CN104479931A - Preparation method of vegetable and fruit washing agent for removing pesticide residues - Google Patents

Preparation method of vegetable and fruit washing agent for removing pesticide residues Download PDF

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Publication number
CN104479931A
CN104479931A CN201410727172.9A CN201410727172A CN104479931A CN 104479931 A CN104479931 A CN 104479931A CN 201410727172 A CN201410727172 A CN 201410727172A CN 104479931 A CN104479931 A CN 104479931A
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China
Prior art keywords
preparation
vegetable
washing agent
parts
fruit washing
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Pending
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CN201410727172.9A
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Chinese (zh)
Inventor
梁宗贵
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Chengdu Shunfa Disinfectant and Washing Technology Co Ltd
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Chengdu Shunfa Disinfectant and Washing Technology Co Ltd
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Priority to CN201410727172.9A priority Critical patent/CN104479931A/en
Publication of CN104479931A publication Critical patent/CN104479931A/en
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Abstract

The invention provides a preparation method of a vegetable and fruit washing agent for removing pesticide residues. The preparation method comprises the following steps: (1) adding 5-10 parts of plant oil, 3-8 parts of an emulsifying agent, 0.5-1 part of dodecyl dimethyl benzyl ammonium chloride and 0.3-0.5 part of a chelating agent in a container, adding 30-40 parts of deionized water, mixing and dissolving, adding 0.5-1 part of enhanceparaben, and mixing until uniform liquid is formed for later use; and (2) adding 0.3-0.5 part of isothiazolinone, 0.3-0.8 part of a liquorice derivative, 0.3-0.5 part of an emollient, 3-5 parts of sodium chloride and 3-5 parts of soluble starch in the liquid of the step (1), continuously mixing to form a uniform liquid so that the vegetable and fruit washing agent is prepared. The vegetable and fruit washing agent prepared by adopting the preparation method can be used for effectively cleaning pesticide residues, dirt and various pathogenic bacteria on the surfaces of the fruits, and is stable in performance and free from polluting the environment; and the preparation method is simple in operation.

Description

A kind of preparation method of pesticide residue vegetables and fruits washing composition of dispelling
Technical field
The present invention relates to washing technology field, particularly a kind of preparation method of pesticide residue vegetables and fruits washing composition of dispelling.
Background technology
Along with the enhancing of people's nutrient health idea, fresh fruits and vegetables have become requisite food on people's dining table.Modern agriculture almost be unable to do without agricultural chemicals, our dining table also almost can not find the vegetables of not spraying agricultural chemicals.So, again how present situation? nearly 2,000 ten thousand people fall ill because of pesticidal contamination every year.The harm of pesticide residue is not only and is caused acute poisoning, and more alarming is chronic poisoning, and carcinogenic, teratogenesis and mutagenesis.Eat with the fruit of remains of pesticide, vegetables, the symptom such as headache, dizziness, vomiting, stomachache, diarrhoea can be there is in acute poisoning person, chronic poisoning except can causing various diseases, pesticide residue at people's cylinder accumulation after 15-20 years, the fatal disease (cancer) that can past medical help.
At present, the Betengent product for vegetable and fruit washing is a lot, but there is a lot of limitation, and can not meet the demand of people, a lot of product is all that clean effect is good, but can not remove the pesticide residue on vegetables and fruits surface.
One section of notification number is disclose a kind of vegetable and fruit special purpose detergent composition in the patent of invention file of CN101985586A, is made up of the water of certain part by weight, dodecyl benzyl dimethyl ammonium chloride, Dodecyl Polyoxyethylene Ether sodium sulfate, fatty alcohol-polyoxyethylene ether, Coconut Fatty Acid Monoethanolamide, essence and sodium-chlor.It has sterilization broad spectrum, have good washing to dispel effect, and security is high, nontoxic residue-free.The invention also discloses the preparation method of this vegetable and fruit special purpose detergent composition, first take said components, then said components is processed in a kettle..Its step is simple, easily implements, process stabilizing, and obtained vegetable and fruit special purpose detergent composition components is even.The germicidal action that can greatly reduce dodecyl benzyl dimethyl ammonium chloride mixed with Dodecyl Polyoxyethylene Ether sodium sulfate of dodecyl benzyl dimethyl ammonium chloride in this invention, Papillary produces antagonism, thus affects the effect of this washing composition.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of pesticide residue vegetables and fruits washing composition of dispelling, the washing composition that the method prepares effectively can clean fruit surface pesticide residue, dirt and various pathogenic bacterium, stable performance, free from environmental pollution, and this preparation method is simple to operate.
For solving the problems of the technologies described above, the present invention is achieved through the following technical solutions.
A preparation method for pesticide residue of dispelling vegetable and fruit washing agent, comprises the steps:
(1) get vegetables oil 5-10 part, emulsifying agent 3-8 part, dodecyl benzyl dimethyl ammonium chloride 0.5-1 part, sequestrant 0.3-0.5, add in container and add 30-40 part deionized water, stirring and dissolving, add 0.5-1 part nipagin esters again, stir until to form uniform liquid for subsequent use;
(2) get isothiazolinone 0.3-0.5 part, Radix Glycyrrhizae derivative 0.3-0.8 part, softener 0.3-0.5 part, sodium-chlor 3-5 part, Zulkovsky starch 3-5 part joins in the liquid of step (1), continue to be stirred to and form uniform liquid and get final product.
Further, in step (1) be nipagin esters is added 1-2 times amount deionized water and stirring dissolve after add again.
Further, be that the liquid heat of step (1) is added nipagin esters again after 60-70 DEG C.
Described vegetables oil is Oleum Cocois, wheatgerm oil, one or more in raisin seed oil, Viscotrol C, rose hip oil, sweet almond oil.
Described emulsifier polyglycerol fatty acid ester, quillaja-saponin, one or more in glycerate, sorbitan-fatty acid ester, propylene glycol fatty acid ester.
Described Radix Glycyrrhizae derivative is Rizinsan K2 A2.
Described softener is one or more in propolis essential oil, water-soluble osso-albumin.
Described sequestrant is disodium ethylene diamine tetraacetate.
Beneficial effect:
Prepared by the inventive method dispel, and the agent of pesticide residue vegetable and fruit washing has excellent washing effect, thoroughly can dispel dirt and the pesticide residue on vegetables and fruits surface, there is sterilization and disinfection broad spectrum, dodecyl benzyl dimethyl ammonium chloride and isothiazolinone composite, there is synergism, decrease the consumption of these two kinds of compositions, cost-saving; Adopt vegetables oil, emulsifying agent, dodecyl benzyl dimethyl ammonium chloride composite, clean effect is good, easy rinsing, and detergent ingredients does not remain; Glycyrrhizin derivative, sodium bicarbonate, sodium-chlor and sequestrant are composite, can remove the various pesticide residue compositions on vegetables and fruits completely.Present method by nipagin esters, dodecyl benzyl dimethyl ammonium chloride is multiple, isothiazolinone is composite, has the effect of synergy, thus greatly reduces the consumption of raw material, cost-saving; Various composition of the present invention is nontoxic, and environmental protection, does not injure HUMAN HEALTH, and oil in water emulsion formula does not hinder skin, is free from side effects.
Embodiment
The present invention is described in detail below in conjunction with specific embodiment.
Embodiment 1
A preparation method for pesticide residue of dispelling vegetable and fruit washing agent, comprises the steps:
(1) get vegetables oil 5 parts, emulsifying agent 3 parts, dodecyl benzyl dimethyl ammonium chloride 0.5 part, sequestrant 0.3, add in container and add 30 parts of deionized waters, stirring and dissolving, add 0.5 part of nipagin esters again, stir until to form uniform liquid for subsequent use;
(2) get isothiazolinone 0.3 part, 0.3 part, Radix Glycyrrhizae derivative, softener 0.3 part, 3 parts, sodium-chlor, Zulkovsky starch 3 parts join in the liquid of step (1), continue to be stirred to and form uniform liquid and get final product.
Embodiment 2
A preparation method for pesticide residue of dispelling vegetable and fruit washing agent, comprises the steps:
(1) get vegetables oil 10 parts, emulsifying agent 8 parts, dodecyl benzyl dimethyl ammonium chloride 1 part, sequestrant 0.5, add in container and add 40 parts of deionized waters, stirring and dissolving, then add 1 part of nipagin esters, stir until to form uniform liquid for subsequent use;
(2) get isothiazolinone 0.5 part, 0.8 part, Radix Glycyrrhizae derivative, softener 0.5 part, 5 parts, sodium-chlor, Zulkovsky starch 5 parts join in the liquid of step (1), continue to be stirred to and form uniform liquid and get final product.
Embodiment 3
A preparation method for pesticide residue of dispelling vegetable and fruit washing agent, comprises the steps:
(1) get vegetables oil 7 parts, emulsifying agent 5 parts, dodecyl benzyl dimethyl ammonium chloride 0.8 part, sequestrant 0.4, add in container and add 35 parts of deionized waters, stirring and dissolving, add 0.8 part of nipagin esters again, stir until to form uniform liquid for subsequent use;
(2) get isothiazolinone 0.4 part, 0.6 part, Radix Glycyrrhizae derivative, softener 0.4 part, 4 parts, sodium-chlor, Zulkovsky starch 4 parts join in the liquid of step (1), continue to be stirred to and form uniform liquid and get final product.
Embodiment 4
A preparation method for pesticide residue of dispelling vegetable and fruit washing agent, comprises the steps:
(1) get vegetables oil 5 parts, emulsifying agent 3 parts, dodecyl benzyl dimethyl ammonium chloride 0.5 part, sequestrant 0.3, add in container and add 30 parts of deionized waters, stirring and dissolving, add 0.5 part of nipagin esters again, stir until to form uniform liquid for subsequent use;
(2) get isothiazolinone 0.3 part, 0.3 part, Radix Glycyrrhizae derivative, softener 0.3 part, 3 parts, sodium-chlor, Zulkovsky starch 3 parts join in the liquid of step (1), continue to be stirred to and form uniform liquid and get final product.Wherein, in step (1) be nipagin esters is added 1-2 times amount deionized water and stirring dissolve after add again.
Embodiment 5
A preparation method for pesticide residue of dispelling vegetable and fruit washing agent, comprises the steps:
(1) get vegetables oil 10 parts, emulsifying agent 8 parts, dodecyl benzyl dimethyl ammonium chloride 1 part, sequestrant 0.5, add in container and add 40 parts of deionized waters, stirring and dissolving, then add 1 part of nipagin esters, stir until to form uniform liquid for subsequent use;
(2) get isothiazolinone 0.5 part, 0.8 part, Radix Glycyrrhizae derivative, softener 0.5 part, 5 parts, sodium-chlor, Zulkovsky starch 5 parts join in the liquid of step (1), continue to be stirred to and form uniform liquid and get final product.Further, be that the liquid heat of step (1) is added nipagin esters again after 60-70 DEG C.
Embodiment 6
A preparation method for pesticide residue of dispelling vegetable and fruit washing agent, comprises the steps:
(1) get vegetables oil 7 parts, emulsifying agent 5 parts, dodecyl benzyl dimethyl ammonium chloride 0.8 part, sequestrant 0.4, add in container and add 35 parts of deionized waters, stirring and dissolving, add 0.8 part of nipagin esters again, stir until to form uniform liquid for subsequent use;
(2) get isothiazolinone 0.4 part, 0.6 part, Radix Glycyrrhizae derivative, softener 0.4 part, 4 parts, sodium-chlor, Zulkovsky starch 4 parts join in the liquid of step (1), continue to be stirred to and form uniform liquid and get final product.Described vegetables oil is Oleum Cocois, wheatgerm oil, one or more in raisin seed oil, Viscotrol C, rose hip oil, sweet almond oil.
Embodiment 7
A preparation method for pesticide residue of dispelling vegetable and fruit washing agent, comprises the steps:
(1) get vegetables oil 5 parts, emulsifying agent 3 parts, dodecyl benzyl dimethyl ammonium chloride 0.5 part, sequestrant 0.3, add in container and add 30 parts of deionized waters, stirring and dissolving, add 0.5 part of nipagin esters again, stir until to form uniform liquid for subsequent use;
(2) get isothiazolinone 0.3 part, 0.3 part, Radix Glycyrrhizae derivative, softener 0.3 part, 3 parts, sodium-chlor, Zulkovsky starch 3 parts join in the liquid of step (1), continue to be stirred to and form uniform liquid and get final product.Described emulsifying agent is polyglycerol fatty acid ester, quillaja-saponin, one or more in glycerate, sorbitan-fatty acid ester, propylene glycol fatty acid ester.
Embodiment 8
A preparation method for pesticide residue of dispelling vegetable and fruit washing agent, comprises the steps:
(1) get vegetables oil 7 parts, emulsifying agent 5 parts, dodecyl benzyl dimethyl ammonium chloride 0.8 part, sequestrant 0.4, add in container and add 35 parts of deionized waters, stirring and dissolving, add 0.8 part of nipagin esters again, stir until to form uniform liquid for subsequent use;
(2) get isothiazolinone 0.4 part, 0.6 part, Radix Glycyrrhizae derivative, softener 0.4 part, 4 parts, sodium-chlor, Zulkovsky starch 4 parts join in the liquid of step (1), continue to be stirred to and form uniform liquid and get final product.Described Radix Glycyrrhizae derivative is Rizinsan K2 A2.
Embodiment 9
A preparation method for pesticide residue of dispelling vegetable and fruit washing agent, comprises the steps:
(1) get vegetables oil 7 parts, emulsifying agent 5 parts, dodecyl benzyl dimethyl ammonium chloride 0.8 part, sequestrant 0.4, add in container and add 35 parts of deionized waters, stirring and dissolving, add 0.8 part of nipagin esters again, stir until to form uniform liquid for subsequent use;
(2) get isothiazolinone 0.4 part, 0.6 part, Radix Glycyrrhizae derivative, softener 0.4 part, 4 parts, sodium-chlor, Zulkovsky starch 4 parts join in the liquid of step (1), continue to be stirred to and form uniform liquid and get final product.
Described softener is one or more in propolis essential oil, water-soluble osso-albumin.
Embodiment 10
A preparation method for pesticide residue of dispelling vegetable and fruit washing agent, comprises the steps:
(1) get vegetables oil 7 parts, emulsifying agent 5 parts, dodecyl benzyl dimethyl ammonium chloride 0.8 part, sequestrant 0.4, add in container and add 35 parts of deionized waters, stirring and dissolving, add 0.8 part of nipagin esters again, stir until to form uniform liquid for subsequent use;
(2) get isothiazolinone 0.4 part, 0.6 part, Radix Glycyrrhizae derivative, softener 0.4 part, 4 parts, sodium-chlor, Zulkovsky starch 4 parts join in the liquid of step (1), continue to be stirred to and form uniform liquid and get final product.
Described sequestrant is disodium ethylene diamine tetraacetate.

Claims (8)

1. a preparation method for pesticide residue of dispelling vegetable and fruit washing agent, is characterized in that: comprise the steps:
(1) get vegetables oil 5-10 part, emulsifying agent 3-8 part, dodecyl benzyl dimethyl ammonium chloride 0.5-1 part, sequestrant 0.3-0.5, add in container and add 30-40 part deionized water, stirring and dissolving, add 0.5-1 part nipagin esters again, stir until to form uniform liquid for subsequent use;
(2) get isothiazolinone 0.3-0.5 part, Radix Glycyrrhizae derivative 0.3-0.8 part, softener 0.3-0.5 part, sodium-chlor 3-5 part, Zulkovsky starch 3-5 part joins in the liquid of step (1), continue to be stirred to and form uniform liquid and get final product.
2. the preparation method of a kind of pesticide residue vegetable and fruit washing agent of dispelling according to claim 1, is characterized in that: in step (1) be nipagin esters is added 1-2 times amount deionized water and stirring dissolve after add again.
3. the preparation method of a kind of pesticide residue vegetable and fruit washing agent of dispelling according to claim 1, is characterized in that: be that the liquid heat of step (1) is added nipagin esters again after 60-70 DEG C.
4. the preparation method of a kind of pesticide residue vegetable and fruit washing agent of dispelling according to claim 1, is characterized in that: described vegetables oil is Oleum Cocois, wheatgerm oil, one or more in raisin seed oil, Viscotrol C, rose hip oil, sweet almond oil.
5. the preparation method of a kind of pesticide residue vegetable and fruit washing agent of dispelling according to claim 1, it is characterized in that: described emulsifier polyglycerol fatty acid ester, quillaja-saponin, one or more in glycerate, sorbitan-fatty acid ester, propylene glycol fatty acid ester.
6. the preparation method of a kind of pesticide residue vegetable and fruit washing agent of dispelling according to claim 1, is characterized in that: described Radix Glycyrrhizae derivative is Rizinsan K2 A2.
7. the preparation method of a kind of pesticide residue vegetable and fruit washing agent of dispelling according to claim 1, is characterized in that: described softener is one or more in propolis essential oil, water-soluble osso-albumin.
8. the preparation method of a kind of pesticide residue vegetable and fruit washing agent of dispelling according to claim 1, is characterized in that: described sequestrant is disodium ethylene diamine tetraacetate.
CN201410727172.9A 2014-12-04 2014-12-04 Preparation method of vegetable and fruit washing agent for removing pesticide residues Pending CN104479931A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106857628A (en) * 2017-01-11 2017-06-20 北京长江脉医药科技有限责任公司 A kind of disinfectant including sterilization and degrading pesticide active component

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1144266A (en) * 1994-10-24 1997-03-05 邹刚毅 Magic detergent
CN102586040A (en) * 2012-01-09 2012-07-18 中国热带农业科学院农产品加工研究所 Preparation method of cleaning agent for residual pesticides on fruits and vegetables
CN103242974A (en) * 2013-04-08 2013-08-14 广州立白企业集团有限公司 Fruit, vegetable and tableware detergent with good rheological property
CN103589536A (en) * 2013-11-27 2014-02-19 骆志明 Licorice-containing skin moistening liquid soap
CN104017668A (en) * 2014-06-05 2014-09-03 广州立白企业集团有限公司 Emulsus dish washing detergent

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1144266A (en) * 1994-10-24 1997-03-05 邹刚毅 Magic detergent
CN102586040A (en) * 2012-01-09 2012-07-18 中国热带农业科学院农产品加工研究所 Preparation method of cleaning agent for residual pesticides on fruits and vegetables
CN103242974A (en) * 2013-04-08 2013-08-14 广州立白企业集团有限公司 Fruit, vegetable and tableware detergent with good rheological property
CN103589536A (en) * 2013-11-27 2014-02-19 骆志明 Licorice-containing skin moistening liquid soap
CN104017668A (en) * 2014-06-05 2014-09-03 广州立白企业集团有限公司 Emulsus dish washing detergent

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万素英等: "《食品防腐与食品防腐剂》", 31 December 1998, 北京:中国轻工业出版社 *
祁鲁梁等: "《水处理药剂及材料实用手册》", 31 December 2006, 北京:中国石化出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106857628A (en) * 2017-01-11 2017-06-20 北京长江脉医药科技有限责任公司 A kind of disinfectant including sterilization and degrading pesticide active component

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Application publication date: 20150401