CN104522877A - Method for manufacturing low temperature cigarette raw materials - Google Patents
Method for manufacturing low temperature cigarette raw materials Download PDFInfo
- Publication number
- CN104522877A CN104522877A CN201410731816.1A CN201410731816A CN104522877A CN 104522877 A CN104522877 A CN 104522877A CN 201410731816 A CN201410731816 A CN 201410731816A CN 104522877 A CN104522877 A CN 104522877A
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- China
- Prior art keywords
- low temperature
- ethyl acetate
- raw materials
- cigarette raw
- cigarette
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a method for manufacturing low temperature cigarette raw materials. The method for manufacturing the low temperature cigarette raw materials includes following steps: 1, heating a stirring container with balls, keeping temperature constant, adding cut tobacco of cigarettes, using the stirring container to stir the balls and the cut tobacco of the cigarettes, heating the cut tobacco of the cigarettes at the constant temperature so as to achieve destructive distillation, guiding generated smoke into a suction filtration container which contains ethyl acetate, and when the smoke is not generated, continuing to heat the cut tobacco of the cigarettes for 8-12min; 2, adding distilled water into the suction filtration container used in the step 1 so as to obtain mixture liquid, pouring the mixture liquid into a separating funnel after shaking the mixture liquid well, separating the mixture liquid after standing so as to obtain ethyl acetate percolate, filtering the percolate, and removing impurities; 3, performing rotary evaporation on the ethyl acetate percolate after being filtered in the step 2 so as to obtain brown oily extractives which are used as the low temperature cigarette raw materials. The method for manufacturing the low temperature cigarette raw materials is simple in technology, uses the constant temperature destructive distillation and ethyl acetate filtration rotary evaporation to fully extract the low temperature cigarette raw materials which can be used in electronic cigarettes and low temperature cigarettes, can not generate tar or harmful smoke, and greatly reduces poison of smoking to a human body.
Description
Technical field
The present invention relates to a kind of preparation method of raw material of cigarette, particularly relate to a kind of method making low temperature cigarette raw material.
Background technology
Under the condition of result of combustion of tobacco, significantly reduce coke tar in cigarette and harmful components burst size further, difficulty is very large, and this mode is difficult to obtain the accreditation of health circle.Therefore, change the traditional consumption mode that tobacco burns and sucks, researching and developing cigarette of new generation, is the important channel fundamentally breaking through tobacco bottleneck.Low temperature cigarette is the novel tobacco product that a class is different from traditional cigarette, and it mainly relies on thermal source to carry out destructive distillation to tobacco sheet base at a lower temperature, thus realizes transmitting flue gas to respiratory system under not burning condition.Low temperature cigarette outward appearance and traditional cigarette similar, only heating but not burning tobacco below 300 degrees Celsius, but satisfaction and Partial Tobacco fragrance can be passed to consumer, can not produce tar and side-stream smoke substantially.
Therefore, market in urgent need is for the preparation method of low temperature cigarette raw material.
Summary of the invention
The object of the invention is to solve deficiency of the prior art, a kind of method making low temperature cigarette raw material is provided.
To achieve these goals, the technical solution of employing is in the present invention: a kind of method making low temperature cigarette raw material, and step is as follows:
One, the stirred vessel containing ball is warming up to 290 ~ 310 DEG C, and keep temperature constant, add cigarette shreds, by stirred vessel, ball and cigarette shreds are stirred, heated at constant temperature makes cigarette shreds destructive distillation, being introduced by the smog of generation is equipped with in the suction filtration container of ethyl acetate, when not having smog to produce, stops heating after still continuing heating 8 ~ 12min;
Two, add distilled water in the suction filtration container in step one, pour separatory funnel into after shaking up, separatory after leaving standstill, obtains ethyl acetate filter liquor, filter liquor is filtered, and removes impurity;
Three, by step 2 filter after ethyl acetate filter liquor at-0.09MPa, 27 ~ 30 DEG C, revolve steaming, obtain brown oil extract and be low temperature cigarette raw material.
Further, the cigarette shreds in described step one refers to and cured tobacco leaf is removed muscle, is cut into pipe tobacco with filament cutter, pipe tobacco width 0.8 ~ 1mm.
Further, in described step one temperature constant at 300 DEG C.
The invention has the beneficial effects as follows: this method technique is simple, utilize constant temperature destructive distillation and ethyl acetate to filter and revolve steaming, extract fully, the raw material of cigarette of extraction can be used for electronic cigarette and low temperature cigarette, do not produce tar and harmful smoke, greatly reduce the murder by poisoning that smoking causes human body.
Detailed description of the invention
embodiment 1
Make a method for low temperature cigarette raw material, step is as follows:
One, the stirred vessel containing ball is warming up to 290 ~ 310 DEG C, and keep temperature constant, add cigarette shreds, by stirred vessel, ball and cigarette shreds are stirred, heated at constant temperature makes cigarette shreds destructive distillation, being introduced by the smog of generation is equipped with in the suction filtration container of ethyl acetate, when not having smog to produce, stops heating after still continuing heating 8 ~ 12min;
Two, add distilled water in the suction filtration container in step one, pour separatory funnel into after shaking up, separatory after leaving standstill, obtains ethyl acetate filter liquor, filter liquor is filtered, and removes impurity;
Three, by step 2 filter after ethyl acetate filter liquor at-0.09MPa, 27 ~ 30 DEG C, revolve steaming, obtain brown oil extract and be low temperature cigarette raw material.
Cigarette shreds in described step one refers to and cured tobacco leaf is removed muscle, is cut into pipe tobacco with filament cutter, pipe tobacco width 0.8 ~ 1mm.
embodiment 2
Make a method for low temperature cigarette raw material, step is as follows:
The there-necked flask of bead is housed with electric jacket heating, and stir bead with electric mixer, by heating temperatures to 300 DEG C in bottle, control temperature is at 300 DEG C simultaneously; From bottleneck add 50 grams of pipe tobaccos (amount of pipe tobacco with agitator can stir bead and pipe tobacco can rotate be advisable), continue heating, stir pipe tobacco and bead continues destructive distillation, open vavuum pump, smog enters the bottle,suction that ethyl acetate is housed simultaneously.
When not having smog to produce in flask, then heat 10 minutes.Stop heating, close vavuum pump.Much filtrate after pipe tobacco destructive distillation is mainly in first and second bottle,suction.
Add 100ml distilled water respectively by two bottle,suctions, shake up (object is dissolved in distilled water water-soluble chemical substance), then pour mixture into separatory funnel, separatory after leaving standstill, obtains ethyl acetate filter liquor, uses Filter paper filtering impurity.
Ethyl acetate filter liquor Rotary Evaporators is revolved steaming (-0.09MPa, 27-30 DEG C), obtains brown oil extract, be low temperature cigarette raw material.
This method technique is simple, and utilize constant temperature destructive distillation and ethyl acetate to filter and revolve steaming, extract fully, the raw material of cigarette of extraction can be used for electronic cigarette and low temperature cigarette, does not produce tar and harmful smoke, greatly reduces the murder by poisoning that smoking causes human body.
Above-mentioned explanation is not limitation of the present invention, and the present invention is also not limited in above-mentioned citing, and the change that those skilled in the art make in essential scope of the present invention, remodeling, interpolation or replacement also should belong to protection scope of the present invention.
Claims (3)
1. make a method for low temperature cigarette raw material, it is characterized in that, step is as follows:
One, the stirred vessel containing ball is warming up to 290 ~ 310 DEG C, and keep temperature constant, add cigarette shreds, by stirred vessel, ball and cigarette shreds are stirred, heated at constant temperature makes cigarette shreds destructive distillation, being introduced by the smog of generation is equipped with in the suction filtration container of ethyl acetate, when not having smog to produce, stops heating after still continuing heating 8 ~ 12min;
Two, add distilled water in the suction filtration container in step one, pour separatory funnel into after shaking up, separatory after leaving standstill, obtains ethyl acetate filter liquor, filter liquor is filtered, and removes impurity;
Three, by step 2 filter after ethyl acetate filter liquor at-0.09MPa, 27 ~ 30 DEG C, revolve steaming, obtain brown oil extract and be low temperature cigarette raw material.
2. the method for making low temperature cigarette raw material according to claim 1, is characterized in that: the cigarette shreds in described step one refers to and cured tobacco leaf is removed muscle, is cut into pipe tobacco with filament cutter, pipe tobacco width 0.8 ~ 1mm.
3. the method for making low temperature cigarette raw material according to claim 1, is characterized in that: in described step one, temperature constant is at 300 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410731816.1A CN104522877B (en) | 2014-12-06 | 2014-12-06 | A kind of method making low temperature cigarette raw material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410731816.1A CN104522877B (en) | 2014-12-06 | 2014-12-06 | A kind of method making low temperature cigarette raw material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104522877A true CN104522877A (en) | 2015-04-22 |
| CN104522877B CN104522877B (en) | 2016-06-08 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410731816.1A Expired - Fee Related CN104522877B (en) | 2014-12-06 | 2014-12-06 | A kind of method making low temperature cigarette raw material |
Country Status (1)
| Country | Link |
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| CN (1) | CN104522877B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105661622A (en) * | 2016-02-16 | 2016-06-15 | 中国农业科学院烟草研究所 | Nicotine liquid raw material of electronic cigarette and preparation device and method of nicotine liquid raw material |
| CN109480327A (en) * | 2017-09-11 | 2019-03-19 | 湖南中烟工业有限责任公司 | A kind of preparation method and applications of tobacco purification high-temperature retorting object |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB302863A (en) * | 1928-03-19 | 1928-12-27 | Basile Seferiadis | Process and device for extracting essential principles or gums from tobaccos of all kinds |
| CN1140035A (en) * | 1995-07-08 | 1997-01-15 | 李吉荣 | Method for preparing liquid cigarette |
| CN2726325Y (en) * | 2004-05-17 | 2005-09-21 | 上海烟草（集团）公司 | Apparatus for extracting fragrance components from tobacco |
| CN1720827A (en) * | 2004-07-12 | 2006-01-18 | 苏少宁 | Non-inflammable smoking articles and extraction method thereof |
| CN102766534A (en) * | 2012-07-16 | 2012-11-07 | 上海烟草集团有限责任公司 | Method for separating alkaline scent ingredients from main stream smoke of cigarettes and application |
| CN103289822A (en) * | 2013-05-23 | 2013-09-11 | 湖北中烟工业有限责任公司 | Spice continuous-extraction instrument for solid tobacco |
| CN203841098U (en) * | 2014-05-06 | 2014-09-24 | 上海烟草集团有限责任公司 | Device for removing volatile organic small molecule compounds from tobacco harm reduction material |
-
2014
- 2014-12-06 CN CN201410731816.1A patent/CN104522877B/en not_active Expired - Fee Related
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB302863A (en) * | 1928-03-19 | 1928-12-27 | Basile Seferiadis | Process and device for extracting essential principles or gums from tobaccos of all kinds |
| CN1140035A (en) * | 1995-07-08 | 1997-01-15 | 李吉荣 | Method for preparing liquid cigarette |
| CN2726325Y (en) * | 2004-05-17 | 2005-09-21 | 上海烟草（集团）公司 | Apparatus for extracting fragrance components from tobacco |
| CN1720827A (en) * | 2004-07-12 | 2006-01-18 | 苏少宁 | Non-inflammable smoking articles and extraction method thereof |
| CN102766534A (en) * | 2012-07-16 | 2012-11-07 | 上海烟草集团有限责任公司 | Method for separating alkaline scent ingredients from main stream smoke of cigarettes and application |
| CN103289822A (en) * | 2013-05-23 | 2013-09-11 | 湖北中烟工业有限责任公司 | Spice continuous-extraction instrument for solid tobacco |
| CN203841098U (en) * | 2014-05-06 | 2014-09-24 | 上海烟草集团有限责任公司 | Device for removing volatile organic small molecule compounds from tobacco harm reduction material |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105661622A (en) * | 2016-02-16 | 2016-06-15 | 中国农业科学院烟草研究所 | Nicotine liquid raw material of electronic cigarette and preparation device and method of nicotine liquid raw material |
| CN105661622B (en) * | 2016-02-16 | 2018-03-23 | 中国农业科学院烟草研究所 | A kind of tobacco juice for electronic smoke raw material and its preparation facilities and method |
| CN109480327A (en) * | 2017-09-11 | 2019-03-19 | 湖南中烟工业有限责任公司 | A kind of preparation method and applications of tobacco purification high-temperature retorting object |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104522877B (en) | 2016-06-08 |
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