CN104666934B - Cordyceps sinensis compound buccal lozenge and preparation method thereof - Google Patents
Cordyceps sinensis compound buccal lozenge and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of cordyceps sinensis compound buccal lozenge and preparation method thereof, is the lyophilized lozenge being prepared by 5 ~ 30 parts by weight of cordyceps sinensis, 5 ~ 60 parts by weight of ganoderma lucidum, 10 ~ 120 parts by weight of Radix Codonopsis, 8 ~ 50 parts by weight of dendrobium candidum, 10 ~ 80 parts by weight of roxburgh anoectochilus terminal bud；The present invention had not only played compound Chinese prescription systemic regulation, synergistic advantage, but also solve security risk of the cordyceps sinensis folk prescription there are heavy metals exceeding standard by the form of Chinese medicine compound prescription compatibility；Made lozenge ensures the activity of active ingredient to the full extent, and appearance uniform, specific surface area is big, loose structure is good, and dissolution velocity is fast；More conducively ensure the release of the cordyceps sinensis elite limit to be taken containing sheet mode, reach the ultimate attainment absorption of human body, be easy to take and store.
Description
Technical field
The present invention relates to a kind of compound preparation of Chinese medicine and preparation method thereof, be specifically cordyceps sinensis compound buccal lozenge and its
Preparation method.
Background technology
Cordyceps sinensis, is that section ergot fungus cordyceps sinensis bacterium colonizes in stroma and larva on Hepialidae insect larvae
The complex of corpse.Sweet in flavor and neutral in nature, return lung kidney channel, main active are cordycepin, cordycepic acid and Cordyceps sinensis polysaccharide, have and adjust
Invigorating the lung and the kidney, preventing phlegm from forming and stopping coughing, adjust immunity of organisms, antitumor and other effects.
Cordyceps sinensis is wild rare medicinal herbs, main product in Jinsha jiang River, the Lancang River, Nujiang Three Rivers regions upstream.East
To the Liangshan Mountain in Sichuan Province, west to the Burang County in Tibet, the Mount Min North gets Gansu Province, the Yulong in south to the Himalayas and Yunnan Province
Snow mountain.The yield of Cordyceps Sinensis From Tibet constitutes about the 41% of national cordyceps yield, and Qinghai Province's yield constitutes about the national winter worm summer
The 33% of Herbage harvest, Yunnan Province and Sichuan Province's cordyceps yield are respectively accounted for above and below 11%-16%.Since cordyceps sinensis is a kind of mushroom
Biology, is influenced by natural growing environment, and content of beary metal fluctuation is big in cordyceps sinensis medicinal material, and resource controllability is low, the worm summer in winter
Security risk of the careless folk prescription as health food there are heavy metals exceeding standard.
Tradition using cordyceps sinensis more take it is pan-fried, boil, stew, soaking, crushing, chewing mode, modern study confirm：The worm summer in winter
Grass with decoct, boil, stew, soak, crush, the conventional method such as chewing is eaten, since the okioplast wall of cordyceps sinensis cannot be broken（Carefully
The nutrition of intracellular and energy account for more than the 80% of its total amount）, absorption of human body utilization rate causes active ingredients of cordyceps sinensis less than 10%
A large amount of wastes.Cordyceps sinensis can cause losing, breaking for many of core essential ingredient by heating, stewing high-temperature process
Bad, effective rate of utilization substantially reduces.
Cordyceps sinensis is famous strengthening by means of tonics medicine, and how its scarcity of resources, develop utilization rate height, convenient to take, makes
With the product of safety, more selections are provided for consumer, are our problems faceds.
The content of the invention
The purpose of the present invention is exactly that there are heavy metals exceeding standard hidden danger, cordyceps sinensis raw material profit in order to overcome existing single preparations of ephedrine
It is low with rate, the problems such as taking inconvenience and a kind of cordyceps sinensis compound buccal lozenge preparation and preparation method thereof is provided；
The cordyceps sinensis compound buccal lozenge of the present invention, is made of the raw material of following weight parts：
5 ~ 30 ganoderma lucidum 5 ~ 60 of cordyceps sinensis
10 ~ 120 dendrobium candidum 8 ~ 50 of Radix Codonopsis
Roxburgh anoectochilus terminal bud 10 ~ 80.
Further preferred solution, is made of the raw material of following weight parts：
10 ~ 20 ganoderma lucidum 10 ~ 40 of cordyceps sinensis
20 ~ 80 dendrobium candidum 20-40 of Radix Codonopsis
Roxburgh anoectochilus terminal bud 20-60.
Further preferred solution, is made of the raw material of following weight parts：
15 ganoderma lucidum 30 of cordyceps sinensis
60 dendrobium candidum 30 of Radix Codonopsis
Roxburgh anoectochilus terminal bud 40.
The preparation method of the cordyceps sinensis compound buccal lozenge, comprises the following steps：
（1）Learn from else's experience cleaning, the cordyceps sinensis of drying process is crushed, and it is micro- to obtain the cordyceps sinensis that mesh number is 300 ~ 1000
Powder；
（2）By ganoderma lucidum, Radix Codonopsis, dendrobium candidum, roxburgh anoectochilus terminal bud is measured, add 8-15 times of water to decoct 1 ~ 3 time, when each 1-3 is small, decoct
Liquid filtering merges, and concentrates of every 1ml equivalent to crude drug 0.5-2g is concentrated under reduced pressure to give at 70 DEG C；
（3）By step（1）Gained aweto micropowder is added into above-mentioned concentrate by formula ratio, is stirred evenly, and obtains the worm summer in winter
Careless compound suspension；
（4）Suspension is placed in stainless steel disc, liquid level 1cm, is placed on the shelf of freeze dryer, first with 1 DEG C/minute
The shelf temperature of freeze dryer is down to -45 DEG C by the speed of clock；When products temperature is down to -40 DEG C, and holding 2 is small；Start to take out afterwards
Vacuum, when vacuum reaches 20-30pa, starts to warm up；Shelf temperature is risen to -10 with 0.1-0.5 DEG C/min of speed
DEG C, after the sample water heading line off of visor position, i.e., shelf temperature is risen to 25 DEG C with 1-2 DEG C/min of speed, setting limit is true
Reciprocal of duty cycle, insulation 6-8 it is small when after, nitrogen charging emptying, that is, obtain cordyceps sinensis compound lyophilized products；It is made using direct power compressing method
Cordyceps sinensis compound buccal lozenge.
The present invention is made of five kinds of cordyceps sinensis, ganoderma lucidum, Radix Codonopsis, dendrobium candidum, roxburgh anoectochilus terminal bud raw materials, wherein cordyceps sinensis：
It is sweet in flavor mild-natured, for the product of flat tonifying lung kidney；Kind energy tonifying lung gas, beneficial lung yin, kidney-replenishing, benefiting essence-blood, and can hemostasis and phlegm；With controlling lung kidney
Two is empty, takes the photograph to receive and haves no right.Modern pharmacology research proves, cordyceps sinensis have antibacterial, immunological regulation, anticancer, anti-inflammatory, improve on kidney
Gland Determination of cortisol, anti-arrhythmia, antifatigue, eliminating phlegm and relieving asthma, tranquilizing soporific etc. act on, and effect is extensive.Ganoderma lucidum therein is certainly
Gu has the reputation of celestial grass, its nature and flavor is sweet, flat, the thoughts of returning home, lung, liver and kidney channel, there is invigorating qi for tranquilization, relieving cough and asthma work(.Modern pharmacology is ground
Study carefully confirmation, ganoderma lucidum has the work such as antitumor, immunological regulation, hypoglycemic, liver protection, anti-aging, anti-inflammatory and antalgic, cardioprotection, anticoagulation
With.Two medicines share, invigorating the lung and the kidney, benefiting qi for tranquillization, play strengthening by means of tonics altogether, consolidate the work(of righting, are altogether monarch drug in a prescription.Radix Codonopsis therein,
Dendrobium candidum blood-nourishing kidney-nourishing, Yin-nourishing and body fluid promoting, are ministerial drug；Two medicines close and with it, with help invigorating Qi and tonifying kidney, blood-nourishing of promoting the production of body fluid effect.Gold thread
Lotus clearing heat and cooling blood, removing dampness and detoxicating, soothing the liver of reinforcing the kidney；All medicines share play altogether Yin Yang balancing, strengthen the body resistance to consolidate the constitution, beauty treatment of promoting the production of body fluid, reconcile gas
Blood, the five internal organs, the work(for supporting longevity macrobiosis；Reach protection liver, improve the immunity of the human body comprehensively, enhancing human body is to the resistance of disease
Effect.
Form of the invention by Chinese medicine compound prescription compatibility, had not only played compound Chinese prescription systemic regulation, synergistic advantage, but also
Solve security risk of the cordyceps sinensis folk prescription there are heavy metals exceeding standard.Compound suspension material is in cryogenic vacuum shape in the present invention
Lyophilization is carried out under state, avoids and the side effects such as foam, oxidation is produced by vapor, ensures active ingredient to the full extent
Activity.The material appearance uniform of freeze-dried preparation, specific surface area is big, loose structure is good, and dissolution velocity is fast.With containing sheet mode
Take and more conducively ensure the release of the cordyceps sinensis elite limit, reach the ultimate attainment absorption of human body.And finished product lozenge is easy to take and stores.
Embodiment
Embodiment 1
（1）Learn from else's experience cleaning, the cordyceps sinensis of drying process is crushed, and it is micro- to obtain the cordyceps sinensis that mesh number is 300 ~ 1000
Powder；
（2）Ganoderma lucidum 30g, Radix Codonopsis 60g, dendrobium candidum 30g, roxburgh anoectochilus terminal bud 40g are taken respectively, add 8-15 times of water to decoct 1 ~ 3 time, often
When secondary 1-3 is small, decocting liquid filtering merges, and concentrates of every 1ml equivalent to 0.5g crude drugs is concentrated under reduced pressure to give at 70 DEG C；
（3）By step（1）Gained aweto micropowder 15g is added into above-mentioned concentrate, is stirred evenly, and obtains cordyceps sinensis compound
Suspension；
（4）Suspension is placed in stainless steel disc, liquid level 1cm, is placed on the shelf of freeze dryer, first with 1 DEG C/minute
The shelf temperature of freeze dryer is down to -45 DEG C by the speed of clock；When products temperature is down to -40 DEG C, and holding 2 is small；Start to take out afterwards
Vacuum, when vacuum reaches 20pa, starts to warm up；Shelf temperature is risen to -10 DEG C with 0.3 DEG C/min of speed, works as visor
After the sample water heading line off of position, i.e., shelf temperature is risen to 25 DEG C with 1 DEG C/min of speed, setting limit vacuum, keeps the temperature 8
After hour, nitrogen charging emptying, that is, obtain cordyceps sinensis compound lyophilized products；Cordyceps sinensis compound is made using direct power compressing method
Lozenge.
Embodiment 2
（1）Learn from else's experience cleaning, the cordyceps sinensis of drying process is crushed, and it is micro- to obtain the cordyceps sinensis that mesh number is 300 ~ 1000
Powder；
（2）Ganoderma lucidum 40g, Radix Codonopsis 80g, dendrobium candidum 40g, roxburgh anoectochilus terminal bud 60g are taken respectively, add 8-15 times of water to decoct 1 ~ 3 time, often
When secondary 1-3 is small, decocting liquid filtering merges, and concentrates of every 1ml equivalent to 1.0g crude drugs is concentrated under reduced pressure to give at 70 DEG C；
（3）By step（1）Gained aweto micropowder 20g is added into above-mentioned concentrate, is stirred evenly, and obtains cordyceps sinensis compound
Suspension；
（4）Suspension is placed in stainless steel disc, liquid level 1cm, is placed on the shelf of freeze dryer, first with 1 DEG C/minute
The shelf temperature of freeze dryer is down to -45 DEG C by the speed of clock；When products temperature is down to -40 DEG C, and holding 2 is small；Start to take out afterwards
Vacuum, when vacuum reaches 30pa, starts to warm up；Shelf temperature is risen to -10 DEG C with 0.5 DEG C/min of speed, works as visor
After the sample water heading line off of position, i.e., shelf temperature is risen to 25 DEG C with 1 DEG C/min of speed, setting limit vacuum, keeps the temperature 6
After hour, nitrogen charging emptying, that is, obtain cordyceps sinensis compound lyophilized products；Cordyceps sinensis compound is made using direct power compressing method
Lozenge.
Embodiment 3
（1）Learn from else's experience cleaning, the cordyceps sinensis of drying process is crushed, and it is micro- to obtain the cordyceps sinensis that mesh number is 300 ~ 1000
Powder；
（2）Ganoderma lucidum 20g, Radix Codonopsis 100g, dendrobium candidum 30g, roxburgh anoectochilus terminal bud 50g are taken respectively, add 8-15 times of water to decoct 1 ~ 3 time,
When 1-3 is small every time, decocting liquid filtering merges, and concentrates of every 1ml equivalent to 2g crude drugs is concentrated under reduced pressure to give at 70 DEG C；
（3）By step（1）Gained aweto micropowder 30g is added into above-mentioned concentrate, is stirred evenly, and obtains cordyceps sinensis compound
Suspension；
（4）Suspension is placed in stainless steel disc, liquid level 1cm, is placed on the shelf of freeze dryer, first with 1 DEG C/minute
The shelf temperature of freeze dryer is down to -45 DEG C by the speed of clock；When products temperature is down to -40 DEG C, and holding 2 is small；Start to take out afterwards
Vacuum, when vacuum reaches 20pa, starts to warm up；Shelf temperature is risen to -10 DEG C with 0.1 DEG C/min of speed, works as visor
After the sample water heading line off of position, i.e., shelf temperature is risen to 25 DEG C with 2 DEG C/min of speed, setting limit vacuum, keeps the temperature 7
After hour, nitrogen charging emptying, that is, obtain cordyceps sinensis compound lyophilized products；Cordyceps sinensis compound is made using direct power compressing method
Lozenge.
Embodiment 4
（1）Learn from else's experience cleaning, the cordyceps sinensis of drying process is crushed, and it is micro- to obtain the cordyceps sinensis that mesh number is 300 ~ 1000
Powder；
（2）Ganoderma lucidum 35g, Radix Codonopsis 75g, dendrobium candidum 25g, roxburgh anoectochilus terminal bud 45g are taken respectively, add 8-15 times of water to decoct 1 ~ 3 time, often
When secondary 1-3 is small, decocting liquid filtering merges, and concentrates of every 1ml equivalent to 1.5g crude drugs is concentrated under reduced pressure to give at 70 DEG C；
（3）By step（1）Gained aweto micropowder 20g is added into above-mentioned concentrate, is stirred evenly, and obtains cordyceps sinensis compound
Suspension；
（4）Suspension is placed in stainless steel disc, liquid level 1cm, is placed on the shelf of freeze dryer, first with 1 DEG C/minute
The shelf temperature of freeze dryer is down to -45 DEG C by the speed of clock；When products temperature is down to -40 DEG C, and holding 2 is small；Start to take out afterwards
Vacuum, when vacuum reaches 25pa, starts to warm up；Shelf temperature is risen to -10 DEG C with 0.3 DEG C/min of speed, works as visor
After the sample water heading line off of position, i.e., shelf temperature is risen to 25 DEG C with 1 DEG C/min of speed, setting limit vacuum, keeps the temperature 8
After hour, nitrogen charging emptying, that is, obtain cordyceps sinensis compound lyophilized products；Cordyceps sinensis compound is made using direct power compressing method
Lozenge.
Embodiment 5
（1）Learn from else's experience cleaning, the cordyceps sinensis of drying process is crushed, and it is micro- to obtain the cordyceps sinensis that mesh number is 300 ~ 1000
Powder；
（2）Ganoderma lucidum 50g, Radix Codonopsis 50g, dendrobium candidum 40g, roxburgh anoectochilus terminal bud 65g are taken respectively, add 8-15 times of water to decoct 1 ~ 3 time, often
When secondary 1-3 is small, decocting liquid filtering merges, and concentrates of every 1ml equivalent to 1.5g crude drugs is concentrated under reduced pressure to give at 70 DEG C；
（3）By step（1）Gained aweto micropowder 30g is added into above-mentioned concentrate, is stirred evenly, and obtains cordyceps sinensis compound
Suspension；
（4）Suspension is placed in stainless steel disc, liquid level 1cm, is placed on the shelf of freeze dryer, first with 1 DEG C/minute
The shelf temperature of freeze dryer is down to -45 DEG C by the speed of clock；When products temperature is down to -40 DEG C, and holding 2 is small；Start to take out afterwards
Vacuum, when vacuum reaches 20pa, starts to warm up；Shelf temperature is risen to -10 DEG C with 0.3 DEG C/min of speed, works as visor
After the sample water heading line off of position, i.e., shelf temperature is risen to 25 DEG C with 2 DEG C/min of speed, setting limit vacuum, keeps the temperature 7
After hour, nitrogen charging emptying, that is, obtain cordyceps sinensis compound lyophilized products；Cordyceps sinensis compound is made using direct power compressing method
Lozenge.
Cordyceps sinensis compound buccal lozenge prepared by above-described embodiment 1-5 is subjected to appearance detection, it is as a result as follows：
The method of inspection：Take appropriate amount of sample to be placed in white porcelain dish, color and luster state is observed under natural light, smells its smell.
Table 1 is cordyceps sinensis compound buccal lozenge appearance test result.
Table 1
As can be seen from the above table, the cordyceps sinensis compound buccal lozenge prepared by the method for the present invention is observed under natural light, outside
Go sightseeing clean, there is uniform color and luster, and remain micro- fishy taste specific to cordyceps sinensis, illustrate to remain work(to the full extent
Imitate the natural characteristic of component.
Cordyceps sinensis compound buccal lozenge prepared by above-described embodiment 1-5 and aweto micropowder raw material are subjected to a huge sum of money respectively
Belong to assay, as a result as shown in table 2, table 3：
Table 2 is the heavy metal analysis result of the cordyceps sinensis compound buccal lozenge prepared by 1-5 of the embodiment of the present invention：
Table 2
Table 3 is heavy metal analysis result in aweto micropowder prepared by the present invention：
Table 3
Table 4 is the pollutant limitation regulation of corresponding generic food in GB 16740-2014 and GB 2762.
Table 4：Pollutant is limited the quantity
From above-mentioned testing result this it appears that：Total arsenic content of beary metal is implicitly present in folk prescription aweto micropowder
The problem of beyond national standard, but the cordyceps sinensis compound buccal lozenge being prepared by the method for the present invention is according to GB 5009.12, GB/T
5009.11st, 5009.17 methods of GB/T detect respectively, and the results show is all up to standard.Illustrate the form with Chinese medicine compound prescription compatibility,
It can be very good to solve security risk of the cordyceps sinensis folk prescription there are heavy metals exceeding standard；Compound Chinese prescription system can also have been played at the same time
Conditioning, synergistic advantage.Suspension material in the present invention carries out lyophilization under cryogenic vacuum state, avoid by
Vapor produces the side effects such as foam, oxidation, ensures the activity of active ingredient to the full extent.The material of freeze-dried preparation
Appearance uniform, specific surface area is big, loose structure is good, and dissolution velocity is fast.More conducively ensure cordyceps sinensis essence to be taken containing sheet mode
Magnificent limit release, reaches the ultimate attainment absorption of human body.And finished product lozenge is easy to take and stores.
Claims (3)
1. cordyceps sinensis compound buccal lozenge, it is characterised in that be made of the raw material of following weight parts：
5 ~ 30 ganoderma lucidum 5 ~ 60 of cordyceps sinensis
10 ~ 120 dendrobium candidum 8 ~ 50 of Radix Codonopsis
Roxburgh anoectochilus terminal bud 10 ~ 80；
The preparation method of above-mentioned cordyceps sinensis compound buccal lozenge is as follows：
（1）Learn from else's experience cleaning, the cordyceps sinensis of drying process is crushed, and obtains the aweto micropowder that mesh number is 300 ~ 1000；
（2）By ganoderma lucidum, Radix Codonopsis, dendrobium candidum, roxburgh anoectochilus terminal bud is measured, 8-15 times of water is added to decoct 1 ~ 3 time, when each 1-3 is small, decocting liquid mistake
Filter merges, and concentrates of every 1ml equivalent to crude drug 0.5-2g is concentrated under reduced pressure to give at 70 DEG C；
（3）By step（1）Gained aweto micropowder is added into above-mentioned concentrate by formula ratio, is stirred evenly, and is obtained cordyceps sinensis and is answered
Square suspension；
（4）Suspension is placed in stainless steel disc, liquid level 1cm, is placed on the shelf of freeze dryer, first with 1 DEG C/min
The shelf temperature of freeze dryer is down to -45 DEG C by speed；When products temperature is down to -40 DEG C, and holding 2 is small；Start to vacuumize afterwards,
When vacuum reaches 20-30pa, start to warm up；Shelf temperature is risen to -10 DEG C with 0.1-0.5 DEG C/min of speed, when regarding
After the sample water heading line off of mirror position, i.e., shelf temperature is risen to 25 DEG C with 1-2 DEG C/min of speed, setting limit vacuum, is protected
After when warm 6-8 is small, nitrogen charging emptying, that is, obtain cordyceps sinensis compound lyophilized products；The worm summer in winter is made using direct power compressing method
Careless compound buccal lozenge.
2. cordyceps sinensis compound buccal lozenge according to claim 1, it is characterised in that be made of the raw material of following weight parts：
10 ~ 20 ganoderma lucidum 10 ~ 40 of cordyceps sinensis
20 ~ 80 dendrobium candidum 20-40 of Radix Codonopsis
Roxburgh anoectochilus terminal bud 20-60.
3. cordyceps sinensis compound buccal lozenge according to claim 1, it is characterised in that be made of the raw material of following weight parts：
15 ganoderma lucidum 30 of cordyceps sinensis
60 dendrobium candidum 30 of Radix Codonopsis
Roxburgh anoectochilus terminal bud 40.
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| CN106722463A (en) * | 2016-11-29 | 2017-05-31 | 柳璐 | The processing method and its fire-dried stoned dates of one breeding spleen stomach invigorating fire-dried stoned dates |
| CN113455651A (en) * | 2021-07-09 | 2021-10-01 | 杨水祥 | A preparation containing stem cell extractive solution for improving metabolism and immunity and improving sub-health |
| CN115154553A (en) * | 2022-07-21 | 2022-10-11 | 福建稻鲜生文旅集团有限公司 | Anoectochilus roxburghii compound blood glucose reducing oral liquid, circulating extraction double-effect concentration preparation device and preparation method thereof |
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