CN104026734B - A kind of preparation method of tobacco flavor electronics tobacco tar - Google Patents

A kind of preparation method of tobacco flavor electronics tobacco tar Download PDF

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Publication number
CN104026734B
CN104026734B CN201410263756.5A CN201410263756A CN104026734B CN 104026734 B CN104026734 B CN 104026734B CN 201410263756 A CN201410263756 A CN 201410263756A CN 104026734 B CN104026734 B CN 104026734B
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tobacco
tobacco leaf
extract
solvent
electronics
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CN104026734A (en
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张雨夏
王萍娟
李志华
田兆福
吴彦
田玉红
冯守爱
刘绍华
黄天辉
黄东业
刘启斌
周俊
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China Tobacco Guangxi Industrial Co Ltd
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China Tobacco Guangxi Industrial Co Ltd
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Abstract

The invention discloses a kind of preparation method of tobacco flavor electronics tobacco tar.First get tobacco leaf to be shredded, be that solvothermal extracts with water or 95% ethanol, obtain tobacco extract through heat filtering and refrigeration sedimentation filtration, concentrate to obtain tobacco leaf extract; Then prepared opium paste is taken: amino acid weight ratio is the prepared opium paste mixture 5g of 10 ~ 2:1, takes mixed solvent 100g, puts in solvent by prepared opium paste mixture, and 80 ~ 100 DEG C of heat times are 3 ~ 12 hours, obtain the maillard reaction product of leaf tobacco extract; By volume percentage measures the Maillard reaction thing of peony transparency liquid: peppermint oil: glycerin monostearate is 1 ~ 25%:0 ~ 40%:0 ~ 1%, and 100% volume supplied by propane diols or polyethylene glycol, stirs and evenly mixs and obtain electronic cigarette oil product.The present invention makes these fragrance components enter electronics tobacco tar, gives electronic cigarette oil smoke grass characteristic perfume, better masks the excitant that Alevaire brings, more can experience the suction of true cigarette close to consumer.

Description

A kind of preparation method of tobacco flavor electronics tobacco tar
Technical field
The present invention relates to a kind of preparation method of electronics tobacco tar, is a kind of electronics tobacco tar with special tobacco flavor.
Background technology
Cigarette burning cracking produces allow thousands of compounds, and most of harmful, and especially tar contains carcinogen, grievous injury smoker and involuntary smoker's health.Along with the development of global Tobacco Control campaign, the cigarette substitute of various relative healths continues to bring out, wherein popular with electronic cigarette (electroniccigarette).Electronic cigarette core is electronics tobacco tar (electroniccigaretteliquid), and tobacco tar produces fog and is similar to true cigarette flue gas under the effect of atomizer, is not but known by people containing the harmful substance such as tar, carbon monoxide.At present, although commercially available electronic cigarette with the addition of leaf tobacco extract, but after consumer's comparation and assessment, larger with the perceptual difference distance of cigarette in fragrance, excitant, mouthfeel etc., especially with the product that various essence and flavoring agent is deployed into, allow people be difficult to accept or be accustomed to its fragrance and taste, even exhaust sensation that is dizzy and that feel sick.Leaf tobacco extract contains the monose such as a large amount of glucose, fructose, can as the provider of carbohydrate in Maillard reaction thing, Maillard reaction can produce various useful flavor matter, in flavouring, comparatively leaf tobacco extract has more superiority, invest tobacco characteristic perfume specific to leaf tobacco extract on the one hand, Maillard reaction thing allows as cigarette additive on the other hand, and security is higher.In future, this perfume (or spice) of tobacco specialized especially is worth further investigation exploitation to electronic cigarette blending.
Summary of the invention
The object of this invention is to provide a kind of maillard reaction product of leaf tobacco extract, be applied in electronics tobacco tar compatibility, make the fragrance closer to cigarette, promote suction mouthfeel, reduce smog and consumer is attracted to the excitant of smoker throat.
Object of the present invention is achieved through the following technical solutions.
A preparation method for tobacco flavor electronics tobacco tar, step is as follows: (1) is first got tobacco leaf and shredded, and is that solvothermal extracts, obtains tobacco extract, concentrate to obtain tobacco leaf extract through heat filtering and refrigeration sedimentation filtration with water or 95% ethanol; (2) weight ratio prepared opium paste is then taken: amino acid is the prepared opium paste mixture 5g of 10 ~ 2:1, solvent takes 100g, prepared opium paste and amino acid are put in solvent, it is 3 ~ 12 hours 80 ~ 120 DEG C of heat times again, obtain the maillard reaction product of tobacco leaf, (3) by the Maillard reaction thing of peony transparency liquid: peppermint oil: glycerin monostearate percent by volume is 1 ~ 25%:0 ~ 40%:0 ~ 1%, supply 100% volume with propane diols or polyethylene glycol again, be uniformly mixed and obtain tobacco flavor electronic cigarette oil product.
Particularly, a kind of preparation method of tobacco flavor electronics tobacco tar, step is as follows:
(1) first get tobacco leaf to be shredded, be solvent 60 ~ 100 DEG C heating extraction 1 ~ 5h with 6 ~ 20 times of water or 95% ethanol, obtain tobacco extract through heat filtering and refrigeration sedimentation filtration, concentrated yield is the tobacco leaf extract of 22.6 ~ 24.%;
(2) then take by weight prepared opium paste: amino acid is the prepared opium paste mixture 5g of 10 ~ 2:1, solvent takes 100g, put in solvent by prepared opium paste and amino acid, 80 ~ 100 DEG C of heat times are 3 ~ 12 hours, obtain the maillard reaction product of leaf tobacco extract;
(3) by the Maillard reaction thing of peony transparency liquid: peppermint oil: glycerin monostearate percent by volume is that 1 ~ 25%:0 ~ 40%:0 ~ 1% mixes, supply 100% volume with propane diols or polyethylene glycol again, be uniformly mixed and obtain electronic cigarette oil product.
Tobacco leaf of the present invention refers to that described tobacco leaf refers to Different sources, different brackets, and the mixing tobacco leaf of one or more in the waste/hypo-tobacco leaf produced in the flue-cured tobacco of different year, suncured tabacco, air-curing of tobacco leaves production process, shredded by large tobacco leaf, size is as subsequent use in sunflower seed.
Described amino acid is one or more in glycine, glutamic acid, proline, alanine, aspartic acid, and addition is 0.1 ~ 0.5 times of prepared opium paste weight.
Described solvent is any two kinds of not miscible two-phase solvent mixed liquors in water, propane diols, polyethylene glycol, glycerine, triacetyl glycerine, preferred two-phase solvent triacetyl glycerine: glycerine is the mixed liquor of 10 ~ 0.5:1, addition is prepared opium paste and amino acid whose 20 times, after reaction terminates, get the Maillard reaction thing being dissolved in glycerin layer and be applied to electronics tobacco tar.
Described peppermint oil be asia peppermint oil, mentha piperita oil one or both.
Described glycerine, propane diols or polyethylene glycol and glycerin monostearate, be edible rank.
The invention has the beneficial effects as follows:
The present invention replaces conventional single phase solvent system directly to leach with any two kinds of immiscible two-phase solvents in water, propane diols, polyethylene glycol, glycerine, triacetyl glycerine, not only as reactant liquor simultaneously but also utilize the difference of the distribution coefficient in two kinds of immiscible solvents of each composition in product and reach separation, the loss of useful aroma component in complicated purification process was decreased.The Maillard reaction of this leaf tobacco extract can newly increase and bake fragrance and popcorn perfume on tobacco perfume base plinth, and when electronics tobacco tar is aspirated, the fragrance of smog increases substantially.This Maillard reaction makes full use of the dead meal that produces in production of cigarettes process as raw materials such as offal, offal, tobacco leaf fragments, and therefore manufacturing expense is very cheap.
Detailed description of the invention
For convenience of understanding the present invention better, be illustrated by following instance.These examples belong to protection scope of the present invention, but do not limit the scope of the invention.
Embodiment 1
First get tobacco leaf to be shredded, extract 5h with the heating of 80 DEG C, 6 times of water, obtain tobacco extract through heat filtering and refrigeration sedimentation filtration, concentrated yield is the tobacco leaf extract of 22.60%; Then weight ratio prepared opium paste is taken: aspartic acid is the prepared opium paste mixture 5g of 10:1, triacetyl glycerine: glycerin weight takes 100g than the mixed solvent for 10:1, prepared opium paste mixture is put in triacetyl glycerine and Glycerol solvents, 80 DEG C of heat times are 8 hours, obtain the maillard reaction product of leaf tobacco extract; By volume percentage measures the Maillard reaction thing of glycerin layer peony transparency liquid: asia peppermint oil is 1mL:25mL, is adding 74mL propane diols, is being uniformly mixed and obtains electronic cigarette oil product.
Embodiment 2
First get tobacco leaf to be shredded, extract 3h with the 60 DEG C of heating of 10 times of 95 ethanol, obtain tobacco extract through heat filtering and refrigeration sedimentation filtration, concentrated yield is the tobacco leaf extract of 24%; Then prepared opium paste is taken: proline weight ratio is the prepared opium paste mixture 5g of 2:1, triacetyl glycerine: glycerin weight takes 100g than the mixed solvent for 1:2, prepared opium paste mixture is put in triacetyl glycerine and Glycerol solvents, 100 DEG C of heat times are 9 hours, obtain the maillard reaction product of leaf tobacco extract; By volume percentage measures the Maillard reaction thing of glycerin layer peony transparency liquid: peppermint oil: glycerin monostearate is 25mL:40mL:1mL, is adding 34mL PEG400, is being uniformly mixed and obtains electronic cigarette oil product.
Embodiment 3
First get tobacco leaf to be shredded, extract 2h with the heating of 100 DEG C, 20 times of water, obtain tobacco extract through heat filtering and refrigeration sedimentation filtration, concentrated yield is the tobacco leaf extract of 23.90%; Then prepared opium paste is taken: kilnitamin weight ratio is 6:15g, triacetyl glycerine: glycerin weight takes 100g than the mixed solvent for 5:1, put into by prepared opium paste mixture in triacetyl glycerine and Glycerol solvents, 90 DEG C of heat times are 8 hours, obtain the maillard reaction product of leaf tobacco extract; By volume percentage measures the Maillard reaction thing of glycerin layer peony transparency liquid: glycerin monostearate is 10mL:0.3mL, is adding 89.7mL propane diols, is being uniformly mixed and obtains electronic cigarette oil product.

Claims (8)

1. the preparation method of a tobacco flavor electronics tobacco tar, it is characterized in that, step is as follows: (1) is first got tobacco leaf and shredded, and is that solvothermal extracts with water or 95% ethanol, obtain tobacco extract through heat filtering and refrigeration sedimentation filtration, concentrate to obtain tobacco leaf extract; (2) weight ratio tobacco leaf extract is then taken: amino acid is the tobacco leaf extract mixture 5g of 10 ~ 2:1, solvent takes 100g, tobacco leaf extract and amino acid are put in solvent, again 80 ~ 120 DEG C of heating 3 ~ 12 hours, obtain the maillard reaction product of tobacco leaf, (3) by the Maillard reaction thing of peony transparency liquid: peppermint oil: glycerin monostearate percent by volume is 1 ~ 25%:0 ~ 40%:0 ~ 1%, supply 100% volume with propane diols or polyethylene glycol again, be uniformly mixed and obtain tobacco flavor electronic cigarette oil product; Solvent described in step (2) is the mixture of two kinds not miscible arbitrarily in water, propane diols, polyethylene glycol, glycerine, triacetyl glycerine.
2. the preparation method of a kind of tobacco flavor electronics tobacco tar according to claim 1, it is characterized in that, step is as follows: (1) is first got tobacco leaf and shredded, be solvent 60 ~ 100 DEG C heating extraction 1 ~ 5h with 6 ~ 20 times of water or 95% ethanol, obtain tobacco extract through heat filtering and refrigeration sedimentation filtration, concentrated yield is the tobacco leaf extract of 22.6 ~ 24%; (2) then take weight ratio tobacco leaf extract: amino acid is the prepared opium paste mixture 5g of 10 ~ 2:1, and solvent takes 100g, puts in solvent by tobacco leaf extract and amino acid, 80 ~ 100 DEG C are heated 3 ~ 12 hours, obtain the maillard reaction product of tobacco leaf; (3) by the Maillard reaction thing of peony transparency liquid: peppermint oil: glycerin monostearate percent by volume is that 1 ~ 25%:0 ~ 40%:0 ~ 1% mixes, supply 100% volume with propane diols or polyethylene glycol again, be uniformly mixed and obtain tobacco flavor electronic cigarette oil product.
3. the preparation method of a kind of tobacco flavor electronics tobacco tar according to claim 1 and 2, it is characterized in that, described solvent is triacetyl glycerine: glycerin weight is than the mixture being 10 ~ 0.5:1.
4. the preparation method of a kind of tobacco flavor electronics tobacco tar according to claim 1 and 2, is characterized in that: described tobacco leaf is flue-cured tobacco, the mixing tobacco leaf of one or more in the waste/hypo-tobacco leaf that produces in suncured tabacco, air-curing of tobacco leaves production process.
5. the preparation method of a kind of tobacco flavor electronics tobacco tar according to claim 1 and 2, is characterized in that: described amino acid is one or more in glycine, glutamic acid, proline, alanine, aspartic acid.
6. the preparation method of a kind of tobacco flavor electronics tobacco tar according to claim 1 and 2, is characterized in that: described peppermint oil be asia peppermint oil, mentha piperita oil one or both.
7. the preparation method of a kind of tobacco flavor electronics tobacco tar according to claim 1 and 2, is characterized in that: described glycerine, propane diols or polyethylene glycol and glycerin monostearate, is edible rank.
8. the preparation method of a kind of tobacco flavor electronics tobacco tar according to claim 1 and 2, it is characterized in that, step is as follows: (1) is first got tobacco leaf and shredded, with 10 times of water or 95% ethanol be solvent 80 DEG C heating extract 5h, obtain tobacco extract through heat filtering and refrigeration sedimentation filtration, concentrated yield is the tobacco leaf extract of 22.6 ~ 24%; (2) weight ratio tobacco leaf extract is then taken: amino acid is the tobacco leaf extract mixture 5g of 3:1, triacetyl glycerine: glycerin weight takes 100g than for 3:2 mixed solvent, tobacco leaf extract and amino acid are put in solvent, 90 DEG C of heat times are 8 hours, obtain the maillard reaction product of tobacco leaf; (3) by the Maillard reaction thing of peony transparency liquid: peppermint oil: glycerin monostearate percent by volume is 15%:25%:0.2% mixing, then supplies 100% volume with propane diols, is uniformly mixed and obtains tobacco flavor electronic cigarette oil product.
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CN104287085B (en) * 2014-10-10 2017-01-25 安徽中烟工业有限责任公司 Electronic cigarette liquid with liquid leakage preventing function
CN105433431B (en) * 2014-11-12 2018-12-07 湖南中烟工业有限责任公司 A kind of electronic cigarette liquid and electronic cigarette
CN104473323A (en) * 2014-12-03 2015-04-01 河南中烟工业有限责任公司 Electronic cigarette atomizing agent
CN105077570B (en) * 2015-08-18 2017-08-29 河南中烟工业有限责任公司 A kind of tobacco leaf extract pyrolysis product, its preparation method and its application
CN105542959A (en) * 2015-12-17 2016-05-04 立场电子科技发展(上海)有限公司 Method for preparing electronic cigarette liquid flavor
CN106820267A (en) * 2016-12-28 2017-06-13 深圳瀚星翔科技有限公司 A kind of electronic cigarette tobacco tar and preparation method thereof
CN106551420A (en) * 2017-01-23 2017-04-05 江苏中烟工业有限责任公司 A kind of method that application cabo prepares tobacco juice for electronic smoke
CN111671134A (en) * 2020-06-22 2020-09-18 福建中烟工业有限责任公司 Mint flue-cured tobacco type tobacco flavor electronic cigarette atomized liquid
CN111671133A (en) * 2020-06-22 2020-09-18 福建中烟工业有限责任公司 Tea-flavored flue-cured tobacco type tobacco flavor electronic cigarette atomized liquid
CN111671131B (en) * 2020-06-22 2022-04-22 福建中烟工业有限责任公司 Electronic cigarette atomized liquid with flue-cured tobacco and tobacco taste and preparation method thereof

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