CN104432448A - Tobacco mildew-proof method for ethanol slow-release sterilization - Google Patents

Tobacco mildew-proof method for ethanol slow-release sterilization Download PDF

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Publication number
CN104432448A
CN104432448A CN201410584452.9A CN201410584452A CN104432448A CN 104432448 A CN104432448 A CN 104432448A CN 201410584452 A CN201410584452 A CN 201410584452A CN 104432448 A CN104432448 A CN 104432448A
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China
Prior art keywords
tobacco
tobacco leaf
mould inhibitor
proof method
cigarette
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Pending
Application number
CN201410584452.9A
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Chinese (zh)
Inventor
苏罗毅
李觅
刘红光
胡伟
飞旭云
袁逢春
李庆华
程昌新
皇普东有
李文鹏
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Hongyun Honghe Tobacco Group Co Ltd
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Hongyun Honghe Tobacco Group Co Ltd
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Application filed by Hongyun Honghe Tobacco Group Co Ltd filed Critical Hongyun Honghe Tobacco Group Co Ltd
Priority to CN201410584452.9A priority Critical patent/CN104432448A/en
Publication of CN104432448A publication Critical patent/CN104432448A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B1/00Preparation of tobacco on the plantation
    • A24B1/02Arrangements in barns for preparatory treatment of the tobacco, e.g. with devices for drying

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  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a tobacco mildew-proof method for ethanol slow-release sterilization. Mixing waste tobacco powder and absolute alcohol according to the ratio of 2-4: 1, the mixture is packaged by a breathable bag to be used as a mildew preventive and is respectively placed in the center and the periphery of a tobacco pile, and the weight ratio of the mildew preventive to tobacco leaves is 1-2: 100. slowly releasing ethanol steam at fixed points in the sealed tobacco pile, so that the tobacco leaves are in the atmosphere containing the ethanol steam for a long time to inhibit or kill putrefying bacteria. The invention improves the safety of alcohol use and the alcohol sterilization efficiency, shortens the tobacco processing time and has simple and convenient operation process.

Description

The tobacco leaf mold-proof method of a kind of ethanol slowly-releasing sterilization
Technical field
The invention belongs to technical field of cigarette processing, be specifically related to the tobacco leaf mold-proof method of a kind of ethanol slowly-releasing sterilization.
Background technology
Tobacco leaf before for production of cigarettes, needs through the storage of 1 ~ 3 year, alcoholization process, and object is to improve quality of tobacco by alcoholization.Because tobacco leaf hygroscopicity is strong, and containing the various nutriments required for growth of microorganism, very easily grow various microorganism in alcoholization phase or lay up period and make tobacco leaf moldy metamorphism, thus had a strong impact on presentation quality and the organoleptic quality of tobacco leaf, reduce the use value of tobacco leaf, especially all the more so in humidity, summer that temperature is high.Tobacco mildew, as the global problem of tobacco, causes massive losses to enterprise and country, is day by day subject to people's attention.
Tobacco mildew main cause is mould growth and breeding on tobacco leaf.The condition of mould breeding has three: nutrition, temperature, humidity.Owing to containing the abundant organic substance such as sugar, protein in tobacco leaf, be the basis of fungus growth breeding, through a series of processes such as just roasting, classification, purchase and packagings, surface and inside have posted a large amount of microorganism attached, under the condition of, high humidity high in temperature, the easiest moisture absorption of tobacco leaf is mouldy.And in hot and humid air, the speed that tobacco leaf absorbs moisture is accelerated further, more the growth and breeding of mould creates favourable condition.Present stage, controlling and preventing the technical measures taked in tobacco mildew from mainly containing two kinds of approach both at home and abroad.One is thoroughly killed by tobacco leaf pathogenic microorganism, and as adopted 60Co-Y ray tobacco leaf irradiation, tobacco leaf is fumigated (as hydrogen phosphide, oxirane and ozone etc.) and reached the object of mildew and insect proof with chemical biocide etc.; Another kind is the water content by controlling tobacco leaf, the temperature of storage environment, humidity and oxygen concentration, and add chemistry and the biological growth pressing down raw agent and suppress causal organism, reach the object delaying tobacco mildew process, as tobacco leaf controlled atmosphere storage (being filled with nitrogen and carbon dioxide), sealed oxygen-reducing (seal or add deoxidier etc. simultaneously).Although these measures serve certain effect to minimizing tobacco mildew, be difficult to reach desirable prevention effect.Control the temperature in storage environment, humidity is very high to the requirement of storehouse, a large amount of conditioning equipment is installed, and a large amount of electric energy will be consumed, there is the defects such as weak effect, investment is large, operating cost is high; Sprinkling is even and comprehensively, thus limited efficiency, is also difficult to the harmful effect avoiding chemical agent to cause environment and food in addition to use chemical agent to be difficult to; Sealed oxygen-reducing requires higher to construction material, so involve great expense, storage cost is high.
Ethanol is commonly called as alcohol, and molecular formula is C 2h 5oH (C 2h 6o), be a kind of inflammable, volatile colourless transparent liquid under normal temperature, normal pressure, its solution has special, pleasant fragrance, and slightly excitant.Having many uses of ethanol, available ethanol manufactures acetic acid, beverage, essence, dyestuff, fuel etc.Ethanol is a kind of conventional disinfection sanitizer in daily life, and it, by infiltrating in bacterial body, absorbs the moisture of bacterioprotein, make the protein coagulating of composition bacterium, cause sex change and the precipitation of protein, thus reach the object of kill bacteria.Because ethanol is liquid, volatile, burning, is therefore only limitted to use in the daily lifes such as medical treatment as disinfection sanitizer, and utilizes ethanol to there is not yet reported success at home and abroad to prevent the method for tobacco mildew.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, utilize the bactericidal property of ethanol, for tobacco leaf storage provides the tobacco leaf mold-proof method of a kind of pollution-free, noresidue, safety, environmental protection.
Object of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage of the present invention is percetage by weight.
The tobacco leaf mold-proof method of a kind of ethanol slowly-releasing sterilization, it is characterized in that: waste tobacco powder is mixed with the weight ratio of absolute alcohol by 2 ~ 4:1, mixture venting bags installs as mould inhibitor, and be placed in Yan Duo center and surrounding, and the weight proportion of mould inhibitor and tobacco leaf is 1 ~ 2:100.
The preferred weight ratio of waste tobacco powder and absolute alcohol is 3:1.
Mould inhibitor adopts uniform mode to place.
When placing mould inhibitor, the amount ratio of Yan Duo center and surrounding is 1:2.
When placing mould inhibitor, the amount ratio that cigarette is stamped towards sunny side and in the shade is 1:7.
The composite membrane that preferred employing is closed or closed chamber Storage tobacco.
Relative to prior art, the present invention has the following advantages:
1, alcohol has fungicidal spectrum extensively, efficiently, pollution-free, the features such as use cost is low.To realizing the clean storage of tobacco leaf, push forward safety in production comprehensively significant.
2, alcohol is volatilizable gas, and in sealed cigarette is stamped, permeability is strong, and diffusivity is good, and even concentration does not have dead angle.
3, the present invention uses waste tobacco powder to adsorb fixing alcohol, make the sterilization of alcohol slow releasing, long for the tobacco leaf storage cycle, environmental change is complicated, existing method can not realize the deficiency of permanently effective control tobacco mildew, improve security and the alcohol germicidal efficiency of alcohol use, shorten the tobacco leaf processing time, operating process is simple and convenient.
Detailed description of the invention
Below by embodiment, the present invention is described in further detail, but embodiment is not limited to the technical solution.Based on any conversion that training centre of the present invention is made, all fall into protection scope of the present invention.
Embodiment 1:
Test site: Kunming Cigarette Factory warehousing department nine reservoir area.
The open-air stack time: in October, 2013-2014 year September
Junior tobacco leaf is open-air stack according to a conventional method, 2.5 tons (50 tobacco bales)/buttress.After implementing by following different modes, open buttress, randomly draw 1000 grams of samples from each cigarette buttress upper, middle and lower different parts, carry out plate count.Add up the tobacco leaf gross weight of each cigarette buttress and tobacco leaf weight of going mouldy, calculate mould variability.
Process one (A1): will containing 95% ethanol be evenly sprayed on cigarette stamp on the outer gunnysack of each tobacco bale, fountain height is 3.5kg, adopts the composite membrane or closed chamber Storage tobacco closed, is formed and seal tobacco leaf stack, Outdoor Storage 11 months.
Process two (A2): load 95% ethanol 0.25kg with container, amount to 14 bottles, bottleneck gauze is sealed, be convenient to alcohol slowly volatilize, be distributed in Yan Duo center and surrounding respectively, adopt the composite membrane or closed chamber Storage tobacco closed, form sealing tobacco leaf stack, Outdoor Storage 11 months.
Process three (A3): the solid netted plastic offal given up in production and absolute alcohol formed by 2:1 mixture is packed good, as slow vaporization cigarette buttress mould inhibitor, mould inhibitor is packed as 1kg specification and 2kg specification, the mould inhibitor made is distributed in Yan Duo center and surrounding respectively, wherein the mould inhibitor of 1 bag of 2kg dress is placed at Yan Duo center, surrounding places the mould inhibitor of 8 bags of 1kg dresses respectively, adopt the composite membrane or closed chamber Storage tobacco closed, form sealing tobacco leaf stack, Outdoor Storage 11 months.
Contrast (CK1): normal storage tobacco leaf method of operating sealed cigarette is stamped, Outdoor Storage 11 months.
The experimental result of process 1-3 is in table 1.
Table 1. different wine precision processing mode experimental result
Result shows, makes differently to carry out alcohol fungus and mildew resistance, and through the Outdoor Storage of 11 months, through sorting two throwings, the percentage accounting for cigarette buttress gross weight with mould cigarette waste product represents mould variability.A3 process makes the mould variability of operation of discarded offal mixed alcohol significantly lower than control group, 85.15% is reduced respectively than contrast, mould content of molds reduces 98.99% than contrast, bacterium content of molds reduces 96.75% than contrast, uses the mould variability of A2 process alcohol sterilization operation, mould content of molds, bacterium content of molds to reduce 74.25%, 91.97% and 94.85% than contrast respectively; The mould variability of A1 process alcohol sterilization operation, mould content of molds, bacterium content of molds is used to reduce 47.56%, 58.58% and 88.83% than contrast respectively; Above-mentioned three kinds of modes inhibit storage tobacco mildew all in various degree, bactericidal effect is obvious, wherein with A3 process, be about to mould inhibitor piled up neatly by solid that in producing, useless offal and absolute alcohol mixture are formed mode best results as slow vaporization cigarette, A1 process and A2 process are slightly poor in mode of operation and effect.
Embodiment 2:
Test site: Kunming Cigarette Factory warehousing department nine reservoir area.
The open-air stack time: in October, 2013-2014 year September
Junior tobacco leaf is open-air stack according to a conventional method, 2.5 tons (50 tobacco bales)/buttress.Each tobacco leaf stack center and stacking surrounding arrange mould inhibitor set-point respectively.After implementing by following different modes, open buttress, randomly draw 1000 grams of samples from each cigarette buttress upper, middle and lower different parts, carry out plate count.Add up the tobacco leaf gross weight of each cigarette buttress and tobacco leaf weight of going mouldy, calculate mould variability.5 kilograms of deciding grade and level are carried out cigarette to smoke panel test and chemical analysis.
Mode one processes (B1): the solid netted plastic offal given up in production and absolute alcohol formed by 2:1 mixture is packed good, as slow vaporization cigarette buttress mould inhibitor, mould inhibitor is packed as 1kg specification and 2kg specification, the mould inhibitor made is distributed in Yan Duo center and surrounding respectively, wherein the mould inhibitor of 1 bag of 2kg dress is placed at Yan Duo center, surrounding places the mould inhibitor of 8 bags of 1kg dresses respectively, adopt the composite membrane or closed chamber Storage tobacco closed, form sealing tobacco leaf stack, Outdoor Storage 11 months.
Mode two processes (B2): the solid netted plastic offal given up in production and absolute alcohol formed by 3:1 mixture is packed good, as slow vaporization cigarette buttress mould inhibitor, mould inhibitor is packed as 1kg specification and 2kg specification, the mould inhibitor made is distributed in Yan Duo center and surrounding respectively, wherein the mould inhibitor of 4 bags of 2kg dresses is placed at Yan Duo center, surrounding places the mould inhibitor of 16 bags of 1kg dresses respectively, adopt the composite membrane or closed chamber Storage tobacco closed, form sealing tobacco leaf stack, Outdoor Storage 11 months.
Mode three processes (B3): the solid netted plastic offal given up in production and absolute alcohol formed by 4:1 mixture is packed good, as slow vaporization cigarette buttress mould inhibitor, mould inhibitor is packed as 1kg specification and 2kg specification, the mould inhibitor made is distributed in Yan Duo center and surrounding respectively, wherein the mould inhibitor of 8 bags of 2kg dresses is placed at Yan Duo center, surrounding places the mould inhibitor of 32 bags of 1kg dresses respectively, adopt the composite membrane or closed chamber Storage tobacco closed, form sealing tobacco leaf stack, Outdoor Storage 11 months.
CK2: normal storage tobacco leaf method of operating sealed cigarette is stamped, Outdoor Storage 11 months.
The experimental result of process 1 ~ 3 is in table 2.
Table 2. different ratio mould inhibitor process experimental result
Result shows, the junior tobacco leaf of above-described embodiment is after placing alcohol bactericide, and through the Outdoor Storage of 11 months, through sorting two throwings, the percentage accounting for cigarette buttress gross weight with mould cigarette waste product represents mould variability.The mould variability of processed group significantly lower than control group, respectively according to reducing 89.84%, 99.10% and 96.02%.The junior tobacco leaf of above-described embodiment is after placing the storage of alcohol bactericide, through the Outdoor Storage of 11 months, the mould content of molds of processed group reduces 99.73%, 99.85% and 99.77% respectively than contrast, and bacterium content of molds reduces 97.39%, 99.02% and 98.81% respectively than contrast.Three kinds of modes inhibit storage tobacco mildew all in various degree, bactericidal effect is obvious, wherein with B2 process, being about to offal useless in producing and absolute alcohol, to press the solid netted plastic that 3:1 mixture formed packed good, piles up neatly the mode best results of mould inhibitor as slow vaporization cigarette.
Embodiment 3:
Test site: Kunming Cigarette Factory warehousing department nine reservoir area.
The open-air stack time: in October, 2013-2014 year September
Junior tobacco leaf is open-air stack according to a conventional method, 2.5 tons (50 tobacco bales)/buttress.The solid netted plastic offal given up in production and absolute alcohol formed by 3:1 mixture is packed good, as slow vaporization cigarette buttress mould inhibitor, mould inhibitor is packed as 1kg specification and 2kg specification, each tobacco leaf stack center and stacking surrounding arrange mould inhibitor set-point by following different modes respectively, buttress is opened after enforcement, randomly draw 1000 grams of samples from each cigarette buttress upper, middle and lower different parts, carry out plate count.Add up the tobacco leaf gross weight of each cigarette buttress and tobacco leaf weight of going mouldy, calculate mould variability.5 kilograms of deciding grade and level are carried out cigarette to smoke panel test and chemical analysis.
Mode one processes (C1): the mould inhibitor made is distributed in Yan Duo center and surrounding respectively, wherein the mould inhibitor of 4 bags of 2kg dresses is placed at Yan Duo center, cigarette stamps the mould inhibitor placing 2 bags of 1kg dresses towards sunny side respectively, and cigarette stamps the mould inhibitor that in the shade is placed 14 bags of 1kg dresses respectively.Adopt the composite membrane or closed chamber Storage tobacco closed, form sealing tobacco leaf stack, Outdoor Storage 11 months.
Mode two processes (C2): the mould inhibitor made is distributed in Yan Duo center and surrounding respectively, wherein the mould inhibitor of 4 bags of 2kg dresses is placed at Yan Duo center, cigarette stamps the mould inhibitor placing 6 bags of 1kg dresses towards sunny side respectively, and cigarette stamps the mould inhibitor that in the shade is placed 10 bags of 1kg dresses respectively.Adopt the composite membrane or closed chamber Storage tobacco closed, form sealing tobacco leaf stack, Outdoor Storage 11 months.
Mode three processes (C3): the mould inhibitor made is distributed in Yan Duo center and surrounding respectively, wherein the mould inhibitor of 4 bags of 2kg dresses is placed at Yan Duo center, cigarette stamps the mould inhibitor placing 8 bags of 1kg dresses towards sunny side respectively, and cigarette stamps the mould inhibitor that in the shade is placed 8 bags of 1kg dresses respectively.Adopt the composite membrane or closed chamber Storage tobacco closed, form sealing tobacco leaf stack, Outdoor Storage 11 months.
Contrast (CK3): normal storage tobacco leaf method of operating sealed cigarette is stamped, Outdoor Storage 11 months.
The experimental result of process 1 ~ 3 is in table 3.
Table 3. cigarette is stamped towards sunny side mould inhibitor consumption different from the shade process experimental result
Result shows, the junior tobacco leaf of above-described embodiment is after placing alcohol bactericide, and through the Outdoor Storage of 11 months, through sorting two throwings, the percentage accounting for cigarette buttress gross weight with mould cigarette waste product represents mould variability.The mould variability of the processed group of three kinds of different modes placement slowly-releasing alcohol bactericide is all remarkable in control group, respectively according to reducing 99.62%, 99.55% and 99.34%.Mould content of molds reduces 99.79%, 99.79% and 99.75% respectively than contrast, and bacterium content of molds reduces 95.60%, 91.77% and 85.23% respectively than contrast.Three kinds of different modes of placing inhibit storage tobacco mildew all in various degree, bactericidal effect is obvious, wherein to process one, be about to useless offal and absolute alcohol in producing press solid slow-release that 3:1 mixture formed and to volatilize bactericide, packed good with netted plastic, Yan Duo places at center the mould inhibitor of 4 bags of 2kg dresses, and cigarette stamps the mould inhibitor placing 2 bags of 1kg dresses towards sunny side respectively, and cigarette stamps the mode best results that in the shade is placed the mould inhibitor of 14 bags of 1kg dresses respectively.

Claims (6)

1. the tobacco leaf mold-proof method of ethanol slowly-releasing sterilization, it is characterized in that: waste tobacco powder is mixed with the weight ratio of absolute alcohol by 2 ~ 4:1, mixture venting bags installs as mould inhibitor, and be placed in Yan Duo center and surrounding, and the weight proportion of mould inhibitor and tobacco leaf is 1 ~ 2:100.
2. tobacco leaf mold-proof method according to claim 1, is characterized in that: the preferred weight ratio of waste tobacco powder and absolute alcohol is 3:1.
3. tobacco leaf mold-proof method according to claim 1, is characterized in that: mould inhibitor adopts uniform mode to place.
4. tobacco leaf mold-proof method according to claim 1, is characterized in that: when placing mould inhibitor, the amount ratio of Yan Duo center and surrounding is 1:2.
5. tobacco leaf mold-proof method according to claim 1, is characterized in that: when placing mould inhibitor, the amount ratio that cigarette is stamped towards sunny side and in the shade is 1:7.
6. tobacco leaf mold-proof method according to claim 1, is characterized in that: adopt the composite membrane or closed chamber Storage tobacco closed.
CN201410584452.9A 2014-10-27 2014-10-27 Tobacco mildew-proof method for ethanol slow-release sterilization Pending CN104432448A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111869917A (en) * 2020-07-31 2020-11-03 云南省烟草公司曲靖市公司 Novel method for preventing and treating mildew rot in tobacco leaf baking process

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CN103704281A (en) * 2013-12-27 2014-04-09 成都新朝阳作物科学有限公司 Pesticide composition containing sophora flavescens and tobacco extracts as well as preparation method and application thereof
TW201414425A (en) * 2012-10-09 2014-04-16 ming-zong Chen Composite insect resist agent for plants
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CN86102596A (en) * 1986-04-10 1986-10-08 李祥麟 The method of strengthen fermentation of tobacco leaf
CN1138416A (en) * 1996-04-18 1996-12-25 陈国才 High effective multicomponent natural plant insecticide
CN1158926C (en) * 1997-08-20 2004-07-28 克罗斯塔工业公司 Environmentally-friendly, controlled-release insect repellent device
CN1276160A (en) * 2000-05-09 2000-12-13 吕世禄 0.36% aqueous matrine solution
CN1596777A (en) * 2004-09-27 2005-03-23 唐建文 Safety broad spectrum high efficiency compound type gas phase mildew proof antiseptic antistaling agent and its manufacturing method and application
CN101897348A (en) * 2010-05-28 2010-12-01 云南省农业科学院农业环境资源研究所 Soil insect control agent and preparation method thereof
CN102450252A (en) * 2010-10-20 2012-05-16 周端午 Green, long-lasting antibacterial, mildew-resistant and insecticidal water-based micro-emulsifier
CN102007945A (en) * 2010-10-22 2011-04-13 北京化工大学 Mothproof and mildewproof agent taking Eupatorium adenophorum as carrier and preparation method thereof
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111869917A (en) * 2020-07-31 2020-11-03 云南省烟草公司曲靖市公司 Novel method for preventing and treating mildew rot in tobacco leaf baking process

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Application publication date: 20150325