CN104649787B - A kind of special amino sour water soluble fertilizers of lemon and preparation method thereof - Google Patents

A kind of special amino sour water soluble fertilizers of lemon and preparation method thereof Download PDF

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CN104649787B
CN104649787B CN201510066122.5A CN201510066122A CN104649787B CN 104649787 B CN104649787 B CN 104649787B CN 201510066122 A CN201510066122 A CN 201510066122A CN 104649787 B CN104649787 B CN 104649787B
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lemon
borax
water soluble
urea
map
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CN104649787A (en
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李进学
岳建强
高俊燕
李晶
刘红明
朱春华
赖新朴
潘黎
杨红霞
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INSTITUTE OF TROPICAL AND SUBTROPICAL CASH CROP YUNNAN ACADEMY OF AGRICULTURAL SCIENCES
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INSTITUTE OF TROPICAL AND SUBTROPICAL CASH CROP YUNNAN ACADEMY OF AGRICULTURAL SCIENCES
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Abstract

The present invention discloses special amino sour water soluble fertilizers of a kind of lemon and preparation method thereof, is made up of urea, MAP, ammonium sulfate, potassium nitrate, full water-soluble humic acid, borax, white vitriol, magnesium sulfate monohydrate, EDTA chelated irons.First urea, MAP, ammonium sulfate, potassium nitrate are crushed respectively; again material A is mixed to get by being humidified, heating progress agglomeration granulation; full water-soluble humic acid, borax, white vitriol, magnesium sulfate monohydrate, EDTA chelated irons are crushed again, it is well mixed to obtain material B;Material A, B are well mixed and are granulated, through drying, screening, cooling.The present invention can make lemon keep nutrition balanced in earsh vegetative growth phase, fruit expanding period, fast and effeciently obtain required nutrient, it is ensured that tree body and fruit healthy development growth, raising tree crown build up the raising with fruit yield and quality.

Description

A kind of special amino sour water soluble fertilizers of lemon and preparation method thereof
Technical field
Prepared the invention belongs to fertilizer and utilize technical field, and in particular to a kind of special amino sour water soluble fertilizers of lemon And preparation method thereof.
Background technology
The important species of lemon category Rutaceae both citrus citron class, in world's citrus planting industry, lemon accounts for the 3rd.Lemon Lemon industry is one of specialty industries in China's modern times Citrus Industry technical system, and its plantation is mainly distributed on the four of south China The regions such as river Anyue, Yunnan Dehong, the Baoshan, lemon have become the advantage specialty economies industry of Southwestern China mountain farming.I State south subtropical zone lemon area vast with the torrid zone, the soil types of its lemon plantation is mainly characteristic of acid red soil, for many years, for a long time Chemical fertilizer or irrational fertilizing management largely are used, it is poor applied to dropper, sprinkling irrigation, the fertilizer dissolubility with filling etc., cause pipeline Block, a large amount of inputs, waste fertilizer, pedo relict pollution.Soil validity magnesium, validity zinc and the boron in this area lemon orchard Content is low, and in this area, soil acidification is serious, the common Chemical Mixed Fertilizer in the lemon long-term use market of plantation, straight fertilizer, causes Soil hardening, Trace Elements in Soil dysequilibrium and cause orchard tree body a large amount of nutritional deficiency symptoms, yellow, tree body growing way occur Weak, irrational Nutrition Management pattern is to limit the Main Factors of lemon industry development.
Therefore, in the more serious lemon producing region of soil acidification, to accelerate lemon body and form tree crown, yield positive results ahead of time, Fruit, characteristic that need to be according to lemon to nutritional need, using scientific and effective big-and-middle micro- instant capacity formula fertilizer, For lemon orchard propose one scientific and efficient, low consumption, safety ecology fertilizer applications.
The content of the invention
To solve balance micro- in hardened south China lemon producing region lemon garden red soil, magnesium in soil, boron, zinc etc. Imbalance;The problems such as lacking the water soluble fertilizer coupling integrated applied to rich water, the present invention provides a kind of special amino acid of lemon Water soluble fertilizer and preparation method thereof, to realize that lemon forms high yield tree crown, beneficial to Fruit ahead of time, improve fruit yield with The purpose of quality.
In order to realize above-mentioned purpose, the present invention uses following technical scheme:A kind of special amino sour water dissolubility fertilizer of lemon Material, is made up of the component of following masses percentage:
Urea 18~42%, MAP 3~12%,
Ammonium sulfate 5~33%, potassium nitrate 6~26%,
Full water-soluble humic acid 1~8%, borax 0.2~3%,
Zinc vitriol 0~3%, magnesium sulfate monohydrate 2~18%,
EDTA chelated irons 0~12%, the summation of above-mentioned each component is 100%.
Above-mentioned EDTA chelated irons are sodium iron ethylene diamine tetra acetate(EDTA-Fe-13 chelated irons), yellow powder.
Another object of the present invention is to provide a kind of preparation method of the special amino sour water soluble fertilizers of lemon, its feature It is by following each step:
(1)Stocked up by the component of following mass percent:
Urea 18~42%, MAP 3~12%,
Ammonium sulfate 5~33%, potassium nitrate 6~26%,
Full water-soluble humic acid 1~8%, borax 0.2~3%,
Zinc vitriol 0~3%, magnesium sulfate monohydrate 2~18%,
EDTA chelated irons 0~12%, the summation of above-mentioned each component is 100%;
(2)By step(1)In urea, MAP, ammonium sulfate, potassium nitrate carry out being crushed to 70~90 mesh respectively, then By being humidified, heating carry out agglomeration granulation, material A is obtained;
(3)By step(1)In full water-soluble humic acid, borax, white vitriol, magnesium sulfate monohydrate, EDTA chelated irons It is well mixed after being crushed, obtains material B;
(4)By step(2)Resulting material A and step(3)Resulting material B is well mixed, then after being granulated, through drying, Screening, cooling, produce the special amino sour water soluble fertilizers of lemon.
The step(2)Heating be heated to 50~55 DEG C.
The step(4)Cooling be to be cooled to 15~30 DEG C.
Dose when the special amino sour water soluble fertilizers of gained lemon are applied is:Tree body is pressed according to special fertilizer dosage is recommended Target is grown to calculate, when taking out the tip for young age lemon different times and starting, every mu of 20~38kg of dose, every 20~35 days one It is secondary, apply fertilizer 4~8 times altogether;During fruiting period swollen for lemon, every mu of 24~48kg of dose, apply fertilizer 2 times, every 20 days once.
The present invention compared with prior art, has advantages below and effect:The present invention is by lemon orchard soil, tree body Nutrient situation and Growth status take away Nutrient Investigation sampling analysis, specify the nutrient obstruction of Influence To Soil lemon Growth status because Son.And investigated and analysed according to orchard soil and determine dose and allocation proportion, while increase full water-soluble humic acid, water solubility Middle and trace element magnesium, boron, zinc, chelating Taiyuan Railway Bureau, solve the problems, such as that current soil lacks organic matter and micro-.The present invention's Raw material sources are extensive, easy to implement the method, easy to operate, and versatility is stronger;The product is water-soluble preferably, may be directly applied to dropper, The coupling integrated systems of rich water such as sprinkling irrigation, more than 30% is saved than traditional fertilization, reduce labour cost 50%, thus it is dirty without environment Dye, production easy to spread.Lemon growth special fertilizer material formula provided by the invention is reasonable, easy to use, and it meets south China And the characteristics of demand of the lemon orchard's soil nutrient of the Great Mekong river sub-region country such as periphery Burma, Thailand, Vietnam.
The special full water-soluble amino acid ammoniacal liquor soluble fertilizers of lemon prepared by the present invention, continuous 4 years in Yunnan Province's Dehong prefecture Ruili City lemon producing region is tested, and in the experiment of 4 years, compared with applying conventional composite fertilizer, three are experimental field applied lemon dedicated water Dissolubility fertilizer yield improves 11.1~25.5% than conventional composite fertilizer;, can using the special water-soluble fertilizer of lemon in terms of lemon quality Dissolubility solid content is higher than applying conventional composite fertilizer content, and significant difference;Improve crushing juice rate and Vc contents simultaneously.The present invention The special full water-soluble amino acid ammoniacal liquor soluble fertilizers of lemon of offer are that south China typical case is red(It is crimson)Earth lemon garden realizes The increase of fruit yield and being obviously improved for quality.
Embodiment
Below by embodiment, the present invention will be further described.
Embodiment 1
(1)Stocked up by the component of following mass percent:
Urea 28.8%, MAP 10.3%,
Ammonium sulfate 27%, potassium nitrate 17.8%,
Full water-soluble humic acid 3%, borax 0.3%,
Zinc vitriol 0.3%, magnesium sulfate monohydrate 12.2%,
EDTA chelated irons 0.3%, the summation of above-mentioned each component is 100%.
(2)By step(1)In urea, MAP, ammonium sulfate, potassium nitrate carries out being crushed to 90 mesh respectively, then passes through It is humidified, is heated to 50 DEG C of progress agglomeration granulations, obtains material A;
(3)By step(1)In full water-soluble humic acid, borax, white vitriol, magnesium sulfate monohydrate, EDTA chelated irons It is well mixed after being crushed, obtains material B;
(4)By step(2)Resulting material A and step(3)Resulting material B is well mixed, then after being granulated, through drying, Sieve, be cooled to 20 DEG C, produce the special amino sour water soluble fertilizers of lemon.
Embodiment 2
(1)Stocked up by the component of following mass percent:
Urea 42%, MAP 6%,
Ammonium sulfate 18%, potassium nitrate 16%,
Full water-soluble humic acid 2%, borax 0.5%,
Zinc vitriol 0.8%, magnesium sulfate monohydrate 14%,
EDTA chelated irons 0.7%, the summation of above-mentioned each component is 100%.
(2)By step(1)In urea, MAP, ammonium sulfate, potassium nitrate carries out being crushed to 70 mesh respectively, then passes through It is humidified, is heated to 55 DEG C of progress agglomeration granulations, obtains material A;
(3)By step(1)In full water-soluble humic acid, borax, white vitriol, magnesium sulfate monohydrate, EDTA chelated irons It is well mixed after being crushed, obtains material B;
(4)By step(2)Resulting material A and step(3)Resulting material B is well mixed, then after being granulated, through drying, Sieve, be cooled to 30 DEG C, produce the special amino sour water soluble fertilizers of lemon.
Embodiment 3
(1)Stocked up by the component of following mass percent:
Urea 26%, MAP 9.6%,
Ammonium sulfate 33%, potassium nitrate 22%,
Full water-soluble humic acid 1%, borax 0.4%,
Magnesium sulfate monohydrate 8%, the summation of above-mentioned each component is 100%.
(2)By step(1)In urea, MAP, ammonium sulfate, potassium nitrate carries out being crushed to 80 mesh respectively, then passes through It is humidified, is heated to 52 DEG C of progress agglomeration granulations, obtains material A;
(3)By step(1)In full water-soluble humic acid, borax, magnesium sulfate monohydrate be well mixed after being crushed, obtain Material B;
(4)By step(2)Resulting material A and step(3)Resulting material B is well mixed, then after being granulated, through drying, Sieve, be cooled to 15 DEG C, produce the special amino sour water soluble fertilizers of lemon.
Embodiment 4
(1)Stocked up by the component of following mass percent:
Urea 33%, MAP 5%,
Ammonium sulfate 31%, potassium nitrate 16%,
Full water-soluble humic acid 3.4%, borax 0.2%,
Zinc vitriol 0.3%, magnesium sulfate monohydrate 10.5%,
EDTA chelated irons 0.6%, the summation of above-mentioned each component is 100%.
(2)By step(1)In urea, MAP, ammonium sulfate, potassium nitrate carry out being crushed to 80~90 mesh respectively, then By being humidified, being heated to 50~52 DEG C of progress agglomeration granulations, material A is obtained;
(3)By step(1)In full water-soluble humic acid, borax, white vitriol, magnesium sulfate monohydrate, EDTA chelated irons It is well mixed after being crushed, obtains material B;
(4)By step(2)Resulting material A and step(3)Resulting material B is well mixed, then after being granulated, through drying, Sieve, be cooled to 18~20 DEG C, produce the special amino sour water soluble fertilizers of lemon.
Embodiment 5
(1)Stocked up by the component of following mass percent:
Urea 38%, MAP 8%,
Ammonium sulfate 24%, potassium nitrate 6%,
Full water-soluble humic acid 4%, borax 3%,
Magnesium sulfate monohydrate 5%, EDTA chelated irons 12%,
The summation of above-mentioned each component is 100%.
(2)By step(1)In urea, MAP, ammonium sulfate, potassium nitrate carries out being crushed to 80 mesh respectively, then passes through It is humidified, is heated to 53~55 DEG C of progress agglomeration granulations, obtains material A;
(3)By step(1)In full water-soluble humic acid, borax, magnesium sulfate monohydrate, EDTA chelated irons mix after being crushed Close uniformly, obtain material B;
(4)By step(2)Resulting material A and step(3)Resulting material B is well mixed, then after being granulated, through drying, Sieve, be cooled to 20~25 DEG C, produce the special amino sour water soluble fertilizers of lemon.
Embodiment 6
(1)Stocked up by the component of following mass percent:
Urea 18%, MAP 12%,
Ammonium sulfate 5%, potassium nitrate 26%,
Full water-soluble humic acid 8%, borax 1%,
Zinc vitriol 3%, magnesium sulfate monohydrate 18%,
EDTA chelated irons 9%, the summation of above-mentioned each component is 100%.
(2)By step(1)In urea, MAP, ammonium sulfate, potassium nitrate carries out being crushed to 90 mesh respectively, then passes through It is humidified, is heated to 53 DEG C of progress agglomeration granulations, obtains material A;
(3)By step(1)In full water-soluble humic acid, borax, white vitriol, magnesium sulfate monohydrate, EDTA chelated irons It is well mixed after being crushed, obtains material B;
(4)By step(2)Resulting material A and step(3)Resulting material B is well mixed, then after being granulated, through drying, Sieve, be cooled to 18 DEG C, produce the special amino sour water soluble fertilizers of lemon.
Embodiment 7
(1)Stocked up by the component of following mass percent:
Urea 30%, MAP 3%,
Ammonium sulfate 25%, potassium nitrate 23%,
Full water-soluble humic acid 5%, borax 2%,
Zinc vitriol 2%, magnesium sulfate monohydrate 2%,
EDTA chelated irons 8%, the summation of above-mentioned each component is 100%.
(2)By step(1)In urea, MAP, ammonium sulfate, potassium nitrate carry out being crushed to 70~80 mesh respectively, then By being humidified, being heated to 53~55 DEG C of progress agglomeration granulations, material A is obtained;
(3)By step(1)In full water-soluble humic acid, borax, white vitriol, magnesium sulfate monohydrate, EDTA chelated irons It is well mixed after being crushed, obtains material B;
(4)By step(2)Resulting material A and step(3)Resulting material B is well mixed, then after being granulated, through drying, Sieve, be cooled to 15~20 DEG C, produce the special amino sour water soluble fertilizers of lemon.
The special full water-soluble amino acid ammonia fertilizer material of lemon of the present invention carries out compliance test result by following experiment:
It is applied to the special full water-soluble amino acid ammonia fertilizer material of lemon using what the embodiment of the present invention 1~7 provided, the fertilizer has Imitating percentage by weight of the element in terms of pure nutrient is:Nitrogen:18~25%;Phosphorus pentoxide:2~10%;Potassium oxide:5~11%;Entirely Fulvo acid:3%;Pure boron:0.3%;Zinc oxide:0.3%th, DTA chelated irons:0.1~0.3%.
Each point is respectively 4 years demonstration areas of lemon water solubility special fertilizer demonstration test:40 mu of Gao Li villager group, brave allusion quotation 50 mu of villager group in 20 mu of villager group, Nanjing.4th year lemon special fertilizer Yunnan producing region popularizing area it is accumulative 6000 mu, 500 mu of Baoshan Longyang District Lu'an coal mine, 300 mu of Puer City billows.Every mu of 20~38kg of dose, take out the tip for lemon different times and open During the beginning, every 20~35 days once, apply fertilizer 4~8 times altogether;During for swollen fruiting period, apply fertilizer 2 times, every 20 days once.4 years lemonades Dissolubility special fertilizer demonstration test citron fruit yield and fruit quality are as follows(Table 1, table 2).
In terms of lemon yield, from First Year to the experiment of 4 years the 4th year in, three experimental field apply lemon it is special water-soluble Property fertilizer yield is higher than conventional composite fertilizer.Compared with applying conventional composite fertilizer, Gao Li villager group First Year and the 3rd year difference Not significantly, Second Year and the 4th year difference are notable;Meng Dian villager group is in addition to First Year significant difference, and three year differences do not show afterwards Write;This on the contrary, in Nanjing villager group except the first year difference not significantly in addition to, behind 3 year differences it is notable.Different Fertilization region, Citron fruit output increased 11.1~25.5%.
The special water-soluble fertilizer of the lemon of table 1 and the Yield comparison of the conventional composite fertilizer of tradition(Unit:Ton/mu)
Note:A, b in table are to represent the significant difference in p < 0.05.
(Two)The special water-soluble formula fertilizer of lemon and influence of the conventional composite fertilizer fertilising to quality
In terms of lemon quality, in Gao Li villager group, Meng Dian villager group and Nanjing villager group three experimental field, 1 year to the 4th year is continuous 4 years, high than applying conventional composite fertilizer content using the special fertile soluble solid of water solubility of lemon, And significant difference;Crushing juice rate and Vc contents difference in the experiment of First Year to Second Year is not notable, the 3rd year to the 4th year It is higher than traditional Chemical Mixed Fertilizer in experiment, and significant difference.
The special water soluble fertilizer of the lemon of table 2 is with custom composite fertilizer to fruit quality impact analysis
Note:A, b in table are to represent the significant difference in p < 0.05;A, B represents the conspicuousness in p < 0.01 Difference.

Claims (3)

1. a kind of preparation method of the special amino sour water soluble fertilizers of lemon, it is characterised in that pass through following each step:
(1)Stocked up by the component of following mass percent:
Urea 38~42%, MAP 3~12%,
Ammonium sulfate 5~33%, potassium nitrate 6~26%,
Full water-soluble humic acid 1~8%, borax 0.2~3%,
Zinc vitriol 0~3%, magnesium sulfate monohydrate 2~18%,
EDTA chelated irons 0~12%, the summation of above-mentioned each component is 100%;
(2)By step(1)In urea, MAP, ammonium sulfate, potassium nitrate carries out being crushed to 70~90 mesh respectively, then passes through It is humidified, is heated to 50~55 DEG C of progress agglomeration granulations, obtains material A;
(3)By step(1)In full water-soluble humic acid, borax, Zinc vitriol, magnesium sulfate monohydrate, EDTA chelated irons enter Row is well mixed after crushing, and obtains material B;
(4)By step(2)Resulting material A and step(3)Resulting material B is well mixed, then after being granulated, through drying, screening, 15~30 DEG C are cooled to, produces the special amino sour water soluble fertilizers of lemon.
2. preparation method according to claim 1, it is characterised in that:The special amino sour water soluble fertilizers of gained lemon are applied When dose be:When taking out the tip for young age lemon different times and starting, every mu of 20~38kg of dose, every 20~35 days one It is secondary, apply fertilizer 4~8 times altogether;During fruiting period swollen for lemon, every mu of 24~48kg of dose, apply fertilizer 2 times, every 20 days once.
A kind of 3. special amino sour water soluble fertilizers of lemon that preparation method according to claim 1 obtains.
CN201510066122.5A 2015-02-09 2015-02-09 A kind of special amino sour water soluble fertilizers of lemon and preparation method thereof Active CN104649787B (en)

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CN105111016A (en) * 2015-08-23 2015-12-02 云南省农业科学院热带亚热带经济作物研究所 Water-soluble humic acid fertilizer and preparation method
CN105111017A (en) * 2015-08-23 2015-12-02 云南省农业科学院热带亚热带经济作物研究所 Humic acid fertilizer for correcting lemon yellowing and preparation method
CN105399577A (en) * 2015-12-07 2016-03-16 河南晋开集团雨露复合肥有限公司 Liquid compound fertilizer for swelling fruit period and preparation method thereof
CN105399576A (en) * 2015-12-07 2016-03-16 河南晋开集团雨露复合肥有限公司 Liquid compound fertilizer for growing period and preparation method thereof

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US6749660B2 (en) * 2001-06-04 2004-06-15 Geovation Technologies, Inc. Solid-chemical composition and method of preparation for the anaerobic bioremediation of environmental contaminants coupled to denitrification
CN1206192C (en) * 2002-12-10 2005-06-15 李兰廷 Humic acid multiple fertilizer with mixed organic and inorganic components as well as its preparation technique
CN1919802A (en) * 2006-08-23 2007-02-28 杭州艾可泰投资有限公司 Humic acid highly effective composite fertilizer and preparation method thereof
CN102503641A (en) * 2011-10-29 2012-06-20 史丹利化肥股份有限公司 Novel green efficient multifunctional humic acid special fertilizer for soybean and preparation method thereof
CN103864497A (en) * 2014-03-14 2014-06-18 华中农业大学 Special fertilizer for oranges in acid soil and preparation method of fertilizer

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