CN103668978A - Textile anti-bacterial finishing agent and preparation method thereof - Google Patents
Textile anti-bacterial finishing agent and preparation method thereof Download PDFInfo
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- CN103668978A CN103668978A CN201310614060.8A CN201310614060A CN103668978A CN 103668978 A CN103668978 A CN 103668978A CN 201310614060 A CN201310614060 A CN 201310614060A CN 103668978 A CN103668978 A CN 103668978A
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Abstract
The invention relates to a textile anti-bacterial finishing agent and a preparation method thereof and belongs to the technical field of textile auxiliary agents. The finishing agent comprises components in parts by weight as follows: 10-15 parts of ethoxyl ether chitosan, 8-12 parts of nano-zinc oxide, 4-7 parts of clove essential oil, 12-25 parts of water-based acrylic resin, 3-6 parts of a dispersing agent and 50-70 parts of water. According to the finishing agent, an inorganic nano anti-bacterial agent and a natural anti-bacterial agent cooperate with each other to realize an anti-bacterial effect, so that a product of the finishing agent is high in heat resistance, strong in anti-bacterial property, safe, reliable and environment-friendly; meanwhile, the clove essential oil is added in the product, so that the anti-bacterial property of the product is enhanced, and a processed textile has the fragrance; and the product is simple in preparation method, so that the product is easy to popularize and apply.
Description
Technical field
The invention belongs to textile auxiliary technical field, be specifically related to a kind of fabric antimicrobial finishing agent and preparation method thereof.
Background technology
Along with growth in the living standard, people more and more pay attention to the quality of life, wish to obtain the clothing of comfort and the living environment of hygiene and health, so people require more and more higher for various textiless, particularly safely, feel at ease, comfortable, healthy, health, " green " formation of idea such as clean, make to arrange to process after antibacterial, the mildew-resistant, deodorization of textiles to be more subject to people's attention.
In life, people inevitably touch the microorganisms such as various bacteriums, fungi, and these microorganisms, under suitable external condition, can breed rapidly, and spread disease by modes such as contacts, affect people's healthy and normal work, studying and living.Fiber belongs to porous material, can form the polylayer forest in countless spaces again, so fabric is easier to adsorb mushroom after stack braiding.Antibiotic finish is exactly to make fabric have the function that suppresses fungus grown, maintains the clothing living environment of health, guarantees health.It is bactericide that traditional antibacterial finishing agent be take the organic chemicals synthesizing, and toxicity is larger.Therefore how overcoming the deficiencies in the prior art is problems that current textile auxiliary technical field is needed solution badly.
Summary of the invention
The object of the invention is, in order to solve the deficiencies in the prior art, provides a kind of fabric antimicrobial finishing agent and preparation method thereof, and this finishing agent heat resistance is high, antibiotic property is strong, safe and reliable, and preparation technology is simple.
The technical solution used in the present invention is as follows:
A fabric antimicrobial finishing agent, comprises the following component according to parts by weight meter: 10 ~ 15 parts of hydroxyethyl ether shitosans, 8 ~ 12 parts of nano zine oxides, 4 ~ 7 parts of clove oils, 12 ~ 25 parts of water-borne acrylic resins, 3 ~ 6 parts of dispersants, 50 ~ 70 parts, water.
Further preferably described dispersant is PEG400.
The preparation method of above-mentioned fabrics antibacterial finishing agent, that hydroxyethyl ether shitosan, nano zine oxide, water-borne acrylic resin are added to the water together with dispersant, high-speed stirred is to mixing, and then to adding clove oil, stirring at low speed, to mixing, obtains fabric antimicrobial finishing agent of the present invention.
Further preferably the mixing speed of described high-speed stirred is 1400 ~ 1600r/min.
Further preferably the mixing speed of described stirring at low speed is 30 ~ 50r/min.
compared with prior art, its beneficial effect is in the present invention:(1) the present invention adopts inorganic nano antiseptic and natural antibacterial agent Synergistic antimicrobial, makes that product heat resistance of the present invention is high, antibiotic property is strong, and safe and reliable, environmental protection; (2) in product, add clove oil, not only strengthened the antibiotic property of product, also made the fabric after processing there is armaticity simultaneously; (3) product preparation method of the present invention is simple, is easy to apply.
Specific embodiment
Below in conjunction with embodiment, the present invention is described in further detail.
Embodiment 1
A fabric antimicrobial finishing agent, comprises the following component according to parts by weight meter: 10 parts of hydroxyethyl ether shitosans, 8 parts of nano zine oxides, 4 parts of clove oils, 12 parts of water-borne acrylic resins, 3 parts of PEG400s, 50 parts, water.
The preparation method of the present embodiment fabric antimicrobial finishing agent, that hydroxyethyl ether shitosan, nano zine oxide, water-borne acrylic resin are added to the water together with PEG400, high-speed stirred is to mixing, high-speed stirred speed is 1400 ~ 1600r/min, and then to adding clove oil stirring at low speed, mixing speed 30 ~ 50r/min, to the fabric antimicrobial finishing agent that mixes and obtain the present embodiment.
Embodiment 2
A fabric antimicrobial finishing agent, comprises the following component according to parts by weight meter: 15 parts of hydroxyethyl ether shitosans, 12 parts of nano zine oxides, 7 parts of clove oils, 25 parts of water-borne acrylic resins, 6 parts of PEG400s, 70 parts, water.
The preparation method of the present embodiment fabric antimicrobial finishing agent is identical with the preparation method of embodiment 1 antibacterial finishing agent.
Embodiment 3
A fabric antimicrobial finishing agent, comprises the following component according to parts by weight meter: 13 parts of hydroxyethyl ether shitosans, 11 parts of nano zine oxides, 5 parts of clove oils, 18 parts of water-borne acrylic resins, 4 parts of PEG400s, 60 parts, water.
The preparation method of the present embodiment fabric antimicrobial finishing agent is identical with the preparation method of embodiment 1 antibacterial finishing agent.
The resulting fabric antimicrobial finishing agent of the embodiment of the present invention 1 ~ 3 is mixed with to the dressing liquid that concentration is 20 grams per liters, adopt citric acid that dressing liquid pH is adjusted to 5-6, then fabric is placed in after dressing liquid infiltration, two soak two rolls, finally take out fabric and at 120 ℃, dry, shape, obtaining antibiotic fabric.
Anti-microbial property to resulting antibiotic fabric is tested, and test result is as shown in table 1.
The anti-microbial property test result of table 1 antibiotic fabric
| ? | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Staphylococcus aureus | 95% | 98% | 99% |
| Escherichia coli | 96% | 94% | 97% |
| Candida albicans | 90% | 93% | 95% |
Claims (5)
1. a fabric antimicrobial finishing agent, is characterized in that comprising the following component according to parts by weight meter: 10 ~ 15 parts of hydroxyethyl ether shitosans, 8 ~ 12 parts of nano zine oxides, 4 ~ 7 parts of clove oils, 12 ~ 25 parts of water-borne acrylic resins, 3 ~ 6 parts of dispersants, 50 ~ 70 parts, water.
2. fabric antimicrobial finishing agent according to claim 1, is characterized in that described dispersant is PEG400.
3. the preparation method of fabric antimicrobial finishing agent claimed in claim 1, it is characterized in that hydroxyethyl ether shitosan, nano zine oxide, water-borne acrylic resin to be added to the water together with dispersant, high-speed stirred is to mixing, and then to adding clove oil, stirring at low speed, to mixing, obtains fabric antimicrobial finishing agent of the present invention.
4. the preparation method of fabric antimicrobial finishing agent according to claim 3, is characterized in that the mixing speed of described high-speed stirred is 1400 ~ 1600r/min.
5. the preparation method of fabric antimicrobial finishing agent according to claim 3, is characterized in that the mixing speed of described stirring at low speed is 30 ~ 50r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201310614060.8A CN103668978B (en) | 2013-11-27 | 2013-11-27 | A kind of fabric antimicrobial finishing agent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310614060.8A CN103668978B (en) | 2013-11-27 | 2013-11-27 | A kind of fabric antimicrobial finishing agent and preparation method thereof |
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| CN103668978A true CN103668978A (en) | 2014-03-26 |
| CN103668978B CN103668978B (en) | 2015-12-30 |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104452289A (en) * | 2014-12-23 | 2015-03-25 | 常熟市华博毛纺织有限公司 | Finishing process of shirt fabric |
| CN104532557A (en) * | 2014-12-23 | 2015-04-22 | 常熟市中宏针织厂 | Finishing process of garment shell fabric |
| CN104594029A (en) * | 2015-02-02 | 2015-05-06 | 苏州爱立方服饰有限公司 | Antibacterial finish method for blended cotton fabric |
| CN105019236A (en) * | 2015-07-13 | 2015-11-04 | 江苏神涛环保科技有限公司 | Composite antibiotic finishing agent for textiles |
| CN105220462A (en) * | 2015-10-30 | 2016-01-06 | 朱忠良 | A kind of textile nano function finishing agent and its preparation method and application |
| CN105780473A (en) * | 2014-12-22 | 2016-07-20 | 常熟市虹桥印染有限公司 | Textile antibacterial finishing agent |
| CN107747217A (en) * | 2017-10-23 | 2018-03-02 | 湖州市星智造服饰有限公司 | Clothing finishing agent and preparation method thereof |
| CN107869057A (en) * | 2017-11-30 | 2018-04-03 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of antibacterial antistatic finishing agent |
| CN109023917A (en) * | 2018-06-26 | 2018-12-18 | 澳洋集团有限公司 | A kind of preparation method of modified cotton fiber material |
| CN109235033A (en) * | 2018-08-10 | 2019-01-18 | 苏州市天翱特种织绣有限公司 | A kind of preparation method of antibacterial fabric deodorization finishing agent |
| CN112063109A (en) * | 2020-09-11 | 2020-12-11 | 石家庄元鼎新材料有限公司 | Nano zinc oxide/artemisia yellow-wormwood volatile oil/epoxy resin high-performance antibacterial material and preparation method thereof |
| CN113279250A (en) * | 2021-05-24 | 2021-08-20 | 广东奔立尔实业集团有限公司 | Environment-friendly antibacterial ultraviolet-proof clothes |
| CN113846483A (en) * | 2021-08-26 | 2021-12-28 | 开滦（集团）有限责任公司 | Polyformaldehyde fiber finishing liquid, finishing method and polyformaldehyde blended fabric |
| ES2904257A1 (en) * | 2020-10-02 | 2022-04-04 | Zapico Rodriguez Ines | Disinfection procedure (Machine-translation by Google Translate, not legally binding) |
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| CN103333571A (en) * | 2013-06-24 | 2013-10-02 | 广州慧谷化学有限公司 | Water-based antimicrobial moldproof hydrophilic paint for heat exchanger fin surface treatment |
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| CN1554810A (en) * | 2003-12-26 | 2004-12-15 | 吉林容大机电技术有限公司 | Biological function materal used in fabric and coating |
| JP2006328624A (en) * | 2005-04-28 | 2006-12-07 | Nicca Chemical Co Ltd | Water-repellent agent, water-repellent finishing method and water-repellent textile product |
| CN1742583A (en) * | 2005-09-23 | 2006-03-08 | 周海燕 | Composite nano anti-biotic material and preparation method |
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Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105780473A (en) * | 2014-12-22 | 2016-07-20 | 常熟市虹桥印染有限公司 | Textile antibacterial finishing agent |
| CN104452289A (en) * | 2014-12-23 | 2015-03-25 | 常熟市华博毛纺织有限公司 | Finishing process of shirt fabric |
| CN104532557A (en) * | 2014-12-23 | 2015-04-22 | 常熟市中宏针织厂 | Finishing process of garment shell fabric |
| CN104594029A (en) * | 2015-02-02 | 2015-05-06 | 苏州爱立方服饰有限公司 | Antibacterial finish method for blended cotton fabric |
| CN105019236A (en) * | 2015-07-13 | 2015-11-04 | 江苏神涛环保科技有限公司 | Composite antibiotic finishing agent for textiles |
| CN105220462A (en) * | 2015-10-30 | 2016-01-06 | 朱忠良 | A kind of textile nano function finishing agent and its preparation method and application |
| CN107747217A (en) * | 2017-10-23 | 2018-03-02 | 湖州市星智造服饰有限公司 | Clothing finishing agent and preparation method thereof |
| CN107869057A (en) * | 2017-11-30 | 2018-04-03 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of antibacterial antistatic finishing agent |
| CN109023917A (en) * | 2018-06-26 | 2018-12-18 | 澳洋集团有限公司 | A kind of preparation method of modified cotton fiber material |
| CN109235033A (en) * | 2018-08-10 | 2019-01-18 | 苏州市天翱特种织绣有限公司 | A kind of preparation method of antibacterial fabric deodorization finishing agent |
| CN109235033B (en) * | 2018-08-10 | 2021-12-17 | 苏州市天翱特种织绣有限公司 | Preparation method of antibacterial and deodorant finishing agent for fabric |
| CN112063109A (en) * | 2020-09-11 | 2020-12-11 | 石家庄元鼎新材料有限公司 | Nano zinc oxide/artemisia yellow-wormwood volatile oil/epoxy resin high-performance antibacterial material and preparation method thereof |
| CN112063109B (en) * | 2020-09-11 | 2023-01-17 | 石家庄元鼎新材料有限公司 | Nano zinc oxide/artemisia yellow-wormwood volatile oil/epoxy resin high-performance antibacterial material and preparation method thereof |
| ES2904257A1 (en) * | 2020-10-02 | 2022-04-04 | Zapico Rodriguez Ines | Disinfection procedure (Machine-translation by Google Translate, not legally binding) |
| CN113279250A (en) * | 2021-05-24 | 2021-08-20 | 广东奔立尔实业集团有限公司 | Environment-friendly antibacterial ultraviolet-proof clothes |
| CN113846483A (en) * | 2021-08-26 | 2021-12-28 | 开滦（集团）有限责任公司 | Polyformaldehyde fiber finishing liquid, finishing method and polyformaldehyde blended fabric |
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|---|---|
| CN103668978B (en) | 2015-12-30 |
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