CN104483344B - 一种防霉剂中富马酸二甲酯的快速判定方法 - Google Patents
一种防霉剂中富马酸二甲酯的快速判定方法 Download PDFInfo
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- CN104483344B CN104483344B CN201510006379.1A CN201510006379A CN104483344B CN 104483344 B CN104483344 B CN 104483344B CN 201510006379 A CN201510006379 A CN 201510006379A CN 104483344 B CN104483344 B CN 104483344B
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- dimethyl fumarate
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- LDCRTTXIJACKKU-ONEGZZNKSA-N dimethyl fumarate Chemical compound COC(=O)\C=C\C(=O)OC LDCRTTXIJACKKU-ONEGZZNKSA-N 0.000 claims description 48
- 229960004419 dimethyl fumarate Drugs 0.000 claims description 47
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- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 4
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- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
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- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 3
- 238000004128 high performance liquid chromatography Methods 0.000 description 3
- ODIGIKRIUKFKHP-UHFFFAOYSA-N (n-propan-2-yloxycarbonylanilino) acetate Chemical compound CC(C)OC(=O)N(OC(C)=O)C1=CC=CC=C1 ODIGIKRIUKFKHP-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
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- 239000001530 fumaric acid Substances 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
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- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
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- XJMWHXZUIGHOBA-UHFFFAOYSA-N azane;propanoic acid Chemical compound N.CCC(O)=O XJMWHXZUIGHOBA-UHFFFAOYSA-N 0.000 description 1
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- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 description 1
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- 238000002203 pretreatment Methods 0.000 description 1
- 235000019260 propionic acid Nutrition 0.000 description 1
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- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
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CN201510006379.1A CN104483344B (zh) | 2015-01-07 | 2015-01-07 | 一种防霉剂中富马酸二甲酯的快速判定方法 |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101318901A (zh) * | 2008-06-17 | 2008-12-10 | 健雄职业技术学院 | 一种富马酸二甲酯的合成新工艺 |
CN102432464A (zh) * | 2011-12-14 | 2012-05-02 | 费近峰 | 一种富马酸二甲酯的连续生产工艺 |
CN102766050A (zh) * | 2012-08-10 | 2012-11-07 | 太仓市运通化工厂 | 一种富马酸二甲酯的合成方法 |
CN103848739A (zh) * | 2014-03-20 | 2014-06-11 | 徐晓宁 | 一种高纯度富马酸二甲酯的生产方法 |
CN104020074A (zh) * | 2014-06-20 | 2014-09-03 | 重庆民泰香料化工有限责任公司 | 混合型饲料添加剂香味剂中水分的检测方法 |
-
2015
- 2015-01-07 CN CN201510006379.1A patent/CN104483344B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101318901A (zh) * | 2008-06-17 | 2008-12-10 | 健雄职业技术学院 | 一种富马酸二甲酯的合成新工艺 |
CN102432464A (zh) * | 2011-12-14 | 2012-05-02 | 费近峰 | 一种富马酸二甲酯的连续生产工艺 |
CN102766050A (zh) * | 2012-08-10 | 2012-11-07 | 太仓市运通化工厂 | 一种富马酸二甲酯的合成方法 |
CN103848739A (zh) * | 2014-03-20 | 2014-06-11 | 徐晓宁 | 一种高纯度富马酸二甲酯的生产方法 |
CN104020074A (zh) * | 2014-06-20 | 2014-09-03 | 重庆民泰香料化工有限责任公司 | 混合型饲料添加剂香味剂中水分的检测方法 |
Non-Patent Citations (3)
Title |
---|
张凤枰等.毛细管气相色谱内标法测定防霉剂中富马酸二甲酯.《粮食储藏》.2007,(第01期), * |
曹华娟等.食品中富马酸二甲酯残留量的GC-MS法测定.《实用预防医学》.2005,(第01期), * |
楚洁.富马酸二甲酯的合成研究.《泰安师专学报》.2001,(第03期), * |
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Address after: 400063 Mintai Road, Jiguan Shilong Industrial Park, Nanan District, Chongqing Patentee after: CHONGQING MINTAI NEW AGROTECH DEVELOPMENT GROUP Co.,Ltd. Address before: 400063 Mintai Road, Jiguan Shilong Industrial Park, Nanan District, Chongqing Patentee before: CHONGQING MINTAI FLAVOR CHEMICAL CO.,LTD. |
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Denomination of invention: A rapid determination method of dimethyl fumarate in fungicide Effective date of registration: 20210219 Granted publication date: 20170510 Pledgee: Chongqing Branch of China Everbright Bank Co.,Ltd. Pledgor: CHONGQING MINTAI NEW AGROTECH DEVELOPMENT GROUP Co.,Ltd. Registration number: Y2021500000005 |
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Denomination of invention: A rapid determination method for dimethyl fumarate in a mold inhibitor Granted publication date: 20170510 Pledgee: Chongqing Branch of China Everbright Bank Co.,Ltd. Pledgor: CHONGQING MINTAI NEW AGROTECH DEVELOPMENT GROUP Co.,Ltd. Registration number: Y2024500000032 |