CN104449130A - Corrosion-oxidation-resistant and environment-friendly waterborne coating for glass door and preparation method of waterborne coating - Google Patents
Corrosion-oxidation-resistant and environment-friendly waterborne coating for glass door and preparation method of waterborne coating Download PDFInfo
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- CN104449130A CN104449130A CN201410568294.8A CN201410568294A CN104449130A CN 104449130 A CN104449130 A CN 104449130A CN 201410568294 A CN201410568294 A CN 201410568294A CN 104449130 A CN104449130 A CN 104449130A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1656—Antifouling paints; Underwater paints characterised by the film-forming substance
- C09D5/1662—Synthetic film-forming substance
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1687—Use of special additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
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Abstract
The invention discloses a corrosion-oxidation-resistant and environment-friendly waterborne coating for a glass door. The waterborne coating is characterized by being prepared from the following raw materials in parts by weight: 8-10 parts of silicone acrylic emulsion, 43-46 parts of acrylic resin emulsion, 15-18 parts of chloride ether resin emulsion, 1-3 parts of triethylene glycol monomethyl ether, 0.3-0.6 part of alkanolamine alkoxy titanate, 0.3-0.5 part of a flatting agent BYK-56, 0.2-0.4 part of polyether-modified organosilicone emulsion, 0.3-0.5 part of lauryl dimethyl amine oxide, 0.3-0.6 part of polyoxyethylene polyoxypropylene oleate, 0.5-1.0 part of garlic polysaccharide, 0.5-1.0 part of tea polyphenol, 3-5 parts of a modified nanometer titanium dioxide photocatalyst, 1-2 parts of a pigment and 10-15 parts of deionized water. By adding the modified nanometer titanium dioxide photocatalyst, the self-cleaning property, antifouling property, mildew resistance, air purifying property and the like of the coating are increased; and by adding the silicone acrylic emulsion, the weather resistance, water resistance, antifouling property, acid-alkali resistance, ultraviolet resistance and the like of the coating are increased. The production operation of the coating is simple and low in production cost, the coating film is non-yellowing and aging-resistant and the coating is safe and environmentally friendly, and is suitable for being used as a coating for decorating the household glass door.
Description
Technical field
The present invention relates to a kind of coating and preparation method thereof, particularly a kind of corrosion-resistant oxidation environment-friendly type glass door use coating and preparation method thereof.
Background technology
Every coating using water as solvent or make dispersion medium, all can be described as water-borne coatings.Water-borne coatings, using water as dispersion medium, only adopts a small amount of hypotoxicity alcohol ether organic solvent, safety and environmental protection, economizes on resources, and eliminates the danger of presence of fire during construction, is conducive to reducing topsoil.Water-borne coatings is very good to material surface adaptability, and can construct equally at wet environment, coating adhesion is strong.Glass and glasswork, because of attractive in appearance and needs that are performance, coating need be applied thereon, glass paint is developed by solvent-borne type hydrotropisms, it is the inexorable trend adapting to environment protection requirement development, the requirement having surmounted traditional decoration far away and beautified, the performances such as wear-resistant to it, anti-zoned quarter, weathering resistance propose requirements at the higher level.
Nano photo-catalytic refers under light illumination, there is not chemical transformation in self, but the material of chemical reaction can be promoted, nano TiO 2 is topmost photocatalyst material, when after the energy that it absorbs in sunlight or other light sources, a series of reaction occurs can become harmless carbonic acid gas and water by oxygenolysis such as most of organism, pollutent, foul smell, bacteriums.If but dispersing technology is not good in the product for nano-titania photocatalyst, thus cause reunion.This reunion directly has influence on photocatalyst activity, reduces the photo-catalysis capability of product, and then loses pollution degraded effect.Binchotan and diatomite support process according to this situation by the present invention, increase specific surface area, nano photo-catalytic is adsorbed on carrier, and utilize cupric ion, silver ions and rare earth element to carry out modification to nano photo-catalytic, increase the function such as sterilization, sterilization, avoid nano photocatalyst catalytic material in coating, disperse uneven generation to reunite and lose light-catalysed ability.
Summary of the invention
The object of this invention is to provide a kind of corrosion-resistant oxidation environment-friendly type glass door use coating and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of corrosion-resistant oxidation environment-friendly type glass door use coating, is made up of the raw material of following weight part: organosilicon crylic acid latex 8-10, Emulsion acrylic resin 43-46, chlorinated polyether resin emulsion 15-18, triethylene glycol monomethyl ether 1-3, hydramine alkoxy titanates 0.3-0.6, flow agent BYK-560.3-0.5, organic silicon modified by polyether emulsion 0.2-0.4, dimethyl dodecyl amine oxide 0.3-0.5, polyoxyethylene oxypropylene oleic acid ester 0.3-0.6, garlic polysaccharide 0.5-1.0, tea-polyphenol 0.5-1.0, modified nano-titanium dioxide photocatalyst 3-5, pigment 1-2, deionized water 10-15;
Described modified nano-titanium dioxide photocatalyst is made up of the raw material of following weight part: nano-titania photocatalyst 40-50, nano silicon 15-20, nano-tourmaline 10-15, binchotan 10-15, rare earth element 0.5-1.0, copper powder 0.7-1.4, silver powder 0.6-1.2, cobalt oxide powder 0.4-0.8, diatomite 8-12, alkylphenol polyoxyethylene 0.6-1.2, Silane coupling agent KH550 0.7-1.4, the salpeter solution 20-40 of 20%, the sodium hydroxide solution 20-40 of 30%, polyvinyl alcohol 1-2, st-yrax n-butyl ether 0.3-0.5, ferric acetyl acetonade 0.2-0.4, distilled water 100, diatomite is ground into particle and binchotan to be added in the salpeter solution of 20% and to soak 20 minutes by preparation method after high-temperature calcination, wash with water in neutral, to be immersed in the solution of the sodium hydroxide of 30% 30 minutes again, wash with water and add copper powder in neutral post-drying, silver powder, it is for subsequent use that cobalt oxide powder and 10-30% Silane coupling agent KH550 grind to form fine powder, again alkylphenol polyoxyethylene is added in distilled water and dissolves, raised temperature to 85 ° about C, add the above-mentioned fine powder worn under 1000-1200 rev/min, stir the uniform mixed solution of formation, add nano-titania photocatalyst again, nano silicon, st-yrax n-butyl ether, ferric acetyl acetonade, rare earth element and remaining Silane coupling agent KH550 grinding distribution 0.5-1.0 hour, dry.
One of the present invention corrosion-resistant oxidation environment-friendly type glass door use coating, be made up of following concrete steps:
(1) deionized water, flow agent BYK-56, organic silicon modified by polyether emulsion, dimethyl dodecyl amine oxide, garlic polysaccharide, tea-polyphenol mixing are added in Scattered Kettle, to stir 3-5 minute under the condition of 600-800 rev/min;
(2) rotating speed is adjusted to 900-1000 rev/min, in Scattered Kettle, adds triethylene glycol monomethyl ether, polyoxyethylene oxypropylene oleic acid ester stirs 6-8 minute;
(3) rotating speed is adjusted to 1400-1600 rev/min, adds organosilicon crylic acid latex, Emulsion acrylic resin, chlorinated polyether resin emulsion stirring 15-25 minute;
(4) rotating speed is adjusted to 1000-1200 rev/min, adds hydramine alkoxy titanates, pigment, modified nano-titanium dioxide photocatalyst uniform stirring 20-30 minute successively;
(5) be added in sand mill and carry out grinding distribution by the material after dispersion, after filtering, fineness is less than 20 μm and packs.
Advantage of the present invention is: the modified nano-titanium dioxide photocatalyst that the present invention adds enhances the performance of the self-cleaning property of coating, antifouling mould resistance, the aspect such as to purify air, the organosilicon crylic acid latex added enhances the feature such as weathering resistance, water tolerance, resistance to crocking, resistance to acids and bases, UV resistant of coating, coating material production of the present invention is simple to operate, film not yellowing is anti-aging, production cost is low, and green safety is suitable for as family's glass door decoration coating.
specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of corrosion-resistant oxidation environment-friendly type glass door use coating, is made up of the raw material of following weight part (kilogram): organosilicon crylic acid latex 10, Emulsion acrylic resin 45, chlorinated polyether resin emulsion 17, triethylene glycol monomethyl ether 3, hydramine alkoxy titanates 0.5, flow agent BYK-560.4, organic silicon modified by polyether emulsion 0.4, dimethyl dodecyl amine oxide 0.4, polyoxyethylene oxypropylene oleic acid ester 0.5, garlic polysaccharide 1.0, tea-polyphenol 0.8, modified nano-titanium dioxide photocatalyst 4, pigment 2, deionized water 14;
Described modified nano-titanium dioxide photocatalyst is made up of the raw material of following weight part (kilogram): nano-titania photocatalyst 44, nano silicon 16, nano-tourmaline 12, binchotan 14, rare earth element 0.5, copper powder 0.8, silver powder 0.7, cobalt oxide powder 0.5, diatomite 10, alkylphenol polyoxyethylene 0.8, Silane coupling agent KH550 0.8, the salpeter solution 36 of 20%, the sodium hydroxide solution 34 of 30%, polyvinyl alcohol 1, st-yrax n-butyl ether 0.3, ferric acetyl acetonade 0.3, distilled water 100, diatomite is ground into particle and binchotan to be added in the salpeter solution of 20% and to soak 20 minutes by preparation method after high-temperature calcination, wash with water in neutral, to be immersed in the solution of the sodium hydroxide of 30% 30 minutes again, wash with water and add copper powder in neutral post-drying, silver powder, it is for subsequent use that cobalt oxide powder and 10-30% Silane coupling agent KH550 grind to form fine powder, again alkylphenol polyoxyethylene is added in distilled water and dissolves, raised temperature to 85 ° about C, add the above-mentioned fine powder worn under 1000-1200 rev/min, stir the uniform mixed solution of formation, add nano-titania photocatalyst again, nano silicon, st-yrax n-butyl ether, ferric acetyl acetonade, rare earth element and remaining Silane coupling agent KH550 grinding distribution 0.5-1.0 hour, dry.
One of the present invention corrosion-resistant oxidation environment-friendly type glass door use coating, be made up of following concrete steps:
(1) deionized water, flow agent BYK-56, organic silicon modified by polyether emulsion, dimethyl dodecyl amine oxide, garlic polysaccharide, tea-polyphenol mixing are added in Scattered Kettle, to stir 3-5 minute under the condition of 600-800 rev/min;
(2) rotating speed is adjusted to 900-1000 rev/min, in Scattered Kettle, adds triethylene glycol monomethyl ether, polyoxyethylene oxypropylene oleic acid ester stirs 6-8 minute;
(3) rotating speed is adjusted to 1400-1600 rev/min, adds organosilicon crylic acid latex, Emulsion acrylic resin, chlorinated polyether resin emulsion stirring 15-25 minute;
(4) rotating speed is adjusted to 1000-1200 rev/min, adds hydramine alkoxy titanates, pigment, modified nano-titanium dioxide photocatalyst uniform stirring 20-30 minute successively;
(5) be added in sand mill and carry out grinding distribution by the material after dispersion, after filtering, fineness is less than 20 μm and packs.
Glass paint sticking power experiment (frame method) of the present invention≤1 grade, snappiness experiment≤1mm, impact experiment: 50cm, hardness: 3H, cut resistance test: 1 grade, water tolerance test (leaching distilled water 600 hours): without exception, resistance to boiling water experiment (100 ° of C >=25 hour): unchanged, ethanol-tolerant experiment (90% soaks 32 hours): without exception, artificial ageing resistance is tested: 1000 hours are non-foaming, do not peel off, flawless.
Claims (2)
1. a corrosion-resistant oxidation environment-friendly type glass door use coating, it is characterized in that, be made up of the raw material of following weight part: organosilicon crylic acid latex 8-10, Emulsion acrylic resin 43-46, chlorinated polyether resin emulsion 15-18, triethylene glycol monomethyl ether 1-3, hydramine alkoxy titanates 0.3-0.6, flow agent BYK-560.3-0.5, organic silicon modified by polyether emulsion 0.2-0.4, dimethyl dodecyl amine oxide 0.3-0.5, polyoxyethylene oxypropylene oleic acid ester 0.3-0.6, garlic polysaccharide 0.5-1.0, tea-polyphenol 0.5-1.0, modified nano-titanium dioxide photocatalyst 3-5, pigment 1-2, deionized water 10-15,
Described modified nano-titanium dioxide photocatalyst is made up of the raw material of following weight part: nano-titania photocatalyst 40-50, nano silicon 15-20, nano-tourmaline 10-15, binchotan 10-15, rare earth element 0.5-1.0, copper powder 0.7-1.4, silver powder 0.6-1.2, cobalt oxide powder 0.4-0.8, diatomite 8-12, alkylphenol polyoxyethylene 0.6-1.2, Silane coupling agent KH550 0.7-1.4, the salpeter solution 20-40 of 20%, the sodium hydroxide solution 20-40 of 30%, polyvinyl alcohol 1-2, st-yrax n-butyl ether 0.3-0.5, ferric acetyl acetonade 0.2-0.4, distilled water 100, diatomite is ground into particle and binchotan to be added in the salpeter solution of 20% and to soak 20 minutes by preparation method after high-temperature calcination, wash with water in neutral, to be immersed in the solution of the sodium hydroxide of 30% 30 minutes again, wash with water and add copper powder in neutral post-drying, silver powder, it is for subsequent use that cobalt oxide powder and 10-30% Silane coupling agent KH550 grind to form fine powder, again alkylphenol polyoxyethylene is added in distilled water and dissolves, raised temperature to 85 ° about C, add the above-mentioned fine powder worn under 1000-1200 rev/min, stir the uniform mixed solution of formation, add nano-titania photocatalyst again, nano silicon, st-yrax n-butyl ether, ferric acetyl acetonade, rare earth element and remaining Silane coupling agent KH550 grinding distribution 0.5-1.0 hour, dry.
2. a kind of corrosion-resistant oxidation environment-friendly type glass door use coating according to claim 1, is characterized in that, be made up of following concrete steps:
(1) deionized water, flow agent BYK-56, organic silicon modified by polyether emulsion, dimethyl dodecyl amine oxide, garlic polysaccharide, tea-polyphenol mixing are added in Scattered Kettle, to stir 3-5 minute under the condition of 600-800 rev/min;
(2) rotating speed is adjusted to 900-1000 rev/min, in Scattered Kettle, adds triethylene glycol monomethyl ether, polyoxyethylene oxypropylene oleic acid ester stirs 6-8 minute;
(3) rotating speed is adjusted to 1400-1600 rev/min, adds organosilicon crylic acid latex, Emulsion acrylic resin, chlorinated polyether resin emulsion stirring 15-25 minute;
(4) rotating speed is adjusted to 1000-1200 rev/min, adds hydramine alkoxy titanates, pigment, modified nano-titanium dioxide photocatalyst uniform stirring 20-30 minute successively;
(5) be added in sand mill and carry out grinding distribution by the material after dispersion, after filtering, fineness is less than 20 μm and packs.
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| CN201410568294.8A CN104449130A (en) | 2014-10-23 | 2014-10-23 | Corrosion-oxidation-resistant and environment-friendly waterborne coating for glass door and preparation method of waterborne coating |
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| CN201410568294.8A CN104449130A (en) | 2014-10-23 | 2014-10-23 | Corrosion-oxidation-resistant and environment-friendly waterborne coating for glass door and preparation method of waterborne coating |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106046991A (en) * | 2016-08-01 | 2016-10-26 | 安庆瑞泰化工有限公司 | Ash-sticking-proof waterborne coating and preparation method thereof |
| CN106147408A (en) * | 2016-08-14 | 2016-11-23 | 安庆市沁之源电器有限公司 | A kind of electric cooker high-temperature resistant coating and preparation method thereof |
| CN108129966A (en) * | 2017-12-19 | 2018-06-08 | 海洋化工研究院有限公司 | A kind of chlorinated polyether emulsion water-based anticorrosive paint |
| CN108952100A (en) * | 2018-08-13 | 2018-12-07 | 浙江云信装饰工程有限公司 | A kind of wall decoration coating plastering construction method |
| CN113861584A (en) * | 2021-09-14 | 2021-12-31 | 浙江亚厦装饰股份有限公司 | PVC (polyvinyl chloride) plate and manufacturing method thereof |
| CN114728215A (en) * | 2019-11-06 | 2022-07-08 | 陶氏东丽株式会社 | Water-soluble silicone defoamer composition and water-based coating containing same |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106046991A (en) * | 2016-08-01 | 2016-10-26 | 安庆瑞泰化工有限公司 | Ash-sticking-proof waterborne coating and preparation method thereof |
| CN106147408A (en) * | 2016-08-14 | 2016-11-23 | 安庆市沁之源电器有限公司 | A kind of electric cooker high-temperature resistant coating and preparation method thereof |
| CN108129966A (en) * | 2017-12-19 | 2018-06-08 | 海洋化工研究院有限公司 | A kind of chlorinated polyether emulsion water-based anticorrosive paint |
| CN108952100A (en) * | 2018-08-13 | 2018-12-07 | 浙江云信装饰工程有限公司 | A kind of wall decoration coating plastering construction method |
| CN114728215A (en) * | 2019-11-06 | 2022-07-08 | 陶氏东丽株式会社 | Water-soluble silicone defoamer composition and water-based coating containing same |
| CN114728215B (en) * | 2019-11-06 | 2023-09-22 | 陶氏东丽株式会社 | Water-soluble organosilicon defoamer composition and water-based paint containing same |
| CN113861584A (en) * | 2021-09-14 | 2021-12-31 | 浙江亚厦装饰股份有限公司 | PVC (polyvinyl chloride) plate and manufacturing method thereof |
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Application publication date: 20150325 |