CN104695222B - Environment-friendly type composite fabric finishing agent and preparation method thereof - Google Patents
Environment-friendly type composite fabric finishing agent and preparation method thereof Download PDFInfo
- Publication number
- CN104695222B CN104695222B CN201510097015.9A CN201510097015A CN104695222B CN 104695222 B CN104695222 B CN 104695222B CN 201510097015 A CN201510097015 A CN 201510097015A CN 104695222 B CN104695222 B CN 104695222B
- Authority
- CN
- China
- Prior art keywords
- extract
- ethanol
- finishing agent
- preparation
- friendly type
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- 239000000675 fabric finishing Substances 0.000 title claims abstract description 22
- 238000009962 finishing (textile) Methods 0.000 title claims abstract description 22
- 239000002131 composite material Substances 0.000 title claims abstract description 20
- 239000000284 extract Substances 0.000 claims abstract description 60
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 37
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims abstract description 34
- 229920001661 Chitosan Polymers 0.000 claims abstract description 25
- DDXLVDQZPFLQMZ-UHFFFAOYSA-M dodecyl(trimethyl)azanium;chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+](C)(C)C DDXLVDQZPFLQMZ-UHFFFAOYSA-M 0.000 claims abstract description 25
- 229940022860 xylitan Drugs 0.000 claims abstract description 25
- 238000002481 ethanol extraction Methods 0.000 claims abstract description 21
- CDOUZKKFHVEKRI-UHFFFAOYSA-N 3-bromo-n-[(prop-2-enoylamino)methyl]propanamide Chemical compound BrCCC(=O)NCNC(=O)C=C CDOUZKKFHVEKRI-UHFFFAOYSA-N 0.000 claims abstract description 18
- 235000019329 dioctyl sodium sulphosuccinate Nutrition 0.000 claims abstract description 18
- 239000007788 liquid Substances 0.000 claims abstract description 16
- 238000013019 agitation Methods 0.000 claims abstract description 10
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 claims description 40
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 18
- 238000000605 extraction Methods 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 8
- 239000012141 concentrate Substances 0.000 claims description 6
- 238000004137 mechanical activation Methods 0.000 claims description 6
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 4
- RZHBMYQXKIDANM-UHFFFAOYSA-N dioctyl butanedioate;sodium Chemical compound [Na].CCCCCCCCOC(=O)CCC(=O)OCCCCCCCC RZHBMYQXKIDANM-UHFFFAOYSA-N 0.000 claims description 3
- 238000009987 spinning Methods 0.000 claims 2
- 239000000469 ethanolic extract Substances 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 abstract description 9
- 230000000845 anti-microbial effect Effects 0.000 abstract description 6
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 230000037303 wrinkles Effects 0.000 abstract description 3
- 239000004744 fabric Substances 0.000 description 9
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 6
- 230000000844 anti-bacterial effect Effects 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 5
- 229910052708 sodium Inorganic materials 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- 239000001384 succinic acid Substances 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 2
- 241000588724 Escherichia coli Species 0.000 description 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 150000004676 glycans Chemical class 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
- 239000005017 polysaccharide Substances 0.000 description 2
- 229910052709 silver Inorganic materials 0.000 description 2
- 239000004332 silver Substances 0.000 description 2
- 230000001629 suppression Effects 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- UPLPHRJJTCUQAY-WIRWPRASSA-N 2,3-thioepoxy madol Chemical compound C([C@@H]1CC2)[C@@H]3S[C@@H]3C[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CC[C@](C)(O)[C@@]2(C)CC1 UPLPHRJJTCUQAY-WIRWPRASSA-N 0.000 description 1
- 241000222122 Candida albicans Species 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229940095731 candida albicans Drugs 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 125000001153 fluoro group Chemical group F* 0.000 description 1
- 229910017053 inorganic salt Inorganic materials 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000009988 textile finishing Methods 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention discloses environment-friendly type composite fabric finishing agent and preparation method thereof, in described dressing liquid xylitan monostearate be 2.5wt% 5wt%, dioctyl sodium sulfosuccinate be 3wt% 6wt%, Dodecyl trimethyl ammonium chloride be 3.5wt% 5.5wt%, aqua armeniacae extract be 4wt% 7wt%, chitosan be 4wt% 8wt%, Radix Sanguisorbae 40wt% ethanol water extract be 5wt% 9wt%, Pollen Typhae ethanol extraction be 3wt% 8wt%, Isosorbide-5-Nitrae butanediol be 6wt% 12wt%, surplus be water.Described preparation method includes mechanical agitation, mixing.The composite fabric finishing agent prepared has that environmental protection, wrinkle resistance be strong, the feature of good antimicrobial effect.
Description
Technical field
The invention belongs to textile finishing field, relate to textile finish and preparation method thereof, particularly relate to environment-friendly type
Textile finish and preparation method thereof.
Background technology
In antibacterial finishing agent, the inorganic salt of metal ion or the inorganic antiseptic kind of complex are most, and purposes is
Many, yield is the most maximum.Being characterized in that antibiotic property and safety are high, heat-resist, antibacterial range is wide, and effect duration is long.Antibiotic finish
In agent, volume antimicrobial component mainly has silver, copper, zinc and compound thereof；Wherein silver and compound thereof are with the most use.At crease-shedding finishing agent
In, the most substantial amounts of employ some compositions that environment is had relatively havoc.Common fabric water-refusing oil-refusing finishing agent mostly is fluorine-containing
Type, it also has bigger destruction to environment.In order to effectively prevent the finishing agent destruction to environment, researcher arranges in environment-friendly type
The developer of agent has more research, but on the premise of ensure that environment-friendly type, the respective performances of its finishing agent prepared is remote
Less than the performance of the finishing agent of chemosynthesis, accordingly, it would be desirable to exploitation is on the premise of ensureing environment-friendly type, the most also have the highest
Wrinkle resistance and the composite fabric finishing agent of bacteriostasis property.
Summary of the invention
Solve the technical problem that: the most common finishing agent mostly is synthesis class finishing agent, and effective ingredient therein mostly is
Chemical composition, has bigger destruction to environment, it is an object of the invention to provide a kind of environmentally safe, environment-friendly type have good
Finishing agent of the most crease-resistant good, antibacterial functions and preparation method thereof.
Technical scheme: the invention discloses environment-friendly type composite fabric finishing agent and preparation method thereof, described environment-friendly type
Composite fabric finishing agent includes the composition of following weight percentage ratio:
Xylitan monostearate 2.5wt%-5wt%,
Dioctyl sodium sulfosuccinate 3wt%-6wt%,
Dodecyl trimethyl ammonium chloride 3.5wt%-5.5wt%,
Aqua armeniacae extract 4wt%-7wt%,
Chitosan 4wt%-8wt%,
Radix Sanguisorbae 40wt% ethanol water extract 5wt%-9wt%,
Pollen Typhae ethanol extraction 3wt%-8wt%,
1,4-butanediol 6wt%-12wt%,
Surplus is water.
It is further preferred that described environment-friendly type composite fabric finishing agent, including the composition of following weight percentage ratio:
Xylitan monostearate 3.5wt%-4.5wt%,
Dioctyl sodium sulfosuccinate 4wt%-5wt%,
Dodecyl trimethyl ammonium chloride 4.5wt%-5wt%,
Aqua armeniacae extract 5wt%-6wt%,
Chitosan 5wt%-7wt%,
Radix Sanguisorbae 40wt% ethanol water extract 6wt%-8wt%,
Pollen Typhae ethanol extraction 5wt%-7wt%,
1,4-butanediol 8wt%-10wt%,
Surplus is water.
Further preferred, described environment-friendly type composite fabric finishing agent, including the composition of following weight percentage ratio:
Xylitan monostearate 4wt%,
Dioctyl sodium sulfosuccinate 4.5wt%,
Dodecyl trimethyl ammonium chloride 4.8wt%,
Aqua armeniacae extract 5.5wt%,
Chitosan 6wt%,
Radix Sanguisorbae 40wt% ethanol water extract 7wt%,
Pollen Typhae ethanol extraction 6wt%,
1,4-butanediol 9wt%,
Surplus is water.
The preparation method of environment-friendly type composite fabric finishing agent, described preparation method comprises the following steps:
Step 1: water intaking and BDO respectively, carries out mechanical agitation to uniformly by water and Isosorbide-5-Nitrae butanediol；Step 2: add
Heat, to 50 DEG C, adds xylitan monostearate, dioctyl sodium sulfosuccinate, Dodecyl trimethyl ammonium chloride, machine
Tool stirs to mix homogeneously；Step 3: finally add aqua armeniacae extract, chitosan, Radix Sanguisorbae 40wt% ethanol water extract, Pollen Typhae second
Alcohol extraction thing, is stirred for uniformly, and in the Final finishing liquid that stirs, xylitan monostearate is 2.5wt%-5wt%, succinum
Sodium dioctyl sulfo is 3wt%-6wt%, Dodecyl trimethyl ammonium chloride is 3.5wt%-5.5wt%, aqua armeniacae extract is
4wt%-7wt%, chitosan are 4wt%-8wt%, Radix Sanguisorbae 40wt% ethanol water extract is 5wt%-9wt%, Pollen Typhae ethanol extraction is
3wt%-8wt%, 1,4-butanediol is 6wt%-12wt%, surplus is water.
The preparation method of described environment-friendly type composite fabric finishing agent, Radix Sanguisorbae 40wt% ethanol in described preparation method
Water extract preparation method is as follows:
After Radix Sanguisorbae is dried, carried out mechanical activation comminution, then be stirred extracting with the ethanol water of 40wt%, extracted
Temperature is 50 DEG C, and extraction time is 120min, and feed liquid weight ratio is 1:7, concentrates, prepare Radix Sanguisorbae 40wt% ethanol after being centrifuged
Water extract.
The preparation method of described environment-friendly type composite fabric finishing agent, Pollen Typhae ethanol extraction in described preparation method
Preparation method is as follows:
After being dried by Pollen Typhae, being carried out mechanical activation comminution, then be stirred extracting with ethanol solution, Extracting temperature is 50
DEG C, extraction time is 3h, and feed liquid weight ratio is 1:9, concentrates, prepare Pollen Typhae ethanol water extract after being centrifuged.
Beneficial effect: the effective ingredient in the environment-friendly type composite fabric finishing agent of the present invention be to environment without destroy and
Pollute, on the premise of environmental protection, effectively raise crease-resistant level and the anti-microbial property of fabric, the wherein addition of aqua armeniacae extract
Effectively raise the crease-resistant level of fabric, it may be possible to owing to albumen contained in aqua armeniacae extract and polysaccharide are to its crease-resistant feelings
Condition creates impact, it addition, the Radix Sanguisorbae 40wt% ethanol water extract added and Pollen Typhae ethanol extraction effectively raise finishing agent
Anti-microbial property, during therefore it can be widely used in the antibacterial of fabric and anti-crease finishing.
Detailed description of the invention
In following embodiment and comparative example, Radix Sanguisorbae 40wt% ethanol water extract preparation method is as follows:
After Radix Sanguisorbae is dried, carried out mechanical activation comminution, then be stirred extracting with the ethanol water of 40wt%, extracted
Temperature is 50 DEG C, and extraction time is 120min, and feed liquid weight ratio is 1:7, concentrates, prepare Radix Sanguisorbae 40wt% ethanol after being centrifuged
Water extract.
Pollen Typhae ethanol extraction preparation method is as follows:
After being dried by Pollen Typhae, being carried out mechanical activation comminution, then be stirred extracting with ethanol solution, Extracting temperature is 50
DEG C, extraction time is 3h, and feed liquid weight ratio is 1:9, concentrates, prepare Pollen Typhae ethanol water extract after being centrifuged.
Embodiment 1
Step 1: water intaking and BDO respectively, carries out mechanical agitation to uniformly by water and Isosorbide-5-Nitrae butanediol；Step 2: add
Heat, to 50 DEG C, adds xylitan monostearate, dioctyl sodium sulfosuccinate, Dodecyl trimethyl ammonium chloride, machine
Tool stirs to mix homogeneously；Step 3: finally add aqua armeniacae extract, chitosan, Radix Sanguisorbae 40wt% ethanol water extract, Pollen Typhae second
Alcohol extraction thing, is stirred for uniformly, and in the Final finishing liquid that stirs, xylitan monostearate is 5wt%, dioctyl succinate
Sodium sulfonate is 3wt%, Dodecyl trimethyl ammonium chloride is 3.5wt%, aqua armeniacae extract is 7wt%, chitosan is 8wt%, Radix Sanguisorbae
40wt% ethanol water extract is 9wt%, Pollen Typhae ethanol extraction be 8wt%, 1,4-butanediol be 12wt%, surplus be water.
Embodiment 2
Step 1: water intaking and BDO respectively, carries out mechanical agitation to uniformly by water and Isosorbide-5-Nitrae butanediol；Step 2: add
Heat, to 50 DEG C, adds xylitan monostearate, dioctyl sodium sulfosuccinate, Dodecyl trimethyl ammonium chloride, machine
Tool stirs to mix homogeneously；Step 3: finally add aqua armeniacae extract, chitosan, Radix Sanguisorbae 40wt% ethanol water extract, Pollen Typhae second
Alcohol extraction thing, is stirred for uniformly, in the Final finishing liquid that stirs xylitan monostearate be 2.5wt%, succinic acid two pungent
Ester sodium sulfonate is 6wt%, Dodecyl trimethyl ammonium chloride is 5.5wt%, aqua armeniacae extract is 4wt%, chitosan is 4wt%,
Elm 40wt% ethanol water extract is 5wt%, Pollen Typhae ethanol extraction be 3wt%, 1,4-butanediol be 6wt%, surplus be water.
Embodiment 3
Step 1: water intaking and BDO respectively, carries out mechanical agitation to uniformly by water and Isosorbide-5-Nitrae butanediol；Step 2: add
Heat, to 50 DEG C, adds xylitan monostearate, dioctyl sodium sulfosuccinate, Dodecyl trimethyl ammonium chloride, machine
Tool stirs to mix homogeneously；Step 3: finally add aqua armeniacae extract, chitosan, Radix Sanguisorbae 40wt% ethanol water extract, Pollen Typhae second
Alcohol extraction thing, is stirred for uniformly, in the Final finishing liquid that stirs xylitan monostearate be 4.5wt%, succinic acid two pungent
Ester sodium sulfonate is 5wt%, Dodecyl trimethyl ammonium chloride is 4.5wt%, aqua armeniacae extract is 6wt%, chitosan is 7wt%,
Elm 40wt% ethanol water extract is 6wt%, Pollen Typhae ethanol extraction be 7wt%, 1,4-butanediol be 10wt%, surplus be water.
Embodiment 4
Step 1: water intaking and BDO respectively, carries out mechanical agitation to uniformly by water and Isosorbide-5-Nitrae butanediol；Step 2: add
Heat, to 50 DEG C, adds xylitan monostearate, dioctyl sodium sulfosuccinate, Dodecyl trimethyl ammonium chloride, machine
Tool stirs to mix homogeneously；Step 3: finally add aqua armeniacae extract, chitosan, Radix Sanguisorbae 40wt% ethanol water extract, Pollen Typhae second
Alcohol extraction thing, is stirred for uniformly, in the Final finishing liquid that stirs xylitan monostearate be 3.5wt%, succinic acid two pungent
Ester sodium sulfonate is 4wt%, Dodecyl trimethyl ammonium chloride is 5wt%, aqua armeniacae extract is 5wt%, chitosan is 5wt%, Radix Sanguisorbae
40wt% ethanol water extract is 8wt%, Pollen Typhae ethanol extraction be 5wt%, 1,4-butanediol be 8wt%, surplus be water.
Embodiment 5
Step 1: water intaking and BDO respectively, carries out mechanical agitation to uniformly by water and Isosorbide-5-Nitrae butanediol；Step 2: add
Heat, to 50 DEG C, adds xylitan monostearate, dioctyl sodium sulfosuccinate, Dodecyl trimethyl ammonium chloride, machine
Tool stirs to mix homogeneously；Step 3: finally add aqua armeniacae extract, chitosan, Radix Sanguisorbae 40wt% ethanol water extract, Pollen Typhae second
Alcohol extraction thing, is stirred for uniformly, and in the Final finishing liquid that stirs, xylitan monostearate is 4wt%, dioctyl succinate
Sodium sulfonate is 4.5wt%, Dodecyl trimethyl ammonium chloride is 4.8wt%, aqua armeniacae extract is 5.5wt%, chitosan is 6wt%,
Radix Sanguisorbae 40wt% ethanol water extract is 7wt%, Pollen Typhae ethanol extraction be 6wt%, 1,4-butanediol be 9wt%, surplus be water.
Comparative example 1
Step 1: water intaking and BDO respectively, carries out mechanical agitation to uniformly by water and Isosorbide-5-Nitrae butanediol；Step 2: add
Heat, to 50 DEG C, adds xylitan monostearate, dioctyl sodium sulfosuccinate, Dodecyl trimethyl ammonium chloride, machine
Tool stirs to mix homogeneously；Step 3: finally add chitosan, Radix Sanguisorbae 40wt% ethanol water extract, Pollen Typhae ethanol extraction, then
Be stirred until homogeneous, in the Final finishing liquid that stirs xylitan monostearate be 5wt%, dioctyl sodium sulfosuccinate be
3wt%, Dodecyl trimethyl ammonium chloride are 3.5wt%, chitosan is 8wt%, Radix Sanguisorbae 40wt% ethanol water extract is 9wt%, Pollen Typhae
Ethanol extraction be 8wt%, 1,4-butanediol be 12wt%, surplus be water.
Comparative example 2
Step 1: water intaking and BDO respectively, carries out mechanical agitation to uniformly by water and Isosorbide-5-Nitrae butanediol；Step 2: add
Heat, to 50 DEG C, adds xylitan monostearate, dioctyl sodium sulfosuccinate, Dodecyl trimethyl ammonium chloride, machine
Tool stirs to mix homogeneously；Step 3: finally add aqua armeniacae extract, chitosan, is stirred for uniformly, whole after stirring
Reason liquid in xylitan monostearate be 5wt%, dioctyl sodium sulfosuccinate be 3wt%, Dodecyl trimethyl ammonium chloride
For 3.5wt%, aqua armeniacae extract be 7wt%, chitosan be 8wt%, 1,4-butanediol be 12wt%, surplus be water.
Take in the finishing agent that pure cotton fabric the most at room temperature immerses the above embodiments 1 to 5, comparative example 1 and 2, immerse
Time is 2h, and two leachings two are rolled, and pick-up is 60%, dry at 85 DEG C.Use AATCC standard measure respectively the above embodiments and
The pure cotton fabric of comparative example is to escherichia coli and the suppression ratio of Candida albicans.Additionally also measured were its crease-resistant intensity.Result is such as
Under:
Table 1 escherichia coli and staphylococcus aureus suppression ratio measurement result
Table 2 wrinkle resistance measurement result
The finishing agent of the present invention effectively raises crease-resistant level and the anti-microbial property of fabric on the premise of environmental protection, wherein
The addition of aqua armeniacae extract effectively raises the crease-resistant level of fabric, it may be possible to due to albumen contained in aqua armeniacae extract
With polysaccharide, its crease-resistant situation is created impact, it addition, the Radix Sanguisorbae 40wt% ethanol water extract added and Pollen Typhae ethanol extraction have
The anti-microbial property that improve finishing agent of effect, during therefore it can be widely used in the antibacterial of fabric and anti-crease finishing.
Claims (6)
1. environment-friendly type composite fabric finishing agent, it is characterised in that described environment-friendly type composite fabric finishing agent includes following heavy
The composition of amount percentage ratio:
Xylitan monostearate 2.5wt%-5wt%,
Dioctyl sodium sulfosuccinate 3wt%-6wt%,
Dodecyl trimethyl ammonium chloride 3.5wt%-5.5wt%,
Aqua armeniacae extract 4wt%-7wt%,
Chitosan 4wt%-8wt%,
Radix Sanguisorbae 40wt% ethanol water extract 5wt%-9wt%,
Pollen Typhae ethanol extraction 3wt%-8wt%,
1,4-butanediol 6wt%-12wt%,
Surplus is water.
Environment-friendly type composite fabric finishing agent the most according to claim 1, it is characterised in that described environment-friendly type Compound spinning
Fabric finishing agent includes the composition of following weight percentage ratio:
Xylitan monostearate 3.5wt%-4.5wt%,
Dioctyl sodium sulfosuccinate 4wt%-5wt%,
Dodecyl trimethyl ammonium chloride 4.5wt%-5wt%,
Aqua armeniacae extract 5wt%-6wt%,
Chitosan 5wt%-7wt%,
Radix Sanguisorbae 40wt% ethanol water extract 6wt%-8wt%,
Pollen Typhae ethanol extraction 5wt%-7wt%,
1,4-butanediol 8wt%-10wt%,
Surplus is water.
Environment-friendly type composite fabric finishing agent the most according to claim 1, it is characterised in that described environment-friendly type Compound spinning
Fabric finishing agent includes the composition of following weight percentage ratio:
Xylitan monostearate 4wt%,
Dioctyl sodium sulfosuccinate 4.5wt%,
Dodecyl trimethyl ammonium chloride 4.8wt%,
Aqua armeniacae extract 5.5wt%,
Chitosan 6wt%,
Radix Sanguisorbae 40wt% ethanol water extract 7wt%,
Pollen Typhae ethanol extraction 6wt%,
1,4-butanediol 9wt%,
Surplus is water.
4. the preparation method of environment-friendly type composite fabric finishing agent, it is characterised in that described preparation method comprises the following steps:
Step 1: water intaking and BDO respectively, carries out mechanical agitation to uniformly by water and BDO；Step 2: heating
To 50 DEG C, add xylitan monostearate, dioctyl sodium sulfosuccinate, Dodecyl trimethyl ammonium chloride, machinery
Stirring is to mix homogeneously；Step 3: finally add aqua armeniacae extract, chitosan, Radix Sanguisorbae 40wt% ethanol water extract, Pollen Typhae ethanol
Extract, is stirred for uniformly, and in the Final finishing liquid that stirs, xylitan monostearate is 2.5wt%-5wt%, succinic acid
Dioctyl ester sodium sulfonate is 3wt%-6wt%, Dodecyl trimethyl ammonium chloride is 3.5wt%-5.5wt%, aqua armeniacae extract is
4wt%-7wt%, chitosan are 4wt%-8wt%, Radix Sanguisorbae 40wt% ethanol water extract is 5wt%-9wt%, Pollen Typhae ethanol extraction is
3wt%-8wt%, 1,4-butanediol is 6wt%-12wt%, surplus is water.
The preparation method of environment-friendly type composite fabric finishing agent the most according to claim 4, it is characterised in that described system
In Preparation Method, Radix Sanguisorbae 40wt% ethanol water extract preparation method is as follows:
After Radix Sanguisorbae is dried, carried out mechanical activation comminution, then be stirred extracting with the ethanol water of 40wt%, Extracting temperature
Being 50 DEG C, extraction time is 120min, and feed liquid weight ratio is 1:7, concentrates, prepare Radix Sanguisorbae 40wt% ethanol water and carry after being centrifuged
Thing.
The preparation method of environment-friendly type composite fabric finishing agent the most according to claim 4, it is characterised in that described system
In Preparation Method, Pollen Typhae ethanol extraction preparation method is as follows:
After being dried by Pollen Typhae, being carried out mechanical activation comminution, then be stirred extracting with ethanol solution, Extracting temperature is 50 DEG C, carries
The time of taking is 3h, and feed liquid weight ratio is 1:9, concentrates, prepare Pollen Typhae ethanol water extract after being centrifuged.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510097015.9A CN104695222B (en) | 2015-03-05 | 2015-03-05 | Environment-friendly type composite fabric finishing agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510097015.9A CN104695222B (en) | 2015-03-05 | 2015-03-05 | Environment-friendly type composite fabric finishing agent and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104695222A CN104695222A (en) | 2015-06-10 |
| CN104695222B true CN104695222B (en) | 2016-08-03 |
Family
ID=53342739
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510097015.9A Expired - Fee Related CN104695222B (en) | 2015-03-05 | 2015-03-05 | Environment-friendly type composite fabric finishing agent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104695222B (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105064010A (en) * | 2015-08-03 | 2015-11-18 | 湖州吉昌丝绸有限公司 | Novel natural antibacterial finishing agent, and preparation method thereof |
| CN105350284A (en) * | 2015-12-18 | 2016-02-24 | 苏州富美纺织科技有限公司 | Preparation method of finishing liquid for fabric |
| CN107474977A (en) * | 2017-09-14 | 2017-12-15 | 苏州经贸职业技术学院 | A kind of cotton wool fabric mothproof soft type detergent and preparation method thereof |
| CN110117902B (en) * | 2019-05-31 | 2021-11-02 | 深圳市北岳海威化工有限公司 | Textile finishing liquor and production process thereof |
| CN111101372B (en) * | 2019-10-25 | 2022-02-15 | 南通大学 | Preparation method of natural cattail wool anti-mosquito cellulose fiber |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103668961A (en) * | 2012-09-21 | 2014-03-26 | 青岛道合生物科技有限公司 | Traditional Chinese medicine antibacterial finishing agent special for cotton fabrics |
| CN103643492B (en) * | 2013-12-02 | 2016-01-20 | 常熟市雄发针织毛绒有限公司 | The preparation method of fabric soft finishing agent |
| CN103741457B (en) * | 2013-12-31 | 2016-03-16 | 吴江市七都镇庙港雅迪针织制衣厂 | Silk fabric antistatic finishing agent |
| CN104228288A (en) * | 2014-09-18 | 2014-12-24 | 青岛玉石制衣有限公司 | Manufacturing method of health-care fabric for skin tightening |
| CN104294579B (en) * | 2014-09-24 | 2016-03-30 | 邓杵娇 | A kind of healthcare face fabric for underpants for women |
-
2015
- 2015-03-05 CN CN201510097015.9A patent/CN104695222B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN104695222A (en) | 2015-06-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104695222B (en) | Environment-friendly type composite fabric finishing agent and preparation method thereof | |
| CN106106522B (en) | A kind of nano zine oxide-load silver chitosan compound anti-bacteria agent and preparation method thereof | |
| CN101720756B (en) | Prochloraz-containing compound suspend emulsion formulation and preparation method | |
| CN105332082B (en) | A kind of antibacterial Fypro based on silver-loaded zirconium phosphate and preparation method thereof | |
| CN105064010A (en) | Novel natural antibacterial finishing agent, and preparation method thereof | |
| CN105603740A (en) | Antibacterial anti-ultraviolet cotton fabric and preparation process thereof | |
| CN104562661A (en) | Cotton and linen fabric finishing process | |
| KR20090121506A (en) | Antimicrobial finishing method of cotton fabrics or cellulosic fabrics | |
| CN111410713A (en) | Plant-derived antibacterial microcapsule emulsion and preparation method thereof | |
| CN106135275A (en) | A kind of preparation method of the sepiolite antimicrobial powder of organically-modified and load silver ion | |
| CN113024687A (en) | Preparation method of quaternary ammonium salinization modified soluble chitosan antibacterial agent, antibacterial agent and antibacterial fiber | |
| CN105274834A (en) | Afterfinish process for knitted fabric | |
| CN101974796A (en) | Method for preparing medical stone cellulose fiber | |
| CN109235036A (en) | A kind of method that decatize heating in-situ preparation-immersion coating prepares bacteriostasis, preservation non-woven fabrics packaging material | |
| CN104695223B (en) | Nano-antibacterial textile finish and preparation method thereof | |
| CN104695214B (en) | A kind of real silk polyphenol finishing agent and preparation method thereof | |
| CN107385910A (en) | Fiber composite natral Anti-bacterial and Crease agent and preparation method thereof | |
| CN103210907A (en) | Zoxamide water suspension and preparation method thereof | |
| CN104452289A (en) | Finishing process of shirt fabric | |
| CN104562656B (en) | A kind of environment-friendly type woollen sweater antibacterial finish agent and preparation method thereof | |
| CN105594699B (en) | A kind of 80% dimethomorph water dispersion granula and preparation method thereof | |
| CN102165958B (en) | Pesticide composite containing bifenazate and triazophos | |
| CN104562639A (en) | Finishing process of sheet fabrics | |
| CN107156182A (en) | A kind of preparation method containing plant saponin biopesticide synergist | |
| CN105648776A (en) | Antibacterial and anti-ultraviolet finishing agent and method for preparing same |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160803 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |