CN104447090B - A kind of ecological organic fertilizer and preparation method thereof - Google Patents
A kind of ecological organic fertilizer and preparation method thereof Download PDFInfo
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- CN104447090B CN104447090B CN201410708931.7A CN201410708931A CN104447090B CN 104447090 B CN104447090 B CN 104447090B CN 201410708931 A CN201410708931 A CN 201410708931A CN 104447090 B CN104447090 B CN 104447090B
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
- C05D9/02—Other inorganic fertilisers containing trace elements
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Pest Control & Pesticides (AREA)
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- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a kind of ecological organic fertilizer, including following parts by weight component：100 150 parts of 70 80 parts of Negundo Chastetree Leaf, 30 40 parts of green manure, 10 20 parts of Dalmatian chrysanthemum, 20 40 parts of molasses, 0.4 0.6 parts of Choline Chloride, 0.1 2 parts of antibacterial peptide, 13 parts of trace element, 5 parts of amino acid/11,14 parts of biological bacteria, 23 parts of dispersant, 3 10 parts of water-loss reducer and water.The present invention has the advantages that low cost, fertilizer efficiency high, prevention and elimination of disease and pests, reduction environmental pollution, improved soil and fertilizer aggreggate utility are high.
Description
Technical field
The present invention relates to environmental protection and technical field of biological fertilizer, more particularly to a kind of ecological organic fertilizer and its making side
Method.
Background technology
China's crop acreage is big, and agricultural provides the basic product of the support development of the national economy and development.Fertilizer
Be can for plant growth provide indispensable nutrition, improve soil property, a horizontal class material of increasing soil fertility, be agriculture
One of material base of industry production.
The long-term use of chemical fertilizer, easily causes all kinds of nutrients ratio imbalances, farmland ecosystem in soil hardening, soil
Destroyed, the profitable strain reduction in soil, less able disease-resistant crops, heavy metal and toxic element increase, agricultural product
Quality decline and the problems such as cause environmental pollution.
Ecological organic fertilier refer to microorganisms with specific functions with mainly with plant and animal residues, such as feces of livestock and poultry, agricultural crop straw
Microbial manure and organic fertilizer effect are had concurrently Deng for source and through the class that harmless treatment, the organic materials for becoming thoroughly decomposed are composited
Fertilizer.Ecological organic fertilier nutrient is complete, can improve soil physical and chemical property, enhancing soil water-retaining, fertilizer conservation, the energy of fertilizer
Power.Beneficial microbe in ecological organic fertilier into forming mutual symbiosis Relationship With Proliferation with Soil Microorganism after soil,
Suppress harmful bacteria growing and be converted into beneficial bacterium, interact, mutually promote, play the synergy of colony, be a kind of environmental protection
Type fertilizer.
Liquid fertilizer is fast with fertilizer efficiency compared with solid fertilizer, will not lump, and application method is various, production, transport and
The advantages of polluting few when using.
Existing ecological organic fertilizer also has that nutritional ingredient is not complete, fertilizer efficiency is poor, the duration is shorter, does not have concurrently or not kills
The shortcomings of bacterium, insecticidal action.
The content of the invention
The invention provides a kind of ecological organic fertilizer and preparation method thereof.The ecological organic fertilier that the present invention is provided has battalion
Form point abundant, long using simple, the fertilizer efficiency duration, the advantages of have sterilized, insecticidal action concurrently.
The present invention provide technical scheme be：
A kind of ecological organic fertilizer, including following parts by weight component：Negundo Chastetree Leaf 70-80 parts, green manure 30-40 parts, remove
10-20 parts of worm chrysanthemum, molasses 20-40 parts, Choline Chloride 0.4-0.6 parts, antibacterial peptide 0.1-2 parts, 1-3 parts of trace element, amino acid
1-5 parts, biological bacteria 1-4 parts, dispersant 2-3 parts, water-loss reducer 3-10 parts and water 100-150 parts.
Preferably, in described ecological organic fertilizer, it is made up of the component of following parts by weight：It is 75 parts of Negundo Chastetree Leaf, green
35 parts of fertilizer, 15 parts of Dalmatian chrysanthemum, 30 parts of molasses, 0.5 part of Choline Chloride, 1 part of antibacterial peptide, 2 parts of trace element, 3 parts of amino acid, biology
125 parts of 3 parts of bacterium, 2.5 parts of dispersant, 6 parts of water-loss reducer and water.
Preferably, in described ecological organic fertilizer, the biological bacteria is thin nitrogen-fixing bacteria, phosphate solubilizing bacteria, potassium solubilizing bacteria, ammonification
Any one or a few in bacterium and nitrobacteria.
Preferably, in described ecological organic fertilizer, the green manure be sweet potato, pea, Cassia, bamboo beans and Gui fiber crops in
Any one or a few, the water content of the green manure is 30-80%.
Preferably, in described ecological organic fertilizer, the trace element is any one in iron, copper, zinc, manganese or boron
Plant or several.
Preferably, in described ecological organic fertilizer, the water is magnetized water.
A kind of preparation method of ecological organic fertilizer, comprises the following steps：
Step one, be to be put into parts by weight in fermentation vat after 75 parts of Negundo Chastetree Leaf is crushed, backward fermentation vat in addition
Parts by weight are 15 parts of molasses and 75 parts of water, are sealed after stirring, and in the 30-40h that fermented at 50-70 DEG C, filtering to send out
Zymotic fluid, it is standby；
Step 2, the zymotic fluid that will be leached in step one are fitted into extraction kettle, start CO 2 high pressure pump, carry out dioxy
Change carbon supercritical extract, after cycling extraction 1-5h, termination of pumping is depressurized to 5-6MPa, extract is collected, it is standby；
Step 3, with the alkaloid that extract surface is floated in siphon pipe extraction step two, collect alkaloid, it is standby；
Step 4, take the Dalmatian chrysanthemum that parts by weight are 15 parts flower dry in the shade after be milled, cross 150-120 mesh sieve take sieve
Lower thing, obtains the attritive powder of Dalmatian chrysanthemum flower, standby；
Step 5, by parts by weight it is 35 parts of green manure and is put into fermentation vat after the root, stem and leaf of 15 parts of Dalmatian chrysanthemum is crushed
In, backward fermentation vat in add parts by weight be 15 parts of molasses and 50 parts of water, sealed after stirring, in 50-70 DEG C
Lower fermentation 30-40h, filters to obtain zymotic fluid, standby；
Step 6, the alkaloid that will be collected in step 3 are put into stirring pool, then to addition Choline Chloride 0.5 in stirring pool
6 parts of part, 1 part of antibacterial peptide, 3 parts of biological bacteria, 2 parts of trace element, 3 parts of amino acid, 2.5 parts of dispersant and water-loss reducer, and step
Gained zymotic fluid in the attritive powder and step 5 of obtained Dalmatian chrysanthemum flower, stirs in four, obtains final product ecological organic fertilizer.
Preferably, in the preparation method of described ecological organic fertilizer, the water-loss reducer is Polyacrylamide Powder.
Preferably, in the preparation method of described ecological organic fertilizer, in the step 2, the carbon dioxide is super to be faced
Boundary extraction reaction condition be：The pressure of supercritical carbon dioxide is 10-18MPa, and flow is 8-20L/h, and extraction kettle temperature is
32-40℃。
The invention provides a kind of ecological organic fertilizer and preparation method thereof.It is first in the alkaloid in extracting Negundo Chastetree Leaf
First by the way of first fermenting, fermentation energy destroys the cell membrane of plant, is conducive to the dissolution of active ingredient, is effectively improved life
The recovery rate of alkaloids, and fermentation energy kills most of harmful microorganism and worm's ovum；Separated by carbon dioxide supercritical extraction again
Active ingredient in extract, supercritical extract using supercritical carbon dioxide as extractant, with nontoxic, residual in the absence of solvent
Stay, free from environmental pollution and extract and separate rate high the advantages of.During the fermentation using molasses as fermentation substrate, molasses are sugaring works
The byproduct of industry, if being underutilized, easily causes environmental pollution and the wasting of resources, and molasses are together with other plant and animal residuess
Fermentation, becomes the value bio-organic fertilizer rich in amino acid, fulvic acid, humic acid etc. very high.Add in liquid fertilizer
Added alkaloid, its play the role of uniqueness except insect pest pharmacological action and promote plant growth；Non- antibiosis is with the addition of in liquid fertilizer
Plain series bactericidal agent-antibacterial peptide, antibacterial peptide has heat endurance good, broad-spectrum antiseptic, the advantages of having no drug resistance；Be with the addition of in liquid fertilizer
Choline Chloride, Choline Chloride is a kind of plant photosynthesis promoter, has obvious effect to increasing yield；Added in liquid fertilizer
The Dalmatian chrysanthemum of botanical pesticide one, Dalmatian chrysanthemum can not only remove mosquito-killing, and can kill crops and forest, the evil of fruit tree
Worm；Beneficial organism bacterium is with the addition of in liquid fertilizer, the biological bacterias such as nitrogen-fixing bacteria, phosphate solubilizing bacteria, potassium solubilizing bacteria is imposed on into plant, decompose it,
The nutrients such as nitrogen, phosphorus, potassium in absorption air, soil, make the comprehensive source of manure of formation life and growth in nature in soil, reach voluntarily fertilizer.
The zymotic fluid of green manure is with the addition of in liquid fertilizer, green manure is a kind of complete biology source of manure of nutrient, can provide abundant supporting for soil
Point, insoluble Nutrient Transformation in soil can be made, it is beneficial to the absorption of crop, the physicochemical property of soil can be improved, promote soil
The activity of microorganism.Water-loss reducer is with the addition of in liquid fertilizer, water-loss reducer is a kind of especially strong functional high-polymer material of water absorbing capacity
Material, it is nontoxic, water, water suction are released repeatedly, moreover it is possible to absorbed fertilizer, agricultural chemicals and slowly discharged, increase fertilizer efficiency, drug effect.Present invention tool
Have that low cost, fertilizer efficiency are high, amount of increase in production is big, prevention and elimination of disease and pests, reduce environmental pollution, improved soil, retain water and nutrients, fertilizer synthesis
Using it is high, crop nutritional quality and yield can be improved the advantages of.
Specific embodiment
With reference to embodiment, the present invention is described in further detail, to make those skilled in the art with reference to specification
Word can be implemented according to this.
Embodiment 1：
A kind of ecological organic fertilizer, including following parts by weight component：70 parts of Negundo Chastetree Leaf, 30 parts of sweet potato, Dalmatian chrysanthemum 10
Part, 20 parts of molasses, 0.4 part of Choline Chloride, 0.1 part of antibacterial peptide, 1 part of trace element, amino acid/11 part, 1 part of nitrogen-fixing bacteria, dispersant 2
100 parts of part, 3 parts of polyacrylamide and magnetized water.
A kind of preparation method of ecological organic fertilizer, comprises the following steps：
Step one, be to be put into parts by weight in fermentation vat after 70 parts of Negundo Chastetree Leaf is crushed, backward fermentation vat in addition
Parts by weight are 10 parts of molasses and 55 parts of magnetized water, are sealed after stirring, and in the 30h that fermented at 50 DEG C, filtering to ferment
Liquid, it is standby；
Step 2, the zymotic fluid that will be leached in step one are fitted into extraction kettle, start CO 2 high pressure pump, to extraction kettle
In be passed through the supercritical carbon dioxide that pressure is 10MPa, control the flow of carbon dioxide for 8L/h, extraction kettle temperature is 32 DEG C,
After cycling extraction 1h, termination of pumping is depressurized to 5MPa, collects extract, standby；
Step 3, with the alkaloid that extract surface is floated in siphon pipe extraction step two, collect alkaloid, it is standby；
Step 4, take the Dalmatian chrysanthemum that parts by weight are 10 parts flower dry in the shade after be milled, cross 120 mesh sieve take sieve under
Thing, obtains the attritive powder of Dalmatian chrysanthemum flower, standby；
Step 5, it is after 30 parts of water content are 30% sweet potato and the root, stem and leaf of 10 parts of Dalmatian chrysanthemum is crushed by parts by weight
Be put into fermentation vat, backward fermentation vat in add parts by weight be 10 parts of molasses and 45 parts of magnetized water, after stirring
Sealing, in the 30h that fermented at 50 DEG C, filters to obtain zymotic fluid, standby；
Step 6, the alkaloid that will be collected in step 3 are put into stirring pool, then to addition Choline Chloride 0.5 in stirring pool
3 parts of part, 0.1 part of antibacterial peptide, 1 part of nitrogen-fixing bacteria, 1 part of trace element, amino acid/11 part, 2 parts of dispersant and polyacrylamide, and
Gained zymotic fluid in the attritive powder and step 5 of obtained Dalmatian chrysanthemum flower, stirs in step 4, obtains final product ecological organic
Liquid fertilizer.
Embodiment 2：
A kind of ecological organic fertilizer, including following parts by weight component：80 parts of Negundo Chastetree Leaf, 40 parts of pea, Dalmatian chrysanthemum 20
Part, 40 parts of molasses, 0.6 part of Choline Chloride, 2 parts of antibacterial peptide, 3 parts of trace element, 5 parts of amino acid, 4 parts of phosphate solubilizing bacteria, dispersant 3
150 parts of part, 10 parts of polyacrylamide and magnetized water.
A kind of preparation method of ecological organic fertilizer, comprises the following steps：
Step one, be to be put into parts by weight in fermentation vat after 80 parts of Negundo Chastetree Leaf is crushed, backward fermentation vat in addition
Parts by weight are 20 parts of molasses and 85 parts of magnetized water, are sealed after stirring, and in the 40h that fermented at 70 DEG C, filtering to ferment
Liquid, it is standby；
Step 2, the zymotic fluid that will be leached in step one are fitted into extraction kettle, start CO 2 high pressure pump, to extraction kettle
In be passed through the supercritical carbon dioxide that pressure is 18MPa, control the flow of carbon dioxide for 20L/h, extraction kettle temperature is 40 DEG C,
After cycling extraction 5h, termination of pumping is depressurized to 6MPa, collects extract, standby；
Step 3, with the alkaloid that extract surface is floated in siphon pipe extraction step two, collect alkaloid, it is standby；
Step 4, take the Dalmatian chrysanthemum that parts by weight are 20 parts flower dry in the shade after be milled, cross 150 mesh sieve take sieve under
Thing, obtains the attritive powder of Dalmatian chrysanthemum flower, standby；
Step 5, it is after 40 parts of water content are 50% pea and the root, stem and leaf of 20 parts of Dalmatian chrysanthemum is crushed by parts by weight
Be put into fermentation vat, backward fermentation vat in add parts by weight be 20 parts of molasses and 65 parts of magnetized water, after stirring
Sealing, in the 40h that fermented at 70 DEG C, filters to obtain zymotic fluid, standby；
Step 6, the alkaloid that will be collected in step 3 are put into stirring pool, then to addition Choline Chloride 0.6 in stirring pool
10 parts of part, 2 parts of antibacterial peptide, 4 parts of phosphate solubilizing bacteria, 3 parts of trace element, 5 parts of amino acid, 3 parts of dispersant and polyacrylamide, Yi Jibu
Gained zymotic fluid in the attritive powder and step 5 of obtained Dalmatian chrysanthemum flower, stirs in rapid four, obtains final product ecological organic liquor
Fertilizer.
Embodiment 3：
A kind of ecological organic fertilizer, including following parts by weight component：75 parts of Negundo Chastetree Leaf, 35 parts of bamboo beans, Dalmatian chrysanthemum 15
Part, 30 parts of molasses, 0.5 part of Choline Chloride, 1 part of antibacterial peptide, 2 parts of trace element, 3 parts of amino acid, 3 parts of nitrobacteria, dispersant
125 parts of 2.5 parts, 6 parts of polyacrylamide and magnetized water.
A kind of preparation method of ecological organic fertilizer, comprises the following steps：
Step one, be to be put into parts by weight in fermentation vat after 75 parts of Negundo Chastetree Leaf is crushed, backward fermentation vat in addition
Parts by weight are 15 parts of molasses and 75 parts of magnetized water, are sealed after stirring, and in the 35h that fermented at 60 DEG C, filtering to ferment
Liquid, it is standby；
Step 2, the zymotic fluid that will be leached in step one are fitted into extraction kettle, start CO 2 high pressure pump, to extraction kettle
In be passed through the supercritical carbon dioxide that pressure is 14MPa, control the flow of carbon dioxide for 14L/h, extraction kettle temperature is 36 DEG C,
After cycling extraction 3h, termination of pumping is depressurized to 5.5MPa, extract is collected, it is standby；
Step 3, with the alkaloid that extract surface is floated in siphon pipe extraction step two, collect alkaloid, it is standby；
Step 4, take the Dalmatian chrysanthemum that parts by weight are 15 parts flower dry in the shade after be milled, cross 130 mesh sieve take sieve under
Thing, obtains the attritive powder of Dalmatian chrysanthemum flower, standby；
Step 5, it is after 35 parts of water content are 80% bamboo beans and the root, stem and leaf of 15 parts of Dalmatian chrysanthemum is crushed by parts by weight
Be put into fermentation vat, backward fermentation vat in add parts by weight be 15 parts of molasses and 50 parts of magnetized water, after stirring
Sealing, in the 35h that fermented at 60 DEG C, filters to obtain zymotic fluid, standby；
Step 6, the alkaloid that will be collected in step 3 are put into stirring pool, then to addition Choline Chloride 0.5 in stirring pool
6 parts of part, 1 part of antibacterial peptide, 3 parts of nitrobacteria, 2 parts of trace element, 3 parts of amino acid, 2.5 parts of dispersant and polyacrylamide, with
And in step 4 in the attritive powder and step 5 of obtained Dalmatian chrysanthemum flower gained zymotic fluid, stir, obtaining final product ecology has
Machine liquid fertilizer.
Although embodiment of the present invention is disclosed as above, it is not restricted to listed in specification and implementation method
With, it can be applied to various suitable the field of the invention completely, for those skilled in the art, can be easily
Other modification is realized, therefore under the universal limited without departing substantially from claim and equivalency range, the present invention is not limited
In specific details and shown here as the embodiment with description.
Claims (3)
1. a kind of preparation method of ecological organic fertilizer, it is characterised in that comprise the following steps：
Step one, be to be put into parts by weight in fermentation vat after 75 parts of Negundo Chastetree Leaf is crushed, backward fermentation vat in add weight
Number is 15 parts of molasses and 75 parts of water, is sealed after stirring, and in the 30-40h that fermented at 50-70 DEG C, filters to obtain zymotic fluid,
It is standby；
Step 2, the zymotic fluid that will be leached in step one are fitted into extraction kettle, start CO 2 high pressure pump, carry out carbon dioxide
Supercritical extract, after cycling extraction 1-5h, termination of pumping is depressurized to 5-6MPa, collects extract, standby；
Step 3, with the alkaloid that extract surface is floated in siphon pipe extraction step two, collect alkaloid, it is standby；
Step 4, take the Dalmatian chrysanthemum that parts by weight are 15 parts flower dry in the shade after be milled, cross 150-120 mesh sieve take sieve under
Thing, obtains the attritive powder of Dalmatian chrysanthemum flower, standby；
Step 5, by parts by weight it is 35 parts of green manure and is put into fermentation vat after the root, stem and leaf of 15 parts of Dalmatian chrysanthemum is crushed, it
The molasses and 50 parts of water that parts by weight are 15 parts are added in backward fermentation vat, is sealed after stirring, in fermentation at 50-70 DEG C
30-40h, filters to obtain zymotic fluid, standby；
Step 6, the alkaloid that will be collected in step 3 are put into stirring pool, then in stirring pool add 0.5 part of Choline Chloride,
6 parts of 1 part of antibacterial peptide, 3 parts of biological bacteria, 2 parts of trace element, 3 parts of amino acid, 2.5 parts of dispersant and water-loss reducer, and in step 4
Gained zymotic fluid, stirs in the attritive powder and step 5 of obtained Dalmatian chrysanthemum flower, obtains final product ecological organic fertilizer.
2. the preparation method of ecology organic fertilizer as claimed in claim 1, it is characterised in that the water-loss reducer is polyacrylamide
Amine powder.
3. the preparation method of ecology organic fertilizer as claimed in claim 1, it is characterised in that in the step 2, described two
The reaction condition of carbonoxide supercritical extract is：The pressure of supercritical carbon dioxide is 10-18MPa, and flow is 8-20L/h, extraction
Kettle temperature degree is taken for 32-40 DEG C.
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| CN104447090A (en) | 2015-03-25 |
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