CN104264473B - A kind of environment-friendly type anophelifuge finishing agent - Google Patents

A kind of environment-friendly type anophelifuge finishing agent Download PDF

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CN104264473B
CN104264473B CN201410525260.0A CN201410525260A CN104264473B CN 104264473 B CN104264473 B CN 104264473B CN 201410525260 A CN201410525260 A CN 201410525260A CN 104264473 B CN104264473 B CN 104264473B
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parts
agent
environment
friendly type
finishing agent
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CN104264473A (en
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周继东
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Haimen he d Intellectual Property Service Co. Ltd.
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Haimen He D Intellectual Property Service Co Ltd
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Abstract

The invention discloses a kind of environment-friendly type anophelifuge finishing agent, in parts by weight, including following components: propylene glycol 20 30 parts, hydroxyethyl cellulose 5 10 parts, 25 parts of lecithin, stearic acid 2 10 parts, Fructus Citri Limoniae oil 25 parts, eucalyptus oil 25 parts, ammonia 23 parts, wetting agent 13 parts, softening agent 5 10 parts, cross-linking agent 5 20 parts, deionized water 50 80 parts.The invention also discloses the preparation method of this environment-friendly type anophelifuge finishing agent, its preparation method is simple, low cost, in preparation process, discharges without noxious substance, beneficially environmental conservation, and repelling effect is lasting.

Description

A kind of environment-friendly type anophelifuge finishing agent
Technical field:
The present invention relates to a kind of anophelifuge finishing agent, be specifically related to a kind of environment-friendly type anophelifuge finishing agent And preparation method thereof.
Background technology:
It is known that mosquito sucks human blood, it is to propagate malaria, filaricide, epidemic encephalitis B inflammation The communication media important with diseases such as dengue fever.Human health is constituted a serious threat by mosquito, So preventing mosquito bite critically important.The environment such as forest, grassland, wilderness are lived, work, The people of tourism, using anophelifuge is main preventive means.The U.S., Singapore, Thailand etc. The anophelifuge that country is equipped with is with diethyltoluamide as main component.Although adding diethyltoluamide to silkworm silk to knit Thing can realize lasting anophelifuge protection, but directly add diethyltoluamide and can not obtain permanent driving Mosquito effect.And diethyltoluamide has zest, diethyltoluamide can be had instead by the skin of some user Should, there is research worker to claim the anophelifuge diethyltoluamide activity to key enzyme a kind of in central nervous system There is inhibitory action.
Silk fabric have the most elegant, feel is soft and smooth, gloss is soft and moisture absorption is ventilative, health care The characteristic that function etc. are excellent, is the senior fabric in garment production.But along with people's living standard Raising and the reinforcement of environmental consciousness, the environment-friendly functionization of silk fabric arranges and also becomes increasingly Important, such as anophelifuge arranges, and becomes the another key factor of silk fabric sustainable development.
Summary of the invention:
For solving the problems referred to above, the invention provides a kind of environment-friendly type anophelifuge finishing agent, this arrangement Agent is nontoxic, beneficially environmental conservation, and repelling effect is lasting.
The purpose of the present invention is achieved through the following technical solutions:
A kind of environment-friendly type anophelifuge finishing agent, includes following components in parts by weight:
Propylene glycol 20-30 part,
Hydroxyethyl cellulose 5-10 part,
Lecithin 2-5 part,
Stearic acid 2-10 part,
Fructus Citri Limoniae oil 2-5 part,
Eucalyptus oil 2-5 part,
Ammonia 2-3 part,
Wetting agent 1-3 part,
Softening agent 5-10 part,
Cross-linking agent 5-20 part,
Deionized water 50-80 part.
Preferred as technique scheme, the environment-friendly type anophelifuge finishing agent of the present invention, with weight Part meter, including following components:
Propylene glycol 20 parts,
Hydroxyethyl cellulose 5 parts,
2 parts of lecithin,
Stearic acid 10 parts,
Fructus Citri Limoniae oil 5 parts,
Eucalyptus oil 3 parts,
Ammonia 2 parts,
Wetting agent 2 parts,
Softening agent 8 parts,
Cross-linking agent 10 parts,
Deionized water 80 parts.
The preparation method of a kind of environment-friendly type anophelifuge finishing agent of the present invention comprises the following steps:
(1) propylene glycol, deionized water and stearic acid are added in homogenizer, stirring Mix homogeneously;
(2) Fructus Citri Limoniae oil, eucalyptus oil, lecithin and hydroxyethyl cellulose are added to high-speed stirring Mix in machine, when 6000-8000 rev/min, stir 2-3h, be sufficiently mixed uniformly;
(3) in homogenizer, add softening agent, wetting agent, cross-linking agent, continue stirring Mix homogeneously;
(4) add ammonia, regulate pH to 6-8, obtain environment-friendly type anophelifuge finishing agent.
Preferred as technique scheme, described in step (3), cross-linking agent is metering system Acid acetoacetoxyethyl AAEM.
Preferred as technique scheme, described in step (4), pH is 7.
Compared with prior art, compared with prior art, the invention have the advantages that
(1) this environment-friendly type anophelifuge finishing agent, preparation method is simple, and cost is relatively low.
(2) this environment-friendly type anophelifuge finishing agent repelling effect is lasting, non-stimulated to skin, and system Discharge without noxious substance during Bei, beneficially environmental conservation.
(3) methacrylic acid acetyl second is used during the preparation of this environment-friendly type anophelifuge finishing agent Acyloxy ethyl ester AAEM cross-linking agent, this cross-linking agent and silk fabric fiber crosslink effect, The thin film that anophelifuge is formed on silk fabric surface is more firm, and carries out whole to silk fabric Bake without heat during reason, it is to avoid the mass energy of consumption, cause air pollution.
Detailed description of the invention:
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the present invention is made the most in detail Stating, this embodiment is only used for explaining the present invention, is not intended that limiting the scope of the present invention.
Embodiment 1
A kind of environment-friendly type anophelifuge finishing agent, in parts by weight, including following components:
Propylene glycol 20 parts, hydroxyethyl cellulose 5 parts,
2 parts of lecithin, stearic acid 2 parts, Fructus Citri Limoniae oil 2 parts,
Eucalyptus oil 2 parts, ammonia 2 parts, wetting agent 1 part,
Softening agent 5 parts, cross-linking agent 5 parts, deionized water 50 parts.
Its preparation method, comprises the following steps:
(1) propylene glycol, deionized water and stearic acid are added in homogenizer, stirring Mix homogeneously;
(2) Fructus Citri Limoniae oil, eucalyptus oil, lecithin and hydroxyethyl cellulose are added to high-speed stirring Mix in machine, when 6000 revs/min, stir 2h, be sufficiently mixed uniformly;
(3) in homogenizer, add softening agent, wetting agent, cross-linking agent, continue stirring Mix homogeneously;
(4) add ammonia, regulate pH to 6, obtain environment-friendly type anophelifuge finishing agent.
Embodiment 2
A kind of environment-friendly type anophelifuge finishing agent, in parts by weight, including following components:
Propylene glycol 30 parts, hydroxyethyl cellulose 10 parts,
5 parts of lecithin, stearic acid 10 parts, Fructus Citri Limoniae oil 5 parts,
Eucalyptus oil 5 parts, ammonia 3 parts, wetting agent 3 parts,
Softening agent 10 parts, cross-linking agent 20 parts, deionized water 80 parts.
Its preparation method, comprises the following steps:
(1) propylene glycol, deionized water and stearic acid are added in homogenizer, stirring Mix homogeneously;
(2) Fructus Citri Limoniae oil, eucalyptus oil, lecithin and hydroxyethyl cellulose are added to high-speed stirring Mix in machine, when 8000 revs/min, stir 3h, be sufficiently mixed uniformly;
(3) in homogenizer, add softening agent, wetting agent, cross-linking agent, continue stirring Mix homogeneously;
(4) add ammonia, regulate pH to 8, obtain environment-friendly type anophelifuge finishing agent.
Embodiment 3
A kind of environment-friendly type anophelifuge finishing agent, in parts by weight, including following components:
Propylene glycol 25 parts, hydroxyethyl cellulose 7 parts,
3 parts of lecithin, stearic acid 5 parts, Fructus Citri Limoniae oil 3 parts,
Eucalyptus oil 3 parts, ammonia 2 parts, wetting agent 2 parts,
Softening agent 7 parts, cross-linking agent 10 parts, deionized water 60 parts.
Its preparation method, comprises the following steps:
(1) propylene glycol, deionized water and stearic acid are added in homogenizer, stirring Mix homogeneously;
(2) Fructus Citri Limoniae oil, eucalyptus oil, lecithin and hydroxyethyl cellulose are added to high-speed stirring Mix in machine, when 7000 revs/min, stir 2h, be sufficiently mixed uniformly;
(3) in homogenizer, add softening agent, wetting agent, cross-linking agent, continue stirring Mix homogeneously;
(4) add ammonia, regulate pH to 7, obtain environment-friendly type anophelifuge finishing agent.
Embodiment 4
A kind of environment-friendly type anophelifuge finishing agent, in parts by weight, including following components:
Propylene glycol 28 parts, hydroxyethyl cellulose 9 parts,
4 parts of lecithin, stearic acid 8 parts, Fructus Citri Limoniae oil 4 parts,
Eucalyptus oil 4 parts, ammonia 3 parts, wetting agent 3 parts,
Softening agent 9 parts, cross-linking agent 15 parts, deionized water 70 parts.
Its preparation method, comprises the following steps:
(1) propylene glycol, deionized water and stearic acid are added in homogenizer, stirring Mix homogeneously;
(2) Fructus Citri Limoniae oil, eucalyptus oil, lecithin and hydroxyethyl cellulose are added to high-speed stirring Mix in machine, when 7800 revs/min, stir 3h, be sufficiently mixed uniformly;
(3) in homogenizer, add softening agent, wetting agent, cross-linking agent, continue stirring Mix homogeneously;
(4) add ammonia, regulate pH to 8, obtain environment-friendly type anophelifuge finishing agent.

Claims (4)

1. an environment-friendly type anophelifuge finishing agent, it is characterised in that include following in parts by weight Component:
Propylene glycol 20-30 part,
Hydroxyethyl cellulose 5-10 part,
Lecithin 2-5 part,
Stearic acid 2-10 part,
Fructus Citri Limoniae oil 2-5 part,
Eucalyptus oil 2-5 part,
Ammonia 2-3 part,
Wetting agent 1-3 part,
Softening agent 5-10 part,
Cross-linking agent 5-20 part,
Deionized water 50-80 part,
Wherein said cross-linking agent is acetoacetoxyethyl methacrylate AAEM.
2. a kind of environment-friendly type anophelifuge finishing agent, it is characterised in that with Weight portion meter, including following components:
Propylene glycol 20 parts,
Hydroxyethyl cellulose 5 parts,
2 parts of lecithin,
Stearic acid 10 parts,
Fructus Citri Limoniae oil 5 parts,
Eucalyptus oil 3 parts,
Ammonia 2 parts,
Wetting agent 2 parts,
Softening agent 8 parts,
Cross-linking agent 10 parts,
Deionized water 80 parts.
The preparation method of a kind of environment-friendly type anophelifuge finishing agent the most as claimed in claim 1, it is special Levy and be to comprise the following steps:
(1) propylene glycol, deionized water and stearic acid are added in homogenizer, stirring Mix homogeneously;
(2) Fructus Citri Limoniae oil, eucalyptus oil, lecithin and hydroxyethyl cellulose are added to high-speed stirring Mix in machine, when 6000-8000 rev/min, stir 2-3h, be sufficiently mixed uniformly;
(3) in homogenizer, add softening agent, wetting agent, cross-linking agent, continue stirring Mix homogeneously;
(4) add ammonia, regulate pH to 6-8, obtain environment-friendly type anophelifuge finishing agent.
The preparation method of a kind of environment-friendly type anophelifuge finishing agent the most as claimed in claim 3, it is special Levy and be: described in step (4), pH is 7.
CN201410525260.0A 2014-10-08 2014-10-08 A kind of environment-friendly type anophelifuge finishing agent Active CN104264473B (en)

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Publication number Priority date Publication date Assignee Title
CN105746501B (en) * 2016-03-24 2019-02-01 江苏金太阳纺织科技股份有限公司 Folium eucalypti oil assistant and preparation method thereof and fabric final finishing working solution
CN105768248B (en) * 2016-04-15 2017-08-25 上海喜眠服饰有限公司 Do not catch a cold underwear and preparation method thereof

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CN1203293A (en) * 1998-07-03 1998-12-30 王雪平 Cold antibiotic fabric and making method thereof
CN1851109A (en) * 2006-05-26 2006-10-25 天津永阔国际贸易有限公司 Fabric finishing liquid for insecticidal medium, and its use method and fabric product
CN101187158B (en) * 2007-12-07 2011-02-09 深圳清华大学研究院 Mosquito-proof finishing agent and preparation method and its uses in mosquito-preventing fabric
CN102451132A (en) * 2010-11-01 2012-05-16 董根荣 Leave-in shower gel with mosquito repelling function and preparation method thereof
CN103255616A (en) * 2013-05-22 2013-08-21 海安县联发张氏色织有限公司 Fabric mosquito repellent

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