CN104666934A - Cordyceps sinensis compound lozenge and preparation method thereof - Google Patents
Cordyceps sinensis compound lozenge and preparation method thereof Download PDFInfo
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- CN104666934A CN104666934A CN201510105925.7A CN201510105925A CN104666934A CN 104666934 A CN104666934 A CN 104666934A CN 201510105925 A CN201510105925 A CN 201510105925A CN 104666934 A CN104666934 A CN 104666934A
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Abstract
The invention discloses a cordyceps sinensis compound lozenge and a preparation method thereof. The cordyceps sinensis compound lozenge is a freeze-dried lozenge which is prepared from the following components in parts by weight: 5-30 parts of cordyceps sinensis, 5-60 parts of lucid ganoderma, 10-120 parts of codonopsis pilosula, 8-50 parts of dendrobium candidum and 10-80 parts of anoectochilus roxburghii. In form of traditional Chinese medicine compound compatibility, the cordyceps sinensis compound lozenge has the advantages of conditioning and synergistic interaction by a traditional Chinese medicine compound system and solves the potential safety hazard that a single cordyceps sinensis contains excessive heavy metals. The prepared lozenge ensures the activity of active ingredients to the maximum extent, and is uniform in appearance, large in specific surface area, good in porous structure and high in dissolving speed; as the cordyceps sinensis compound lozenge is orally taken in form of the lozenge, cordyceps sinensis essence is extremely released and extremely absorbed by a human body, so that the lozenge is easy to take and store.
Description
Technical field
The present invention relates to compound preparation of a kind of Chinese crude drug and preparation method thereof, specifically Cordyceps compound buccal lozenge and preparation method thereof.
Background technology
Cordyceps is that section ergot fungus cordyceps sinensis bacterium colonizes in Stroma on Hepialidae insect larvae and larva cadaveric complex.Nature and flavor are sweet flat, and return lung kidney channel, main active is cordycepin, cordycepic acid and Cordyceps polysaccharide, has adjustment invigorating the lung and the kidney, preventing phlegm from forming and stopping coughing, effect such as adjustment immunity of organisms, antitumor etc.
Cordyceps is wild rare medicinal herbs, main product in Jinsha jiang River, the Lancang River, Nujiang Three Rivers regions upstream.To the east of the Liangshan Mountain in Sichuan Province, to the Burang County in Tibet, North gets the Mount Min in Gansu Province, reach the Yulong Xueshan in the Himalayas and Yunnan Province in the south.The output of Cordyceps Sinensis From Tibet accounts for greatly 41% of national cordyceps yield, and Qinghai Province's output accounts for greatly 33% of national cordyceps yield, and it is upper and lower that Yunnan Province and Sichuan Province's cordyceps yield respectively account for 11%-16%.Because Cordyceps is that a kind of mushroom is biological, by the impact of self-sow environment, in Cordyceps medical material, content of beary metal fluctuation is large, and resource controllability is low, and Cordyceps folk prescription exists the potential safety hazard of heavy metals exceeding standard as health food.
Tradition uses Cordyceps to take to decoct more, boil, stew, soak, pulverize, chew food mode, modern study confirms: Cordyceps eats with decocting, boiling, stew, soak, pulverize, chew the traditional methods such as food, due to the okioplast wall (intracellular nutrition and energy account for more than 80% of its total amount) of Cordyceps can not be broken, absorption of human body utilization rate, less than 10%, causes a large amount of wastes of active ingredients of cordyceps sinensis.Cordyceps boils through heating, stewing loss, the destruction that high-temperature process can cause wherein multiple core essential ingredient, and effective rate of utilization reduces greatly.
Cordyceps is famous strengthening by means of tonics medicine, and how its scarcity of resources, develop utilization rate high, taking convenience, the product of use safety, for consumer provides more selection, is our problems faced.
Summary of the invention
There is heavy metals exceeding standard hidden danger to overcome existing single preparations of ephedrine in object of the present invention, Cordyceps raw material availability low exactly, takes the problems such as inconvenience and provide a kind of Cordyceps compound buccal lozenge preparation and preparation method thereof;
Cordyceps compound buccal lozenge of the present invention, is made up of the raw material of following weight parts:
Cordyceps 5 ~ 30 Ganoderma 5 ~ 60
Radix Codonopsis 10 ~ 120 Herba Dendrobii 8 ~ 50
Herba Anoectochili roxburghii 10 ~ 80.
Further preferred version, is made up of the raw material of following weight parts:
Cordyceps 10 ~ 20 Ganoderma 10 ~ 40
Radix Codonopsis 20 ~ 80 Herba Dendrobii 20-40
Herba Anoectochili roxburghii 20-60.
Further preferred version, is made up of the raw material of following weight parts:
Cordyceps 15 Ganoderma 30
Radix Codonopsis 60 Herba Dendrobii 30
Herba Anoectochili roxburghii 40.
The preparation method of described Cordyceps compound buccal lozenge, comprises the steps:
(1) learn from else's experience cleaning, dried Cordyceps pulverize, obtain the aweto micropowder that order number is 300 ~ 1000;
(2) by measuring Ganoderma, Radix Codonopsis, Herba Dendrobii, Herba Anoectochili roxburghii, add 8-15 times of soak by water 1 ~ 3 time, each 1-3 hour, decocting liquid filters and merges, and at 70 DEG C, concentrating under reduced pressure obtains the concentrated solution that every 1ml is equivalent to crude drug 0.5-2g;
(3) step (1) gained aweto micropowder is added in above-mentioned concentrated solution by formula ratio, stirs evenly, obtain Cordyceps compound recipe suspension;
(4) suspension is placed in stainless steel disc, liquid level is 1cm, is placed on the shelf of freeze dryer, first with the speed of 1 DEG C/min, the shelf temperature of freeze dryer is down to-45 DEG C; When products temperature is down to-40 DEG C, keep 2 hours; Start evacuation afterwards, when vacuum reaches 20-30pa, start to heat up; Shelf temperature is risen to-10 DEG C with the speed of 0.1-0.5 DEG C/min, when after the sample water heading line off of visor position, rises to 25 DEG C by shelf temperature with the speed of 1-2 DEG C/min, setting final vacuum, be incubated after 6-8 hour, fill nitrogen emptying, namely obtain Cordyceps compound recipe lyophilized products; Direct power compressing method is adopted namely to make Cordyceps compound buccal lozenge.
The present invention is made up of Cordyceps, Ganoderma, Radix Codonopsis, Herba Dendrobii, Herba Anoectochili roxburghii five kinds of raw materials, wherein Cordyceps: sweet in the mouth is put down, and is the product of flat tonifying the lung kidney; Kind energy tonifying the lung gas, lung benefiting is cloudy, kidney-replenishing, benefiting essence-blood, energy hemostasis and phlegm of holding concurrently; With controlling deficiency of both the lung and kidney, taking the photograph to receive and having no right.Modern pharmacology research proves, Cordyceps have antibacterial, immunomodulating, anticancer, antiinflammatory, improve the effects such as adrenal cortex alcohol content, arrhythmia, resisting fatigue, eliminating phlegm and relieving asthma, tranquilizing soporific, effect is extensively.Ganoderma wherein has the reputation of Herba mesonae chinensis from ancient times, and its nature and flavor are sweet, flat, and GUIXIN, lung, liver, kidney channel, have invigorating QI and tranquilization, the merit of relieving cough and asthma.Modern pharmacology research confirms, the effects such as Ganoderma has antitumor, immunomodulating, blood sugar lowering, protects the liver, defying age, anti-inflammatory and antalgic, cardioprotection, anticoagulation.Two medicines share, and invigorating the lung and the kidney, benefiting vital QI for tranquillizing, plays strengthening by means of tonics altogether, consolidates the merit of righting, is monarch drug altogether.Radix Codonopsis wherein, Herba Dendrobii nourish blood kidney tonifying, Yin-nourishing and body fluid promoting, are ministerial drug; Two medicines close and with it, to help vital energy benefiting and the kidney invigorating, the effect nourished blood of promoting the production of body fluid.Herba Anoectochili roxburghii clearing away heat and cooling blood, removing dampness and detoxicating, reinforce the kidney suppressing the hyperactive liver; All medicines share and play Yin Yang balancing, strengthening the body resistance, skin care of promoting the production of body fluid, QI and blood regulating, the five internal organs altogether, support the longevity merit of prolonging life; Reach the liver protecting, improve body immunity comprehensively, strengthen human body to the effect of the resistance of disease.
The present invention, by the form of Chinese medicine compound compatibility, had both played the advantage of compound Chinese prescription systemic regulation, Synergistic, had solved again the potential safety hazard that Cordyceps folk prescription exists heavy metals exceeding standard.In the present invention, compound recipe suspension material carries out sublimation drying under cryogenic vacuum state, avoids and produces the side effect such as foam, oxidation by steam, ensures the activity of effective ingredient to the full extent.Through material appearance uniform prepared by lyophilization, specific surface area is large, loose structure good, and dissolution velocity is fast.Be more conducive to ensure the release of the Cordyceps elite limit to take containing sheet mode, reach the ultimate attainment absorption of human body.And finished product buccal tablet is easy to take and store.
Detailed description of the invention
Embodiment 1
(1) learn from else's experience cleaning, dried Cordyceps pulverize, obtain the aweto micropowder that order number is 300 ~ 1000;
(2) get Ganoderma 30g, Radix Codonopsis 60g, Herba Dendrobii 30g, Herba Anoectochili roxburghii 40g respectively, add 8-15 times of soak by water 1 ~ 3 time, each 1-3 hour, decocting liquid filters and merges, and at 70 DEG C, concentrating under reduced pressure obtains the concentrated solution that every 1ml is equivalent to 0.5g crude drug;
(3) step (1) gained aweto micropowder 15g is added in above-mentioned concentrated solution, stirs evenly, obtain Cordyceps compound recipe suspension;
(4) suspension is placed in stainless steel disc, liquid level is 1cm, is placed on the shelf of freeze dryer, first with the speed of 1 DEG C/min, the shelf temperature of freeze dryer is down to-45 DEG C; When products temperature is down to-40 DEG C, keep 2 hours; Start evacuation afterwards, when vacuum reaches 20pa, start to heat up; Shelf temperature is risen to-10 DEG C with the speed of 0.3 DEG C/min, when after the sample water heading line off of visor position, rises to 25 DEG C by shelf temperature with the speed of 1 DEG C/min, setting final vacuum, be incubated after 8 hours, fill nitrogen emptying, namely obtain Cordyceps compound recipe lyophilized products; Direct power compressing method is adopted namely to make Cordyceps compound buccal lozenge.
Embodiment 2
(1) learn from else's experience cleaning, dried Cordyceps pulverize, obtain the aweto micropowder that order number is 300 ~ 1000;
(2) get Ganoderma 40g, Radix Codonopsis 80g, Herba Dendrobii 40g, Herba Anoectochili roxburghii 60g respectively, add 8-15 times of soak by water 1 ~ 3 time, each 1-3 hour, decocting liquid filters and merges, and at 70 DEG C, concentrating under reduced pressure obtains the concentrated solution that every 1ml is equivalent to 1.0g crude drug;
(3) step (1) gained aweto micropowder 20g is added in above-mentioned concentrated solution, stirs evenly, obtain Cordyceps compound recipe suspension;
(4) suspension is placed in stainless steel disc, liquid level is 1cm, is placed on the shelf of freeze dryer, first with the speed of 1 DEG C/min, the shelf temperature of freeze dryer is down to-45 DEG C; When products temperature is down to-40 DEG C, keep 2 hours; Start evacuation afterwards, when vacuum reaches 30pa, start to heat up; Shelf temperature is risen to-10 DEG C with the speed of 0.5 DEG C/min, when after the sample water heading line off of visor position, rises to 25 DEG C by shelf temperature with the speed of 1 DEG C/min, setting final vacuum, be incubated after 6 hours, fill nitrogen emptying, namely obtain Cordyceps compound recipe lyophilized products; Direct power compressing method is adopted namely to make Cordyceps compound buccal lozenge.
Embodiment 3
(1) learn from else's experience cleaning, dried Cordyceps pulverize, obtain the aweto micropowder that order number is 300 ~ 1000;
(2) get Ganoderma 20g, Radix Codonopsis 100g, Herba Dendrobii 30g, Herba Anoectochili roxburghii 50g respectively, add 8-15 times of soak by water 1 ~ 3 time, each 1-3 hour, decocting liquid filters and merges, and at 70 DEG C, concentrating under reduced pressure obtains the concentrated solution that every 1ml is equivalent to 2g crude drug;
(3) step (1) gained aweto micropowder 30g is added in above-mentioned concentrated solution, stirs evenly, obtain Cordyceps compound recipe suspension;
(4) suspension is placed in stainless steel disc, liquid level is 1cm, is placed on the shelf of freeze dryer, first with the speed of 1 DEG C/min, the shelf temperature of freeze dryer is down to-45 DEG C; When products temperature is down to-40 DEG C, keep 2 hours; Start evacuation afterwards, when vacuum reaches 20pa, start to heat up; Shelf temperature is risen to-10 DEG C with the speed of 0.1 DEG C/min, when after the sample water heading line off of visor position, rises to 25 DEG C by shelf temperature with the speed of 2 DEG C/min, setting final vacuum, be incubated after 7 hours, fill nitrogen emptying, namely obtain Cordyceps compound recipe lyophilized products; Direct power compressing method is adopted namely to make Cordyceps compound buccal lozenge.
Embodiment 4
(1) learn from else's experience cleaning, dried Cordyceps pulverize, obtain the aweto micropowder that order number is 300 ~ 1000;
(2) get Ganoderma 35g, Radix Codonopsis 75g, Herba Dendrobii 25g, Herba Anoectochili roxburghii 45g respectively, add 8-15 times of soak by water 1 ~ 3 time, each 1-3 hour, decocting liquid filters and merges, and at 70 DEG C, concentrating under reduced pressure obtains the concentrated solution that every 1ml is equivalent to 1.5g crude drug;
(3) step (1) gained aweto micropowder 20g is added in above-mentioned concentrated solution, stirs evenly, obtain Cordyceps compound recipe suspension;
(4) suspension is placed in stainless steel disc, liquid level is 1cm, is placed on the shelf of freeze dryer, first with the speed of 1 DEG C/min, the shelf temperature of freeze dryer is down to-45 DEG C; When products temperature is down to-40 DEG C, keep 2 hours; Start evacuation afterwards, when vacuum reaches 25pa, start to heat up; Shelf temperature is risen to-10 DEG C with the speed of 0.3 DEG C/min, when after the sample water heading line off of visor position, rises to 25 DEG C by shelf temperature with the speed of 1 DEG C/min, setting final vacuum, be incubated after 8 hours, fill nitrogen emptying, namely obtain Cordyceps compound recipe lyophilized products; Direct power compressing method is adopted namely to make Cordyceps compound buccal lozenge.
Embodiment 5
(1) learn from else's experience cleaning, dried Cordyceps pulverize, obtain the aweto micropowder that order number is 300 ~ 1000;
(2) get Ganoderma 50g, Radix Codonopsis 50g, Herba Dendrobii 40g, Herba Anoectochili roxburghii 65g respectively, add 8-15 times of soak by water 1 ~ 3 time, each 1-3 hour, decocting liquid filters and merges, and at 70 DEG C, concentrating under reduced pressure obtains the concentrated solution that every 1ml is equivalent to 1.5g crude drug;
(3) step (1) gained aweto micropowder 30g is added in above-mentioned concentrated solution, stirs evenly, obtain Cordyceps compound recipe suspension;
(4) suspension is placed in stainless steel disc, liquid level is 1cm, is placed on the shelf of freeze dryer, first with the speed of 1 DEG C/min, the shelf temperature of freeze dryer is down to-45 DEG C; When products temperature is down to-40 DEG C, keep 2 hours; Start evacuation afterwards, when vacuum reaches 20pa, start to heat up; Shelf temperature is risen to-10 DEG C with the speed of 0.3 DEG C/min, when after the sample water heading line off of visor position, rises to 25 DEG C by shelf temperature with the speed of 2 DEG C/min, setting final vacuum, be incubated after 7 hours, fill nitrogen emptying, namely obtain Cordyceps compound recipe lyophilized products; Direct power compressing method is adopted namely to make Cordyceps compound buccal lozenge.
Cordyceps compound buccal lozenge prepared by above-described embodiment 1-5 is carried out outward appearance detection, and result is as follows:
The method of inspection: get appropriate amount of sample and be placed in white porcelain dish, observe color and luster state under natural light, smell its abnormal smells from the patient.
Table 1 is Cordyceps compound buccal lozenge appearance test result.
Table 1
As can be seen from the above table, Cordyceps compound buccal lozenge prepared by the inventive method is observed under natural light, and smooth appearance has uniform color and luster, and remain micro-fishy taste specific to Cordyceps, the natural characteristic remaining functional component is to the full extent described.
Cordyceps compound buccal lozenge prepared by above-described embodiment 1-5 and aweto micropowder raw material are carried out content of beary metal mensuration respectively, and result is as shown in table 2, table 3:
Table 2 is heavy metal analysis results of the Cordyceps compound buccal lozenge prepared by embodiment of the present invention 1-5:
Table 2
Table 3 is heavy metal analysis results in the aweto micropowder prepared by the present invention:
Table 3
Table 4 is pollutant limitation regulations of corresponding generic food in GB 16740-2014 and GB 2762.
Table 4: pollutant are limited the quantity
Can obviously find out from above-mentioned testing result: in folk prescription aweto micropowder, really there is the problem that total arsenic content of beary metal exceeds GB, but the Cordyceps compound buccal lozenge prepared by the inventive method is detected respectively according to GB 5009.12, GB/T 5009.11, GB/T 5009.17 method, result display is all up to standard.The form using Chinese medicine compound compatibility is described, the potential safety hazard that Cordyceps folk prescription exists heavy metals exceeding standard can well be solved; The advantage of compound Chinese prescription systemic regulation, Synergistic can also have been played simultaneously.Suspension material in the present invention carries out sublimation drying under cryogenic vacuum state, avoids and produces the side effect such as foam, oxidation by steam, ensures the activity of effective ingredient to the full extent.Through material appearance uniform prepared by lyophilization, specific surface area is large, loose structure good, and dissolution velocity is fast.Be more conducive to ensure the release of the Cordyceps elite limit to take containing sheet mode, reach the ultimate attainment absorption of human body.And finished product buccal tablet is easy to take and store.
Claims (4)
1. Cordyceps compound buccal lozenge, is characterized in that being made up of the raw material of following weight parts:
Cordyceps 5 ~ 30 Ganoderma 5 ~ 60
Radix Codonopsis 10 ~ 120 Herba Dendrobii 8 ~ 50
Herba Anoectochili roxburghii 10 ~ 80.
2. Cordyceps compound buccal lozenge according to claim 1, is characterized in that being made up of the raw material of following weight parts:
Cordyceps 10 ~ 20 Ganoderma 10 ~ 40
Radix Codonopsis 20 ~ 80 Herba Dendrobii 20-40
Herba Anoectochili roxburghii 20-60.
3. Cordyceps compound buccal lozenge according to claim 1, is characterized in that being made up of the raw material of following weight parts:
Cordyceps 15 Ganoderma 30
Radix Codonopsis 60 Herba Dendrobii 30
Herba Anoectochili roxburghii 40.
4. the preparation method of the Cordyceps compound buccal lozenge according to any one of claim 1 ~ 3, is characterized in that comprising the steps:
(1) learn from else's experience cleaning, dried Cordyceps pulverize, obtain the aweto micropowder that order number is 300 ~ 1000;
(2) by measuring Ganoderma, Radix Codonopsis, Herba Dendrobii, Herba Anoectochili roxburghii, add 8-15 times of soak by water 1 ~ 3 time, each 1-3 hour, decocting liquid filters and merges, and at 70 DEG C, concentrating under reduced pressure obtains the concentrated solution that every 1ml is equivalent to crude drug 0.5-2g;
(3) step (1) gained aweto micropowder is added in above-mentioned concentrated solution by formula ratio, stirs evenly, obtain Cordyceps compound recipe suspension;
(4) suspension is placed in stainless steel disc, liquid level is 1cm, is placed on the shelf of freeze dryer, first with the speed of 1 DEG C/min, the shelf temperature of freeze dryer is down to-45 DEG C; When products temperature is down to-40 DEG C, keep 2 hours; Start evacuation afterwards, when vacuum reaches 20-30pa, start to heat up; Shelf temperature is risen to-10 DEG C with the speed of 0.1-0.5 DEG C/min, when after the sample water heading line off of visor position, rises to 25 DEG C by shelf temperature with the speed of 1-2 DEG C/min, setting final vacuum, be incubated after 6-8 hour, fill nitrogen emptying, namely obtain Cordyceps compound recipe lyophilized products; Direct power compressing method is adopted namely to make Cordyceps compound buccal lozenge.
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| CN106722463A (en) * | 2016-11-29 | 2017-05-31 | 柳璐 | The processing method and its fire-dried stoned dates of one breeding spleen stomach invigorating fire-dried stoned dates |
| CN113455651A (en) * | 2021-07-09 | 2021-10-01 | 杨水祥 | A preparation containing stem cell extractive solution for improving metabolism and immunity and improving sub-health |
| CN115154553A (en) * | 2022-07-21 | 2022-10-11 | 福建稻鲜生文旅集团有限公司 | Anoectochilus roxburghii compound blood glucose reducing oral liquid, circulating extraction double-effect concentration preparation device and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106389870A (en) * | 2016-08-28 | 2017-02-15 | 广西吉光生态科技有限公司 | Anoectochilus roxburghii pill and preparation method thereof |
| CN106722463A (en) * | 2016-11-29 | 2017-05-31 | 柳璐 | The processing method and its fire-dried stoned dates of one breeding spleen stomach invigorating fire-dried stoned dates |
| CN113455651A (en) * | 2021-07-09 | 2021-10-01 | 杨水祥 | A preparation containing stem cell extractive solution for improving metabolism and immunity and improving sub-health |
| CN115154553A (en) * | 2022-07-21 | 2022-10-11 | 福建稻鲜生文旅集团有限公司 | Anoectochilus roxburghii compound blood glucose reducing oral liquid, circulating extraction double-effect concentration preparation device and preparation method thereof |
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