CN104323396A - Natural antioxidant and preparation method thereof - Google Patents
Natural antioxidant and preparation method thereof Download PDFInfo
- Publication number
- CN104323396A CN104323396A CN201410540765.4A CN201410540765A CN104323396A CN 104323396 A CN104323396 A CN 104323396A CN 201410540765 A CN201410540765 A CN 201410540765A CN 104323396 A CN104323396 A CN 104323396A
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- CN
- China
- Prior art keywords
- parts
- natural
- pressure
- propolis
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- 230000003078 antioxidant effect Effects 0.000 title claims abstract description 11
- 239000003963 antioxidant agent Substances 0.000 title claims abstract description 8
- 238000002360 preparation method Methods 0.000 title claims abstract description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000000463 material Substances 0.000 claims abstract description 8
- 244000037364 Cinnamomum aromaticum Species 0.000 claims abstract description 7
- 235000014489 Cinnamomum aromaticum Nutrition 0.000 claims abstract description 7
- 240000008790 Musa x paradisiaca Species 0.000 claims abstract description 7
- 235000018290 Musa x paradisiaca Nutrition 0.000 claims abstract description 7
- 241000241413 Propolis Species 0.000 claims abstract description 7
- 244000269722 Thea sinensis Species 0.000 claims abstract description 7
- 235000006468 Thea sinensis Nutrition 0.000 claims abstract description 7
- 235000020279 black tea Nutrition 0.000 claims abstract description 7
- 239000000843 powder Substances 0.000 claims abstract description 7
- 229940069949 propolis Drugs 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims abstract description 4
- 238000002156 mixing Methods 0.000 claims description 9
- 240000004510 Agastache rugosa Species 0.000 claims description 6
- 239000004115 Sodium Silicate Substances 0.000 claims description 6
- 229920002678 cellulose Polymers 0.000 claims description 6
- 239000001913 cellulose Substances 0.000 claims description 6
- 235000013305 food Nutrition 0.000 claims description 6
- 239000011259 mixed solution Substances 0.000 claims description 6
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 6
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 6
- 235000009917 Crataegus X brevipes Nutrition 0.000 claims description 4
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 claims description 4
- 235000009685 Crataegus X maligna Nutrition 0.000 claims description 4
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 claims description 4
- 235000009486 Crataegus bullatus Nutrition 0.000 claims description 4
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 claims description 4
- 235000009682 Crataegus limnophila Nutrition 0.000 claims description 4
- 235000004423 Crataegus monogyna Nutrition 0.000 claims description 4
- 240000000171 Crataegus monogyna Species 0.000 claims description 4
- 235000002313 Crataegus paludosa Nutrition 0.000 claims description 4
- 235000009840 Crataegus x incaedua Nutrition 0.000 claims description 4
- 239000012141 concentrate Substances 0.000 claims description 3
- 238000000605 extraction Methods 0.000 claims description 3
- 238000000855 fermentation Methods 0.000 claims description 3
- 230000004151 fermentation Effects 0.000 claims description 3
- 238000004108 freeze drying Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 230000000630 rising effect Effects 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- 241001529821 Agastache Species 0.000 abstract 1
- 241001162994 Rugosus Species 0.000 abstract 1
- 238000000874 microwave-assisted extraction Methods 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 description 2
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3562—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/358—Inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Inorganic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
The present invention discloses a natural antioxidant which comprises the following components by weight: 22-24 parts of black tea leaf, 12-14 parts of agastache rugosus, 13-15 parts of banana skin, 5-7 parts of cassia twig and 3-6 parts of propolis, the preparation method comprises the following steps: crushing the components by weight, adding the powder into 70-85vol% ethanol in the ratio of material to liquid of 1:4-6, soaking for 2-3H, performing microwave-assisted extraction for 1-2H, the raw materials of the natural antioxidant are easy to obtain, the antioxidant effect is good, the ratio is reasonable, and application range is wide.
Description
Technical field
The present invention relates to food additives field, specifically belong to natural.
Background technology
Antioxidant stops after making an addition to food or postpones Food Oxidation, and improve the stability of food quality and extend the material of storage period, the antioxidant in market mostly is Prof. Du Yucang.
Summary of the invention
The object of this invention is to provide a kind of natural, raw material is natural to be easy to get, and antioxidant effect is good, reasonable mixture ratio applied range.
Technical scheme of the present invention is as follows:
Natural, comprises following component according to parts by weight: black tea leaf 22 ~ 24 parts, cellulose 5 ~ 7 parts, sodium silicate 2-5 part, wrinkled giant hyssop 12 ~ 14 parts, banana skin 13 ~ 15 parts, cassia twig 5 ~ 7 parts, 3 ~ 6 parts of propolis.
A preparation method for natural, is made up of following steps:
(1), fresh black tea leaf, cellulose, sodium silicate, wrinkled giant hyssop, banana skin, coffee, leaves of Hawthorn and cassia twig, propolis are cleaned, drain away the water, steam pressure fermentation stage is carried out after mixing, comprise vacuum, boosting, constant temperature and pressure and buck stage, the parameter in each stage and process are: vacuum: 0 ~ 0.04MPa, and the pumpdown time is 0.8 ~ 0.9h; Boosting: 0.08 ~ 1.0MPa, pressure rising time is 1.2 ~ 1.8h; Constant temperature and pressure: 0.7MPa, constant voltage time is 3 ~ 5h, and thermostat temperature is 145 ~ 160 DEG C; Step-down: drop to normal pressure, dip time is 1.2 ~ 1.5h, then is ground into powder, for subsequent use;
(2) be, that 1:4 ~ 6 join in 70 ~ 85vol% ethanol and soak after 2 ~ 3h by the powder obtained in step 1 by solid-liquid ratio, microwave abstracting 1 ~ 2h, extraction temperature is 40 DEG C ~ 50 DEG C, microwave frequency 1000MHz ~ 1450MHz, obtain mixed solution, the mixed solution Rotary Evaporators obtained concentrates and reclaims ethanol, obtains dark mixing material;
(3), the dark mixing material freeze drying that will obtain in step 2, be antioxidant from natural food.
Natural of the present invention utilizes natural Chinese herbal medicine or natural products to make, and raw material is natural to be easy to get, and antioxidant effect is good, reasonable mixture ratio applied range.Avoid the harm of traditional chemical additive to human body, thus ensure the health of human body and the hygiene and health of diet.
Detailed description of the invention
Natural, comprises following component according to parts by weight: black tea leaf 22 ~ 24 parts, cellulose 5 ~ 7 parts, sodium silicate 2-5 part, wrinkled giant hyssop 12 ~ 14 parts, banana skin 13 ~ 15 parts, cassia twig 5 ~ 7 parts, 3 ~ 6 parts of propolis.
A preparation method for natural, is made up of following steps:
(1), fresh black tea leaf, cellulose, sodium silicate, wrinkled giant hyssop, banana skin, coffee, leaves of Hawthorn and cassia twig, propolis are cleaned, drain away the water, steam pressure fermentation stage is carried out after mixing, comprise vacuum, boosting, constant temperature and pressure and buck stage, the parameter in each stage and process are: vacuum: 0 ~ 0.04MPa, and the pumpdown time is 0.8 ~ 0.9h; Boosting: 0.08 ~ 1.0MPa, pressure rising time is 1.2 ~ 1.8h; Constant temperature and pressure: 0.7MPa, constant voltage time is 3 ~ 5h, and thermostat temperature is 145 ~ 160 DEG C; Step-down: drop to normal pressure, dip time is 1.2 ~ 1.5h, then is ground into powder, for subsequent use;
(2) be, that 1:4 ~ 6 join in 70 ~ 85vol% ethanol and soak after 2 ~ 3h by the powder obtained in step 1 by solid-liquid ratio, microwave abstracting 1 ~ 2h, extraction temperature is 40 DEG C ~ 50 DEG C, microwave frequency 1000MHz ~ 1450MHz, obtain mixed solution, the mixed solution Rotary Evaporators obtained concentrates and reclaims ethanol, obtains dark mixing material;
(3), the dark mixing material freeze drying that will obtain in step 2, be antioxidant from natural food.
Claims (2)
1. natural, is characterized in that comprising following component according to parts by weight: black tea leaf 22 ~ 24 parts, cellulose 5-7 part, sodium silicate 2-5 part, wrinkled giant hyssop 12 ~ 14 parts, banana skin 13 ~ 15 parts, coffee 4 ~ 6 parts, leaves of Hawthorn 3 ~ 5 parts, cassia twig 5 ~ 7 parts, 3 ~ 6 parts of propolis.
2. a preparation method for natural according to claim 1, is characterized in that being made up of following steps:
(1), fresh black tea leaf, cellulose, sodium silicate, wrinkled giant hyssop, banana skin, coffee, leaves of Hawthorn and cassia twig, propolis are cleaned, drain away the water, steam pressure fermentation stage is carried out after mixing, comprise vacuum, boosting, constant temperature and pressure and buck stage, the parameter in each stage and process are: vacuum: 0 ~ 0.04MPa, and the pumpdown time is 0.8 ~ 0.9h; Boosting: 0.08 ~ 1.0MPa, pressure rising time is 1.2 ~ 1.8h; Constant temperature and pressure: 0.7MPa, constant voltage time is 3 ~ 5h, and thermostat temperature is 145 ~ 160 DEG C; Step-down: drop to normal pressure, dip time is 1.2 ~ 1.5h, then is ground into powder, for subsequent use;
(2) be, that 1:4 ~ 6 join in 70 ~ 85vol% ethanol and soak after 2 ~ 3h by the powder obtained in step 1 by solid-liquid ratio, microwave abstracting 1 ~ 2h, extraction temperature is 40 DEG C ~ 50 DEG C, microwave frequency 1000MHz ~ 1450MHz, obtain mixed solution, the mixed solution Rotary Evaporators obtained concentrates and reclaims ethanol, obtains dark mixing material;
(3), the dark mixing material freeze drying that will obtain in step 2, be antioxidant from natural food.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410540765.4A CN104323396A (en) | 2014-10-14 | 2014-10-14 | Natural antioxidant and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410540765.4A CN104323396A (en) | 2014-10-14 | 2014-10-14 | Natural antioxidant and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104323396A true CN104323396A (en) | 2015-02-04 |
Family
ID=52398327
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410540765.4A Pending CN104323396A (en) | 2014-10-14 | 2014-10-14 | Natural antioxidant and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104323396A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104856188A (en) * | 2015-04-25 | 2015-08-26 | 安徽蜂献蜂业有限公司 | Natural honey antioxidant and preparation method thereof |
| CN104886590A (en) * | 2015-04-25 | 2015-09-09 | 安徽蜂献蜂业有限公司 | Natural propolis antioxidant and preparation method thereof |
| CN105166378A (en) * | 2015-09-15 | 2015-12-23 | 安徽天泽饲料有限责任公司 | Premixed meat meal for anti-oxidization feed |
| CN106417445A (en) * | 2016-10-31 | 2017-02-22 | 广州嘉德乐生化科技有限公司 | Cake powder modifier and preparation method thereof |
-
2014
- 2014-10-14 CN CN201410540765.4A patent/CN104323396A/en active Pending
Non-Patent Citations (1)
| Title |
|---|
| 迟玉杰: "《食品添加剂》", 30 April 2013, 中国轻工业出版社 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104856188A (en) * | 2015-04-25 | 2015-08-26 | 安徽蜂献蜂业有限公司 | Natural honey antioxidant and preparation method thereof |
| CN104886590A (en) * | 2015-04-25 | 2015-09-09 | 安徽蜂献蜂业有限公司 | Natural propolis antioxidant and preparation method thereof |
| CN105166378A (en) * | 2015-09-15 | 2015-12-23 | 安徽天泽饲料有限责任公司 | Premixed meat meal for anti-oxidization feed |
| CN106417445A (en) * | 2016-10-31 | 2017-02-22 | 广州嘉德乐生化科技有限公司 | Cake powder modifier and preparation method thereof |
| CN106417445B (en) * | 2016-10-31 | 2019-10-29 | 广州嘉德乐生化科技有限公司 | A kind of cake powder modifier and preparation method thereof |
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| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150204 |