CN104586644A - Toothpaste capable of removing extrinsic dental stains - Google Patents

Toothpaste capable of removing extrinsic dental stains Download PDF

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Publication number
CN104586644A
CN104586644A CN201510037867.9A CN201510037867A CN104586644A CN 104586644 A CN104586644 A CN 104586644A CN 201510037867 A CN201510037867 A CN 201510037867A CN 104586644 A CN104586644 A CN 104586644A
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sodium
toothpaste
mottle
powder
essence
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CN201510037867.9A
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CN104586644B (en
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唐献兰
蒙衍强
文胜
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Guangzhou Qiancai Cosmetic Co ltd
Xi'an Silk Road Zhixing Technology Service Co ltd
Guangxi Science and Technology Normal University
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Guangxi Science and Technology Normal University
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Abstract

The invention discloses toothpaste capable of removing extrinsic dental stains and relates to the technical field of toothpaste. The toothpaste is prepared from the following raw materials in percentage by weight: 20%-30% of sorbitol, 0.0-6.0% of glycerinum, 0.0-4.0% of propylene glycol, 35%-40.00% of high-whiteness mountain flour, 8%-12.00% of epidesmine powder, 1%-5% of moso bamboo powdered carbon, 2.00% of thickener silicon dioxide, 0.6% of sodium carboxymethylcellulose, 0.6% of hydroxyethyl cellulose, 2.20% of sodium lauryl sulfate, 0.20% of saccharin sodium, 0.5%-0.76% of sodium monofluorophosphate, 0.35% of trisodium phosphate, 0.30% of sodium dihydrogen phosphate, 0.8%-1.0% of an essence and purified water. The toothpaste has a good effect of removing extrinsic dental stains of teeth, is capable of thoroughly removing dental plaques, food remains and surface dirt, is safe, mild, and suitable for long-term use; and the defects such as aching and limp teeth and oral mucosa injuries easily caused by other chemical stain removing methods are overcome.

Description

To dispel exogenous mottle toothpaste
Technical field
The present invention relates to a kind of toothpaste, especially one is dispelled exogenous mottle toothpaste.
Background technology
Dental exogenous mottle refers to the mottle that dental surface adheres to or calculus.The formation of mottle is from tooth rete.Tooth rete is the rete of one deck no cell structure, and it is formed because enamel absorbs glycoprotein from saliva.If do not use friction-type toothpaste to remove rete, it can thicken 11 microns in every 7 days, and final thickness can reach 100 microns.As still do not obtained removing in time, effectively after 30 days, interference-free rete can become mottle.The rete of new deposition by calcification, painted, the degeneration of glycoprotein and crosslinkedly change into ripe rete.The reason of rete quality is a lot, smoking, and the long-term edible food being rich in tannic acid as tea, red wine etc., and uses some cationic formulation such as hibitane or multivalent metal salt such as stannum, ferrum etc. all can impel the formation of exogenous mottle.Smoking has surprising effect for rete is painted: in smoking population, and medium or seriously painted ratio is three times of non-smoking crowd.These mottles can be attached to tooth enamel surface securely, then develop into dental calculus or the dental plaque of more difficult removal gradually.
Generally accept such fact now: brush teeth correctly, frequently and contribute to dental health.Its effect helps to remove bacterial plaque and residual food.Comparatively speaking, comparatively bacterial plaque is more difficult removes from dental surface for colored film.Use the toothpaste of toothbrush and water or low friction valve both cannot remove this kind of mottle, their growth in teeth surfaces can not be prevented.Whitening toothpaste is generally realize the effect of functions of whitening teeth by three approach: one is use the abrasive that friction value is high, granule is large, as dentifrice etc. in the past; Two is use strong acid or highly basic to carry out bleaching teeth, as phytic acid.Phytic acid can with the ganoid main component hydroxyapatite of dental surface (Ca 10(PO 4) 6(OH) 2) generate stable complex, the enamel surface of tooth formed one deck smooth, the osmotic protection film with ion selectivity, thus the formation again of cigarette stain, tea stain and other color dirt can be prevented, to reach effect that tooth protection cleans the teeth; Three is use peroxide release active oxygen bleaching tooth.In addition, also have in toothpaste and add fluoride, pyrophosphate, sodium tripolyphosphate etc. and become to assign to carry out stain whitening.
But traditional abrasivus does not have effect substantially to deep layer tinter, and the enamel of dental surface can be destroyed by the toothpaste of particle friction, make dental surface become coarse, in addition, the stability of second-rate abrasivus and poor with the compatibility of other raw materials, thus affect the total quality of toothpaste.
Summary of the invention
The problem that the present invention solves is to provide a kind ofly to be had good removal dental exogenous mottle effect and thoroughly can remove the exogenous mottle toothpaste of dispelling of dental plaque, food remains and surface smut and tooth-whitening.
In order to solve the problems of the technologies described above, the technical solution adopted in the present invention is: its material composition is made up of the raw material of following percentage by weight:
Sorbitol 20%-30%; Glycerol 0.0%-6.0%; Propylene glycol 0.0%-4.0%; High whiteness stone powder 35%-40.00%; Epidesmine powder 8%-12 .00%; Phyllostachys pubescens Mazei ex H.de Lebaie powdered carbon 1-5%; Thickening type silicon dioxide 2.00%; Sodium carboxymethyl cellulose 0.6%; Hydroxyethyl-cellulose 0.6%; Sodium lauryl sulfate 2.20%; Saccharin sodium 0.20%; Sodium monofluorophosphate 0.5%-0.76%; Tertiary sodium phosphate 0.35%; Sodium dihydrogen phosphate 0.30%; Essence 0.8%-1.0%; Pure water surplus.
In technique scheme, scheme can also be more specifically: its material composition is made up of the raw material of following percentage by weight:
Sorbitol 20%; Propylene glycol 4.0%; High whiteness stone powder 40%; Epidesmine powder 8%; Phyllostachys pubescens Mazei ex H.de Lebaie powdered carbon 5%; Thickening type silicon dioxide 2.00%; Sodium carboxymethyl cellulose 0.6%; Hydroxyethyl-cellulose 0.6%; Sodium lauryl sulfate 2.20%; Saccharin sodium 0.20%; Sodium monofluorophosphate 0.5%; Tertiary sodium phosphate 0.35%; Sodium dihydrogen phosphate 0.30%; Essence 0.8%; Pure water surplus.
Further: its material composition is made up of the raw material of following percentage by weight:
Sorbitol 30%; Glycerol 6.0%; High whiteness stone powder 35%; Epidesmine powder 12 .00%; Phyllostachys pubescens Mazei ex H.de Lebaie powdered carbon 1%; Thickening type silicon dioxide 2.00%; Sodium carboxymethyl cellulose 0.6%; Hydroxyethyl-cellulose 0.6%; Sodium lauryl sulfate 2.20%; Saccharin sodium 0.20%; Sodium monofluorophosphate 0.76%; Tertiary sodium phosphate 0.35%; Sodium dihydrogen phosphate 0.30%; Essence 1.0%; Pure water surplus.
Further: its material composition is made up of the raw material of following percentage by weight:
Sorbitol 25%; Glycerol 0.3%; Propylene glycol 2.0%; High whiteness stone powder 38%; Epidesmine powder 10%; Phyllostachys pubescens Mazei ex H.de Lebaie powdered carbon 3.0%; Thickening type silicon dioxide 2.00%; Sodium carboxymethyl cellulose 0.6%; Hydroxyethyl-cellulose 0.6%; Sodium lauryl sulfate 2.20%; Saccharin sodium 0.20%; Sodium monofluorophosphate 0.65%; Tertiary sodium phosphate 0.35%; Sodium dihydrogen phosphate 0.30%; Essence 0.9%; Pure water surplus.
Further: described high whiteness stone powder crosses 425 mesh sieves.
The said epidesmine of the present invention (Stellerite) its structure is moisture rack-like aluminosilicate, its chemical composition (%): SiO 258.76, Al 2o 314.13, CaO8.80, K 2o 0.11, Na 2o 0.18, Fe 2o 30.44, H 2o +16.87, H 2o -1.25, chemistry formula is: (K 0. 017na 0. 042ca 1. 13) 1. 189[Al 1. 997si 7. 05o 18] 6. 75H 2o).Natural parastilbite is the aluminium silicate mineral of a kind of moisture alkali metal or alkaline-earth metal, the tectosilicate be made up of silicon-oxy tetrahedron and aluminum-oxygen tetrahedron, there are cavity and the passage of many openings in mineral inside, there is very large specific surface area, hole and duct account for 45% of cumulative volume, making it have stronger ion-exchange capacity and absorbability, is good adsorbing material and antibacterial.Natural parastilbite Mohs' hardness 3-4.
The said Phyllostachys pubescens Mazei ex H.de Lebaie charcoal of the present invention, Mao bamboo timber high temperature, anoxia or restrictive pass into the condition of oxygen under, make bamboo wood decomposes and the solid matter that obtains, bamboo charcoal inside forms all kinds of hole, have micropore, mesopore and macropore, thus bamboo charcoal specific surface area is up to 300m 2/ g, makes it have good absorbability, can kill multiple harmful levels of pathogens in oral cavity.
The present invention, compared with existing whitening toothpaste, has following beneficial effect:
1, owing to adding red meeting zeolite powder and Phyllostachys pubescens Mazei ex H.de Lebaie carbon dust in toothpaste matrix, toothpaste has good removal dental exogenous mottle effect, thoroughly can remove dental plaque, food remains and surface smut and tooth-whitening;
2, the lotion of toothpaste produced is fine and smooth, and the fragrance thoroughly property sent out is high, and quality meets toothpaste GB GB8372-2008 completely;
3, the component that the present invention uses makes tooth whitening overcome other chemical speckle dispelling and easily causes the drawbacks such as tooth is aching and limp, oral mucosa damage, and safety is gentle, is applicable to life-time service; Mastic cost is low;
4, epidesmine abrasivus and Phyllostachys pubescens Mazei ex H.de Lebaie charcoal belong to local natural material, and itself has no side effect, and raw material is easy to get.
Detailed description of the invention
Below in conjunction with embodiment, the present invention will be further described.In following each embodiment, involved percentage ratio except as otherwise noted, is all calculate by weight percentage.
One, to dispel the preparation of exogenous mottle toothpaste:
By high-purity natural stellerite ore, through ball mill pulverizing, flour crosses 325 mesh sieves, for subsequent use;
High whiteness stone powder is crossed 425 mesh sieves, for subsequent use;
By broken for Phyllostachys pubescens Mazei ex H.de Lebaie powdered carbon, cross 200 ~ 325 mesh sieves, for subsequent use;
Powder, liquid material (except essence) are accurately claimed respectively in two containers by formula, premix is even;
Above-mentioned powder and liquid material are added in Manufacturing medicine extract machine, after mixing, opens blender, vacuum pump, homogenizing 20 min; By formula precise essence, and add Manufacturing medicine extract machine, homogenizing 15 min, complete cream initial vacuum processed degree and maintain more than 0.092MPa;
Mastic is used multiple tube fill.
two, dispel exogenous mottle toothpaste constitutive material and weight percent content in embodiment 1 to 3 are as following table 1:
three, clinical trial part:
1. method
1. 1 test period: 60 natural life-spans
1.2 subjects inclusive criteria and exclusion standards
Inclusive criteria: have creamy white speckle problem; Healthy, and agree to coordinate inspection on time; The oral hygiene measures provided in duration of test maintenance every day use is provided, does not use other toothpaste; To oral cavity health care products without allergies.
Exclusion standard: the trouble tooth of endogenous mottle; Current long-term taking chemicals; Antibiotic, immune formulation, collutory etc. need be used at duration of test; Wear artificial tooth or orthodontic appliance; Scaling need be carried out at duration of test, scrape the treatment of influence index observations such as controlling, dental body filled.
1.3 test specimen
Self-control is unguentum, and outward appearance mark is consistent, and be marked with A, B printed words respectively, wherein A sample is formula toothpaste of the present invention, and B sample is reference substance, and not containing epidesmine powder and Phyllostachys pubescens Mazei ex H.de Lebaie powdered carbon raw material in formula, shared by it, formula ratio part is supplied with Paris white.Toothbrush is soft bristle tooth brush.
1.4 test method
1.4.1 EXPERIMENTAL DESIGN
Adopt double blinding, Method of Random Test.
1.4.2 test index
Carrying out examination of mouth by well-trained Dentist, is index tooth with each study subject 33,32,31,41,42,43, presses the scoring of Lobene mottle index classification scoring method respectively to the area of its stain on the tooth surface and color.Before test, correction experiment is carried out to examiner.
Area standards of grading are as follows:
0-exists without mottle;
1-mottle is no more than the l/3 of facing;
2-mottle is no more than 2/3 of facing;
3-mottle is greater than 2/3 of facing.
Color area standards of grading are as follows:
0-exists without mottle;
1-is slight mottle (yellow or yellowish-brown);
2-moderate mottle (moderate is brown);
3-severe mottle (dark-brown or black) mottle is greater than 2/3 of facing.
1.4.3 experiment process
Record each study subject teeth stains index, use toothpaste check after 4 weeks.
Test grouping: screening meets inclusive criteria and exclusion standard person, and be divided into A, B two groups by random table, two groups substantially identical in health, the index creamy white speckle order of severity, age, sex ratio.
1.5 statistical analysis
In this result of the test, before and after using toothpaste in group, 4 weekly datas compare, and two groups of result covariance method analyses, significance level is 0.05。
2. result of the test
Have 50 people and complete experimental study, male 34 people, female 16 people, 20 ~ 58 years old age.
2.1 interpretation of result
2.1.1 two groups of experimenters test front and back index tooth Lobene mottle Index area classification score result of variations
See the following form 2:
table 2 index tooth Lobene mottle Index area classification score change comparison sheet
As seen from Table 2, after each experimenter uses the toothpaste surrounding of adding epidesmine Phyllostachys pubescens Mazei ex H.de Lebaie carbon, the area of experimenter's index creamy white speckle can reduce by 50.4%; With with compared with organizing when baseline checks, exogenous mottle area have dropped 59.4%.
2.1.2 two groups of experimenters test front and back index tooth Lobene mottle index color grading score result of variations
In table 3.
Front and back index tooth Lobene mottle index color grading score result of variations table tested by table 3:
As seen from Table 3, after treating 4 weeks, both index tooth Lobene mottle index colors compare decline 49.0% (P< 0.05).Compared with when checking with baseline, add epidesmine powder and bamboo carbon powder toothpaste reduction toothpaste exogenous mottle index color 59.1%.
Clinical trial shows, the toothpaste containing enough natural parastilbites and Phyllostachys pubescens Mazei ex H.de Lebaie powdered carbon can effectively remove dental surface mottle, has effect of tooth whitening.

Claims (5)

1. to dispel an exogenous mottle toothpaste, it is characterized in that: its material composition is made up of the raw material of following percentage by weight:
Sorbitol 20%-30%; Glycerol 0.0%-6.0%; Propylene glycol 0.0%-4.0%; High whiteness stone powder 35%-40.00%; Epidesmine powder 8%-12 .00%; Phyllostachys pubescens Mazei ex H.de Lebaie powdered carbon 1-5%; Thickening type silicon dioxide 2.00%; Sodium carboxymethyl cellulose 0.6%; Hydroxyethyl-cellulose 0.6%; Sodium lauryl sulfate 2.20%; Saccharin sodium 0.20%; Sodium monofluorophosphate 0.5%-0.76%; Tertiary sodium phosphate 0.35%; Sodium dihydrogen phosphate 0.30%; Essence 0.8%-1.0%; Pure water surplus.
2. exogenous mottle toothpaste of dispelling according to claim 1, is characterized in that its material composition is made up of the raw material of following percentage by weight:
Sorbitol 20%; Propylene glycol 4.0%; High whiteness stone powder 40%; Epidesmine powder 8%; Phyllostachys pubescens Mazei ex H.de Lebaie powdered carbon 5%; Thickening type silicon dioxide 2.00%; Sodium carboxymethyl cellulose 0.6%; Hydroxyethyl-cellulose 0.6%; Sodium lauryl sulfate 2.20%; Saccharin sodium 0.20%; Sodium monofluorophosphate 0.5%; Tertiary sodium phosphate 0.35%; Sodium dihydrogen phosphate 0.30%; Essence 0.8%; Pure water surplus.
3. exogenous mottle toothpaste of dispelling according to claim 1, is characterized in that its material composition is made up of the raw material of following percentage by weight:
Sorbitol 30%; Glycerol 6.0%; High whiteness stone powder 35%; Epidesmine powder 12 .00%; Phyllostachys pubescens Mazei ex H.de Lebaie powdered carbon 1%; Thickening type silicon dioxide 2.00%; Sodium carboxymethyl cellulose 0.6%; Hydroxyethyl-cellulose 0.6%; Sodium lauryl sulfate 2.20%; Saccharin sodium 0.20%; Sodium monofluorophosphate 0.76%; Tertiary sodium phosphate 0.35%; Sodium dihydrogen phosphate 0.30%; Essence 1.0%; Pure water surplus.
4. exogenous mottle toothpaste of dispelling according to claim 1, is characterized in that its material composition is made up of the raw material of following percentage by weight:
Sorbitol 25%; Glycerol 0.3%; Propylene glycol 2.0%; High whiteness stone powder 38%; Epidesmine powder 10%; Phyllostachys pubescens Mazei ex H.de Lebaie powdered carbon 3.0%; Thickening type silicon dioxide 2.00%; Sodium carboxymethyl cellulose 0.6%; Hydroxyethyl-cellulose 0.6%; Sodium lauryl sulfate 2.20%; Saccharin sodium 0.20%; Sodium monofluorophosphate 0.65%; Tertiary sodium phosphate 0.35%; Sodium dihydrogen phosphate 0.30%; Essence 0.9%; Pure water surplus.
5. the exogenous mottle toothpaste of dispelling according to claim 1 or 2 or 3 or 4, is characterized in that: described high whiteness stone powder crosses 425 mesh sieves.
CN201510037867.9A 2015-01-26 2015-01-26 Dispel exogenous color spot toothpaste Active CN104586644B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115040465A (en) * 2022-07-06 2022-09-13 浙江爱尚日用品有限公司 Whitening toothpaste capable of effectively removing dental plaque and tartar
CN115645291A (en) * 2022-09-29 2023-01-31 广东省九科生物科技有限公司 Zeolite toothpaste

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115040465A (en) * 2022-07-06 2022-09-13 浙江爱尚日用品有限公司 Whitening toothpaste capable of effectively removing dental plaque and tartar
CN115040465B (en) * 2022-07-06 2023-01-24 浙江爱尚日用品有限公司 Whitening toothpaste capable of effectively removing dental plaque and tartar
US11771644B1 (en) 2022-07-06 2023-10-03 Zhejiang Airsun Commodity Co., Ltd. Whitening toothpaste capable of effectively removing dental plaque and tartar
CN115645291A (en) * 2022-09-29 2023-01-31 广东省九科生物科技有限公司 Zeolite toothpaste
CN115645291B (en) * 2022-09-29 2024-03-19 广东省九科生物科技有限公司 Zeolite toothpaste

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