CN104629929A - Camellia saponin natural dishwashing liquid - Google Patents
Camellia saponin natural dishwashing liquid Download PDFInfo
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- CN104629929A CN104629929A CN201510110695.3A CN201510110695A CN104629929A CN 104629929 A CN104629929 A CN 104629929A CN 201510110695 A CN201510110695 A CN 201510110695A CN 104629929 A CN104629929 A CN 104629929A
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Abstract
The invention provides camellia saponin natural dishwashing liquid which is prepared from the following components in parts by weight: 6-10 parts of camellia saponin, 1-2 parts of platycodon grandiflorum total saponin, 1-2 parts of vigna umbellata saponin, 1-2 parts of quillaic acid, 5-10 parts of ethanol, 0.1-0.5 part of citric acid, 0.1-0.5 part of sodium citrate, 0.1-0.5 part of sodium chloride and 40-50 parts of deionized water. The plant saponins such as camellia saponin, platycodon grandiflorum total saponin, vigna umbellata saponin and quillaic acid are used as surfactants which are combined with safe components such as sodium citrate and ethanol to develop a kind of natural kitchen dishwashing liquid. With the components such as multiple different plant saponins and sodium citrate, the camellia saponin natural dishwashing liquid has good effects of emulsifying, greasy dirt cleaning, sterilization and the like as well as high stability; and since the components are natural plant components, the camellia saponin natural dishwashing liquid has perfect safety and is good natural kitchen dishwashing liquid.
Description
Technical field
The present invention relates to a kind of Sasanguasaponin Natural cleanser essence, particularly with the liquid detergent that the saponin such as Sasanguasaponin, Radix Platycodi total saponins, Semen Phaseoli saponin(e, quillajic acid form for tensio-active agent.
Background technology
Sasanguasaponin is the class natural sugar glycoside compound contained in Camellia Plants.Being made up of hydrophilic sugared body and hydrophobic coordinating group in Sasanguasaponin molecule, is a kind of natural nonionic surface active agent.Paramethyl red is obviously in acid, belong to pentacyclic triterpenoid, solvable in moisture hot alcohol and Glacial acetic acid, the pyridine of aceticanhydride arsenic, and show the characteristic of Saponin/TSM foaming, in soluble in water and alkali aqueous solution, be insoluble to benzene chloroform and ether, have biological activity and the surfactivitys such as desinsection, sterilization, stimulating plant growth.
Liquid detergent is daily cosmetics of everyday use, its demand is increasing, but because most of liquid detergent all contains tensio-active agent and other biochemical components of synthesis, when wash dining set, the skin of opponent produces dry, the impact such as to chap, all produces certain negative impact to the security of tableware and environment, and therefore natural, safe liquid detergent is more by the attention of people.And the present invention just adopts natural plant composition to obtain a kind of natural safe liquid detergent.
Summary of the invention
The object of the present invention is to provide a kind of Sasanguasaponin Natural cleanser essence, with vegetalitas saponin(es such as Sasanguasaponin, Radix Platycodi total saponins, Semen Phaseoli saponin(e, quillajic acids for tensio-active agent, add that u'eno tea oil, Trisodium Citrate, ethanol etc. are natural, security elements is developed to a kind of natural kitchen essence.Be made up of components such as multiple different vegetalitas saponin(e, Trisodium Citrates, having effect of emulsification, degreasing, sterilization, is a kind of good Natural cleanser essence.
The technical solution used in the present invention is for achieving the above object, its formula material by following weight fraction ratio is, Sasanguasaponin 6-10 part, Radix Platycodi total saponins 1-2 part, Semen Phaseoli saponin(e 1-2 part, quillajic acid 1-2, ethanol 5-10 part, citric acid 0.1-0.5 part, Trisodium Citrate 0.1-0.5 part, sodium-chlor 0.1-0.5 part, deionized water 40-50 part.
The preparation method of Sasanguasaponin is: get the dry Oil-tea-cake of 10g and first pulverize, with 50wt.% alcohol steep 5h, extracting condition be material liquid volume than 1:6, temperature 55 DEG C, lixiviate terminates to filter, and carries out rotary evaporation and is concentrated into 2ml.
The preparation method of described quillajic acid is: get 10g drying soap grass, pulverize, carry out 60 DEG C of lixiviate 4h with 45wt.% methyl alcohol, filter, rotary evaporation is concentrated to 2ml.
The preparation method of described Radix Platycodi total saponins is: get the dry balloonflower root of 10g, and material liquid volume is than being 1:10, lixiviate 30min under ultrasonic wave, and temperature is 35 DEG C, and filter, rotary evaporation is concentrated to 2ml.
The preparation method of described Semen Phaseoli saponin(e is: the Semen Phaseoli getting 10g drying and crushing, and material liquid volume carries out 60 DEG C of lixiviate 4h than 1:10, and filter, rotary evaporation is concentrated into 2ml.
The preparation flow of the natural kitchen essence of Sasanguasaponin is: deionized water is heated to 60 DEG C and adds different saponin(es, in process, temperature controls at 60 DEG C ~ 65 DEG C, stir evenly 30min, temperature drops to 40 DEG C, add 95wt.% ethanol, Trisodium Citrate, use lemon acid for adjusting pH, finally add sodium-chlor adjusting viscosity again.
The invention has the advantages that: in Natural cleanser essence composition of the present invention: Sasanguasaponin is pentacyclic triterpene saponins is a kind of well nonionogenic tenside, can the effect such as emulsification, foaming, dispersion, degreasing, HLB value 16 energy emulsification not Activities of Some Plants, animal oil, there is germicidal action, mould is suppressed best; Radix Platycodi total saponins just has obvious surfactivity when 1.89mg/ml; Semen Phaseoli saponin(e has good surfactivity active, generates stable foam, and has certain Scavenging activity to the protein in grease, so there is good cleaning action; Quillajic acid has good surfactivity foaming abundancy can play foam enhancing effect, have outstanding emulsifying property, has good synergistic effect, the cleaning action of doing well to nonionogenic tensides such as theasaponins, also has Antimicrobial preservative effect; Ethanol has good solubilizing effect; Trisodium Citrate has good complexation of metal ions ability, well thickening power, can also remove the pesticide residue in fruits and vegetables class.The reasonable combination of various natural component, not only improves the security of use, has good degreasing, cleaning, germicidal action to kitchenware fruits and vegetables, also reduces common liquid detergent and uses the harm brought to environment in a large number.
Embodiment
embodiment 1
1, Sasanguasaponin 6 parts, Radix Platycodi total saponins 2 parts, Semen Phaseoli saponin(e 2 parts, quillajic acid 2 parts, ethanol 10 parts, citric acid 0.3 part, Trisodium Citrate 0.5 part, 0.5 part, sodium-chlor, deionized water 45 parts is got.
Deionized water is heated to 60 DEG C and adds different saponin(es, and in process, temperature controls, at 60 DEG C, to stir evenly 30min, and temperature drops to 40 DEG C, adds ethanol, Trisodium Citrate, regulates pH7.5 with citric acid, finally adds sodium-chlor adjusting viscosity again.
Embodiment 2
2, by following weight fraction ratio be, Sasanguasaponin 10 parts, Radix Platycodi total saponins 1 part, Semen Phaseoli saponin(e 1 part, quillajic acid 1, ethanol 5 parts, citric acid 0.1 part, Trisodium Citrate 0.1 part, 0.1 part, sodium-chlor, deionized water 40 parts.
Deionized water is heated to 60 DEG C and adds different saponin(es, and in process, temperature controls, at 65 DEG C, to stir evenly 30min, and temperature drops to 40 DEG C, adds ethanol, Trisodium Citrate, uses lemon acid for adjusting pH, finally adds sodium-chlor adjusting viscosity again.
Embodiment 3
3, be prepared by following weight fraction, Sasanguasaponin 8 parts, Radix Platycodi total saponins 2 parts, Semen Phaseoli saponin(e 1 part, quillajic acid 1 part, ethanol 7 parts, citric acid 0.3 part, Trisodium Citrate 0.3 part, 0.3 part, sodium-chlor, deionized water 45 parts.Deionized water is heated to 60 DEG C and adds different saponin(es, and in process, temperature controls, at 63 DEG C, to stir evenly 30min, and temperature drops to 40 DEG C, adds ethanol, Trisodium Citrate, uses lemon acid for adjusting pH, finally adds sodium-chlor adjusting viscosity again.
embodiment 4 liquid detergent characteristic and effect measuring
1, stability
respectively placing 24h under three kinds of liquid detergents are placed subzero 3 DEG C, 40 DEG C conditions, all there is not layering, precipitation, crystallization or changes the changes such as color in result, and embodying liquid detergent has good stability.
2, spumescence
Adopt Roche Latherometer to measure, and contrast with daily carving board liquid detergent, result is as table 1, and result represents that this product has higher foaming power and foam has higher stability.
Table 1 liquid detergent latherability and Stability Determination result
3, detersive power
Adopt the deoil rate method in GB9985-2000 to measure, and adopt conventional carving board liquid detergent in contrast, the result of mensuration is as table 2, and result shows, and the liquid detergent of three kinds of schemes all has higher deoil rate, has good scourability.
Table 2 liquid detergent soil removal efficiency measurement result
4, sterilization effect
Measuring method, experimental group is that three kinds of Natural cleanser essence dilute 10 times afterwards for sterilizing agent acts on streptococcus aureus, colibacillary experiment bacterium liquid, sampling also pours into inoculation with agar, control group does same operation after then diluting 10 times with carving board liquid detergent, and cultivate 48h together under 37 DEG C of conditions, and observations.
Result is as table 3, and result shows, Natural cleanser essence of the present invention has well suppression and sterilization effect, improves the safety in utilization of tableware, thus reduces the quantity of bacterium when using tableware.
The sterilization effect of table 3 liquid detergent
The foregoing is only preferred embodiment of the present invention, all equalizations done according to the present patent application the scope of the claims change and modify, and all should belong to covering scope of the present invention.
Claims (6)
1. a Sasanguasaponin Natural cleanser essence, it is characterized in that: raw material by following weight fraction ratio is, Sasanguasaponin 6-10 part, Radix Platycodi total saponins 1-2 part, Semen Phaseoli saponin(e 1-2 part, quillajic acid 1-2 part, ethanol 5-10 part, citric acid 0.1-0.5 part, Trisodium Citrate 0.1-0.5 part, sodium-chlor 0.1-0.5 part, deionized water 40-50 part.
2. a kind of Sasanguasaponin Natural cleanser essence according to claim 1, it is characterized in that: the preparation method of Sasanguasaponin is: get the dry Oil-tea-cake of 10g and first pulverize, with 50wt.% alcohol steep 5h, extracting condition is that material liquid volume is than 1:6, temperature 55 DEG C, lixiviate terminates to filter, and carries out rotary evaporation and is concentrated into 2ml.
3. a kind of Sasanguasaponin Natural cleanser essence according to claim 1, is characterized in that: the preparation method of described quillajic acid is: get 10g drying soap grass, pulverize, carry out 60 DEG C of lixiviate 4h with 45wt.% methyl alcohol, filter, rotary evaporation is concentrated to 2ml.
4. a kind of Sasanguasaponin Natural cleanser essence according to claim 1, is characterized in that: the preparation method of described Radix Platycodi total saponins is: get the dry balloonflower root of 10g, and material liquid volume is than being 1:10, lixiviate 30min under ultrasonic wave, temperature is 35 DEG C, and filter, rotary evaporation is concentrated to 2ml.
5. a kind of Sasanguasaponin Natural cleanser essence according to claim 1, it is characterized in that: the preparation method of described Semen Phaseoli saponin(e is: the Semen Phaseoli getting 10g drying and crushing, material liquid volume carries out 60 DEG C of lixiviate 4h than 1:10, and filter, rotary evaporation is concentrated into 2ml.
6. a kind of Sasanguasaponin Natural cleanser essence according to claim 1, it is characterized in that: the preparation flow of the natural kitchen essence of Sasanguasaponin is: deionized water is heated to 60 DEG C and adds different saponin(es, in process, temperature controls at 60 DEG C ~ 65 DEG C, stir evenly 30min, temperature drops to 40 DEG C, add 95wt.% ethanol, Trisodium Citrate, use lemon acid for adjusting pH, finally add sodium-chlor adjusting viscosity again.
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| CN201510110695.3A CN104629929A (en) | 2015-03-14 | 2015-03-14 | Camellia saponin natural dishwashing liquid |
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| CN201510110695.3A CN104629929A (en) | 2015-03-14 | 2015-03-14 | Camellia saponin natural dishwashing liquid |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106085611A (en) * | 2016-06-03 | 2016-11-09 | 潘星辑 | A kind of cleaning agent containing tea saponin and preparation method thereof |
| CN106947610A (en) * | 2017-03-24 | 2017-07-14 | 福建师范大学泉港石化研究院 | A kind of antibacterial detergent of environment-friendly type and preparation method thereof |
| CN113183655A (en) * | 2021-05-17 | 2021-07-30 | 中山市富日印刷材料有限公司 | All-round thermosetting alcohol-free fountain solution and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106085611A (en) * | 2016-06-03 | 2016-11-09 | 潘星辑 | A kind of cleaning agent containing tea saponin and preparation method thereof |
| CN106947610A (en) * | 2017-03-24 | 2017-07-14 | 福建师范大学泉港石化研究院 | A kind of antibacterial detergent of environment-friendly type and preparation method thereof |
| CN113183655A (en) * | 2021-05-17 | 2021-07-30 | 中山市富日印刷材料有限公司 | All-round thermosetting alcohol-free fountain solution and preparation method thereof |
| CN113183655B (en) * | 2021-05-17 | 2022-10-11 | 中山市富日印刷材料有限公司 | All-round thermosetting alcohol-free fountain solution and preparation method thereof |
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