CN105926270A - Fabric antibacterial finishing agent and preparing method thereof - Google Patents
Fabric antibacterial finishing agent and preparing method thereof Download PDFInfo
- Publication number
- CN105926270A CN105926270A CN201610291808.9A CN201610291808A CN105926270A CN 105926270 A CN105926270 A CN 105926270A CN 201610291808 A CN201610291808 A CN 201610291808A CN 105926270 A CN105926270 A CN 105926270A
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- CN
- China
- Prior art keywords
- parts
- finishing agent
- fabric
- antimicrobial finishing
- ytterbium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000004744 fabric Substances 0.000 title claims abstract description 57
- 238000000034 method Methods 0.000 title claims description 9
- 230000000844 anti-bacterial effect Effects 0.000 title abstract description 16
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 39
- NEHNMFOYXAPHSD-UHFFFAOYSA-N citronellal Chemical compound O=CCC(C)CCC=C(C)C NEHNMFOYXAPHSD-UHFFFAOYSA-N 0.000 claims abstract description 36
- 229920002101 Chitin Polymers 0.000 claims abstract description 19
- 229930003633 citronellal Natural products 0.000 claims abstract description 18
- 235000000983 citronellal Nutrition 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 15
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 15
- 150000001225 Ytterbium Chemical class 0.000 claims abstract description 12
- 229910052769 Ytterbium Inorganic materials 0.000 claims abstract description 3
- 230000000845 anti-microbial effect Effects 0.000 claims description 31
- 238000002360 preparation method Methods 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 8
- CKLHRQNQYIJFFX-UHFFFAOYSA-K ytterbium(III) chloride Chemical group [Cl-].[Cl-].[Cl-].[Yb+3] CKLHRQNQYIJFFX-UHFFFAOYSA-K 0.000 claims description 8
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 5
- 230000006196 deacetylation Effects 0.000 claims description 5
- 238000003381 deacetylation reaction Methods 0.000 claims description 5
- 229920002565 Polyethylene Glycol 400 Polymers 0.000 claims description 3
- 229960003511 macrogol Drugs 0.000 claims description 3
- JLFNLZLINWHATN-UHFFFAOYSA-N pentaethylene glycol Chemical compound OCCOCCOCCOCCOCCO JLFNLZLINWHATN-UHFFFAOYSA-N 0.000 claims description 3
- UZLYXNNZYFBAQO-UHFFFAOYSA-N oxygen(2-);ytterbium(3+) Chemical compound [O-2].[O-2].[O-2].[Yb+3].[Yb+3] UZLYXNNZYFBAQO-UHFFFAOYSA-N 0.000 claims description 2
- NAWDYIZEMPQZHO-UHFFFAOYSA-N ytterbium Chemical compound [Yb] NAWDYIZEMPQZHO-UHFFFAOYSA-N 0.000 claims description 2
- 229940075624 ytterbium oxide Drugs 0.000 claims description 2
- 229910003454 ytterbium oxide Inorganic materials 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims 1
- 229940093429 polyethylene glycol 6000 Drugs 0.000 claims 1
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims 1
- 241000191967 Staphylococcus aureus Species 0.000 abstract description 2
- 241000588724 Escherichia coli Species 0.000 abstract 1
- 239000003899 bactericide agent Substances 0.000 abstract 1
- 239000000675 fabric finishing Substances 0.000 abstract 1
- 238000009962 finishing (textile) Methods 0.000 abstract 1
- 230000003115 biocidal effect Effects 0.000 description 8
- 210000002268 wool Anatomy 0.000 description 7
- 229910052761 rare earth metal Inorganic materials 0.000 description 6
- 239000013068 control sample Substances 0.000 description 4
- -1 rare earth ion Chemical class 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 239000004753 textile Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 241000233866 Fungi Species 0.000 description 2
- 239000013522 chelant Substances 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 238000011056 performance test Methods 0.000 description 2
- 229940113115 polyethylene glycol 200 Drugs 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 208000030507 AIDS Diseases 0.000 description 1
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 108010054033 Chitin deacetylase Proteins 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009954 braiding Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000002781 deodorant agent Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000007730 finishing process Methods 0.000 description 1
- 230000001408 fungistatic effect Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- KUBYTSCYMRPPAG-UHFFFAOYSA-N ytterbium(3+);trinitrate Chemical compound [Yb+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O KUBYTSCYMRPPAG-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/17—Halides of elements of Groups 3 or 13 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/165—Ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention relates to a fabric antibacterial finishing agent. The fabric antibacterial finishing agent is prepared from, by weight, 5-8 parts of chitin, 3-5 parts of ytterbium salt, 3-5 parts of citronellal, 10-15 parts of polyethylene glycol and 50-70 parts of water. The suitable element-ytterbium is selected and cooperates with specific bactericide to obtain the fabric finishing agent with broad-spectrum antibacterial activity, and the antibacterial property to staphylococcus aureus and escherichia coli of fabric finished by the fabric antibacterial finishing agent reaches 95% or more and still reaches 92% or more after the fabric is washed by 50 times.
Description
Technical field
The invention belongs to technical field of textile auxiliary agent, be specifically related to a kind of fabric antimicrobial finishing agent and preparation method thereof.
Background technology
Along with growth in the living standard, people increasingly pay attention to the quality of life, it would be desirable to obtain the clothing having comfort
And the living environment of hygiene and health, so people require more and more higher for various textiles, the safest, peace
The formation of " green " ideas such as the heart, comfortable, healthy, health, cleaning, makes antibacterial, the mildew-resistant of textile, deodorant Final finishing process more
Add and be subject to people's attention.
In life, people inevitably touch the microorganisms such as various antibacterial, fungus, and these microorganisms exist
Suitably under external condition, can breed rapidly, and be spread disease by modes such as contacts, affect the healthy and normal of people
Work, studying and living.Fiber belongs to porous material, can form again the polylayer forest in countless space, therefore after superposition braiding
Fabric is easier to adsorb mushroom.Antibiotic finish is exactly the function making fabric have suppression fungus grown, and the clothing maintaining health is raw
Ever-changing environment, it is ensured that health.
Rare earth element has the biological activitys such as reasonable antibacterial, antitumor, anti-AIDS.Owing to rare earth ion has relatively
High charge number (+3) and bigger ionic radius (85～106pm), thus rare earth ion during the antibiotic finish of fabric
Chelate may be formed with the coordination atom such as oxygen, nitrogen in fabric, form coordination compound or chelate with antibacterial the most again, make antibacterial
Agent is combined with fabric securely；Meanwhile, between different antibacterial, with rare earth ion as tie-point, produce collaborative antibacterial work
With, cause fabric to have again the fungistatic effect of spectrum.
This area needs a kind of fabric antimicrobial finishing agent of exploitation, and it can play the effect of rare earth ion, improve fabric
Antibacterial activity.
Summary of the invention
It is an object of the invention to provide a kind of fabric antimicrobial finishing agent, according to parts by weight, described antibiotic finish of the fabric
Agent includes following component:
Chitin 5～8 parts
Ytterbium salt 2～3 parts
Citronellal 3～5 parts
Polyethylene Glycol 3～6 parts
Water 50～70 parts.
Preferably, the deacetylation of described chitin is 50～more than 60%, preferably 56%.
Preferably, described ytterbium salt is selected from Ytterbium trichloride, Ytterbium(III) nitrate. or ytterbium oxide, preferably Ytterbium trichloride.
Preferably, described citronellal purity is more than 70%, such as 75%, 80%, 85%, 90% etc..
Preferably, described Polyethylene Glycol is selected from polyethylene glycol 200, PEG400, Macrogol 2000 or Polyethylene Glycol
Any a kind or the combination of at least 2 kinds in 6000.
Preferably, described fabric antimicrobial finishing agent includes following component:
Chitin 7 parts
Ytterbium salt 4 parts
Citronellal 4 parts
Polyethylene Glycol 13 parts
60 parts of water.
The two of the object of the invention are to provide the preparation method of a kind of fabric antimicrobial finishing agent as described in one of purpose, described
Method is in the water that the chitin of formula ratio, ytterbium salt add together with Polyethylene Glycol formula ratio, high-speed stirred to mix homogeneously,
Then adding citronellal, stirring at low speed, to mix homogeneously, obtains described fabric antimicrobial finishing agent.
Preferably, the mixing speed of described high-speed stirred is 1700～2000r/min.
Preferably, the mixing speed of described stirring at low speed is 60～80r/min.
Compared with prior art, the method have the advantages that
The present invention, by selecting suitable Rare earth element ytterbium, coordinates chitin and citronellal, has obtained for fabric
The finishing agent with broad spectrum antibiotic activity arranged；Use fabric antimicrobial finishing agent finish fabric of the present invention, after arrangement
Fabric to staphylococcus aureus and colibacillary antibiotic property more than 95%, and through 50 washings, its antibiotic property is still
So more than 90%.
Detailed description of the invention
Technical scheme is further illustrated below by detailed description of the invention.
Those skilled in the art, it will be clearly understood that the only help of described embodiment understands the present invention, are not construed as this
Bright concrete restriction.
Embodiment 1
A kind of fabric antimicrobial finishing agent, includes following component by weight:
Chitin (deacetylation is 55%) 7 parts
Ytterbium trichloride 4 parts
Citronellal 4 parts
PEG400 13 parts
60 parts of water；
Preparation method is: described method is that the chitin of formula ratio, ytterbium salt are added together with Polyethylene Glycol formula ratio
In water, 1800r/min high-speed stirred, to mix homogeneously, then adds citronellal, 70r/min stirring at low speed to mix homogeneously,
Obtain described fabric antimicrobial finishing agent.
Embodiment 2
A kind of fabric antimicrobial finishing agent, includes following component by weight:
Chitin deacetylase degree 50% 5 parts
Ytterbium trichloride 3 parts
Citronellal 3 parts
Macrogol 2000 10 parts
50 parts of water；
Preparation method is: described method is that the chitin of formula ratio, ytterbium salt are added together with Polyethylene Glycol formula ratio
In water, 1700r/min high-speed stirred, to mix homogeneously, then adds citronellal, 60r/min stirring at low speed to mix homogeneously,
Obtain described fabric antimicrobial finishing agent.
Embodiment 3
A kind of fabric antimicrobial finishing agent, includes following component by weight:
Chitin (deacetylation 60%) 8 parts
Ytterbium trichloride 5 parts
Citronellal 5 parts
Polyethylene glycol 200 15 parts
70 parts of water；
Preparation method is: described method is that the chitin of formula ratio, ytterbium salt are added together with Polyethylene Glycol formula ratio
In water, 2000r/min high-speed stirred, to mix homogeneously, then adds citronellal, 80r/min stirring at low speed to mix homogeneously,
Obtain described fabric antimicrobial finishing agent.
Comparative example
A kind of fabric antimicrobial finishing agent, includes following component by weight:
Chitin 10 parts
Ytterbium trichloride 6 parts
Citronellal 6 parts
Polyethylene Glycol 5 parts
60 parts of water；
Preparation method is: described method is in the water that the chitin of formula ratio adds together with Polyethylene Glycol formula ratio,
1800r/min high-speed stirred, to mix homogeneously, then adds citronellal, and 70r/min stirring at low speed, to mix homogeneously, obtains institute
State fabric antimicrobial finishing agent.
Performance test
Wool fabric is immersed in the fabric antimicrobial finishing agent that embodiment and comparative example provide, regulation pH value to 3～4,
At 60～70 DEG C, soak 1.5h, take out wool fabric, distilled water wash afterwards, obtain through fabric antimicrobial finishing agent arrangement
Wool fabric, tests.
Antibiotic property: by the wool fabric arranged through fabric antimicrobial finishing agent and control sample 1 (without antibiotic finish of the fabric
The wool fabric that agent arranges) it is placed in triangular flask, inoculate with test organisms, constant temperature culture, measure clump count；Control sample 1 clump count
It is 100；
Washing fastness: by (whole without antibacterial fabric to the wool fabric arranged through fabric antimicrobial finishing agent and control sample 2
The wool fabric that reason agent arranges) wash 50 times, it is subsequently placed in triangular flask, inoculates with test organisms, constant temperature culture, measure bacterium colony
Number；Control sample 2 clump count is 105；.
The performance test results:
In comparative example, owing to chitin content is higher, cause stock dispersion bad, affect antibacterial effect.
Applicant states, the present invention illustrates the process of the present invention by above-described embodiment, but the present invention not office
It is limited to above-mentioned processing step, does not i.e. mean that the present invention has to rely on above-mentioned processing step and could implement.Art
Technical staff is it will be clearly understood that any improvement in the present invention, and equivalence to raw material selected by the present invention is replaced and auxiliary element
Interpolation, concrete way choice etc., within the scope of all falling within protection scope of the present invention and disclosure.
Claims (10)
1. a fabric antimicrobial finishing agent, it is characterised in that according to parts by weight, described fabric antimicrobial finishing agent includes following group
Point:
Chitin 5～8 parts
Ytterbium salt 3～5 parts
Citronellal 3～5 parts
Polyethylene Glycol 10～15 parts
Water 50～70 parts.
2. fabric antimicrobial finishing agent as claimed in claim 1, it is characterised in that the deacetylation of described chitin be 50～
60%.
3. fabric antimicrobial finishing agent as claimed in claim 1 or 2, it is characterised in that the deacetylation of described chitin is
56%.
4. the fabric antimicrobial finishing agent as described in one of claims 1 to 3, it is characterised in that described ytterbium salt is selected from Ytterbium trichloride, nitre
Acid ytterbium or ytterbium oxide, preferably Ytterbium trichloride.
5. the fabric antimicrobial finishing agent as described in one of Claims 1 to 4, it is characterised in that described citronellal purity is 70%
Above.
6. the fabric antimicrobial finishing agent as described in one of Claims 1 to 5, it is characterised in that described Polyethylene Glycol is selected from poly-second
Any a kind or the combination of at least 2 kinds in glycol 200, PEG400, Macrogol 2000 or polyethylene glycol 6000.
7. the fabric antimicrobial finishing agent as described in one of claim 1～6, it is characterised in that described fabric antimicrobial finishing agent bag
Include following component:
Chitin 7 parts
Ytterbium salt 4 parts
Citronellal 4 parts
Polyethylene Glycol 13 parts
60 parts of water.
8. the preparation method of the fabric antimicrobial finishing agent as described in one of claim 1～6, it is characterised in that described side
Method is that in the water that the chitin of formula ratio, ytterbium salt add together with Polyethylene Glycol formula ratio, high-speed stirred is to mix homogeneously, so
After add citronellal, stirring at low speed, to mix homogeneously, obtains described fabric antimicrobial finishing agent.
9. preparation method as claimed in claim 8, it is characterised in that the mixing speed of described high-speed stirred be 1700～
2000r/min。
10. as claimed in claim 8 or 9 preparation method, it is characterised in that the mixing speed of described stirring at low speed be 60～
80r/min。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610291808.9A CN105926270A (en) | 2016-05-05 | 2016-05-05 | Fabric antibacterial finishing agent and preparing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610291808.9A CN105926270A (en) | 2016-05-05 | 2016-05-05 | Fabric antibacterial finishing agent and preparing method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105926270A true CN105926270A (en) | 2016-09-07 |
Family
ID=56835183
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610291808.9A Pending CN105926270A (en) | 2016-05-05 | 2016-05-05 | Fabric antibacterial finishing agent and preparing method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105926270A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107119453A (en) * | 2017-06-28 | 2017-09-01 | 顾秋军 | A kind of fabric antimicrobial finishing agent and preparation method thereof |
| CN107313256A (en) * | 2017-06-28 | 2017-11-03 | 顾秋军 | A kind of fabric antimicrobial finishing agent and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103866651A (en) * | 2014-03-31 | 2014-06-18 | 宋旭 | Wallpaper with air purifying function and preparation method |
| CN105133308A (en) * | 2015-09-14 | 2015-12-09 | 合肥学院 | Method of preparing flame-resisting and antibacterial non-woven paper with impregnation method |
| CN105178012A (en) * | 2015-07-28 | 2015-12-23 | 苏州科淼新材料有限公司 | Preparation method for anti-microbial cotton material |
-
2016
- 2016-05-05 CN CN201610291808.9A patent/CN105926270A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103866651A (en) * | 2014-03-31 | 2014-06-18 | 宋旭 | Wallpaper with air purifying function and preparation method |
| CN105178012A (en) * | 2015-07-28 | 2015-12-23 | 苏州科淼新材料有限公司 | Preparation method for anti-microbial cotton material |
| CN105133308A (en) * | 2015-09-14 | 2015-12-09 | 合肥学院 | Method of preparing flame-resisting and antibacterial non-woven paper with impregnation method |
Non-Patent Citations (1)
| Title |
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| 吴红福等: "新型抗菌防臭纤维的主要品种及其应用", 《中国纤检》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107119453A (en) * | 2017-06-28 | 2017-09-01 | 顾秋军 | A kind of fabric antimicrobial finishing agent and preparation method thereof |
| CN107313256A (en) * | 2017-06-28 | 2017-11-03 | 顾秋军 | A kind of fabric antimicrobial finishing agent and preparation method thereof |
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Application publication date: 20160907 |