CN104644503A - Massage cream capable of deeply retaining water and moisturizing and resisting long-wavelength ultraviolet rays - Google Patents
Massage cream capable of deeply retaining water and moisturizing and resisting long-wavelength ultraviolet rays Download PDFInfo
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Abstract
The invention relates to the field of daily chemicals and in particular relates to massage cream capable of deeply retaining water and moisturizing and resisting long-wavelength ultraviolet rays. The massage cream capable of deeply retaining water and moisturizing and resisting the long-wavelength ultraviolet rays is prepared from the following components: licoflavone lipid nanoemulsion, tea extract, salviae miltiorrhizae aqueous extract, vitamin C, water, glyceryl monostearate, hexadecyl alcohol, squalane, Vaseline, white oil, lanolin alcohol, vitamin E, microcrystalline wax and polyvinylpyrrolidone. The massage cream provided by the invention has the effects of deeply retaining water and moisturizing and resisting long-wavelength ultraviolet rays, sensitization is obviously reduced, wherein licoflavone is added in a nanoemulsion form, sun-proof effect of the massage cream can be improved, melanin inhibitory ratio can be increased, and tyrosinase activity inhibiting effect is obviously improved. After the massage cream provided by the invention is respectively continuously used by 100 persons of 30-55 years old, results show that symptoms such as rough skin, scurf increase, stratum corneum thinning, antianaphylaxis and lines are obviously alleviated.
Description
Technical field
The present invention relates to household chemicals field, particularly pure natural freckle removing and whitening compositions, especially a kind of degree of depth water conservation moisturizing and resist the massage cream of long wave ultraviolet.
Background technology
After skin accepts ultraviolet overexposure, meeting lesional epidermis cell; Activation Tyrosinase, accelerates pigment synthesis, destroys the moisture-keeping functions of skin, makes skin become dry, makes the elastic fibers in skin corium impaired, microgroove is produced.Under acute irradiation, also can cause skin inflammation, burn.When having abnormal case, then can become pigmentosa skin carcinoma etc.
Sunscreen cream kind is more in the market, is mainly reflected on sun-screening function, generally in out using, but be not suitable for when indoor using, because common sunscreen frost does not moisten and maintenance effect skin, coating time is oversize, increase skin loadings, skin is tarnished.
Find through retrieval, publication number is that the application for a patent for invention of CN104042481 discloses a kind of skin moistening moisturizing sun cream, this sunscreen cream is made up of the raw material of following parts by weight: glycerol 20-40 part, palm acid ethyl own fat 10-20 part, butanediol 3-6 part, squalane 3-6 part, stearin 2-5 part, shea butter 4-8 part, polydimethylsiloxane 3-6 part, active certain kind of berries polyphenol 3-7 part, chitin 2-5 part, Mentholum 1-3 part, octyl methoxycinnamate 15-25 part, ethylhexyl salicylate 5-10 part, menthyl lactate 6-12 part, cetearyl alcohol 3-9 part, xanthan gum 8-16 part, methyl hydroxybenzoate 4-6 part, titanium dioxide 3-6 part, distilled water 40-80 part.
Along with the development of cosmetics industry, natural plants series products due to use safety, action temperature and, the advantage such as successful and being welcome.Be generally the plant extract obtaining containing effective ingredient by corresponding processing, and add in cosmetics.
Wherein, licoflavone is a kind of natural whiting agent, has Huang of dispelling significantly, whitening, effect of dispelling spots.Natural sun-prevention series products such as tea polyphenols has removing toxic substances and radiation resistance, radioactive substance can be effectively stoped to invade bone marrow, and strontium 90 and Co 60 can be made to excrete rapidly, be described as " radiation jinx " by healthy and medical circle, similar material also has Radix Rhodiolae, Herba Saussureae Involueratae etc., and the plant extract of these materials has good antioxidation, radioprotective characteristic.
Find through retrieval, publication number is the whitening cosmetics that the application for a patent for invention of CN103989598A, CN103919707A, CN103932953A, CN103989617A individually discloses containing Radix Rhodiolae extract, Radix Ginseng Rubra extract, Radix Ginseng extract, Cordyceps extract, but the component of Chinese medicine extract and the equal more complicated of preparation method.
Summary of the invention
The object of this invention is to provide a kind of pure natural freckle removing and whitening compositions resisting long wave ultraviolet, especially a kind of degree of depth water conservation moisturizing and resist the massage cream of long wave ultraviolet.
For achieving the above object, the technical scheme that concrete employing is following:
Resist a pure natural freckle removing and whitening compositions for long wave ultraviolet, its raw material percentage composition by weight, comprise the licoflavone lipid nanoemulsion of 5 ~ 50%, the anioxidant phytochemicals of 0.1 ~ 5%; The content of described licoflavone lipid nanometer Ruzhong licoflavone is 0.01 ~ 10%.
Preferably, its raw material percentage composition by weight, comprises the licoflavone lipid nanoemulsion of 5 ~ 25%, the anioxidant phytochemicals of 0.1 ~ 5%; The content of described licoflavone lipid nanometer Ruzhong licoflavone is 0.1-3%.
More preferably, its raw material percentage composition by weight, comprises the licoflavone lipid nanoemulsion of 5 ~ 25%, the anioxidant phytochemicals of 0.1 ~ 5%; The content of described licoflavone lipid nanometer Ruzhong licoflavone is 1.5%.
As a kind of embodiment of the best, described licoflavone lipid nanoemulsion percentage composition by weight, comprise component A and B component, described component A comprises the licoflavone of 1.5%, the phospholipid of 3.5%, the soybean oil of 5%, the caprylic/capric triglyceride of 20%, the polyglycerol monooleate of 2%, the sorbester p17 of 0.5%, the glycerol of 5%, the propylene glycol of 5%; Described B component comprises the Tween 80 of 0.5%, and the polyoxyethylene castor oil of 2%, water complements to 100%.
Further, the preparation method of described licoflavone lipid nanoemulsion comprises the following steps:
(1) by component A, high speed shear, without the visible solid content of naked eyes to system;
(2) B component is added step (1) products therefrom, high speed shear, obtains colostrum, and colostrum, through high pressure homogenizer process, obtains licoflavone lipid nanoemulsion.
Resist in the pure natural freckle removing and whitening compositions of long wave ultraviolet provided by the invention, concrete, described anioxidant phytochemicals is selected from one or more in Herba Saussureae Involueratae extract, Radix Rhodiolae extract, Radix Salviae Miltiorrhizae extract or tea extract.More specifically, described extract is water extract.
The present invention is by selecting the licoflavone lipid nanoemulsion of good water solubility, with the plant extract efficient combination with antioxidant activity, obtain one not containing chemical ultraviolet absorbers, the pure natural freckle removing and whitening compositions resisting long wave ultraviolet using plant extract as functional component, this freckle removing and whitening compositions has effect of degree of depth water conservation moisturizing.
The pure natural freckle removing and whitening compositions resisting long wave ultraviolet provided by the invention can commonly use substrate in conjunction with cosmetics, is prepared into suntan lotion, massage cream and massage cream.
Concrete, described suntan lotion, by weight percentage composition, shown in it is composed as follows:
Preferably, percentage composition by weight, shown in it is composed as follows:
The preparation method of described suntan lotion can adopt any technical scheme of the prior art, and preferably, its preparation method is: after B component being heated to 70 DEG C, and after waxy substance is melted, add component A when being cooled to 50 DEG C, 300rpm stirs 10min, and homogenizing, to obtain final product.
Described degree of depth water conservation moisturizing and resist the massage cream of long wave ultraviolet, percentage composition by weight, shown in it is composed as follows:
Preferably, percentage composition by weight, shown in it is composed as follows:
The preparation method of the moisturizing of described degree of depth water conservation and the massage cream of resisting long wave ultraviolet can adopt any technical scheme of the prior art, preferably, its preparation method is: B component is heated to 75 DEG C, after waxy substance is melted, add component C when being cooled to 50 DEG C, 300rpm stirs 10min, adds component A after being cooled to room temperature, homogenizing, to obtain final product.Massage cream of the present invention has the moisturizing of degree of depth water conservation and resists effect of long wave ultraviolet, massage cream of the present invention respectively through 30-55 year 100 personnel within 30 days on probation, find continuously, the situations such as pachylosis, scurf increase, angleplied laminate thinning, antiallergic, microgroove are significantly improved.
Described massage cream, by weight percentage composition, shown in it is composed as follows:
Preferably, percentage composition by weight, shown in it is composed as follows:
The preparation method of described massage cream can adopt any technical scheme of the prior art, and preferably, its preparation method is: B component is heated to 75 DEG C, and after waxy substance is melted, add component A when being cooled to 50 DEG C, 300rpm stirs 10min, and homogenizing, to obtain final product.
Detailed description of the invention
Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.Unreceipted actual conditions person in embodiment, the condition of conveniently conditioned disjunction manufacturer suggestion is carried out.Raw materials used, reagent or the unreceipted production firm person of instrument, being can by the conventional products of commercial acquisition.
Embodiment 1: licoflavone lipid nanoemulsion
The preparation method of this lipid nanoemulsion is as follows:
1) by above-mentioned prescription, by component A, high speed shear under 9000rpm condition, without the visible solid content of naked eyes to system;
2) B component being joined step 1) in products therefrom, high speed shear under 13000rpm condition, obtains colostrum, and colostrum is through high pressure homogenizer process, and pressure 2000bar used, circulates 9 times, obtains transparent clear shape licoflavone lipid nanoemulsion.
Embodiment 2: suntan lotion
The preparation method of this suntan lotion is as follows:
After B component being heated to 70 DEG C, after waxy substance is melted, add component A when being cooled to 50 DEG C, 300rpm stirs 10min, and homogenizing, to obtain final product.
Embodiment 3: massage cream
The preparation method of this massage cream is as follows:
B component is heated to 75 DEG C, after waxy substance is melted, add component C when being cooled to 50 DEG C, 300rpm stirs 10min, adds component A, homogenizing, to obtain final product after being cooled to room temperature.
Embodiment 4: massage cream
The preparation method of this massage cream is as follows:
B component is heated to 75 DEG C, after waxy substance is melted, add component A when being cooled to 50 DEG C, 300rpm stirs 10min, and homogenizing, to obtain final product.
Embodiment 5: massage cream
Embodiment 5 and the difference of embodiment 3 be the component of nano-emulsion and content different, in the present embodiment, licoflavone lipid nanoemulsion specifically composed as follows, the preparation method of licoflavone lipid nanoemulsion is with embodiment 1.
Embodiment 6: massage cream
Embodiment 6 and the difference of embodiment 3 be the component of nano-emulsion and content different, in the present embodiment, licoflavone lipid nanoemulsion specifically composed as follows, the preparation method of licoflavone lipid nanoemulsion is with embodiment 1.
Embodiment 7-8: suntan lotion
Embodiment 7-8 and embodiment 2 are distinguished and are only that the content of component is different, specific as follows:
Embodiment 9-10: massage cream
Embodiment 9-10 and embodiment 3 are distinguished and are only that the content of component is different, specific as follows:
Embodiment 11-12: massage cream
Embodiment 11-12 and embodiment 4 are distinguished and are only that the content of component is different, specific as follows:
Experimental example 1: sensitization is tested
Experimental technique: choose 12 Cavia porcelluss of body weight between 350 ~ 450g, be divided into A, B two groups at random.
The sample that A group selects embodiment 3 to prepare; B group is control sample, is according to embodiment 3, licoflavone lipid nanoemulsion is changed into the OctMet of Isodose, all the other components and preparation method constant.
In test, guinea pig back is shaved hair, respectively about 0.2 gram of sample, reference substance are smeared to 1cm × 1cm region.Observe after 18h and smear cosmetics area skin situation, the results are shown in Table shown in 1:
Guinea pig back change of skin after cosmetics smeared by table 1
| Quantity | No change | Erythema, infiltration or pimple | Edematous erythema, pimple | Remarkable redness, companion's bulla |
| Sample | 6 | 0 | 0 | 0 |
| Reference substance | 1 | 3 | 2 | 0 |
As shown in Table 1, ultraviolet absorber (OctMet) is changed the licoflavone lipid nanoemulsion of same amount, corresponding cosmetics sensitization significantly declines.
Experimental example 2: sun-proof result is tested
Test method: the pertinent regulations detected with reference to spf value in " cosmetics health specification " (version in 2002).30 healthy volunteers are chosen, each 15 of men and women in test, IV type skin (namely seldom tan severely, but easily tanned skin quality), unglazed allergies.30 volunteers are divided into 3 groups, often organize 10 people.
The product of trial target prepared by embodiment of the present invention 2-6 is as sample 1-5;
Reference substance 1-5, respectively according to embodiment 2-6, will wherein plant anti-oxidation thing remove, appropriate section with water polishing, all the other prescriptions and preparation method constant.
Reference substance 6: by the prescription of embodiment 3, replaces with the licoflavone alcoholic solution of active component identical (licoflavone) by licoflavone lipid nanoemulsion, all the other compositions and preparation method constant.
Reference substance 7: by the prescription of embodiment 3, replaces with the licoflavone phosphatide complexes of the CN102949440A of active component identical (licoflavone) by licoflavone lipid nanoemulsion, all the other compositions and preparation method constant.
Reference substance 8: by the prescription of embodiment 3, replaces with the commercially available licoflavone of active component identical (licoflavone) by licoflavone lipid nanoemulsion, all the other compositions and preparation method constant.
Experimental result is in table 2.
The different sample spf value of table 2
| Sample 1 | Sample 2 | Sample 3 | Sample 4 | Sample 5 | Contrast 1 | Contrast 2 | |
| SPF | 11.5 | 13.8 | 16.5 | 13.5 | 12.6 | 7.5 | 8 |
| Contrast 3 | Contrast 4 | Contrast 5 | Contrast 6 | Contrast 7 | Contrast 8 | -- | |
| SPF | 11 | 6.5 | 7.8 | 10.5 | 11.1 | 8.5 | -- |
Can be seen by table 2, add the sunscreen product of plant extract antioxidant, spf value is compared with reference substance 1-5, and licoflavone adds with the form of nano-emulsion and more can improve its sun-proof result.
Experimental example 3:MTT activity test
Take the logarithm the human epidermal cell HEK-n of trophophase, according to 1 × 10
5the concentration of cells/mL inoculates 96 orifice plates, every pore volume 200 μ L, after normal cultivation 24h, in protection group cell culture fluid, adds trial target respectively, after 5min, adopts 1mM H respectively
2o
2carry out oxidative damage process 6h.After oxidative damage process terminates, take out 96 well culture plates, abandon supernatant, after carefully rushing 2-3 time with PBS, then add the fresh medium of 200 μ L containing 0.5mg/mL MTT, continue, at 37 DEG C, under 5%CO2 condition, to cultivate 4h.After cultivation terminates, discard MTT solution, every hole adds 100 μ LDMSO, vibration mixing, surveys each hole absorbance (A490) that wavelength is 490nm, calculates cell survival rate, the results are shown in Table 3.
The product of trial target prepared by embodiment of the present invention 2-6 is as sample 1-5; Reference substance 1-5, respectively according to embodiment 2-6, will wherein licoflavone lipid nanoemulsion and plant extract antioxidant remove, appropriate section with water polishing, all the other prescriptions and preparation method constant.
Reference substance 6-8 is with experimental example 2.
Table 3MTT activity test
| Sample 1 | Sample 2 | Sample 3 | Sample 4 | Sample 5 | Contrast 1 | Contrast 2 | |
| Cell survival rate % | 65.2 | 83.4 | 81.9 | 72.5 | 75.9 | 26.1 | 26.3 |
| Contrast 3 | Contrast 4 | Contrast 5 | Contrast 6 | Contrast 7 | Contrast 8 | -- | |
| Cell survival rate % | 25.9 | 20.3 | 21.9 | 53.2 | 62.3 | 50.8 | -- |
As shown in Table 3, compared with reference substance, containing the sample of licoflavone and plant extract antioxidant, greatly can improve cell viability.
Experimental example 4: melanin inhibition test
By B16 melanocyte with 1 × 10
5the density of individual/mL is inoculated in 6 orifice plates.Every hole 3ml, after hatching 24h, abandons supernatant, adds medicine to be measured, after drug effect 3d, abandons supernatant, and PBS washs, and every hole adds 0.5mL trypsin digestion cell 3min, and every hole adds 2ml maintenance medium and stops digestion.After piping and druming mixing, often kind of concentration is taken out 0.5mL and is made cell counting.All the other cell suspension, with the centrifugal 5min of 2500r/min, abandon supernatant, add sodium hydroxide solution, melanin is dissolved in precipitation, select 490nm wavelength to survey absorbance on enzyme-linked immunosorbent assay instrument, calculate melanin generating suppression, the results are shown in Table 4.
The product of trial target prepared by embodiment of the present invention 2-6 is as sample 1-5; Reference substance 1-5, respectively according to embodiment 2-6, removes licoflavone lipid nanoemulsion, appropriate section with water polishing, all the other prescriptions and preparation method constant.
Reference substance 6-8 is with experimental example 2.
Melanin generating suppression=[1-(medicine hole absorbance ÷ medicine porocyte density) ÷ (control wells absorbance ÷ control wells cell density] × 100%
Table 4 melanin generating suppression %
| Sample 1 | Sample 2 | Sample 3 | Sample 4 | Sample 5 | Contrast 1 | Contrast 2 | |
| Suppression ratio % | 32.8 | 37.3 | 33.6 | 28.9 | 29.3 | 20.3 | 20.1 |
| Contrast 3 | Contrast 4 | Contrast 5 | Contrast 6 | Contrast 7 | Contrast 8 | -- | |
| Suppression ratio % | 20.5 | 19.6 | 18.9 | 25.3 | 26.8 | 25.6 | -- |
As shown in Table 4, compared with reference substance, the sample containing licoflavone lipid nanoemulsion, greatly can strengthen melanin generating suppression.
Experimental example 5: tryrosinase vitality test
By B16 melanocyte with 1 × 10
5the density of individual/mL is inoculated in 96 orifice plates.Every hole 100 μ L, after hatching 24h, abandons supernatant, adds medicine to be measured, after drug effect 3d, abandon supernatant, PBS washing twice, and every hole adds the PBS of 90 μ L containing 1% (volume fraction) Triton X-100.Ultrasonication in ice bath, every hole adds the L-dopa of 10 μ L 10mmoL/L, hatches 60min for 37 DEG C, and in 475nm place colorimetric, blank well returns to zero, and surveys each hole absorbance, calculates inhibitory activity against tyrosinase, the results are shown in Table 5.
The product of trial target prepared by embodiment of the present invention 2-6 is as sample 1-5; Reference substance 1-5, respectively according to embodiment 2-6, removes licoflavone lipid nanoemulsion, appropriate section with water polishing, all the other prescriptions and preparation method constant.
Reference substance 6-8 is with experimental example 2.
Suppression ratio=(1-medicine group mean absorbance values ÷ matched group mean absorbance values) × 100%.
Table 5 inhibitory activity against tyrosinase %
As shown in Table 5, compared with reference substance, containing the sample of licoflavone lipid nanoemulsion, to tyrosinase activity inhibitory action, be significantly improved.
Although above the present invention is described in detail with a general description of the specific embodiments, on basis of the present invention, can make some modifications or improvements it, this will be apparent to those skilled in the art.Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, all belong to the scope of protection of present invention.
Claims (10)
1. resist a pure natural freckle removing and whitening compositions for long wave ultraviolet, it is characterized in that: its raw material percentage composition by weight, comprise the licoflavone lipid nanoemulsion of 5 ~ 50%, the anioxidant phytochemicals of 0.1 ~ 5%; Described licoflavone lipid nanometer Ruzhong, the content of licoflavone is 0.01 ~ 10%.
2. the pure natural freckle removing and whitening compositions resisting long wave ultraviolet according to claim 1, is characterized in that: its raw material percentage composition by weight, comprises the licoflavone lipid nanoemulsion of 5 ~ 25%, the anioxidant phytochemicals of 0.1 ~ 5%; Described licoflavone lipid nanometer Ruzhong, the content of licoflavone is 1.5%.
3. the pure natural freckle removing and whitening compositions resisting long wave ultraviolet according to claim 1 and 2, is characterized in that: described licoflavone lipid nanoemulsion percentage composition by weight, comprises component A and B component,
Described component A comprises the licoflavone of 1.5%, the phospholipid of 3.5%, the soybean oil of 5%, the caprylic/capric triglyceride of 20%, the polyglycerol monooleate of 2%, the sorbester p17 of 0.5%, the glycerol of 5%, the propylene glycol of 5%;
Described B component comprises the Tween 80 of 0.5%, and the polyoxyethylene castor oil of 2%, water complements to 100%.
4. the pure natural freckle removing and whitening compositions resisting long wave ultraviolet according to claim 3, it is characterized in that, the preparation method of described licoflavone lipid nanoemulsion comprises the following steps:
(1) by component A, high speed shear, without the visible solid content of naked eyes to system;
(2) B component is added step (1) products therefrom, high speed shear, obtains colostrum, and colostrum, through high pressure homogenizer process, obtains licoflavone lipid nanoemulsion.
5. the pure natural freckle removing and whitening compositions resisting long wave ultraviolet according to claim 1, is characterized in that: described anioxidant phytochemicals is selected from one or more in Herba Saussureae Involueratae extract, Radix Rhodiolae extract, Radix Salviae Miltiorrhizae extract or tea extract; Particularly, described plant extract is water extract.
6. the pure natural freckle removing and whitening compositions resisting long wave ultraviolet according to any one of claim 1-5, is characterized in that: described in resist long wave ultraviolet pure natural freckle removing and whitening compositions be suntan lotion, massage cream and massage cream.
7. the pure natural freckle removing and whitening compositions resisting long wave ultraviolet according to claim 6, is characterized in that: described suntan lotion percentage composition by weight, comprises component A and B component,
Described component A comprises 5 ~ 25% licoflavone lipid nanoemulsions, 0.1 ~ 1.5% Herba Saussureae Involueratae water extract, 0.1 ~ 1.5% Radix Rhodiolae water extract, 3 ~ 8% glycerol, 0.1 ~ 3% vitamin C, and water is mended to 100%;
Described B component comprises 0.5 ~ 5% almond oil, 2 ~ 4% silicone oil, 0.1 ~ 3% vitamin E, 0.5 ~ 1.5%PEG-100 stearate, 2 ~ 4% hexadecanol, 4 ~ 8% vaseline.
8. the pure natural freckle removing and whitening compositions resisting long wave ultraviolet according to claim 6, it is characterized in that, described massage cream percentage composition by weight, comprises component A, B component and component C,
Described component A comprises 5 ~ 25% licoflavone lipid nanoemulsions, 0.2 ~ 2% tea extract, 0.1 ~ 1% radix Salviae Miltiorrhizae water extract, 0.1 ~ 3% vitamin C, 5 ~ 10% water;
Described B component comprises 0.5 ~ 5% glyceryl monostearate, 2 ~ 5% hexadecanol, 3 ~ 7% squalanes, 3 ~ 10% vaseline, 3 ~ 10% white oils, 0.2 ~ 5% lanolin alcohol, 0.1 ~ 3% vitamin E, 0.5 ~ 2% microwax;
Described component C comprises 0.2 ~ 1% polyvinylpyrrolidone, and water is mended to 100%.
9. the pure natural freckle removing and whitening compositions resisting long wave ultraviolet according to claim 8, it is characterized in that, described massage cream percentage composition by weight, comprises component A, B component and component C,
Described component A comprises 25% licoflavone lipid nanoemulsion, 0.5% tea extract, 0.2% radix Salviae Miltiorrhizae water extract, 0.5% vitamin C, 5% water;
Described B component comprises 2% glyceryl monostearate, 4% hexadecanol, 5% squalane, 6% vaseline, 8% white oil, 1.5% lanolin alcohol, 1% vitamin E, 2% microwax;
Described component C comprises 0.5% polyvinylpyrrolidone, and water is mended to 100%.
10. the pure natural freckle removing and whitening compositions resisting long wave ultraviolet according to claim 6, it is characterized in that, described massage cream percentage composition by weight, comprises component A and B component,
Described component A comprises 5 ~ 25% licoflavone lipid nanoemulsions, 0.1 ~ 3% vitamin C, 0.5 ~ 1.5% Radix Rhodiolae extract, 0.5 ~ 1.5% tea extract, and purified water is mended to 100%;
Described B component comprises 3 ~ 15% titanium dioxide, 5 ~ 15% microwaxes, 0.2 ~ 5% Cera Flava, 3 ~ 10% vaseline, 3 ~ 10% lanolines, 20 ~ 40% Squalenes, 2 ~ 10% oleins, 2 ~ 10% adipic acid C
16alkane ester.
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| CN105724367B (en) * | 2016-02-05 | 2018-06-26 | 沈阳吉强生态农业有限公司 | A kind of Multifunctional protective aqua, preparation method and its application method for farm-forestry crop |
| CN108113926A (en) * | 2017-12-29 | 2018-06-05 | 吉林农业科技学院 | A kind of Herba Saussureae Involueratae ultrasonic extraction process |
| CN111759774A (en) * | 2020-08-17 | 2020-10-13 | 刘婷 | Whitening anti-wrinkle essence |
| WO2023274654A1 (en) * | 2021-06-28 | 2023-01-05 | Firmenich Sa | Flavor nanoemulsions for beverage and personal care applications |
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