CN104388472B - A kind of method of liquid alcohol fermented beer mixed straw cellulose dry distilled spirit - Google Patents
A kind of method of liquid alcohol fermented beer mixed straw cellulose dry distilled spirit Download PDFInfo
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- CN104388472B CN104388472B CN201410594745.5A CN201410594745A CN104388472B CN 104388472 B CN104388472 B CN 104388472B CN 201410594745 A CN201410594745 A CN 201410594745A CN 104388472 B CN104388472 B CN 104388472B
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- liquid
- fermented beer
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- alcohol
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
- C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
- C12P7/06—Ethanol, i.e. non-beverage
- C12P7/08—Ethanol, i.e. non-beverage produced as by-product or from waste or cellulosic material substrate
- C12P7/10—Ethanol, i.e. non-beverage produced as by-product or from waste or cellulosic material substrate substrate containing cellulosic material
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
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- General Chemical & Material Sciences (AREA)
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- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
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- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
The invention discloses a kind of method of liquid alcohol fermented beer mixed straw cellulose dry distilled spirit, comprise the following steps, step 1, the containing cellulose dry such as stalk is broken into the segment that length is 1 20mm, obtains raw material B；Step 2, liquid alcohol fermented beer is put into screw feeder blender with raw material B and just mixed with liquid yeast bacterium, spiral ribbon mixer is entered back into and is sufficiently mixed uniformly, obtain mixture C；Step 3：Put mixture C into solid-state fermenter to be fermented, obtain solid-state fermented grain；Step 4：Solid-state fermented grain is continually fed into automatic continuous wine distilling machine and steams faints；Step 5：Faints is subjected to conventional rectification, obtains finished product alcohol.By using this technique productions alcohol, without the discharge of liquid vinasse and sewage, solve the problems, such as that the refractory reason of liquid vinasse pollution and Alcohol Production cost are high existing for prior art, meet market needs.
Description
Technical field
The present invention relates to Alcohol Production technical field, and in particular to a kind of liquid alcohol fermented beer mixed straw cellulose is done
The method of material distilled spirit.
Background technology
The technique of production alcohol is broadly divided into two major classes at present, and the first kind is that liquid phase process prepares alcohol, i.e., with starchiness
Matter or blackstrap are raw material, and caused alcohol distillation waste liquid, liquid vinasse are difficult to administer in still-process, are brought to environment
Larger destruction and pollution；Second class is that solid state process prepares alcohol, i.e., using sugar grass as raw material, producing alcohol by solid-state fermentation, though
There is no the discharge of liquid vinasse, but because sugar grass sugar content is not high enough, cause production cost too high；The third method is to utilize
Cellulase production alcohol, because the cellulose in raw material and lignin separation difficulty are big, although national policy is supported, but by
Too high in cost, manufacturing enterprise is difficult to maintain production, at present still in conceptual phase.
The content of the invention
It is an object of the invention to propose that the cellulosic materials such as one kind liquid alcohol fermented beer mixed straw, sawdust distill
The method of alcohol, solve the problems, such as that the refractory reason of liquid vinasse pollution and Alcohol Production cost are high existing for prior art.
To achieve the above object, the invention provides a kind of distillation of liquid alcohol fermented beer mixed straw cellulose dry
The method of alcohol, it is characterised in that comprise the following steps：
Step 1：Stalk cellulose dry is broken into the segment that length is 1-20mm, obtains raw material B；
Step 2：Liquid alcohol fermented beer is with raw material B with 5：2-4 ratio mixing put into mixer with liquid ferment
Female bacterium just mix for the first time, is just sufficiently mixed uniformly into spiral ribbon mixer after mixing, obtains mixture C, carried out twice
It is well mixed that mixing preferably makes sugar and moisture fully dissolve；
Step 3：Put mixture C into solid-state fermenter and carry out solid state fermentation, obtain solid-state fermented grain；
Step 4：Solid-state fermented grain is put into automatic continuous wine distilling machine and steams faints, alcohol content 20-60%；
Step 5：The faints obtained in step 4 is subjected to conventional rectification, obtains finished product alcohol.Preferably, step
Stalk cellulose dry described in one is maize straw, more than the one or more in broomcorn straw, rice straw, rice husk, hay.
Preferably, described maize straw, broomcorn straw, rice straw, rice husk, hay moisture are less than 16%.
Preferably, sawdust is included in the raw material B described in step 1.
Preferably, the liquid alcohol fermented beer described in step 2 is to be fermented using starchiness or blackstrap as raw material
40-70h is made, described alcohol fermented beer, alcoholic strength 4-16%, and residual sugar amount is less than 0.5%；
Preferably, liquid alcohol fermented beer described in step 2 can add blackstrap mixing again with raw material B with 5：2-4 ratio
Example mixing is put into screw feeder blender and with liquid yeast bacterium just mix for the first time, is just filled after mixing into spiral ribbon mixer
Divide and be well mixed, obtain mixture C；
Preferably, solid content is 20-50% in the mixture C described in step 2.
Beneficial effect of the present invention：The present invention mixes alcohol fermented beer with blackstrap, and blackstrap can be by alcohol fermented beer
In fermentability sugared content bring up to 0-25%, solve the problems, such as the sugar content deficiency that solid state process prepares alcohol, improve
Alcoholic strength；Liquid alcohol fermented beer mixes with dry containing stalk cellulose, liquid is become solid matter, steams solid after drinking
State thing can be used as Fertilizer application；Solid state fermentation make liquid be changed into solid-state solve in still-process discharge drunk fish to ring
Pollution problem caused by border；Blackstrap can also be turned waste into wealth, improve the added value of blackstrap deep processing；Liquid alcoholic fermentation
Wine with dregs is combined the new way of production alcohol with dry containing stalk cellulose, can reduce production cost.
Brief description of the drawings
Fig. 1 is the method flow of liquid alcohol fermented beer mixed straw cellulose dry distilled spirit of the present invention
Figure.
Embodiment
The present invention is described in further detail below in conjunction with the accompanying drawings, to make those skilled in the art with reference to specification
Word can be implemented according to this.
Embodiment 1
A kind of method of liquid alcohol fermented beer mixed straw cellulose dry distilled spirit, comprises the following steps：
Step 1：Using corn as raw material, the liquid alcohol fermented beer of maturation is prepared through everfermentation 50h, alcoholic strength is
11%, residual sugar amount is less than 0.5%；Liquid alcohol fermented beer mixes with the blackstrap that acidification is crossed again, makes liquid alcoholic fermentation
Fermentability sugared content in wine with dregs is adjusted to 2%, obtains mixture A；
Step 2：It is the small of 5-10mm that the corn stalk fiber element dry that moisture is 14% is broken into length
Section, obtains the raw material of dry containing stalk cellulose B；
Step 3：The mixture A that step 1 the obtains and raw material B that step 2 obtains is mixed to put into 5: 3 ratio and stirred
Mix in blender and with liquid yeast bacterium just mix for the first time, be just sufficiently mixed uniformly, obtain into spiral ribbon mixer after mixing
To mixture C, it is 45% to make C object amounts containing solid, alcoholic strength 9%；
Step 4：Put mixture C into solid-state fermenter and carry out solid state fermentation, obtain solid-state fermented grain；
Step 5：The solid-state fermented grain that step 4 obtains is put into automatic continuous wine distilling machine and steams faints, alcohol content
For 40%；
Step 6：The faints obtained in step 5 is distilled through conventional distillation technology, obtains finished product alcohol.
Embodiment 2
A kind of method of liquid state fermentation wine with dregs mixed straw cellulose dry distilled spirit, comprises the following steps：
Step 1：Using Tapioca chips as raw material, the liquid alcohol fermented beer of maturation, alcoholic strength are prepared through everfermentation 58h
For 12.5%, residual sugar amount is less than 0.2%；Liquid alcohol fermented beer mixes with the blackstrap that acidification is crossed again, makes liquid alcohol
Fermentability sugared content in karusen is adjusted to 4%, obtains mixture A；
Step 2：The rice straw that moisture is 14% is broken into 1-5mm segment, remixes and accounts for rice straw 10%
Rice husk obtains the raw material of dry containing stalk cellulose B；
Step 3：The mixture A that step 1 the obtains and raw material B that step 2 obtains is mixed to put into 5: 2 ratio and stirred
Mix in blender and with liquid yeast bacterium just mix for the first time, be just sufficiently mixed uniformly, obtain into spiral ribbon mixer after mixing
To mixture C, it is 40% to make C object amounts containing solid, alcoholic strength 14.8%；
Step 4：The mixture C that step 3 is obtained is put solid-state fermenter into and fermented, and obtains solid-state fermented grain；
Step 5：The solid-state fermented grain that step 4 obtains is put into automatic continuous wine distilling machine and steams faints, alcohol content
For 50%；
Step 6：The faints obtained in step 5 is distilled through conventional distillation technology, obtains finished product alcohol.
Embodiment 3
A kind of method of liquid state fermentation wine with dregs mixed straw cellulose dry distilled spirit, comprises the following steps：
Step 1：Using corn as raw material, the liquid alcohol fermented beer of maturation is prepared through everfermentation 65h, alcoholic strength is
14%, residual sugar amount is less than 0.2%；Liquid alcohol fermented beer mixes with the blackstrap that acidification is crossed again, makes liquid alcoholic fermentation
Fermentability sugared content in wine with dregs is adjusted to 4%, obtains mixture A；
Step 2：It is 5-20mm that cotton stalk that moisture is 14%, bagasse are broken into length in 1: 2 ratio
Segment, then mixed with sawdust, obtain the raw material of dry containing stalk cellulose B；
Step 3：The mixture A that step 1 the obtains and raw material B that step 2 obtains is mixed with 5: 2.5 ratio and put into
With liquid yeast bacterium just mix for the first time in mixer, be just sufficiently mixed uniformly into spiral ribbon mixer after mixing,
Mixture C is obtained, it is 42% to make C object amounts containing solid, alcoholic strength 16.9%；
Step 4：The mixture C that step 3 is obtained is put solid-state fermenter into and fermented, and obtains solid-state fermented grain；
Step 5：The solid-state fermented grain that step 4 obtains is put into automatic continuous wine distilling machine and steams faints, alcohol content
For 60%；
Step 6：The faints obtained in step 5 is distilled through conventional distillation technology, obtains finished product alcohol.
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed
With it can be applied to various suitable the field of the invention completely, can be easily for those skilled in the art
Other modification is realized, therefore under the universal limited without departing substantially from claim and equivalency range, it is of the invention and unlimited
In specific details.
Claims (4)
- A kind of 1. method of liquid alcohol fermented beer mixed straw cellulose dry distilled spirit, it is characterised in that including with Lower step：Step 1：Stalk cellulose dry is broken into the segment that length is 1-20mm, obtains raw material B；Described stalk is fine It is more than the one or more in maize straw, broomcorn straw, rice straw, rice husk, hay to tie up plain dry；Wherein, described jade Rice stalk, broomcorn straw, rice straw, rice husk, hay moisture are less than 16%；Include sawdust in described raw material B；Step 2：Liquid alcohol fermented beer is with raw material B with 5：2-4 ratio mixing is put into screw feeder blender and and liquid yeast Bacterium just mix for the first time, is just sufficiently mixed uniformly into spiral ribbon mixer after mixing, obtains mixture C；Step 3：Put mixture C into solid-state fermenter and carry out solid state fermentation, obtain solid-state fermented grain；Step 4：Solid-state fermented grain is put into automatic continuous wine distilling machine and steams faints；Step 5：The faints obtained in step 4 is subjected to conventional rectification, obtains finished product alcohol.
- 2. the method for liquid alcohol fermented beer mixed straw cellulose dry distilled spirit according to claim 1, its It is characterised by, the liquid alcohol fermented beer described in step 2 is to carry out 40-70h systems of fermenting as raw material using starchiness or blackstrap .
- 3. the method for liquid alcohol fermented beer mixed straw cellulose dry distilled spirit according to claim 1, its Be characterised by, liquid alcohol fermented beer described in step 2 can add blackstrap mixing again with raw material B with 5：2-4 ratio mixing Put into screw feeder blender and with liquid yeast bacterium just mix for the first time, be just sufficiently mixed after mixing into spiral ribbon mixer Uniformly, mixture C is obtained.
- 4. the method for liquid alcohol fermented beer mixed straw cellulose dry distilled spirit according to claim 1, its It is characterised by, solid content is 20-50% in the mixture C described in step 2.
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| CN201410594745.5A CN104388472B (en) | 2014-10-29 | 2014-10-29 | A kind of method of liquid alcohol fermented beer mixed straw cellulose dry distilled spirit |
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| CN201410594745.5A CN104388472B (en) | 2014-10-29 | 2014-10-29 | A kind of method of liquid alcohol fermented beer mixed straw cellulose dry distilled spirit |
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| CN104388472A CN104388472A (en) | 2015-03-04 |
| CN104388472B true CN104388472B (en) | 2018-01-12 |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104805134A (en) * | 2015-04-27 | 2015-07-29 | 梁利和 | Method for synchronous alcoholic fermentation by applying straw and production of edible fungus culture medium material |
| CN104830915A (en) * | 2015-04-27 | 2015-08-12 | 梁利和 | Method utilizing mixture of straw and molasses to prepare alcohol and using vinasse to modify saline-alkali soil |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005065695A (en) * | 2003-08-07 | 2005-03-17 | Tokyo Univ Of Agriculture | Production method and production system for ethanol |
| EP1954798B1 (en) * | 2005-09-30 | 2010-02-24 | Dong Energy Generation A/S | Non-pressurised pre-treatment, enzymatic hydrolysis and fermentation of waste fractions |
| CN102703518A (en) * | 2012-06-19 | 2012-10-03 | 姜蓉生 | Method for producing alcohol and cultivating edible fungus by solid fermentation through mixing manioc waste with treacle |
| CN104109695A (en) * | 2014-08-06 | 2014-10-22 | 梁利 | Method for producing alcohol through solid fermentation on mixed waste molasses containing cellulose substances |
-
2014
- 2014-10-29 CN CN201410594745.5A patent/CN104388472B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005065695A (en) * | 2003-08-07 | 2005-03-17 | Tokyo Univ Of Agriculture | Production method and production system for ethanol |
| EP1954798B1 (en) * | 2005-09-30 | 2010-02-24 | Dong Energy Generation A/S | Non-pressurised pre-treatment, enzymatic hydrolysis and fermentation of waste fractions |
| CN102703518A (en) * | 2012-06-19 | 2012-10-03 | 姜蓉生 | Method for producing alcohol and cultivating edible fungus by solid fermentation through mixing manioc waste with treacle |
| CN104109695A (en) * | 2014-08-06 | 2014-10-22 | 梁利 | Method for producing alcohol through solid fermentation on mixed waste molasses containing cellulose substances |
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