CN104649845A - Amino acid organic fertilizer using hairs as raw materials and preparation method thereof - Google Patents
Amino acid organic fertilizer using hairs as raw materials and preparation method thereof Download PDFInfo
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- CN104649845A CN104649845A CN201410321891.0A CN201410321891A CN104649845A CN 104649845 A CN104649845 A CN 104649845A CN 201410321891 A CN201410321891 A CN 201410321891A CN 104649845 A CN104649845 A CN 104649845A
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- amino acid
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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Abstract
The invention discloses an amino acid organic fertilizer using hairs as raw materials and a preparation method of the amino acid organic fertilizer. The method comprises the following steps: hydrolyzing the hairs such as pig hairs, hairs and the like used as raw materials by adding acid to prepare an amino acid liquid; uniformly stirring microbial-organics, micro-elements, nitrogen-phosphorus-potassium total nutrients, secondary elements and the amino acid liquid; and drying and screening to prepare the amino acid organic fertilizer. The amino acid organic fertilizer comprises the following components in percentage by mass: 15-30 percent of microbial-organics, 15-30 percent of nitrogen-phosphorus-potassium total nutrients, 0.1-5 percent of microelements, 5-30 percent of secondary elements, 8-20 percent of amino acid liquid, and 5-20 percent of water contents. According to the amino acid organic fertilizer, a soil structure can be improved, the soil is activated, the cost is reduced, the environment pollution is reduced, the nutrition is complete and the utilization rate of the fertilizer is high.
Description
Technical field
The present invention relates to a kind of organic fertilizer and preparation method thereof, be specifically related to a kind of with the hairs such as human hair, pig hair amino acid organic fertilizer that is raw material and preparation method thereof.
Background technology
In amino acid fertilizer, amino acid is present in fertilizer as the smallest molecule forming protein, is easy to absorbed by crops; Also be improved fertilising object disease resistance, improve the function of fertilising crop quality.Can supplement plant essential amino acid containing amino acid whose organic fertilizer, stimulation and regulating plant grow fast, impel plant-growth healthy and strong, promote the absorption to nutritive substance, strengthen the metabolic function of plant, improve photosynthesis, promote that root system of plant is flourishing, accelerate plant-growth breeding.Traditional fertilizer has its advantage, but fertilizer efficiency is slow, utilization ratio is low, easily pollutes.And major ingredient is keratoprotein in the hairs such as pig hair, hair, account for 97%, keratoprotein is then made up of amino acid.Using the amino acid that extracts in the hairs such as pig hair, the hair raw material as amino acid fertilizer, can reduce and obtain amino acid whose cost, as the amino acid whose raw material of important component made for raw material with materials such as hair, pig hairs in amino acid fertilizer, also fertilizer cost of manufacture can be reduced.
Publication number is patent discloses " a kind of amino acid biological fish fertilizer and making method " of CN101836692A, although be also for raw material production amino acid powder in this technical scheme with hair etc., and also containing trace element, but this biological fish-fertilizer is the growth characteristics for the fish in aquaculture and food organism, and be not suitable for the growth characteristics of farm crop, the process of simultaneously also not drying in preparation process.
Summary of the invention
The object of the present invention is to provide a kind of growth characteristics for farm crop and what research and develop take hair as the amino acid fertilizer that raw material is made.
Another object of the present invention is that providing a kind of is the aminoacids solution that raw material is made with hair, then adds the preparation method that amino acid fertilizer made by various auxiliary material.
For meeting above-mentioned purpose, technical scheme of the present invention is: a kind of take hair as the amino acid fertilizer of raw material, it is made up of by mass percentage following raw material: biological organic matter 15%-30%, N P and K total nutrient 15%-30%, trace element 0.1%-5%, moderate-element 5%-30%, amino acid 8%-20%, moisture content 5%-20%.Described N P and K total nutrient bag Nitrogen element, phosphoric, potassium element; Wherein nitrogen element source is in urea, and phosphoric derives from monoammonium phosphate fertilizer, and potassium element derives from potassium sulphate fertilizer.Described biological organic matter is acid-sludge and the rapeseed cake mixture through spontaneous fermentation, and wherein the mass ratio of acid-sludge and rapeseed cake is 1:2; Described trace element comprises at least one in ferro element, manganese element, zinc element, copper, molybdenum element, boron; Described moderate-element comprises element silicon, calcium constituent, magnesium elements, element sulphur; Wherein element silicon derives from silicate, and calcium constituent is at least one in peroxophosphoric acid calcareous fertilisers, lime nitrogen and fused(calcium magnesium)phosphate; Magnesium elements derives from least one in potash magnesium sulphate fertilizer, magnesium sulfate fertilizer, fused(calcium magnesium)phosphate; Element sulphur derives from sulfate radical salt.
Further, the arsenic of described amino acid fertilizer, lead, cadmium, mercury, chromium total content are less than 0.02%.
Of the present invention is that the preparation method of the amino acid fertilizer of raw material comprises the steps: with hair
A. amino acid whose production:
A. hair, hydrochloric acid and water join in reactor according to mass ratio 1:2.5:1.2, and wherein concentration of hydrochloric acid is 35%, at 120 DEG C-150 DEG C, react 8h-10h;
B. normal temperature is cooled to;
C. first time neutralization, adds the neutralization of a certain amount of liquefied ammonia, until pH value is 2.5-3.5;
D. first time filters, and retains filtrate, and decolours to filtrate;
E. second time neutralization, adds the neutralization of a certain amount of liquefied ammonia, until pH value is 3.5-4.5;
F. second time is filtered, and retains filtrate, and to for subsequent use after filtrate decolouring;
B. the production of amino acid fertilizer:
A. biological organic matter is pulverized, then add N P and K total nutrient, trace element, moderate-element stir, in the process stirred, add aminoacids solution, until stir;
B. send into dryer, at the temperature of 60 DEG C-80 DEG C, dryer is rotated in front, opens moisture rapid steamer simultaneously, continues 1-3 minute;
C. reverse side rotates dryer, until moisture content is not more than 20%;
D. screen, open vibrating screener, isolate the finished product that particle diameter is 2mm-5mm;
E. check;
F. pack;
G. put in storage.
Owing to have employed above technical scheme, the following beneficial effect of tool of the present invention is:
1, improve crop yield, containing the amino acid required for farm crop in product, medium trace element etc., are conducive to the absorption of farm crop, improve the output of farm crop.
2, comprehensive nutrition, utilization rate of fertilizer is high.Trace element, moderate-element play an active part in carbohydrate and portein metabolism in plant materials, as boron, promote carbohydrate transport, be conducive to the synthesis of protein and the fertilization of seed can be promoted, manganese, can promote Amino acid synthesis, be conducive to protein synthesis, can promote the raw amino acid of hydrolase polypeptide and the tissue of fortune new life and organ; Zinc, zinc can promote that carbohydrate synthesizes; Molybdenum, can promote leguminous crop fixed nitrogen; Calcium, can strengthen resistance against diseases, is conducive to formation and the growth of plant cell wall, promotes that ginseng hydrate transforms and metabolism; Magnesium, plays activation to a lot of enzymes in crop, affects photosynthetic, respiration.
3, Soil structure is improved, activating soil.Biological organic matter can make cohesive soil become loose, sandy soil can be made to reunite, improve the physical properties of soil, can adsorb a large amount of positively charged ion side moisture, improve the ability of soil fertilizer retaining, extend and improve fertilizer efficiency.
4, reduce costs.With hair, pig hair for raw material production amino acid fertilizer, greatly can must reduce amino acid whose acquisition cost, thus reduce the production cost of amino acid fertilizer; And biological organic matter adopts rapeseed cake and acid-sludge etc. again to utilize material, also reduces cost to a certain extent.
5, environmental pollution is reduced.Amino acid fertilizer has the characteristic of farm manure, and wherein ingredient origin is in soil, reduces in soil, reaches a benign cycle structure, thus reaches and safeguard ecotope object.
Accompanying drawing explanation
Fig. 1 is amino acid whose process flow sheet.
Fig. 2 is the explained hereafter schema of amino acid fertilizer.
Embodiment
Take hair as the amino acid fertilizer that raw material is made, be made up of according to mass ratio following raw material:
Table 1 is for being the amino acid fertilizer formula that raw material is made with hair;
Table 1 embodiment unit: mass percent
Described N P and K total nutrient bag Nitrogen element, phosphoric, potassium element; Wherein nitrogen element source is in urea, and phosphoric derives from monoammonium phosphate fertilizer, and potassium element derives from potassium sulphate fertilizer.
Described biological organic matter is acid-sludge and the rapeseed cake mixture through spontaneous fermentation, and wherein the mass ratio of acid-sludge and rapeseed cake is 1:2.Described trace element comprises at least one in ferro element, manganese element, zinc element, copper, molybdenum element, boron; Described moderate-element comprises element silicon, calcium constituent, magnesium elements, element sulphur; Wherein element silicon derives from silicate, and calcium constituent is at least one in peroxophosphoric acid calcareous fertilisers, lime nitrogen and fused(calcium magnesium)phosphate; Magnesium elements derives from least one in potash magnesium sulphate fertilizer, magnesium sulfate fertilizer, fused(calcium magnesium)phosphate; Element sulphur derives from sulfate radical salt.
The total content of the arsenic in described amino acid fertilizer, lead, cadmium, mercury, chromium is less than 0.02%.
Preparation method's concrete steps of the present invention are as follows:
First be amino acid whose production (see Fig. 1): a. hair, hydrochloric acid and water join in reactor according to mass ratio 1:2.5:1.2, and wherein hydrochloric acid volumetric concentration is 35%, react 8h or 9h or 10h at 120 DEG C or 130 DEG C or 150 DEG C; B. normal temperature is cooled to; C. first time neutralization, adds the neutralization of a certain amount of liquefied ammonia, until pH value is 2.5 or 3 or 3.5; D. first time filters, and retains filtrate, and decolours to filtrate; E. second time neutralization, adds the neutralization of a certain amount of liquefied ammonia, until pH value is 3.5 or 4 or 4.5; H. second time is filtered, and retains filtrate, and to for subsequent use after filtrate decolouring;
Secondly be the production (see Fig. 2) of amino acid fertilizer: biological organic matter is pulverized by a., add N P and K total nutrient, trace element, moderate-element again, then stir, in the process stirred, add aminoacids solution for subsequent use, until stir; B. dryer is rotated in front, at the temperature of 60 DEG C or 70 DEG C or 80 DEG C, opens moisture rapid steamer simultaneously, continues 1min or 2min or 3min; C. send into dryer, reverse side rotates dryer, until moisture content is not more than 20%; D. screen, open vibrating screener, isolate the finished product that particle diameter is 2mm-5mm; E. check; F. pack; G. put in storage.
1. the weather condition requirement of the use of pair farm crop product of the present invention
The weather condition such as the growth of farm crop and humidity, illumination and temperature have close relationship.
2. manurial experiment and effect
Applicant of the present invention has carried out to 2 of identical area mu of age of trees sand pear of more than 5 years tree the test executing common amino acid fertilizer and amino acid fertilizer of the present invention in March, 2011-October, and contrasts ultimate capacity, sugariness.During the 3-10 month, need to execute twice fertilizer.
Table 2 is for using amino acid fertilizer of the present invention and the fertile impact on sand pear tree output of common amino acid.
Table 2
As can be seen from Table 2, use the output that amino acid fertilizer of the present invention makes sand pear set and be obtained for very large raising.
Table 3 is for using amino acid fertilizer of the present invention and common amino acid fertilizer on the impact of sand pear tree sugariness.
Table 3
As can be seen from Table 3, amino acid fertilizer of the present invention is used to the sugariness that sand pear the is set effect of improving a lot.
Cultivate application example
Cultivate application example 1
Within 2009, to set up the application of the Sugarcane amino acid fertilizer of the present invention of 20 mu in Zigong City Rong County, Sichuan Province: within 2009,20 mu of white sugarcane fields are divided into two pieces in Zigong City Rong County, Sichuan Province and implement ground: A sugarcane field and B sugarcane field.In on February 4th, 2009 according to every mu of 5400 strains about white sugarcane seed is planted in A sugarcane field and B sugarcane field, by the end of March A sugarcane field is imposed according to every mu of 50kg and add amino acid fertilizer of the present invention, B sugarcane field is imposed according to every mu of 50kg and adds existing common amino acid fertilizer; By the end of July according to every mu, 15kg amino acid fertilizer of the present invention is applied to A, B sugarcane field is used and applies 15kg common amino acid fertilizer of the prior art according to every mu; Gather mid-December.In A sugarcane field, the output of white sugarcane is average every mu of 6500kg, and sugariness is 23.2; In B sugarcane field, the output of white sugarcane is average every mu of 6050kg, and sugariness is 22.A sugarcane field is for B sugarcane field, and white sugarcane yield is every mu of increase 450kg on average, and sugariness on average increases by 1.3%.
Cultivate application example 2
2011 corn fields setting up 80 mu in Bi Jiang county of Tongren district Guizhou Province city use the application of amino acid fertilizer of the present invention: within 2011, be equally divided into two pieces of ground at Tongren district Guizhou Province to 80 mu of corn fields: first corn field and second corn field.Inside the first corn field of to plant application according to the maize seedling about every mu of 4200 strains on April 5th, 2011 and second corn field, first corn field is used to the amino acid fertilizer of this product simultaneously according to every mu of 45kg, according to every mu of 45kg, common amino acid fertilizer of the prior art is used to corn field; Then mid-June the amino acid fertilizer of this product is added inside corn field according to every mu of 25kg to first corn field, according to every mu of 25kg, common amino acid of the prior art is applied to second corn field fertile; In gathering by the end of August.Output on average every mu of 710kg of first corn, second corn field output on average every mu be 568kg, first corn field and second corn field comparatively speaking, on average every mu of volume increase 20%.
Cultivate application example 3
Within 2013, set up the application of 60 mu of rice application amino acid fertilizers of the present invention in Lixian County, Hunan Province: 2013 are equally divided into the first rice terrace and the second rice terrace in Lixian County, Hunan Province to 60 mu of rice terraces.In the first rice terrace, amino acid fertilizer of the present invention is applied according to every mu of 50kg on April 6th, 2013, fertile to applying common amino acid of the prior art according to every mu of 50kg in the second rice terrace;
And with mid-May by be highly the seedling transplantation of about 8cm in the first rice terrace after applying fertilizer and the second rice terrace, and about ensureing every mu of rice transplanting 1.1-1.3 ten thousand pocket; Common amino acid fertilizer of the prior art, to applying in the first rice terrace according to every mu of 35kg by amino acid fertilizer of the present invention, applies in the second rice terrace according to every mu of 35kg by April 17 simultaneously; Gathered at the beginning of 9 months.Output in first rice terrace is every mu of 690kg on average, mean vol on average every mu of 545kg in the second rice terrace, every mu of volume increase 21%.
Claims (7)
1. be an amino acid fertilizer for raw material with hair, it is made up of by mass percentage following raw material:
Biological organic matter 15%-30% N P and K total nutrient 15%-30%
Trace element 0.1%-5% moderate-element 5%-30%
Amino acid 8%-20% moisture content 5%-20%
Described biological organic matter is acid-sludge and the rapeseed cake mixture through spontaneous fermentation, and wherein the mass ratio of acid-sludge and rapeseed cake is 1:2;
Described N P and K total nutrient bag Nitrogen element, phosphoric, potassium element; Wherein nitrogen element source is in urea, and phosphoric derives from monoammonium phosphate fertilizer, and potassium element derives from potassium sulphate fertilizer;
Described trace element comprises at least one in ferro element, manganese element, zinc element, copper, molybdenum element, boron;
Described moderate-element comprises element silicon, calcium constituent, magnesium elements, element sulphur; Wherein element silicon derives from silicate, and calcium constituent is at least one in peroxophosphoric acid calcareous fertilisers, lime nitrogen and fused(calcium magnesium)phosphate; Magnesium elements derives from least one in potash magnesium sulphate fertilizer, magnesium sulfate fertilizer, fused(calcium magnesium)phosphate; Element sulphur derives from vitriol.
2. amino acid fertilizer according to claim 1, is characterized in that: the arsenic in described amino acid fertilizer, lead, cadmium, mercury, chromium total content are less than 0.02%.
3. amino acid fertilizer according to claim 1, is characterized in that described amino acid fertilizer is made up of according to mass ratio following raw material:
Biological organic matter 21.9% N P and K total nutrient 30%
Trace element 0.1% moderate-element 20%
Amino acid 8% moisture content 20%.
4. amino acid fertilizer according to claim 1, is characterized in that described amino acid fertilizer is made up of according to mass ratio following raw material:
Biological organic matter 21% N P and K total nutrient 25%
Trace element 2% moderate-element 25%
Amino acid/11 2% moisture content 15%.
5. amino acid fertilizer according to claim 1, is characterized in that described amino acid fertilizer is made up of according to mass ratio following raw material:
Biological organic matter 18% N P and K total nutrient 25%
Trace element 1% moderate-element 30%
Amino acid/11 6% moisture content 10%.
6. amino acid fertilizer according to claim 1, is characterized in that described amino acid fertilizer is made up of according to mass ratio following raw material:
Biological organic matter 20% N P and K total nutrient 30%
Trace element 5% moderate-element 15%
Amino acid 20% moisture content 10%.
7. the preparation method of amino acid fertilizer according to claim 1, its step system is:
A. amino acid whose production:
A. hair, hydrochloric acid and water join in reactor according to mass ratio 1:2.5:1.2, and wherein concentration of hydrochloric acid is 35%, at 120 DEG C-150 DEG C, react 8h-10h;
B. normal temperature is cooled to;
C. first time neutralization, adds the neutralization of a certain amount of liquefied ammonia, until pH value is 2.5-3.5;
D. first time filters, and retains filtrate, and decolours to filtrate;
E. second time neutralization, adds the neutralization of a certain amount of liquefied ammonia, until pH value is 3.5-4.5;
F. second time is filtered, and retains filtrate, and to for subsequent use after filtrate decolouring;
B. the production of amino acid fertilizer:
A. biological organic matter is pulverized, then add N P and K total nutrient, trace element, moderate-element stir, in the process stirred, add aminoacids solution for subsequent use, until stir;
B. send into dryer, at the temperature of 60 DEG C-80 DEG C, dryer is rotated in front, opens moisture rapid steamer simultaneously, continues 1-3 minute;
C. reverse side rotates dryer, until moisture content is not more than 20%;
D. screen, open vibrating screener, isolate the finished product that particle diameter is 2mm-5mm;
E. check;
F. pack;
G. put in storage.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105037052A (en) * | 2015-09-06 | 2015-11-11 | 柳建 | Modifying agent used for repairing soil obstacles of protected area and preparation method thereof |
| CN106116807A (en) * | 2016-06-21 | 2016-11-16 | 刘月华 | A kind of ornamental trees and shrubs dedicated fertilizer and preparation technology thereof |
| CN107417437A (en) * | 2017-09-27 | 2017-12-01 | 界首市明亮种植专业合作社 | The preparation method of one boar hair ferment fertilizer |
| CN109089806A (en) * | 2018-08-30 | 2018-12-28 | 安徽双花生态农业开发有限公司 | A kind of implantation methods of the bletilla striata |
| CN109384595A (en) * | 2018-12-12 | 2019-02-26 | 龙永久 | A kind of amino acid Eco-fertilizer and preparation method thereof |
| CN109627091A (en) * | 2019-01-10 | 2019-04-16 | 盐源地金源农业服务有限公司 | A kind of plant health fertilizer and preparation method thereof |
| CN109796290A (en) * | 2019-04-04 | 2019-05-24 | 陕西开耘生态农业股份有限公司 | A kind of compound fertilizer containing potassium fulvate |
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| CN1342627A (en) * | 2001-10-30 | 2002-04-03 | 刘润发 | Organic-inorganic mixed multi-element fertilizer in chelate state |
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| CN103086795A (en) * | 2013-01-24 | 2013-05-08 | 广西大学 | Amino-acid chelated organic fertilizer and production method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105037052A (en) * | 2015-09-06 | 2015-11-11 | 柳建 | Modifying agent used for repairing soil obstacles of protected area and preparation method thereof |
| CN106116807A (en) * | 2016-06-21 | 2016-11-16 | 刘月华 | A kind of ornamental trees and shrubs dedicated fertilizer and preparation technology thereof |
| CN107417437A (en) * | 2017-09-27 | 2017-12-01 | 界首市明亮种植专业合作社 | The preparation method of one boar hair ferment fertilizer |
| CN109089806A (en) * | 2018-08-30 | 2018-12-28 | 安徽双花生态农业开发有限公司 | A kind of implantation methods of the bletilla striata |
| CN109384595A (en) * | 2018-12-12 | 2019-02-26 | 龙永久 | A kind of amino acid Eco-fertilizer and preparation method thereof |
| CN109627091A (en) * | 2019-01-10 | 2019-04-16 | 盐源地金源农业服务有限公司 | A kind of plant health fertilizer and preparation method thereof |
| CN109796290A (en) * | 2019-04-04 | 2019-05-24 | 陕西开耘生态农业股份有限公司 | A kind of compound fertilizer containing potassium fulvate |
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