CN104695219B - Creasing anti-bacterial finishing agent and preparation method thereof, purposes - Google Patents
Creasing anti-bacterial finishing agent and preparation method thereof, purposes Download PDFInfo
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- CN104695219B CN104695219B CN201510097071.2A CN201510097071A CN104695219B CN 104695219 B CN104695219 B CN 104695219B CN 201510097071 A CN201510097071 A CN 201510097071A CN 104695219 B CN104695219 B CN 104695219B
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- finishing agent
- ethyl acetate
- kaempferia galanga
- perilla frutescens
- preparation
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- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 27
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 46
- 244000062241 Kaempferia galanga Species 0.000 claims abstract description 36
- 235000013421 Kaempferia galanga Nutrition 0.000 claims abstract description 36
- 239000000203 mixture Substances 0.000 claims abstract description 31
- 244000124853 Perilla frutescens Species 0.000 claims abstract description 30
- 235000004348 Perilla frutescens Nutrition 0.000 claims abstract description 30
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000000469 ethanolic extract Substances 0.000 claims abstract description 22
- 239000002024 ethyl acetate extract Substances 0.000 claims abstract description 22
- 229920000223 polyglycerol Polymers 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229920001661 Chitosan Polymers 0.000 claims abstract description 14
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 claims abstract description 14
- ODLHGICHYURWBS-LKONHMLTSA-N trappsol cyclo Chemical compound CC(O)COC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](COCC(C)O)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](COCC(C)O)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](COCC(C)O)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](COCC(C)O)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)COCC(O)C)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1COCC(C)O ODLHGICHYURWBS-LKONHMLTSA-N 0.000 claims abstract description 14
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 claims abstract description 10
- 238000010008 shearing Methods 0.000 claims abstract description 10
- 238000000605 extraction Methods 0.000 claims description 28
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 21
- 239000007788 liquid Substances 0.000 claims description 19
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 239000004744 fabric Substances 0.000 claims description 14
- 239000000843 powder Substances 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 10
- 239000006228 supernatant Substances 0.000 claims description 9
- 229920000742 Cotton Polymers 0.000 claims description 8
- 239000012141 concentrate Substances 0.000 claims description 7
- 239000013049 sediment Substances 0.000 claims description 7
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 150000004676 glycans Chemical class 0.000 claims 1
- 230000001153 anti-wrinkle effect Effects 0.000 abstract description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 10
- 239000000284 extract Substances 0.000 description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 5
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 5
- 229910052739 hydrogen Inorganic materials 0.000 description 5
- 239000001257 hydrogen Substances 0.000 description 5
- 229910052708 sodium Inorganic materials 0.000 description 5
- 239000011734 sodium Substances 0.000 description 5
- 239000004753 textile Substances 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- 241000222122 Candida albicans Species 0.000 description 3
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 230000000845 anti-microbial effect Effects 0.000 description 3
- 229940095731 candida albicans Drugs 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 230000002401 inhibitory effect Effects 0.000 description 3
- 229920000728 polyester Polymers 0.000 description 3
- 241000191967 Staphylococcus aureus Species 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 241000233866 Fungi Species 0.000 description 1
- 230000000721 bacterilogical effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000003834 intracellular effect Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000003204 osmotic effect Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses creasing anti-bacterial finishing agent and preparation method thereof, purposes, finishing agent includes that azelaic acid 0.8wt% 2.6wt%, disodium hydrogen phosphate 1.6wt% 3.2wt%, carboxymethyl chitosan 2.5wt% 4wt%, hydroxypropyl beta cyclodextrin 3.3wt% 5.6wt%, Perilla frutescens ethyl acetate extract 3wt% 6wt%, Kaempferia galanga ethanol extract 3.5wt% 7wt%, polyglycerol monooleate 6wt% 12wt%, surplus are water；Preparation method is such as: (1) prepares Perilla frutescens ethyl acetate extract；(2) Kaempferia galanga ethanol extract is prepared；(3) taking above-mentioned each composition the most respectively and carry out mix and blend, shear treatment, for the creasing anti-bacterial finishing agent of preparation after shearing.The finishing agent of preparation has the advantage that anti-wrinkle effect is good, bacteriostasis property is strong, applied widely.
Description
Technical field
The invention belongs to textile finshing agent field, relate to finishing agent and preparation method thereof, purposes, particularly relate to crease-resistant anti-
Bacterium finishing agent and preparation method thereof, purposes.
Background technology
Antibacterial finishing agent is firstly the need of having good security, and secondly it can be to the bacterium removed on fabric, fungi
Produce inhibitory action with mould etc., and bacteriological aftergrowth and breeding can be prevented, need the antibacterial effect with wide spectrum.Antibacterial finishing agent
The cell membrane of bacterium can be destroyed, owing to intracellular osmotic pressure is 20 ~ 30 times of born of the same parents' exosmosis pressure, therefore membranolysis, endochylema
Beyond the region of objective existence is let out, and terminates the metabolic process of microorganism, makes microorganism cannot grow and breed.
The development time of crease-shedding finishing agent is longer, uses Lauxite and formaldehyde etc. to carry out arranging once right and wrong and usually sees
A kind of finishing technique, along with science and technology progress, increasing formaldehydeless finishing agent also arises at the historic moment.Develop new nothing dirty
Dye, environmental protection, crease-shedding finishing agent to human body fanout free region become the recent tendency of a finishing agent development.
Summary of the invention
Solve the technical problem that: the conventional clothing after crease-shedding finishing agent arrangement can occur the change of intensity, and
The antibacterial effect of conventional finishing agent is poor, can not effectively suppress Candida albicans, it is an object of the invention to provide one
Novel creasing anti-bacterial finishing agent and preparation method thereof, purposes.
Technical scheme: the invention discloses creasing anti-bacterial finishing agent and preparation method thereof, purposes, described creasing anti-bacterial is whole
Reason agent includes the composition of following weight percentage:
Azelaic acid 0.8wt%-2.6wt%,
Disodium hydrogen phosphate 1.6wt%-3.2wt%,
Carboxymethyl chitosan 2.5wt%-4wt%,
HP-β-CD 3.3wt%-5.6wt%,
Perilla frutescens ethyl acetate extract 3wt%-6wt%,
Kaempferia galanga ethanol extract 3.5wt%-7wt%,
Polyglycerol monooleate 6wt%-12wt%,
Surplus is water.
Preferably, described creasing anti-bacterial finishing agent, including the composition of following weight percentage:
Azelaic acid 1.2wt%-2.0wt%,
Disodium hydrogen phosphate 2.1wt%-2.7wt%,
Carboxymethyl chitosan 3.0wt%-3.5wt%,
HP-β-CD 4wt%-5wt%,
Perilla frutescens ethyl acetate extract 4wt%-5wt%,
Kaempferia galanga ethanol extract 4.5wt%-6wt%,
Polyglycerol monooleate 8wt%-11wt%,
Surplus is water.
It is further preferred that described creasing anti-bacterial finishing agent, including the composition of following weight percentage:
Azelaic acid 1.8wt%,
Disodium hydrogen phosphate 2.4wt%,
Carboxymethyl chitosan 3.3wt%,
HP-β-CD 4.5wt%,
Perilla frutescens ethyl acetate extract 4.5wt%,
Kaempferia galanga ethanol extract 5.5wt%,
Polyglycerol monooleate 10wt%,
Surplus is water.
The preparation method of creasing anti-bacterial finishing agent, preparation method comprises the following steps:
(1) mechanical crushing after Perilla frutescens being vacuum dried, is stirred Perilla frutescens powder ethyl acetate extracting, extracts
Temperature is 45 DEG C, and extraction time is 3h, and feed liquid weight ratio is 1:5, stands after extraction, takes supernatant liquor and concentrates, white for prepare
Perillaseed ethyl acetate extract；
(2) pulverizing dried for Kaempferia galanga with pulverizer again, be stirred Kaempferia galanga powder ethanol extracting, Extracting temperature is
50 DEG C, extraction time is 2h, and feed liquid weight ratio is 1:8, centrifugal after extraction, removes lower sediment, after being concentrated by supernatant liquor is
The Kaempferia galanga ethanol extract of preparation；
(3) take the most respectively azelaic acid be 0.8wt%-2.6wt%, disodium hydrogen phosphate be 1.6wt%-3.2wt%,
Carboxymethyl chitosan is 2.5wt%-4wt%, HP-β-CD is 3.3wt%-5.6wt%, Perilla frutescens ethyl acetate extract
For 3wt%-6wt%, Kaempferia galanga ethanol extract be 3.5wt%-7wt%, polyglycerol monooleate be 6wt%-12wt%, surplus be water；
Above-mentioned each composition is carried out mix and blend, after stirring 10min, carries out shear treatment with cutter, crease-resistant for prepare after shearing
Antibacterial finishing agent.
The preparation method of described creasing anti-bacterial finishing agent, during described shear treatment, shearing rotating speed is 3000-
5000rpm, shear time is 20-40min.
The purposes of the creasing anti-bacterial finishing agent described in any of the above, described purposes is included in pure cotton fabric, blend fabric
In purposes.
Beneficial effect: pure cotton fabric and textile polyester fibre containing textile were arranged by the creasing anti-bacterial finishing agent of the present invention
After, the wrinkle resistance of two kinds of fabrics is obtained for and is greatly enhanced, and remains the highest ultimate strength.The arrangement of the present invention
Agent also creates the strongest inhibitory action to Candida albicans and staphylococcus aureus.Can be as a kind of novel finishing agent
For pure cotton fabric or the crease-resistant and antibiotic finish of other textiles.
Detailed description of the invention
Embodiment 1
(1) mechanical crushing after Perilla frutescens being vacuum dried, is stirred Perilla frutescens powder ethyl acetate extracting, extracts
Temperature is 45 DEG C, and extraction time is 3h, and feed liquid weight ratio is 1:5, stands after extraction, takes supernatant liquor and concentrates, white for prepare
Perillaseed ethyl acetate extract；(2) pulverize dried for Kaempferia galanga with pulverizer again, be stirred carrying by Kaempferia galanga powder ethanol
Taking, Extracting temperature is 50 DEG C, and extraction time is 2h, and feed liquid weight ratio is 1:8, centrifugal after extraction, removes lower sediment, by upper strata
Clear liquid is the Kaempferia galanga ethanol extract of preparation after concentrating；(3) take the most respectively azelaic acid be 2.6wt%, phosphoric acid hydrogen two
Sodium is 1.6wt%, carboxymethyl chitosan is 4wt%, HP-β-CD is 5.6wt%, Perilla frutescens ethyl acetate extract is
6wt%, Kaempferia galanga ethanol extract are 7wt%, polyglycerol monooleate is 12wt%, surplus is water；Above-mentioned each composition is mixed
Close stirring, after stirring 10min, carry out shear treatment with cutter, for the creasing anti-bacterial finishing agent of preparation after shearing.
Embodiment 2
(1) mechanical crushing after Perilla frutescens being vacuum dried, is stirred Perilla frutescens powder ethyl acetate extracting, extracts
Temperature is 45 DEG C, and extraction time is 3h, and feed liquid weight ratio is 1:5, stands after extraction, takes supernatant liquor and concentrates, white for prepare
Perillaseed ethyl acetate extract；(2) pulverize dried for Kaempferia galanga with pulverizer again, be stirred carrying by Kaempferia galanga powder ethanol
Taking, Extracting temperature is 50 DEG C, and extraction time is 2h, and feed liquid weight ratio is 1:8, centrifugal after extraction, removes lower sediment, by upper strata
Clear liquid is the Kaempferia galanga ethanol extract of preparation after concentrating；(3) take the most respectively azelaic acid be 0.8wt%, phosphoric acid hydrogen two
Sodium is 3.2wt%, carboxymethyl chitosan is 2.5wt%, HP-β-CD is 3.3wt%, Perilla frutescens ethyl acetate extract
For 3wt%, Kaempferia galanga ethanol extract be 3.5wt%, polyglycerol monooleate be 6wt%, surplus be water；Above-mentioned each composition is entered
Row mix and blend, carries out shear treatment with cutter after stirring 10min, for the creasing anti-bacterial finishing agent of preparation after shearing.
Embodiment 3
(1) mechanical crushing after Perilla frutescens being vacuum dried, is stirred Perilla frutescens powder ethyl acetate extracting, extracts
Temperature is 45 DEG C, and extraction time is 3h, and feed liquid weight ratio is 1:5, stands after extraction, takes supernatant liquor and concentrates, white for prepare
Perillaseed ethyl acetate extract；(2) pulverize dried for Kaempferia galanga with pulverizer again, be stirred carrying by Kaempferia galanga powder ethanol
Taking, Extracting temperature is 50 DEG C, and extraction time is 2h, and feed liquid weight ratio is 1:8, centrifugal after extraction, removes lower sediment, by upper strata
Clear liquid is the Kaempferia galanga ethanol extract of preparation after concentrating；(3) take the most respectively azelaic acid be 1.2wt%, phosphoric acid hydrogen two
Sodium is 2.7wt%, carboxymethyl chitosan is 3.5wt%, HP-β-CD is 5wt%, Perilla frutescens ethyl acetate extract is
4wt%, Kaempferia galanga ethanol extract are 6wt%, polyglycerol monooleate is 8wt%, surplus is water；Above-mentioned each composition is mixed
Close stirring, after stirring 10min, carry out shear treatment with cutter, for the creasing anti-bacterial finishing agent of preparation after shearing.
Embodiment 4
(1) mechanical crushing after Perilla frutescens being vacuum dried, is stirred Perilla frutescens powder ethyl acetate extracting, extracts
Temperature is 45 DEG C, and extraction time is 3h, and feed liquid weight ratio is 1:5, stands after extraction, takes supernatant liquor and concentrates, white for prepare
Perillaseed ethyl acetate extract；(2) pulverize dried for Kaempferia galanga with pulverizer again, be stirred carrying by Kaempferia galanga powder ethanol
Taking, Extracting temperature is 50 DEG C, and extraction time is 2h, and feed liquid weight ratio is 1:8, centrifugal after extraction, removes lower sediment, by upper strata
Clear liquid is the Kaempferia galanga ethanol extract of preparation after concentrating；(3) take the most respectively azelaic acid be 2.0wt%, phosphoric acid hydrogen two
Sodium is 2.1wt%, carboxymethyl chitosan is 3.0wt%, HP-β-CD is 4wt%, Perilla frutescens ethyl acetate extract is
5wt%, Kaempferia galanga ethanol extract are 4.5wt%, polyglycerol monooleate is 11wt%, surplus is water；Above-mentioned each composition is carried out
Mix and blend, carries out shear treatment with cutter after stirring 10min, for the creasing anti-bacterial finishing agent of preparation after shearing.
Embodiment 5
(1) mechanical crushing after Perilla frutescens being vacuum dried, is stirred Perilla frutescens powder ethyl acetate extracting, extracts
Temperature is 45 DEG C, and extraction time is 3h, and feed liquid weight ratio is 1:5, stands after extraction, takes supernatant liquor and concentrates, white for prepare
Perillaseed ethyl acetate extract；(2) pulverize dried for Kaempferia galanga with pulverizer again, be stirred carrying by Kaempferia galanga powder ethanol
Taking, Extracting temperature is 50 DEG C, and extraction time is 2h, and feed liquid weight ratio is 1:8, centrifugal after extraction, removes lower sediment, by upper strata
Clear liquid is the Kaempferia galanga ethanol extract of preparation after concentrating；(3) take the most respectively azelaic acid be 1.8wt%, phosphoric acid hydrogen two
Sodium is 2.4wt%, carboxymethyl chitosan is 3.3wt%, HP-β-CD is 4.5wt%, Perilla frutescens ethyl acetate extract
For 4.5wt%, Kaempferia galanga ethanol extract be 5.5wt%, polyglycerol monooleate be 10wt%, surplus be water；By above-mentioned each composition
Carry out mix and blend, after stirring 10min, carry out shear treatment with cutter, for the creasing anti-bacterial finishing agent of preparation after shearing.
Comparative example
Take the most respectively azelaic acid be 2.6wt%, disodium hydrogen phosphate be 1.6wt%, carboxymethyl chitosan be
4wt%, polyglycerol monooleate are 12wt%, surplus is water；Above-mentioned each composition is carried out mix and blend, uses after stirring 10min
Cutter carries out shear treatment, for the creasing anti-bacterial finishing agent of preparation after shearing.
Pure cotton fabric and cotton polyester fiber mixed fabrics are carried out whole with the finishing agent of embodiment 1 to 5 and comparative example respectively
Reason, the immersion time is 1h, and two leachings two are rolled, and pick-up is 50%, dry at 80 DEG C.The recovery angle and the ultimate strength that measure fabric are protected
Stay rate, and measure fabric to staphylococcus aureus and the inhibiting rate of Candida albicans.Result is as follows:
Crease-resistant and the anti-microbial property of table 1 pure cotton fabric
Crease-resistant and the anti-microbial property of table 2 cotton polyester fiber mixed fabrics
Learning from Comparative result, the finishing agent of the present invention has that anti-wrinkle effect is good, anti-microbial property strong, applied widely
Advantage.
Claims (5)
1. creasing anti-bacterial finishing agent, it is characterised in that described creasing anti-bacterial finishing agent includes the composition of following weight percentage:
Azelaic acid 0.8wt%-2.6wt%,
Disodium hydrogen phosphate 1.6wt%-3.2wt%,
Carboxymethyl chitosan 2.5wt%-4wt%,
Hydroxy propyl-Beta-cyclodextrin 3.3wt%-5.6wt%,
Perilla frutescens ethyl acetate extract 3wt%-6wt%,
Kaempferia galanga ethanol extract 3.5wt%-7wt%,
Polyglycerol monooleate 6wt%-12wt%,
Surplus is water；
The preparation method of described creasing anti-bacterial finishing agent comprises the following steps:
(1) mechanical crushing after Perilla frutescens being vacuum dried, is stirred Perilla frutescens powder ethyl acetate extracting, Extracting temperature
Being 45 DEG C, extraction time is 3h, and feed liquid weight ratio is 1:5, stands after extraction, takes supernatant liquor and concentrates, for the Perilla frutescens of preparation
Ethyl acetate extract；
(2) pulverizing dried for Kaempferia galanga with pulverizer again, be stirred Kaempferia galanga powder ethanol extracting, Extracting temperature is 50
DEG C, extraction time is 2h, and feed liquid weight ratio is 1:8, centrifugal after extraction, removes lower sediment, for system after being concentrated by supernatant liquor
Standby Kaempferia galanga ethanol extract；
(3) take the most respectively azelaic acid be 0.8wt%-2.6wt%, disodium hydrogen phosphate be 1.6wt%-3.2wt%, carboxylic first
Base enclosure glycan is 2.5wt%-4wt%, hydroxy propyl-Beta-cyclodextrin is 3.3wt%-5.6wt%, Perilla frutescens ethyl acetate extract is
3wt%-6wt%, Kaempferia galanga ethanol extract are 3.5wt%-7wt%, polyglycerol monooleate is 6wt%-12wt%, surplus is water；Will
Above-mentioned each composition carries out mix and blend, carries out shear treatment with cutter after stirring 10min, crease-resistant for prepare after shearing
Antibacterial finishing agent.
Creasing anti-bacterial finishing agent the most according to claim 1, it is characterised in that under described creasing anti-bacterial finishing agent includes
State the composition of percentage by weight:
Azelaic acid 1.2wt%-2.0wt%,
Disodium hydrogen phosphate 2.1wt%-2.7wt%,
Carboxymethyl chitosan 3.0wt%-3.5wt%,
HP-β-CD 4wt%-5wt%,
Perilla frutescens ethyl acetate extract 4wt%-5wt%,
Kaempferia galanga ethanol extract 4.5wt%-6wt%,
Polyglycerol monooleate 8wt%-11wt%,
Surplus is water.
Creasing anti-bacterial finishing agent the most according to claim 1, it is characterised in that under described creasing anti-bacterial finishing agent includes
State the composition of percentage by weight:
Azelaic acid 1.8wt%,
Disodium hydrogen phosphate 2.4wt%,
Carboxymethyl chitosan 3.3wt%,
HP-β-CD 4.5wt%,
Perilla frutescens ethyl acetate extract 4.5wt%,
Kaempferia galanga ethanol extract 5.5wt%,
Polyglycerol monooleate 10wt%,
Surplus is water.
Creasing anti-bacterial finishing agent the most according to claim 1, it is characterised in that during described shear treatment, shears rotating speed
For 3000-5000rpm, shear time is 20-40min.
5. according to the purposes of the arbitrary described creasing anti-bacterial finishing agent of claims 1 to 3, it is characterised in that described purposes bag
Include the purposes in pure cotton fabric, blend fabric.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510097071.2A CN104695219B (en) | 2015-03-05 | 2015-03-05 | Creasing anti-bacterial finishing agent and preparation method thereof, purposes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510097071.2A CN104695219B (en) | 2015-03-05 | 2015-03-05 | Creasing anti-bacterial finishing agent and preparation method thereof, purposes |
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| CN104695219B true CN104695219B (en) | 2016-08-24 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105064020A (en) * | 2015-09-08 | 2015-11-18 | 湖州吉昌丝绸有限公司 | Novel Chinese yam compound anti-bacterial deodorizing finishing agent as well as preparation method and fiber treatment method thereof |
| CN106480714A (en) * | 2016-10-27 | 2017-03-08 | 苏州经贸职业技术学院 | A kind of preparation method of environment-friendly type antibiotic functional finishing agent |
| CN107345364B (en) * | 2017-07-11 | 2020-03-17 | 苏州新民丝绸有限公司 | Fabric functional agent and application thereof |
| CN107858830A (en) * | 2017-11-23 | 2018-03-30 | 苏州经贸职业技术学院 | A kind of linen Anti-bacterial and Crease method |
| CN108035146A (en) * | 2018-01-05 | 2018-05-15 | 苏州经贸职业技术学院 | A kind of Environment Compatible Textiles finishing agent and preparation method thereof |
| CN108486882A (en) * | 2018-04-08 | 2018-09-04 | 苏州经贸职业技术学院 | A kind of preparation method of antibacterial crease-resistant Silk Finishing agent |
| CN108823961A (en) * | 2018-05-21 | 2018-11-16 | 合肥云都棉花有限公司 | A kind of modified cotton fiber and its non-ironing cloth of preparation |
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| DE10356095A1 (en) * | 2003-11-27 | 2005-06-30 | Deutsches Textilforschungszentrum Nord-West E.V. | Finishing textiles, e.g. to provide active agent binding or releasing properties, by applying halotriazinyl-substituted cyclodextrin and other functional finishing agent and reacting to cause covalent bonding |
| CN101147496A (en) * | 2007-08-31 | 2008-03-26 | 深圳清华大学研究院 | Antibiotic agent for textile and preparation method and application thereof |
| CN102002854B (en) * | 2010-12-06 | 2012-01-25 | 中原工学院 | Multifunctional textile finishing agent, preparation method thereof and cotton textile finishing method |
| CN102605630A (en) * | 2012-04-06 | 2012-07-25 | 南通市嘉宇斯纺织集团有限公司 | Traditional Chinese medicine inclusion compound with antibacterial effect and textile finishing method of traditional Chinese medicine inclusion compound |
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