CN104446803B - high nitrogen type water-soluble fertilizer containing fulvic acid - Google Patents
high nitrogen type water-soluble fertilizer containing fulvic acid Download PDFInfo
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- CN104446803B CN104446803B CN201410742221.6A CN201410742221A CN104446803B CN 104446803 B CN104446803 B CN 104446803B CN 201410742221 A CN201410742221 A CN 201410742221A CN 104446803 B CN104446803 B CN 104446803B
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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Abstract
The invention discloses a kind of high nitrogen type water-soluble fertilizer containing fulvic acid, it includes the element of following weight percent：Nitrogen 25% 35%, phosphorus 5% 15%, potassium 5% 15%, zinc 0.01% 0.3%, boron 0.01% 0.3%, magnesium 0.01% 0.3%, manganese 0.01% 0.3%, ferrum 0.01% 0.3%, fulvic acid 0.5% 2%.The water-soluble chemical fertilizer of high nitrogen type containing fulvic acid of the present invention, comprehensive nutrition are balanced, meet needed for plant growing, wherein containing appropriate fulvic acid, can be effectively promoted the absorption nutritional labeling of plant, quickly grow vigorously.
Description
Technical field
The present invention relates to a kind of full nutritive element water-soluble fertilizer containing fulvic acid, belongs to agricultural fertilizer technical field.
Background technology
As the development of chemical industry, the consumption of chemical fertilizer increase sharply, its life-time service generates very big shadow to soil
Ring, the part for utilizing absorbed by crops also only accounts for the 30%-40% of sowing amount, and remaining is present in soil, contaminated soil, shadow
Agricultural ecological is rung, when serious, even the salinization of soil is directly resulted in.Plus for a long time, Planting household applies N, P, K a great number of elements partially
Fertilizer, ignores the supplement of middle trace element, causes the nutritional labeling in soil unbalance so that plant effectively cannot absorb.
While planting cost is greatly increased, income does not but effectively improve.With the development of high-efficiency agriculture in recent years, sprinkling irrigation,
The application of drip irrigation technique, more and more extensive therefore new, the unique full nutrition unit of high-load, complete water-soluble Fertilizer application
Plain water-soluble fertilizer research and development are very urgent.
In recent years, increasing enterprise participates in the research and development of water soluble fertilizer and produces with mechanism, production technology
It is similar with the selection of raw material.Using primary raw material have carbamide, ammonium sulfate, ammonium chloride, MAP, Diammonium phosphate (DAP),
Potassium dihydrogen phosphate, magnesium potassium sulfate, water soluble organic substance and middle trace element etc., these raw materials through pulverization process, according to certain
Ratio mix homogeneously makes corresponding water soluble fertilizer.
The water-soluble fertilizer product of prior art mixture is primarily present following problem:(1) outward appearance is bad.Be mainly reflected in color and luster,
In the discordance of granularity.(2) product high humidity, causes caking, impact to use and sell.
In recent years, biochemical fertilizer is gradually valued by the people with its unique growth-promoting effect.Wherein fulvic acid is with plant
Growth regulating, drought resisting are projected against growth, are particularly taken seriously.Traditional fulvic acid is extracted from low-grade coal
, also there is the biochemical fulvic acid obtained through biofermentation.But the easy moisture absorption of fulvic acid itself, is simply added to water-soluble fertilizer
In, easily there is the problems such as mixing inequality, high humidity, in the case that chemical fertilizer storage condition is not good, even more easily occur a large amount of
Caking, has a strong impact on the use of chemical fertilizer.
Chinese patent CN102351604A discloses a kind of Fulvic acid organic fertilizer material, it include nitrogen 3%～7%, phosphorus 3%～
7%th, potassium 3%～7%, aminoacid 8%～12%, organic matter 25%～35%, fulvic acid 15%～25% and plant growing is adjusted
Section agent 4%～6%.Containing active very strong organic component, microorganism growth can be greatly promoted, promote plant growing.But
Substantial amounts of aminoacid, organic matter and fulvic acid are wherein used, is extremely easily made moist, back plate of making moist is formed block and is difficult with.And
And, as the fulvic acid addition for wherein using is very big, after fertilising, fulvic acid utilization rate is not high, and microorganism growth excessively goes back shadow
Oxygen content in soil is rung, is unfavorable for plant growing on the contrary.
Chinese patent CN102381922A discloses a kind of potassium fulvate fertilizer, and it includes：Nitrogen 10%～15%, biological clamps
2%～6%, aminoacid 0.5%～3%, Organic substance 25%～35%, fulvic acid 10%～15%, trace element 11%～
15%th, rare earth 3%～6%, swelling agent 0.1%～2%, vegetable protein 0.1%～2% and chitin 0.1%～3%.Its energy
Enough promote plant stalk healthy and strong, improve fruit quality, strengthen plant cold tolerance, but equally exist hygroscopic component content mistake
Big problem, it is difficult to long-term to preserve.And after applying fertilizer, microorganism easily occur and excessively increase sharply, plant growing is affected, fulvic acid is reduced
The problem of utilization rate.
In addition, existing chemical fertilizer mostly is single fertilizer, even a few nutrient is generally also only contained in compound fertilizer, and
Indivedual micronutrient levelss it is low even without.Especially water soluble fertilizer product, more than 90% is only nitrogenous, phosphorus, potassium and part are micro-
To for water-soluble chemical fertilizer, secondary element, requires that high drip irrigation agricultural production causes serious restriction.
The content of the invention
It is an object of the invention to overcome in prior art chemical fertilizer nutrient easily not occur inhaling in complete, fulvic acid application
A kind of deficiency of wet caking, there is provided full nutritive element water-soluble fertilizer containing fulvic acid.Overcome water-soluble fertilizer element in prior art
Incomplete, application effect is not good, the defect or deficiency of fulvic acid chemical fertilizer easily caking.
In order to realize foregoing invention purpose, the invention provides technical scheme below：
A kind of high nitrogen type water-soluble fertilizer containing fulvic acid, it includes the element or composition of following weight percent：Nitrogen
25%-35%, phosphorus 5%-15%, potassium 5%-15%, zinc 0.01%-0.3%, boron 0.01%-0.3%, magnesium 0.01%-0.3%,
Manganese 0.01%-0.3%, ferrum 0.01%-0.3%, fulvic acid 0.5%-2%.
It is preferred that nitrogen 28-32%, phosphorus 7%-12%, potassium 7-12%, zinc 0.01%-0.1%, boron 0.01%-0.1%, magnesium
0.01%-0.1%, manganese 0.01%-0.1%, ferrum 0.01%-0.1%, fulvic acid 1%-1.5%.
Further, the nitrogen with：The form addition of one or more compoundings in carbamide, MAP and potassium nitrate
In fertilizer.
Further, the P elements are added in fertilizer in the form of potassium dihydrogen phosphate and/or MAP.
Further, the potassium element is with the shape of any one or a few compounding in potassium nitrate, potassium dihydrogen phosphate and potassium sulfate
In formula addition fertilizer.
Further, the trace element zinc, boron, magnesium, manganese, ferrum respectively with：Zinc sulfate, Borax, magnesium sulfate, manganese sulfate, sulfur
The form of sour ferrum is added in fertilizer.
Further, the high nitrogen type water-soluble fertilizer containing fulvic acid, it is made up of the composition of following weight percent
's：Carbamide 60-70 parts, potassium nitrate 0-19 parts, MAP 9-26 parts, potassium dihydrogen phosphate 10-27 parts, potassium sulfate 0-10 parts.It is excellent
Select carbamide 62-64 parts, MAP 20-24 parts, potassium dihydrogen phosphate 10-12 parts, potassium sulfate 8-10 parts.
Present invention also offers a kind of method for preparing above-mentioned chemical fertilizer, it comprises the following steps：
(1) part weighs raw material by weight proportion, is placed in Sealing Arrangement and mixes；
(2) raw material of mix homogeneously is crushed in air drying type disintegrating apparatus；
(3) by subpackage in the raw material drying environment after crushing, (air Jing dehumidification treatments, humidity had both obtained finished product less than 20%)
Chemical fertilizer.
Compared with prior art, beneficial effects of the present invention：
The water-soluble chemical fertilizer of high nitrogen type containing fulvic acid of the present invention, comprehensive nutrition are balanced, meet needed for plant growing, wherein containing
There is appropriate fulvic acid, the absorption nutritional labeling of plant can be effectively promoted, quickly grown vigorously.And the present invention's is water-soluble
In chemical fertilizer, each component can be mutually coordinated, not there is a problem of that local moisture absorption is too strong, effectively solve chemical fertilizer after being uniformly dispersed
Easy moisture absorption caking, the problem for affecting to use during storage.
Specific embodiment
With reference to test example and specific embodiment, the present invention is described in further detail.But this should not be understood
Scope for above-mentioned theme of the invention is only limitted to below example, and all technologies realized based on present invention belong to this
The scope of invention.In the present invention, not specified percentage ratio is weight percentage.
Embodiment 1
Take carbamide 60kg, potassium nitrate 10kg, MAP 15kg, potassium dihydrogen phosphate 20kg, Borax 0.2kg, zinc sulfate
0.3kg, iron sulfate 1.3kg, manganese sulfate 0.1 and magnesium sulfate 0.93kg are placed in Sealing Arrangement and mix, in air drying type disintegrating apparatus
Crush 20 mesh sieves, add fulvic acid 1.5kg, mix homogeneously, in dry environment, subpackage (humidity is less than 16%), is distributed into 5kg
Per bag (common plasticses bag), obtains high nitrogen type (N>30%) finished product chemical fertilizer about 109kg.
Embodiment 2
Take carbamide 68kg, MAP 20kg, potassium dihydrogen phosphate 10kg, potassium sulfate 10kg, Borax 0.2kg, zinc sulfate
0.3kg, iron sulfate 0.6kg, manganese sulfate 1.8 and magnesium sulfate 0.93kg are placed in Sealing Arrangement and mix, in air drying type disintegrating apparatus
20 mesh sieves were crushed, adds fulvic acid 1.5kg, mix homogeneously in dry environment (humidity is less than 16%), to be distributed into per bag of 5kg
(common plasticses bag), obtains high nitrogen type (N>33%) finished product chemical fertilizer 113kg.
Embodiment 3
Take carbamide 70kg, MAP 9kg, potassium dihydrogen phosphate 27kg, potassium sulfate 4kg, Borax 0.2kg, zinc sulfate
0.4kg, iron sulfate 0.6kg, manganese sulfate 1.8 and magnesium sulfate 1.03kg are placed in Sealing Arrangement and mix, in air drying type disintegrating apparatus
20 mesh sieves were crushed, fulvic acid 1.7kg was added, mix homogeneously, subpackage in dry environment were distributed into per bag of 5kg (common plasticses
Bag), obtain finished product chemical fertilizer about 114kg (N>33%, P>7%, K>8%).
Embodiment 4
Take carbamide 114kg, potassium nitrate 19kg, MAP 47kg, potassium dihydrogen phosphate 24kg, potassium sulfate 7kg, Borax
0.2kg, zinc sulfate 0.4kg, iron sulfate 0.6kg, manganese sulfate 1.8 and magnesium sulfate 1.03kg are placed in Sealing Arrangement and mix, and air-dry
20 mesh sieves were crushed in formula disintegrating apparatus, fulvic acid 1.7kg was added, mix homogeneously, subpackage in dry environment were distributed into 5kg every
Bag (common plasticses bag), obtains finished product chemical fertilizer about 114kg (N>28%, P>8%, K>8%).
Comparative example 1
Take carbamide 10kg, it is potassium nitrate 30kg, aminoacid 2kg, fulvic acid 12kg, zinc sulfate 0.5kg, iron sulfate 0.2kg, swollen
Big agent 0.1kg, vegetable protein 0.5kg and chitin 0.6kg, after crushing 20 mesh sieves respectively, mix homogeneously divides in dry environment
Dress, is distributed into per bag of 5kg (common plasticses bag), obtains finished product chemical fertilizer about 55kg.
Wettability test
The bagged chemical fertilizer of Example 1-4 and comparative example is each 10 bags, in being placed in ambient humidity more than 95% dark environment,
Per group of 5 bags of identical chemical fertilizer are stacked into perpendicular row, and chemical fertilizer heap bottom is supported with smooth plastic stent, and 15cm is high from the ground, and chemical fertilizer must not
Contact with wall, must not contact between adjacent chemical fertilizer heap, mutual spacing at least 40cm.Took from chemical fertilizer heap every 1 week topmost
One bag, open observation caking situation.Before test, free-running property is designated as 10 points, note 7-9 that slight caking handss can be twisted into pieces later
Point, note 4-6 that part caking apparatus can be crushed point, overall 1-3 point of fine broken note of luming, entirety ties closely knit lump and difficulty
With 0 point of the note destroyed, remaining.Statistical result is as follows：
The fertilizer of the present invention occurs in that local caking in the first Zhou Shijun, but is mainly being close to the surface fertilizer of packaging bag
There is caking, caking growth is more slow in 4 weeks afterwards, there is no to occur the complete hardened situation into closely knit piece.And contrast
Example then occurs in that serious agglomeration problems, has formed closely knit piece completely at 3 weeks, has lost substantially use value.It can be seen that send out
Bright full nutrition water-soluble fertilizer solves the problems, such as easy moisture absorption caking in fulvic acid addition chemical fertilizer well.
Caulis et Folium Brassicae capitatae applies water yield element water-soluble fertilizer field demonstration test
1 materials and methods
1.1 for examination soil：Experimental plot ground is in Pingba, has a moderate climate, abundant rainfall；For try soil belong to rice soil subclass,
Ooze and educate greyish brown damp field penus, greyish brown damp sand mud field soil species, in topsoil quality, earth, soil fertility level are medium.
1.2 for examination fertilizer：Water soluble fertilizer prepared by 3 mode of embodiment
1.3 for studying thing：Caulis et Folium Brassicae capitatae (kind is West Garden)
1.4 demonstration tests are designed
Water-soluble fertilizer demonstration prepared by 3 mode of foliage-spray embodiment, area 5.6 are carried out on the basis of conventional fertilizer application
Mu, Caulis et Folium Brassicae capitatae are sprayed after transplanting 30 days for the first time, spray altogether three times later spray every 10 days once, and per mu is used a great number of elements water-soluble every time
75 grams of fertilizer converts 60 kilograms of clear water.5 fields are selected in demonstration area, same field contrast test is carried out.At contrast test arranges 2
Reason, is processed, trench digging isolation between process, and protection row is stopped around test field, selects the Caulis et Folium Brassicae capitatae of ad eundem to transplant, and process content is such as
Under：
(1) (Caulis et Folium Brassicae capitatae sprays after transplanting 30 days for the first time conventional fertilizer application, sprays altogether three times later spray every 15 days once, and per mu every
60 kilograms of secondary use clear water.
(2) the water-soluble fertilizer that prepared by 3 mode of conventional fertilizer application+embodiment (Caulis et Folium Brassicae capitatae transplant 30 days after spray for the first time, later every
Spray in 15 days sprays once, altogether three times, per mu every time with a great number of elements water-soluble fertilizer 75 grams convert 60 kilograms of clear water.
Whole district's harvesting method is taken to harvest with field contrast test and demonstration field.
2nd, result and analysis
The impact of water-soluble fertilizer prepared by 2.1 administration 3 modes of embodiment to Caulis et Folium Brassicae capitatae biological character
The contrast field Caulis et Folium Brassicae capitatae of table 1 applies the biological economy character analysis of water-soluble fertilizer
Unit：Kilogram
The Caulis et Folium Brassicae capitatae growing way for spraying the mu model field of water-soluble fertilizer prepared by 3 mode of embodiment is vigorous, Caulis et Folium Brassicae capitatae no matter plant height, list
Strain commodity weight is superior to clear water control (table 1).
The impact of water-soluble fertilizer prepared by 2.2 administration 3 modes of embodiment to Caulis et Folium Brassicae capitatae yield
2 Caulis et Folium Brassicae capitatae of table applies water-soluble fertilizer comparative test result
Unit：Kg/acre
Caulis et Folium Brassicae capitatae is applied the comparative test result of water-soluble fertilizer prepared by 3 mode of embodiment and is shown in Table 2.Caulis et Folium Brassicae capitatae foliage-spray is water-soluble
4595.9 kilograms of the average yield per mu of fertilizer, more flat than clear water control mu to increase production 358.5 kilograms, amount of increase in production reaches 8.5%.Jing t are surveyed
Examination, processes average yield difference between 1 and process 2 and reaches pole significant level (t=6.24>t0.01).Illustrate that foliage-spray is water-soluble
Fertilizer is to Caulis et Folium Brassicae capitatae growth with facilitation.
Demonstration area also achieves and same field contrast test identical result.5.6 mu of model field Caulis et Folium Brassicae capitataes average yield per mu 4506.2
Kilogram, average mu increases production 347.5 kilograms, rate of growth 8.1%.
2.3 economic benefits for applying water-soluble fertilizer
3 Caulis et Folium Brassicae capitatae of table applies the performance analysis of water-soluble fertilizer contrast test
Unit：Kilogram
Remarks：Drug prices of market：2.0 yuan/kilogram of Caulis et Folium Brassicae capitatae, 4.5 yuan/kilogram of a great number of elements water-soluble fertilizer, foliage-spray
Once 5.0 yuan of calculating of every mu of labour cost.
Although from Economic and Efficiency Analysis as can be seen that Caulis et Folium Brassicae capitatae sprays water-soluble fertilizer prepared by 3 mode of embodiment than clear water pair
According to increased fertilizers input, but good return is obtained.Result of the test shows, sprays 717.0 yuan of mu new output value after the fertilizer,
701.0 yuan of the newly-increased net income of mu, produces and throws than being 44.8：1 (table 3).5.6 mu of model field Caulis et Folium Brassicae capitataes are total to 3892.0 yuan of new output value, newly
Increase 3802.4 yuan of net income.
Claims (4)
1. a kind of high nitrogen type water-soluble fertilizer containing fulvic acid, it includes the element of following weight percent：Nitrogen 25%-35%, phosphorus
5%-15%, potassium 5%-15%, zinc 0.01%-0.3%, boron 0.01%-0.3%, magnesium 0.01%-0.3%, manganese 0.01%-0.3%, ferrum 0.01%-
0.3%, fulvic acid 0.5%-2%；
The nitrogen is added in fertilizer in the form of one or more compoundings in carbamide, MAP and potassium nitrate；
The P elements are added in fertilizer in the form of potassium dihydrogen phosphate and/or MAP；
The potassium element is to add fertilizer in the form of any one or a few compounding in potassium nitrate, potassium dihydrogen phosphate and potassium sulfate
In.
2. the high nitrogen type water-soluble fertilizer of fulvic acid is contained as claimed in claim 1, it is characterised in that it includes following percentage by weight
The element of example：Nitrogen 28-32%, phosphorus 7%-12%, potassium 7-12%, zinc 0.01%-0.1%, boron 0.01%-0.1%, magnesium 0.01%-0.1%, manganese
0.01%-0.1%, ferrum 0.01%-0.1%, fulvic acid 1%-1.5%.
3. the high nitrogen type water-soluble fertilizer of fulvic acid is contained as claimed in claim 1 or 2, it is characterised in that the trace element zinc,
Boron, magnesium, manganese, ferrum respectively with：Zinc sulfate, Borax, magnesium sulfate, manganese sulfate, the form of iron sulfate are added in fertilizer.
4. the high nitrogen type water-soluble fertilizer of fulvic acid is contained as claimed in claim 1 or 2, it is characterised in that the height containing fulvic acid
Nitrogen type water-soluble fertilizer, including made by the composition of following weight portion：Carbamide 60-70 parts, potassium nitrate 0-19 parts, MAP 9-26
Part, potassium dihydrogen phosphate 10-27 parts, potassium sulfate 0-10 parts.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105130676B (en) * | 2015-07-03 | 2018-06-22 | 河南晋开化工投资控股集团有限责任公司 | A kind of liquid fertilizer of drought-resistant water-preserving fertilizer conservation and preparation method thereof |
| CN105110861A (en) * | 2015-08-07 | 2015-12-02 | 安徽省文胜生物工程股份有限公司 | Water-soluble organic-inorganic compounded fertilizer and preparation method therefor |
| CN105036987A (en) * | 2015-08-19 | 2015-11-11 | 青海省农林科学院 | Special water-soluble fertilizer for young wolfberry |
| CN110498717A (en) * | 2018-05-17 | 2019-11-26 | 广西桂平市焱焱肥业有限公司 | A kind of mineral resources potassium fulvate water-soluble fertilizer and preparation method thereof |
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