CN104594029A - Antibacterial finish method for blended cotton fabric - Google Patents
Antibacterial finish method for blended cotton fabric Download PDFInfo
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- CN104594029A CN104594029A CN201510053180.4A CN201510053180A CN104594029A CN 104594029 A CN104594029 A CN 104594029A CN 201510053180 A CN201510053180 A CN 201510053180A CN 104594029 A CN104594029 A CN 104594029A
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Abstract
The invention discloses an antibacterial finish method for a blended cotton fabric. The antibacterial finish method comprises the following steps: (1) grinding sabina chinensis, extracting the sabina chinensis in ethanol aqueous solution after grinding, performing centrifugal separation after extracting, and concentrating the supernatant, thereby obtaining a sabina chinensis extract; (2) additionally taking green tangerine peel, drying and grinding the green tangerine peel, extracting the green tangerine peel in the ethanol aqueous solution, performing centrifugal separation after extracting, and concentrating the supernatant, thereby obtaining the green tangerine peel extract; (3) taking chitosan, nanometer titania, the sabina chinensis extract, the green tangerine peel extract and water according to the weight, dissolving the chitosan, nanometer titania, sabina chinensis extract and green tangerine peel extract by using water, and stirring to be uniform after dissolving; and (4) immersing a blended cotton fabric in the mixed solution, soaking, soaking twice and padding twice, and drying, thereby obtaining the antibacterial blended cotton fabric. The prepared blended cotton fabric has high antibacterial performance.
Description
Technical field
The invention belongs to textile dyeing and finishing field, relate to a kind of antibiotic finishing method of weaving face fabric, particularly relate to a kind of antibiotic finishing method of blending cotton face fabric.
Background technology
It is excellent that spandex has good elasticity, and its strength ratio rubber latex thread is high, and line density is also thinner, and more chemically-resistant degraded.The resistance to acids and bases of spandex, sweat proof, sea water resistance, dry cleaning resistance, ABRASION RESISTANCE are all better.The ratio that spandex is used on general clothes is lower.All can add other fibers in use in a large number as cotton, polyester blended, so that gloss is reduced to minimum degree.
Terylene has the high feature of intensity.Staple fibre intensity is 2.6 ~ 5.7cN/dtex, and high-tenacity fiber is 5.6 ~ 8.0cN/dtex.And its hygroscopicity is lower, its wet strength is substantially identical with dry strength.Impact strength is higher than polyamide fibre 4 times, higher than viscose 20 times.The second, good springiness.Elasticity is close to wool.Crease resistance exceedes other fibers, i.e. fabric not wrinkle, good stability of the dimension.Modulus of elasticity is 22 ~ 141cN/dtex, higher than polyamide fibre 2 ~ 3 times.
Dacron has higher intensity and elastic recovery capability.Cotton and terylene and spandex blended yarn woven fabric does not have good bacteriostasis property, easily by the pollution such as Escherichia coli and staphylococcus aureus, affects the dress of people.In order to improve the bacteriostasis rate of blending cotton face fabric, need to carry out effective antibiotic finish to blending cotton face fabric.
Summary of the invention
The technical problem solved: the antibacterial strength of the blended yarn woven fabric of cotton and spandex or terylene is lower, be easy to be contaminated by bacterial and encroach on, improve the antibacterial strength of blending cotton face fabric, need to carry out antibiotic finish to blending cotton face fabric, to improve the anti-microbial property of blending cotton face fabric to Escherichia coli, staphylococcus aureus.
Technical scheme: the antibiotic finishing method that the invention discloses a kind of blending cotton face fabric, described antibiotic finishing method step is as follows:
(1) pulverized by Chinese juniper, add ethanol water after pulverizing and extract, centrifugation after extracting, will prepare Chinese juniper extract after supernatant concentration;
(2) separately get rascal, by rascal crushed after being dried, add ethanol water and extract, centrifugation after extracting, prepares peel extract by after supernatant concentration;
(3) get that the peel extract that the Chinese juniper extract that shitosan is 5-13 part, nano titanium oxide is 3-6 part, prepared by step (1) is 3-5 part, prepared by step (2) is 2-5 part, water is 145-165 part by weight, shitosan, nano titanium oxide, Chinese juniper extract and peel extract water are dissolved, is stirred to evenly after dissolving;
(4) be immersed into by blending cotton face fabric in the mixed liquor of step (3), temperature is room temperature, soaks 3h, and two leachings two are rolled, and pick-up is 50-70%, dry at 90 DEG C, is antibacterial blending cotton face fabric after dry.
The antibiotic finishing method of described a kind of blending cotton face fabric, described Chinese juniper method for preparing extractive is as follows: pulverized by Chinese juniper, the ethanol water of 20-40wt% is added after pulverizing, feed liquid weight ratio is 1:6-1:9, Extracting temperature is 55-65 DEG C, extraction time is 3-5h, and centrifugation after extracting, will prepare Chinese juniper extract after supernatant concentration.
The antibiotic finishing method of described a kind of blending cotton face fabric, described peel extract preparation method is as follows: by rascal crushed after being dried, add the ethanol water of 40-60wt%, feed liquid weight ratio is 1:4-6, Extracting temperature 40-60 DEG C, extraction time is 2-3h, and centrifugation after extracting, prepares peel extract by after supernatant concentration.
The antibiotic finishing method of described a kind of blending cotton face fabric, in described blending cotton face fabric, cotton content is 60-80%.
The antibiotic finishing method of described a kind of blending cotton face fabric, in described blending cotton face fabric except cotton, residue fabric is spandex or terylene.
The antibiotic finishing method of described a kind of blending cotton face fabric, described shitosan purity is more than 90%.
The antibiotic finishing method of described a kind of blending cotton face fabric, pick-up is 60%.
Beneficial effect: the antibiotic finishing method of blending cotton face fabric of the present invention very effectively can improve the anti-microbial property of the fabric after cotton and spandex, blend polyester, the antimicrobial component such as natural extract and inorganic antiseptic is included in antibiotic finishing method of the present invention, it is after adding rascal extraction, highly significant improve its antibacterial strength to Escherichia coli and staphylococcus aureus, effectively can arrange blending cotton face fabric, to improve its antibacterial strength.
Detailed description of the invention
Embodiment 1
(1) pulverized by Chinese juniper, add the ethanol water of 20wt% after pulverizing, feed liquid weight ratio 1:9, Extracting temperature is 65 DEG C, and extraction time is 5h, and centrifugation after extracting, will prepare Chinese juniper extract after supernatant concentration;
(2) by rascal crushed after being dried, add the ethanol water of 60wt%, feed liquid weight ratio is 1:6, Extracting temperature 60 DEG C, and extraction time is 3h, and centrifugation after extracting, prepares peel extract by after supernatant concentration;
(3) get that the peel extract that the Chinese juniper extract that shitosan is 13 parts, nano titanium oxide is 6 parts, prepared by step (1) is 5 parts, prepared by step (2) is 5 parts, water is 145 parts by weight, shitosan, nano titanium oxide, Chinese juniper extract and peel extract water are dissolved, is stirred to evenly after dissolving;
(4) be immersed in the mixed liquor of step (3) by 60% blending cotton face fabric that is cotton, 40% spandex, temperature is room temperature, soaks 3h, and two leachings two are rolled, and pick-up is 70%, dry at 90 DEG C, is antibacterial blending cotton face fabric after dry.
Embodiment 2
(1) pulverized by Chinese juniper, add the ethanol water of 40wt% after pulverizing, feed liquid weight ratio is 1:6, and Extracting temperature is 55 DEG C, and extraction time is 3h, and centrifugation after extracting, will prepare Chinese juniper extract after supernatant concentration;
(2) by rascal crushed after being dried, add the ethanol water of 40wt%, feed liquid weight ratio is 1:4, Extracting temperature 40 DEG C, and extraction time is 2h, and centrifugation after extracting, prepares peel extract by after supernatant concentration;
(3) get that the peel extract that the Chinese juniper extract that shitosan is 5 parts, nano titanium oxide is 3 parts, prepared by step (1) is 3 parts, prepared by step (2) is 2 parts, water is 165 parts by weight, shitosan, nano titanium oxide, Chinese juniper extract and peel extract water are dissolved, is stirred to evenly after dissolving;
(4) be immersed in the mixed liquor of step (3) by 80% blending cotton face fabric that is cotton, 20% spandex, temperature is room temperature, soaks 3h, and two leachings two are rolled, and pick-up is 50%, dry at 90 DEG C, is antibacterial blending cotton face fabric after dry.
Embodiment 3
(1) pulverized by Chinese juniper, add the ethanol water of 40wt% after pulverizing, feed liquid weight ratio is 1:6, and Extracting temperature is 55 DEG C, and extraction time is 3h, and centrifugation after extracting, will prepare Chinese juniper extract after supernatant concentration;
(2) by rascal crushed after being dried, add the ethanol water of 40wt%, feed liquid weight ratio is 1:4, Extracting temperature 40 DEG C, and extraction time is 2h, and centrifugation after extracting, prepares peel extract by after supernatant concentration;
(3) get that the peel extract that the Chinese juniper extract that shitosan is 7 parts, nano titanium oxide is 5 parts, prepared by step (1) is 4 parts, prepared by step (2) is 4 parts, water is 160 parts by weight, shitosan, nano titanium oxide, Chinese juniper extract and peel extract water are dissolved, is stirred to evenly after dissolving;
(4) be immersed in the mixed liquor of step (3) by 60% blending cotton face fabric that is cotton, 40% terylene, temperature is room temperature, soaks 3h, and two leachings two are rolled, and pick-up is 50%, dry at 90 DEG C, is antibacterial blending cotton face fabric after dry.
Embodiment 4
(1) pulverized by Chinese juniper, add the ethanol water of 40wt% after pulverizing, feed liquid weight ratio is 1:6, and Extracting temperature is 55 DEG C, and extraction time is 3h, and centrifugation after extracting, will prepare Chinese juniper extract after supernatant concentration;
(2) by rascal crushed after being dried, add the ethanol water of 40wt%, feed liquid weight ratio is 1:4, Extracting temperature 40 DEG C, and extraction time is 2h, and centrifugation after extracting, prepares peel extract by after supernatant concentration;
(3) get that the peel extract that the Chinese juniper extract that shitosan is 10 parts, nano titanium oxide is 4 parts, prepared by step (1) is 5 parts, prepared by step (2) is 2 parts, water is 150 parts by weight, shitosan, nano titanium oxide, Chinese juniper extract and peel extract water are dissolved, is stirred to evenly after dissolving;
(4) be immersed in the mixed liquor of step (3) by 80% blending cotton face fabric that is cotton, 20% terylene, temperature is room temperature, soaks 3h, and two leachings two are rolled, and pick-up is 50%, dry at 90 DEG C, is antibacterial blending cotton face fabric after dry.
Embodiment 5
(1) pulverized by Chinese juniper, add the ethanol water of 30wt% after pulverizing, feed liquid weight ratio is 1:7, and Extracting temperature is 60 DEG C, and extraction time is 4h, and centrifugation after extracting, will prepare Chinese juniper extract after supernatant concentration;
(2) by rascal crushed after being dried, add the ethanol water of 50wt%, feed liquid weight ratio is 1:5, Extracting temperature 50 DEG C, and extraction time is 3h, and centrifugation after extracting, prepares peel extract by after supernatant concentration;
(3) get that the peel extract that the Chinese juniper extract that shitosan is 8 parts, nano titanium oxide is 4 parts, prepared by step (1) is 5 parts, prepared by step (2) is 3 parts, water is 155 parts by weight, shitosan, nano titanium oxide, Chinese juniper extract and peel extract water are dissolved, is stirred to evenly after dissolving;
(4) be immersed in the mixed liquor of step (3) by 80% blending cotton face fabric that is cotton, 20% terylene, temperature is room temperature, soaks 3h, and two leachings two are rolled, and pick-up is 60%, dry at 90 DEG C, is antibacterial blending cotton face fabric after dry.
Comparative example
(1) pulverized by Chinese juniper, add the ethanol water of 20wt% after pulverizing, feed liquid weight ratio 1:9, Extracting temperature is 65 DEG C, and extraction time is 5h, and centrifugation after extracting, will prepare Chinese juniper extract after supernatant concentration;
(2) get that the Chinese juniper extract that shitosan is 13 parts, nano titanium oxide is 6 parts, prepared by step (1) is 5 parts, water is 145 parts by weight, shitosan, nano titanium oxide, Chinese juniper extract and peel extract water are dissolved, is stirred to evenly after dissolving;
(3) be immersed in the mixed liquor of step (2) by 60% blending cotton face fabric that is cotton, 40% spandex, temperature is room temperature, soaks 3h, and two leachings two are rolled, and pick-up is 70%, dry at 90 DEG C, is antibacterial blending cotton face fabric after dry.
Measured by the anti-microbial property of embodiment 1 to 5 and comparative example, its bacteriostasis rate result is as follows:
| Escherichia coli inhibiting rate | Staphylococcus aureus inhibiting rate | |
| Embodiment 1 | 87％ | 85％ |
| Embodiment 2 | 87％ | 86％ |
| Embodiment 3 | 90％ | 90％ |
| Embodiment 4 | 91％ | 88％ |
| Embodiment 5 | 96％ | 94％ |
| Comparative example | 75％ | 79％ |
From the gap of the bacteriostasis rate of comparative example and embodiment, the antibiotic finishing method of blended yarn woven fabric of the present invention, by adding peel extract, and then effectively raises the bacteriostasis rate of blending cotton face fabric to Escherichia coli and staphylococcus aureus.
Claims (7)
1. an antibiotic finishing method for blending cotton face fabric, is characterized in that described antibiotic finishing method step is as follows:
(1) pulverized by Chinese juniper, add ethanol water after pulverizing and extract, centrifugation after extracting, will prepare Chinese juniper extract after supernatant concentration;
(2) separately get rascal, by rascal crushed after being dried, add ethanol water and extract, centrifugation after extracting, prepares peel extract by after supernatant concentration;
(3) get that the peel extract that the Chinese juniper extract that shitosan is 5-13 part, nano titanium oxide is 3-6 part, prepared by step (1) is 3-5 part, prepared by step (2) is 2-5 part, water is 145-165 part by weight, shitosan, nano titanium oxide, Chinese juniper extract and peel extract water are dissolved, is stirred to evenly after dissolving;
(4) be immersed into by blending cotton face fabric in the mixed liquor of step (3), temperature is room temperature, soaks 3h, and two leachings two are rolled, and pick-up is 50-70%, dry at 90 DEG C, is antibacterial blending cotton face fabric after dry.
2. the antibiotic finishing method of a kind of blending cotton face fabric according to claim 1, it is characterized in that described Chinese juniper method for preparing extractive is as follows: pulverized by Chinese juniper, the ethanol water of 20-40wt% is added after pulverizing, feed liquid weight ratio is 1:6-1:9, Extracting temperature is 55-65 DEG C, extraction time is 3-5h, and centrifugation after extracting, will prepare Chinese juniper extract after supernatant concentration.
3. the antibiotic finishing method of a kind of blending cotton face fabric according to claim 1, it is characterized in that described peel extract preparation method is as follows: by rascal crushed after being dried, add the ethanol water of 40-60wt%, feed liquid weight ratio is 1:4-6, Extracting temperature 40-60 DEG C, extraction time is 2-3h, and centrifugation after extracting, prepares peel extract by after supernatant concentration.
4. the antibiotic finishing method of a kind of blending cotton face fabric according to claim 1, is characterized in that, in described blending cotton face fabric, cotton content is 60-80%.
5. the antibiotic finishing method of a kind of blending cotton face fabric according to claim 4, is characterized in that in described blending cotton face fabric except cotton, and residue fabric is spandex or terylene.
6. the antibiotic finishing method of a kind of blending cotton face fabric according to claim 1, is characterized in that described shitosan purity is more than 90%.
7. the antibiotic finishing method of a kind of blending cotton face fabric according to claim 1, is characterized in that pick-up is 60%.
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105239413A (en) * | 2015-11-12 | 2016-01-13 | 长兴千尺度纺织品有限公司 | Application of ecological auxiliary in finishing of cashmere sweater |
| CN105256590A (en) * | 2015-11-12 | 2016-01-20 | 长兴千尺度纺织品有限公司 | Ecological textile auxiliary |
| CN105256568A (en) * | 2015-11-12 | 2016-01-20 | 长兴千尺度纺织品有限公司 | Application of ecological auxiliary to woolen sweater finishing |
| CN105623481A (en) * | 2016-02-24 | 2016-06-01 | 刘操 | Polyester powder coating with sterilizing effect and preparation method and application thereof |
| CN105671942A (en) * | 2016-01-07 | 2016-06-15 | 江苏天章医用卫生新材料有限公司 | Method for preparing medical antibacterial cotton gauze |
| CN107794757A (en) * | 2017-11-30 | 2018-03-13 | 苏州绣艳天下刺绣工艺有限公司 | A kind of preparation method embroidered with antifungal gene finishing agent |
| CN108797108A (en) * | 2018-05-23 | 2018-11-13 | 宁波必博母婴科技有限公司 | A kind of preparation method of antibacterial green textile fabric for baby |
| CN108978179A (en) * | 2018-07-10 | 2018-12-11 | 安徽玉然经编科技有限公司 | A kind of plasma of dacron-chitosan base load silver-nano-titanium oxide antibacterial hydrophilic finiss technique |
| CN108978196A (en) * | 2018-07-23 | 2018-12-11 | 含山县海达服饰有限公司 | A kind of processing method of antibacterial gym suit fabric |
| CN110219171A (en) * | 2019-06-04 | 2019-09-10 | 吴江市恒腾纺织有限公司 | A kind of processing method of high F number spring Asia textile fabric |
| CN110578253A (en) * | 2019-09-17 | 2019-12-17 | 常州大学 | Preparation method of antibacterial textile based on polydopamine/nano-silver |
| CN112853755A (en) * | 2020-12-23 | 2021-05-28 | 南通雅文纺织品有限公司 | Antibacterial fabric for sofa cushion and production process thereof |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105239413A (en) * | 2015-11-12 | 2016-01-13 | 长兴千尺度纺织品有限公司 | Application of ecological auxiliary in finishing of cashmere sweater |
| CN105256590A (en) * | 2015-11-12 | 2016-01-20 | 长兴千尺度纺织品有限公司 | Ecological textile auxiliary |
| CN105256568A (en) * | 2015-11-12 | 2016-01-20 | 长兴千尺度纺织品有限公司 | Application of ecological auxiliary to woolen sweater finishing |
| CN105671942A (en) * | 2016-01-07 | 2016-06-15 | 江苏天章医用卫生新材料有限公司 | Method for preparing medical antibacterial cotton gauze |
| CN105623481A (en) * | 2016-02-24 | 2016-06-01 | 刘操 | Polyester powder coating with sterilizing effect and preparation method and application thereof |
| CN107794757A (en) * | 2017-11-30 | 2018-03-13 | 苏州绣艳天下刺绣工艺有限公司 | A kind of preparation method embroidered with antifungal gene finishing agent |
| CN108797108A (en) * | 2018-05-23 | 2018-11-13 | 宁波必博母婴科技有限公司 | A kind of preparation method of antibacterial green textile fabric for baby |
| CN108978179A (en) * | 2018-07-10 | 2018-12-11 | 安徽玉然经编科技有限公司 | A kind of plasma of dacron-chitosan base load silver-nano-titanium oxide antibacterial hydrophilic finiss technique |
| CN108978196A (en) * | 2018-07-23 | 2018-12-11 | 含山县海达服饰有限公司 | A kind of processing method of antibacterial gym suit fabric |
| CN110219171A (en) * | 2019-06-04 | 2019-09-10 | 吴江市恒腾纺织有限公司 | A kind of processing method of high F number spring Asia textile fabric |
| CN110578253A (en) * | 2019-09-17 | 2019-12-17 | 常州大学 | Preparation method of antibacterial textile based on polydopamine/nano-silver |
| CN110578253B (en) * | 2019-09-17 | 2022-03-08 | 常州大学 | Preparation method of antibacterial textile based on polydopamine/nano-silver |
| CN112853755A (en) * | 2020-12-23 | 2021-05-28 | 南通雅文纺织品有限公司 | Antibacterial fabric for sofa cushion and production process thereof |
| CN112853755B (en) * | 2020-12-23 | 2022-03-25 | 南通雅文纺织品有限公司 | Antibacterial fabric for sofa cushion and production process thereof |
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