mollis diels in hormone regulation. The elaeagnus mollis diels oil-lepidium meyenii walp compound tablet aims at regulating the human body nutritional balance, besides, can play roles in improving human body immunity, eliminating fatigue, regulating blood lipid and improving sexual functions, and is especially for sub-healthy people.
Description
Technical field
The present invention relates to a kind of exploitation of health food, be specifically related to a kind of Myriopteron extensum (Wight) K. Schum Maca composite sheet and preparation method thereof.
Technical background
Elaeagnus mollis (Elaeagnus mollis Diels) is Elaeangnaceae oleaster; for deciduous tree or shrub; system's one of remaining Relict Plant of getting off after the glacial action of the 4th century; its natural range is limited; belong to the distinctive seeds of China, be listed in Chinese Second Class Key Protected Plant at present.Research shows, Myriopteron extensum (Wight) K. Schum core rich in nutritive value, and oil content reaches more than 45%, and protein content is 32.21%, is made up of 17 seed amino acids, wherein has 7 kinds of essential amino acids.Myriopteron extensum (Wight) K. Schum core is the significant points of storing plant albumen, mainly containing albumin, globulin, especially the highest with content of glutamic acid, reaches 61.9 mg/g, and be secondly arginine and winter propylhomoserin, content is respectively 42.8mg/g and 35.1 mg/g.Containing abundant ferrum, zinc, calcium, magnesium, selenium and other trace elements, simultaneously also containing sterols material.Myriopteron extensum (Wight) K. Schum has antioxidation, improves body immunity, reduces the effect of low density lipoprotein, LDL in blood.
Lepidinm meyenii Walp (Lepidium meyenii Walp.) is Cruciferae separate row Vegetable spp plant, and originate in the mountain area, Andean of Peru's height above sea level more than 4000 meters, local Inca, used as tonic, is called Peru's Radix Ginseng.This plant can make people increase muscle power, eliminates anxiety, and improve sexual function, its health care receives international genus order and concern day by day.1992 food and agricultural organization of Lepidinm meyenii Walp united state (FAO) recommend to the whole world as supplementary.Ministry of Health of the People's Republic of China's No. 13 bulletin approval Lepidinm meyenii Walp in 2011 is new resource food.American Space General Administration (NASA) is using the space food of Lepidinm meyenii Walp as spaceman.After Lepidinm meyenii Walp maturation, root is the root of the similar turnip of expanding, and diameter 2 ~ 8cm not etc., is not the main edible part of Lepidinm meyenii Walp.Be rich in the effective ingredient such as the alkaloid of macamide (macamides) and Lepidinm meyenii Walp alkene (macaenes) and some structure uniquenesses, glucosinolate and benzyl isothiocyanate thereof in Lepidinm meyenii Walp root, thus Lepidinm meyenii Walp has significant effect in raising fertility, sexual desire promoting etc.
Myriopteron extensum (Wight) K. Schum and Lepidinm meyenii Walp are with the health-care effect of its uniqueness, gradually, known, occur commercially with the health food that Myriopteron extensum (Wight) K. Schum or Lepidinm meyenii Walp are raw material, major part is using Myriopteron extensum (Wight) K. Schum or the full powder of Lepidinm meyenii Walp as raw material, health-care effect is single, can not by the active substance in Myriopteron extensum (Wight) K. Schum or Lepidinm meyenii Walp abundant Appropriate application, reduce the effective rate of utilization of Myriopteron extensum (Wight) K. Schum or Maca reactive composition.
Summary of the invention
The object of the present invention is to provide a kind of Myriopteron extensum (Wight) K. Schum Maca composite sheet and preparation method thereof, utilize modern nutrition elite extraction process, by Myriopteron extensum (Wight) K. Schum and Lepidinm meyenii Walp is composite reaches synergism, make it play optimal efficacy.
For achieving the above object, the technical solution used in the present invention is: provide a kind of Myriopteron extensum (Wight) K. Schum Maca composite sheet, its composition comprises: samara extract, Maca extract and suitable adjuvant, wherein adjuvant comprises slow releasing agent, disintegrating agent and lubricant.Its concrete formulation weight number proportioning is as follows:
Samara extract: 30 ~ 70 parts;
Maca extract: 10 ~ 40 parts;
Microcrystalline Cellulose: 5 ~ 25 parts;
Functional oligose: 1 ~ 10 part;
Magnesium stearate: 0.1 ~ 1 part.
Described samara extract and Maca extract all adopt supercritical carbon dioxide extraction method to extract: wherein, samara extract need get full seed evenly, free from insect pests, without the rotten Myriopteron extensum (Wight) K. Schum kernel that goes rotten, shelling, pulverizing, entering supercritical carbon dioxide extraction equipment, is that extractant extracts with carbon dioxide; Maca extract, by Lepidinm meyenii Walp root through pulverizing, need soak, entering supercritical carbon dioxide extraction equipment, being entrainer, extracting in the supercritical state with ethanol water in basifier.
Described functional oligose comprises the one or several arbitrarily in oligomeric isomaltose, oligofructose, oligomeric xylose, oligomeric galactose, Chitosan Oligosacchaides, soybean oligo saccharide, stachyose.
The concrete grammar preparing above-mentioned Myriopteron extensum (Wight) K. Schum Maca composite sheet is as follows:
(1) prepare samara oil extract: choose full seed evenly, free from insect pests, without the rotten Myriopteron extensum (Wight) K. Schum kernel that goes rotten, shell, be crushed to 20 ~ 40 orders, enter supercritical carbon dioxide extraction equipment, be that extractant extracts with carbon dioxide, abstraction technique parameter is: CO
2flow 5 ~ 10L/h, extracting pressure 25 ~ 50Mpa, extraction temperature 30 ~ 60 DEG C, extraction 1 ~ 4h after, be decompressed to 10 ~ 15Mpa, temperature is down to the drying of 20 ~ 40 DEG C of gained solid contents and is samara extract, and baking temperature is 20 DEG C ~ 50 DEG C;
(2) prepare Maca extract: get Lepidinm meyenii Walp root, be crushed to 20 ~ 60 orders, in basifier, soak 12 ~ 24h, enter supercritical carbon dioxide extraction equipment, be entrainer with ethanol water, extract in the supercritical state, abstraction technique parameter is: CO
2flow 15 ~ 30L/h, extracting pressure 25 ~ 50Mpa, extraction temperature 30 ~ 70 DEG C, after extraction 1 ~ 4h, be decompressed to 10 ~ 25Mpa, temperature is down to 20 ~ 50 DEG C, carbon dioxide and extract are thoroughly separated after drying and obtain Maca extract, baking temperature is 20 DEG C ~ 60 DEG C;
(3) sieve, tabletting: samara extract, Maca extract are sieved respectively, get appropriate and add microcrystalline Cellulose, functional oligose, magnesium stearate mixing, tabletting, be i.e. obtained Myriopteron extensum (Wight) K. Schum Maca composite sheet.
In described step (2) in preparation Maca extract process, selected basifier is the one in diethylamine or ammonia; Selected entrainer concentration of alcohol is 50% ~ 95%, and entrainer consumption is 1.5mL/g.
Samara extract, Maca extract, microcrystalline Cellulose, functional oligose, magnesium stearate whole mistake 60 ~ 100 mesh sieve in described step (3).
Myriopteron extensum (Wight) K. Schum kernel is rich in multivitamin, protein, aminoacid, polysaccharide and trace element, fat content reaches more than 45%, wherein unsaturated fatty acid accounts for more than 75% of fatty acid, and the ratio of linoleic acid plus linolenic acid is close to breast milk Linoleic acid and linolenic ratio 1:7.The fatty acid of odd number carbon has active anticancer, and fatty acid 1, the 2-methyl-Semen Myristicae containing odd number carbon in samara oil and heptadecanoic acid, the content of vitamin C and E is 10 times of Semen Tritici aestivi germ oil.
Containing carbohydrate 59%, protein 11%, fat 2.2%, phytosterol, calcium, ferrum, zinc, magnesium, copper, 18 seed amino acids and unsaturated fatty acid in Lepidinm meyenii Walp, containing abundant nutritional labeling.Wherein two kinds of unique active substances of the distinctive macamide of Lepidinm meyenii Walp and Lepidinm meyenii Walp Xi Shi U.S. botanist Zheng of Chinese origin B.L discovery, are described as " natural vigour nutrient ", " hormone electromotor " by scientist.
The invention has the beneficial effects as follows: adopt supercritical carbon dioxide extraction Myriopteron extensum (Wight) K. Schum, Maca extract, optionally can retain the anti-oxidation function composition such as flavone in Myriopteron extensum (Wight) K. Schum, Myriopteron extensum (Wight) K. Schum alkaloid, and active substance macamides in Lepidinm meyenii Walp and Lepidinm meyenii Walp alkene isoreactivity material; Myriopteron extensum (Wight) K. Schum and the composite of Lepidinm meyenii Walp can play synergism, and in Myriopteron extensum (Wight) K. Schum kernel, rich in protein compensate for the less shortcoming of Lepidinm meyenii Walp protein content, and the distinctive active component macamide of Lepidinm meyenii Walp and Lepidinm meyenii Walp alkene compensate for the deficiency of Myriopteron extensum (Wight) K. Schum in hormonal regulation; With the addition of functional oligose especially, scalable intestinal microecology balance, promotion beneficial bacteria of intestinal tract are bred, do not rely on insulin metabolism, are promoted trace elements absorption, caries prevention.The present invention can play the effect improving body immunity, allaying tiredness, adjusting blood lipid, raising sexual function while being intended to regulate human body balanced in nutrition.Especially be applicable to sub-health population to take.
Detailed description of the invention
embodiment 1:
A kind of Myriopteron extensum (Wight) K. Schum Maca composite sheet, comprises the raw material of following portions by weight proportioning: samara extract 30 parts, Maca extract 40 parts, microcrystalline Cellulose 20 parts, oligofructose 9 parts, magnesium stearate 1 part.
Myriopteron extensum (Wight) K. Schum Maca composite piece preparation method:
(1) preparation of samara extract: choose full seed evenly, free from insect pests, without the rotten Myriopteron extensum (Wight) K. Schum kernel that goes rotten, slough outer kind of shell, grinding particle size be 20 orders, enter supercritical carbon dioxide extraction equipment, take carbon dioxide as extractant, CO
2flow 2L/h.Important technological parameters: extracting pressure 25Mpa, extraction temperature 45 DEG C, after extraction 2h, be decompressed to 10Mpa, temperature is down to 20 DEG C of gained solid contents, and under 25 DEG C of conditions, drying is samara extract;
(2) preparation of Maca extract: getting Lepidinm meyenii Walp root is raw material, and grinding particle size is 20 orders, soaks 24h in basifier ammonia, enter supercritical carbon dioxide extraction equipment, extract in the supercritical state, extracting pressure controls at 30Mpa, extraction temperature controls at 30 DEG C, CO
2flow 15L/h, entrainer concentration of alcohol is 70%, and entrainer consumption is 1.5ml/g, extraction 1h, and be decompressed to 10Mpa, temperature is down to 20 DEG C, is thoroughly separated by carbon dioxide with extract, dry Maca extract under 30 DEG C of conditions;
(3) recipe quantity Maca extract, samara extract, microcrystalline Cellulose, oligofructose, magnesium stearate are always sneaked out 80 mesh sieves, tabletting, obtained Myriopteron extensum (Wight) K. Schum Maca composite sheet.
embodiment 2:
A kind of Myriopteron extensum (Wight) K. Schum Maca composite sheet, comprises the raw material of following portions by weight proportioning: samara extract 40 parts, Maca extract 25 parts, microcrystalline Cellulose 20 parts, oligomeric galactose 14.1 parts, magnesium stearate 0.9 part.
Myriopteron extensum (Wight) K. Schum Maca composite piece preparation method:
(1) preparation of samara extract: choose full seed evenly, free from insect pests, without the rotten Myriopteron extensum (Wight) K. Schum kernel that goes rotten, slough outer kind of shell, grinding particle size be 40 orders, enter supercritical carbon dioxide extraction equipment, take carbon dioxide as extractant, CO
2flow 10L/h, important technological parameters: extracting pressure 40Mpa, extraction temperature 30 DEG C, after extraction 3h, be decompressed to 15Mpa, under temperature is down to 10 DEG C of gained solid contents, 45 DEG C of conditions, drying is samara extract;
(2) preparation of Maca extract: getting Lepidinm meyenii Walp root is raw material, grinding particle size is 40 orders, 12h is soaked in basifier ethylenediamine, enter supercritical carbon dioxide extraction equipment, with 60% ethanol water for entrainer, extract in the supercritical state, extracting pressure controls at 40Mpa, extraction temperature controls at 25 DEG C, CO
2flow 20L/h, entrainer concentration of alcohol is 75%, and entrainer consumption is 1ml/g, extraction 2h, and be decompressed to 15Mpa, temperature is down to 10 DEG C, is thoroughly separated by carbon dioxide with extract, dry Maca extract under 50 DEG C of conditions;
(3) recipe quantity Maca extract, samara extract, microcrystalline Cellulose, oligomeric galactose, magnesium stearate are always sneaked out 60 mesh sieves, tabletting, obtained Myriopteron extensum (Wight) K. Schum Maca composite sheet.
embodiment 3:
A kind of Myriopteron extensum (Wight) K. Schum Maca composite sheet, comprises the raw material of following portions by weight proportioning: samara extract 55 parts, Maca extract 15 parts, microcrystalline Cellulose 18 parts, oligomeric xylose 11.1 parts, magnesium stearate 0.9 part.
Myriopteron extensum (Wight) K. Schum Maca composite piece preparation method is as follows:
(1) preparation of samara extract: choose full seed evenly, free from insect pests, without the rotten Myriopteron extensum (Wight) K. Schum kernel that goes rotten, slough outer kind of shell, grinding particle size be 20 orders, enter supercritical carbon dioxide extraction equipment, take carbon dioxide as extractant, CO
2flow 5L/h, important technological parameters: extracting pressure 40Mpa, extraction temperature 30 DEG C, after extraction 3h, be decompressed to 15Mpa, temperature is down to 10 DEG C of gained solid contents, and under 30 DEG C of conditions, drying is samara extract;
(2) preparation of Maca extract: getting Lepidinm meyenii Walp root is raw material, and grinding particle size is 40 orders, enters supercritical carbon dioxide extraction equipment, extracts in the supercritical state, and extracting pressure controls at 30Mpa, and extraction temperature controls at 35 DEG C, CO
2flow 10L/h, entrainer concentration of alcohol is 65%, adds a certain amount of ammonia, and entrainer consumption is 3ml/g, extraction 3h, and be decompressed to 6Mpa, temperature is down to 20 DEG C, is thoroughly separated by carbon dioxide with extract, dry Maca extract under 45 DEG C of conditions;
(3) recipe quantity samara extract, Maca extract, microcrystalline Cellulose, oligomeric xylose, magnesium stearate are always sneaked out 100 mesh sieves, tabletting, obtained Myriopteron extensum (Wight) K. Schum Maca composite sheet.
A series of detailed description listed is above only illustrating for feasibility embodiment of the present invention; and be not used to limit the scope of the invention, all do not depart from the skill of the present invention equivalent implementations done of spirit or change all should be included within protection scope of the present invention.
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present invention or basic feature, the present invention can be realized in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present invention is limited by claims instead of above-mentioned explanation, and that is therefore intended in the implication of the equivalency by dropping on claim and scope is all.
Claims (5)
1. a Myriopteron extensum (Wight) K. Schum Maca composite sheet, is characterized in that, composition comprises: samara extract, Maca extract and suitable adjuvant, and wherein adjuvant comprises slow releasing agent, disintegrating agent and lubricant, and concrete formulation weight number proportioning is:
Samara extract: 30 ~ 70 parts;
Maca extract: 10 ~ 40 parts;
Microcrystalline Cellulose: 5 ~ 25 parts;
Functional oligose: 1 ~ 10 part;
Magnesium stearate: 0.1 ~ 1 part;
Described samara extract and Maca extract all adopt supercritical carbon dioxide extraction method to extract;
The samara extract that described employing supercritical carbon dioxide extraction method extracts need get full seed evenly, free from insect pests, without the rotten Myriopteron extensum (Wight) K. Schum kernel that goes rotten, shelling, to pulverize, entering supercritical carbon dioxide extraction equipment, is that extractant extracts with carbon dioxide;
The Maca extract that described employing supercritical carbon dioxide extraction method extracts, by Lepidinm meyenii Walp root through pulverizing, need soak, entering supercritical carbon dioxide extraction equipment, being entrainer, extracting in the supercritical state with ethanol water in basifier;
Described functional oligose comprises the one or several arbitrarily in oligomeric isomaltose, oligofructose, oligomeric xylose, oligomeric galactose, Chitosan Oligosacchaides, soybean oligo saccharide, stachyose.
2. a kind of Myriopteron extensum (Wight) K. Schum Maca composite sheet according to claim 1, it is characterized in that, preparation method concrete steps comprise following content:
(1) prepare samara oil extract: choose full seed evenly, free from insect pests, without the rotten Myriopteron extensum (Wight) K. Schum kernel that goes rotten, shell, be crushed to 20 ~ 40 orders, enter supercritical carbon dioxide extraction equipment, be that extractant extracts with carbon dioxide, abstraction technique parameter is: CO
2flow 5 ~ 10L/h, extracting pressure 25 ~ 50Mpa, extraction temperature 30 ~ 60 DEG C, extraction 1 ~ 4h after, be decompressed to 10 ~ 15Mpa, temperature is down to the drying of 20 ~ 40 DEG C of gained solid contents and is samara extract, and baking temperature is 20 DEG C ~ 50 DEG C;
(2) prepare Maca extract: get Lepidinm meyenii Walp root, be crushed to 20 ~ 60 orders, in basifier, soak 12 ~ 24h, enter supercritical carbon dioxide extraction equipment, be entrainer with ethanol water, extract in the supercritical state, abstraction technique parameter is: CO
2flow 15 ~ 30L/h, extracting pressure 25 ~ 50Mpa, extraction temperature 30 ~ 70 DEG C, after extraction 1 ~ 4h, be decompressed to 10 ~ 25Mpa, temperature is down to 20 ~ 50 DEG C, and carbon dioxide and extract are thoroughly separated after drying and obtain Maca extract, baking temperature is 20 DEG C ~ 60 DEG C;
(3) sieve, tabletting: samara extract, Maca extract are sieved respectively, get appropriate and add microcrystalline Cellulose, functional oligose, magnesium stearate mixing, tabletting, be i.e. obtained Myriopteron extensum (Wight) K. Schum Maca composite sheet.
3. a kind of Myriopteron extensum (Wight) K. Schum Maca composite piece preparation method according to claim 2, is characterized in that, in step (2) in preparation Maca extract process, selected basifier is the one in diethylamine or ammonia.
4. a kind of Myriopteron extensum (Wight) K. Schum Maca composite piece preparation method according to claim 2, is characterized in that, in step (2) in preparation Maca extract process, selected entrainer concentration of alcohol is 50% ~ 95%, and entrainer consumption is 1.5mL/g.
5. a kind of Myriopteron extensum (Wight) K. Schum Maca composite piece preparation method according to claim 2, is characterized in that, samara extract, Maca extract, microcrystalline Cellulose, functional oligose, magnesium stearate whole mistake 60 ~ 100 mesh sieve in step (3).
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Cited By (5)
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| CN105105267A (en) * | 2015-09-18 | 2015-12-02 | 谱尼测试集团股份有限公司 | Drink combination |
| CN105536962A (en) * | 2015-12-02 | 2016-05-04 | 桂龙药业(安徽)有限公司 | Method for separating seed wing and seed kernel of seed of oroxylum indicum |
| CN106174571A (en) * | 2016-07-27 | 2016-12-07 | 王旭东 | A kind of samara oil buccal tablet and preparation method thereof |
| CN107668720A (en) * | 2017-09-28 | 2018-02-09 | 山西琪尔康翅果生物制品有限公司 | It is a kind of that there is samara oil Submicron Emulsion for alleviating physical fatigue and preparation method thereof |
| CN109527576A (en) * | 2018-11-06 | 2019-03-29 | 张家界仙踪林农业科技开发有限公司 | A kind of compound fine maca tablets formula for the strong waist that reinforces the kidney and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105105267A (en) * | 2015-09-18 | 2015-12-02 | 谱尼测试集团股份有限公司 | Drink combination |
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| CN107668720A (en) * | 2017-09-28 | 2018-02-09 | 山西琪尔康翅果生物制品有限公司 | It is a kind of that there is samara oil Submicron Emulsion for alleviating physical fatigue and preparation method thereof |
| CN109527576A (en) * | 2018-11-06 | 2019-03-29 | 张家界仙踪林农业科技开发有限公司 | A kind of compound fine maca tablets formula for the strong waist that reinforces the kidney and preparation method thereof |
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