CN104479513A - 一种海洋气候端羧基溴碳聚酯树脂防火涂料及制备方法 - Google Patents

一种海洋气候端羧基溴碳聚酯树脂防火涂料及制备方法 Download PDF

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CN104479513A
CN104479513A CN201410741554.7A CN201410741554A CN104479513A CN 104479513 A CN104479513 A CN 104479513A CN 201410741554 A CN201410741554 A CN 201410741554A CN 104479513 A CN104479513 A CN 104479513A
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CN104479513B (zh
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张和庆
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Jiangsu Dayang Marine Equipment Co., Ltd.
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Abstract

本发明涉及一种海洋气候端羧基溴碳聚酯树脂防火涂料及制备方法，由下列原料按质量比组成：端羧基溴碳聚酯树脂80-90份、三乙醇胺3.5-4份、三聚氰胺10-15份、钛白粉5-10份、膨胀珍珠岩8-14份、羟乙基纤维素8-12份、甲基硅醇钠3-6份、硫酸铝4-7份。首先将端羧基溴碳聚酯树脂与三乙醇胺进行混合，再加入三聚氰胺、钛白粉、膨胀珍珠岩、羟乙基纤维素进行混合成原浆，将甲基硅醇钠、硫酸铝混合调配后加入原浆进行混合，最后依次经挤出机熔融挤出、粉碎得到涂料。

Description

一种海洋气候端羧基溴碳聚酯树脂防火涂料及制备方法
技术领域
本发明涉及一种防火涂料，具体说是一种海洋气候端羧基溴碳聚酯树脂防火涂料及其制备方法。
背景技术
聚酯粉末涂料具有良好的物理机械性能，可广泛用于金属表面的装饰和保护，在海洋气候下船舶上要求涂料防火、耐水、耐腐蚀性能较高，现有市场上的聚酯粉末涂料大都只在防火上性能优异，但是无法满足海洋气候特殊要求的使用。
发明内容
针对现有技术中的上述不足，本发明提供了一种制造方便，成本低，防火、耐水、耐腐蚀性能较好的一种海洋气候端羧基溴碳聚酯树脂防火涂料及制备方法。
本发明采用的技术方案是：一种海洋气候端羧基溴碳聚酯树脂防火涂料，由下列原料按质量比组成：端羧基溴碳聚酯树脂80-90份、三乙醇胺3.5-4份、三聚氰胺10-15份、钛白粉5-10份、膨胀珍珠岩8-14份、羟乙基纤维素8-12份、甲基硅醇钠3-6份、硫酸铝4-7份。
一种海洋气候端羧基溴碳聚酯树脂防火涂料的制备方法，包括以下步骤：首先将端羧基溴碳聚酯树脂与三乙醇胺进行混合，再加入三聚氰胺、钛白粉、膨胀珍珠岩、羟乙基纤维素进行混合成原浆，将甲基硅醇钠、硫酸铝混合调配后加入原浆进行混合，最后依次经挤出机熔融挤出、粉碎得到涂料。
    一种海洋气候端羧基溴碳聚酯树脂防火涂料，由下列原料按质量比组成：端羧基溴碳聚酯树脂80-85份、三乙醇胺3.5-4份、三聚氰胺10-15份、钛白粉5-10份、膨胀珍珠岩8-14份、羟乙基纤维素8-12份、甲基硅醇钠3-6份、硫酸铝4-7份。
    一种海洋气候端羧基溴碳聚酯树脂防火涂料，由下列原料按质量比组成：端羧基溴碳聚酯树脂85份、三乙醇胺3.6份、三聚氰胺12份、钛白粉7份、膨胀珍珠岩11份、羟乙基纤维素10份、甲基硅醇钠4份、硫酸铝5份。
本发明在端羧基溴碳聚酯树脂中加入三乙醇胺、三聚氰胺、钛白粉、膨胀珍珠岩、羟乙基纤维素，配以甲基硅醇钠和硫酸铝，能兼顾防火、耐水、耐腐蚀性能，适合海洋气候下特殊使用要求。
具体实施方式
以下结合实施例对本发明作进一步说明。
实施例一
一种海洋气候端羧基溴碳聚酯树脂防火涂料，由下列原料按质量比组成：端羧基溴碳聚酯树脂80份、三乙醇胺3.5份、三聚氰胺10份、钛白粉5份、膨胀珍珠岩8份、羟乙基纤维素8份、甲基硅醇钠3份、硫酸铝4份。制备方法包括以下步骤：首先将端羧基溴碳聚酯树脂与三乙醇胺进行混合，再加入三聚氰胺、钛白粉、膨胀珍珠岩、羟乙基纤维素进行混合成原浆，将甲基硅醇钠、硫酸铝混合调配后加入原浆进行混合，最后依次经挤出机熔融挤出、粉碎得到涂料。
实施例二
一种海洋气候端羧基溴碳聚酯树脂防火涂料，由下列原料按质量比组成：端羧基溴碳聚酯树脂90份、三乙醇胺4份、三聚氰胺15份、钛白粉10份、膨胀珍珠岩14份、羟乙基纤维素12份、甲基硅醇钠6份、硫酸铝7份。制备方法包括以下步骤：首先将端羧基溴碳聚酯树脂与三乙醇胺进行混合，再加入三聚氰胺、钛白粉、膨胀珍珠岩、羟乙基纤维素进行混合成原浆，将甲基硅醇钠、硫酸铝混合调配后加入原浆进行混合，最后依次经挤出机熔融挤出、粉碎得到涂料。
实施例三
一种海洋气候端羧基溴碳聚酯树脂防火涂料，由下列原料按质量比组成：端羧基溴碳聚酯树脂85份、三乙醇胺3.6份、三聚氰胺12份、钛白粉7份、膨胀珍珠岩11份、羟乙基纤维素10份、甲基硅醇钠4份、硫酸铝5份。制备方法包括以下步骤：首先将端羧基溴碳聚酯树脂与三乙醇胺进行混合，再加入三聚氰胺、钛白粉、膨胀珍珠岩、羟乙基纤维素进行混合成原浆，将甲基硅醇钠、硫酸铝混合调配后加入原浆进行混合，最后依次经挤出机熔融挤出、粉碎得到涂料。

Claims (4)

1.一种海洋气候端羧基溴碳聚酯树脂防火涂料，由下列原料按质量比组成：端羧基溴碳聚酯树脂80-90份、三乙醇胺3.5-4份、三聚氰胺10-15份、钛白粉5-10份、膨胀珍珠岩8-14份、羟乙基纤维素8-12份、甲基硅醇钠3-6份、硫酸铝4-7份。
2.一种海洋气候端羧基溴碳聚酯树脂防火涂料，由下列原料按质量比组成：端羧基溴碳聚酯树脂80-85份、三乙醇胺3.5-4份、三聚氰胺10-15份、钛白粉5-10份、膨胀珍珠岩8-14份、羟乙基纤维素8-12份、甲基硅醇钠3-6份、硫酸铝4-7份。
3.一种海洋气候端羧基溴碳聚酯树脂防火涂料，由下列原料按质量比组成：端羧基溴碳聚酯树脂85份、三乙醇胺3.6份、三聚氰胺12份、钛白粉7份、膨胀珍珠岩11份、羟乙基纤维素10份、甲基硅醇钠4份、硫酸铝5份。
4.一种海洋气候端羧基溴碳聚酯树脂防火涂料的制备方法，包括以下步骤：首先将端羧基溴碳聚酯树脂与三乙醇胺进行混合，再加入三聚氰胺、钛白粉、膨胀珍珠岩、羟乙基纤维素进行混合成原浆，将甲基硅醇钠、硫酸铝混合调配后加入原浆进行混合，最后依次经挤出机熔融挤出、粉碎得到涂料。
CN201410741554.7A 2014-12-09 2014-12-09 一种海洋气候端羧基溴碳聚酯树脂防火涂料及制备方法 Active CN104479513B (zh)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1380370A (zh) * 2002-03-25 2002-11-20 葛明槽 防火粉末涂料及其生产工艺
CN1729226A (zh) * 2002-10-22 2006-02-01 阿什兰公司 溴化聚酯树脂、含有溴化聚酯树脂的树脂组合物以及层状组合物
CN101255310A (zh) * 2007-09-11 2008-09-03 兰州理工大学 含溴碳聚酯的粉末防火涂料及其制备方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1380370A (zh) * 2002-03-25 2002-11-20 葛明槽 防火粉末涂料及其生产工艺
CN1729226A (zh) * 2002-10-22 2006-02-01 阿什兰公司 溴化聚酯树脂、含有溴化聚酯树脂的树脂组合物以及层状组合物
CN101255310A (zh) * 2007-09-11 2008-09-03 兰州理工大学 含溴碳聚酯的粉末防火涂料及其制备方法

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