CN102451132A - Leave-in shower gel with mosquito repelling function and preparation method thereof - Google Patents
Leave-in shower gel with mosquito repelling function and preparation method thereof Download PDFInfo
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- CN102451132A CN102451132A CN2010105280354A CN201010528035A CN102451132A CN 102451132 A CN102451132 A CN 102451132A CN 2010105280354 A CN2010105280354 A CN 2010105280354A CN 201010528035 A CN201010528035 A CN 201010528035A CN 102451132 A CN102451132 A CN 102451132A
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Abstract
The invention discloses leave-in shower gel with a mosquito repelling function and a preparation method thereof. The shower gel is prepared from an anionic surfactant, an ampholytic surfactant, sophora flavescens, raw kusnezoff monkshood root and other medicinal extracts, a moisturizing agent and a preservative. The shower gel is used for repelling mosquitoes by applying active components of a pure Chinese herbal medicinal preparation, and enabling the effective components of the medicament to be attached to a skin surface for a long time by adopting a leave-in shower gel mode, the effective components of the Chinese herbal medicament can be slowly volatilized to play a role in repelling mosquitoes and avoiding insects, and also can play roles in nourishing and moistening skin, and the pollution to environment and side effect to a human body of a chemical preparation can be solved.
Description
Technical field
The present invention relates to a kind of disposable bathing and reveal and preparation method thereof, belong to filed of daily-use chemical industry with function of driving mosquitoes.
Background technology
Mosquito not only harasses people's life, and influence people and have a rest, or the main media of some communicate illnesss (like encephalitis B, malaria, yellow fever, filaricide, dengue fever etc.) propagation, seriously influenced public health problem.In the registered 535 kinds of worm enzymophathy poison of China, just there are 265 kinds from what the mosquito apoplexy due to endogenous wind was separated to, account for 49.53% of known arbovirus sum.World Health Organization (WHO) report: the whole world was only just surpassed 3,000,000 by the people of malaria infection in 2009, caused nearly 10,000 people's death, and nearly 90% is child below five years old among the dead person.Tend to make after mosquito is wanted surely bring people's redness, scytitis such as the pain of itching; The lighter disappears a couple of days, and is heavy then to change inflammatory skins such as dermatitis, eczema into sick, and the eczema sickness rate is up to 20%; China also is not less than 15%; Particularly southern area is owing to the sultry weather in supermarket, and the eczema sickness rate is high always, accounts for 15～25% of department of dermatologry outpatient service amount.Mosquito bite is the major incentive that causes eczema, and therefore country drops into substantial contribution every year for this reason, but produces little effect.Make a general survey of various anophelifuge methods, the mosquito-repellent water kind is more on the market, but it is antibacterial in the anophelifuge process, can not to carry out antiinflammatory; Chemicals mosquito killing worm is effective, longer duration and being widely used, but mosquito is prone to produce resistance to it, and life-time service can cause serious environmental to pollute, and human body is had side effects.Therefore how to utilize plant anophelifuge active component to become the focus that people pay close attention to gradually in recent years.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of disposable bathing with function of driving mosquitoes to reveal and preparation method thereof; The present invention not only adopts the active component anophelifuge of pure Chinese herbal and crude drugs preparations; Also adopted the form of disposable bath gel to make the effective ingredient of medicine can be attached to skin surface for a long time; Play the skin moisturizing and the effect of preserving moisture again, also solved chemicals, thereby overcome the deficiency of prior art to the pollution of environment and to the side effect of human body.
For solving the problems of the technologies described above; The present invention adopts following technical scheme: a kind of disposable bathing with function of driving mosquitoes is revealed; Calculate by weight, it is to be prepared from 2～15 portions of anion surfactants, 1～10 part of amphoteric surfactant, 5～10 parts of drug extracts, 1～5 part of wetting agent and 0.005～0.5 portion of antiseptic.
Aforesaid a kind of disposable bathing dew with function of driving mosquitoes is preferably: it is to be prepared from 10 portions of anion surfactants, 5 parts of amphoteric surfactantes, 8 parts of drug extracts, 3 parts of wetting agents and 0.3 portion of antiseptic.
Aforesaid drug extract prepares according to following method: calculate by weight; Accurately take by weighing 25～35 parts of Radix Sophorae Flavescentiss, 15～25 parts of Radix Aconiti Kusnezoffii, 5～15 parts of Herba Senecionis Scandentiss, 5～15 parts of Radixs Stemonae, 5～15 portions of Oleum menthae, 5～15 portions of Oleum Caryophyllis, 3～8 parts of Borneolum Syntheticums; Decocte with water 3 times; The each decoction 1 hour filters, and merging filtrate gets drug extract.
Aforesaid drug extract is preferably according to method for preparing: calculate by weight; Accurately take by weighing 30 parts of Radix Sophorae Flavescentiss, 20 parts of Radix Aconiti Kusnezoffii, 10 parts of Herba Senecionis Scandentiss, 10 parts of Radixs Stemonae, 10 portions of Oleum menthae, 10 portions of Oleum Caryophyllis, 5 parts of Borneolum Syntheticums, decocte with water 3 times adds 6 times of water gagings for the first time; Second and third time respectively adds 5 times of water gagings; The each decoction 1 hour filters, and merging filtrate gets drug extract.
Aforesaid anion surfactant is one or more in sulfuric acid, lignosulfonates and the alkyl glyceryl ether sulfonate of polyoxyethylene alkyl ether sulfate salt, derivative of fatty acid; Amphoteric surfactant is one or more in imidazolidine derivatives, betanin derivative and the alanine derivatives; Wetting agent be in hyaluronic acid, chitosan, Aloe glue, glycerol and the propylene glycol one or more; Antiseptic is one or more in benzoic acid and sodium benzoate, sorbic acid and its esters and the P-hydroxybenzoic acid lipid.
The method for preparing that described disposable bathing with function of driving mosquitoes is revealed comprises following steps:
(1) gets anion surfactant according to aforementioned weight and amphoteric surfactant is soluble in water, stir, add drug extract then, continue to stir and make its mix homogeneously;
(2) according to aforementioned weight antiseptic is joined in the wetting agent, fully stir and make its dissolving;
(3) (1) and (2) two parts solution is mixed, and the stirring that homogenizes promptly gets.
The method for preparing that aforesaid disposable bathing with function of driving mosquitoes is revealed is specially:
(1) gets anion surfactant and amphoteric surfactant according to aforementioned weight, and be dissolved in 10～50 parts of water, stir, add drug extract then, continue stirring and make its mix homogeneously;
(2) according to aforementioned weight antiseptic is joined in the wetting agent, fully stir and make its dissolving;
(3) (1) and (2) two parts solution being mixed, and regulate pH=5～7 with citric acid, is to stir 30～60 minutes under 3000～10000rmp in homogenizing speed.
Add in 4～6 portions of skin protectant and 0.3～0.6 part of viscosifier one or both in the method for preparing preparation process (2) that aforesaid disposable bathing with function of driving mosquitoes is revealed.
Aforesaid skin protectant is one or more in stearic acid, olive oil, vaseline, lecithin and the liquid paraffin.
Aforesaid viscosifier are one or more in hydroxyethyl-cellulose, methylcellulose, sodium carboxymethyl cellulose and the polyvinylpyrrolidone.
Among the present invention Radix Sophorae Flavescentis because of the function that has anophelifuge and keep away worm, repellent antipruritic as monarch drug; Radix Aconiti Kusnezoffii have activating blood circulation and unblocking obstruction, anophelifuge parasite killing, reducing swelling and alleviating pain function and as ministerial drug; Playing a role with the accessory drugs principal drug assistance, is adjuvant drug with ability heat-clearing and toxic substances removing, the Herba Senecionis Scandentis of reducing swelling and alleviating pain, the Radix Stemonae, Oleum menthae, Oleum Caryophylli, goes out to assist monarch drug better to bring into play outside the curative effect; And can treat accompanied symptoms and enlarging application range, again with the anticorrosion itching relieving Borneolum Syntheticum of understand things pain-stopping as messenger drug, keep away effects such as worm, anti-inflammation detumescence, killing parasites for relieving itching thereby make above each medicine play anophelifuge altogether.
In the present invention; Adopt suspension to carry out quantitative disinfecting test; In the in-vitro antibacterial test; Act on 1 minute,, Candida albicans false unicellular only to golden yellow Fructus Vitis viniferae bacillus, Aerugo and colibacillary average kill ratio are greater than 99%, to Salmonella typhi effect 2 minutes, and average kill ratio places 50 ℃ incubator to carry out bacteriostatic test in 10 days product greater than 99%; Experimental result proof Gram-positive bacillus, gram negative bacilli, staphylococcus saprophyticus and enterococcus etc. all produce tangible inhibition zone, prove that product of the present invention has persistent insurgent group sterilizing function.
Bath gel directly contacts with skin in addition, and will be detained a period of time at skin surface, so need three groups of tests are carried out in its safety and toxicology:
1 acute irritation property tuerculoderma
8 rabbit spinal column diamond wools are cut, do not damaged epidermis, left and right each the about 3cm * 3cm of QUMAO scope.8 rabbit are divided into A, B group at random; Get and tried the about 0.5ml of thing and directly be coated on the skin that (the A group is coated with bath gel; The B group is coated with 10 times of concentration bath gel), (2.5cm * 2.5cm) cover with 1 layer of cellophane, reuse nonirritant adhesive plaster and binder are fixed to use 2 layers of gauze then.Opposite side skin is as contrast.Adopt blocking test, the application time is 4h.After removing is tried thing 1,24,48,72h observes and to smear the position dermoreaction; Carry out the dermoreaction scoring by " cosmetics health standard " (2007) specified standard; Meansigma methods with the animal subject integration is carried out overall merit; Top average according to 24,48, during 72h is judged skin irritation intensity.
More than 2 skin irritation test
Back part of animal spinal column both sides are cut each 3cm * 3cm of QUMAO scope, application area 2.5cm * 2.5cm by hair before the test.Get and tried the about 0.5ml of thing and spread upon on the side skin (the A group is coated with bath gel, and the B group is coated with 10 times of concentration bath gel), opposite side is coated with deionized water as contrast, smears every day 1 time, smears 14d continuously.Since the 2nd day, smear preceding cropping at every turn, remove the residual thing that tried with deionized water.Observed result behind the 1h, by the scoring of " cosmetics health standard " (2007) specified standard, check plot and trial zone are handled equally.
The test of 3 eye irritations
8 rabbit are divided into A, B group at random; Open the palpebra inferior of rabbit one branch hole eyeball gently, will be tried thing 0.1ml (100mg) and splash into (the A group is coated with bath gel, and the B group is coated with 10 times of concentration bath gel) in (or being coated with) conjunctival sac; Make the passive closed 1s of upper and lower eyelid, to prevent that being tried thing loses.The opposite side eyes are not handled, and make own control.Splash into and tried not wash eyes in the 24h behind the thing.Clinical examination and scoring: splash into tried thing after 1,24,48,72h and animal eyes being checked in the 4th day and the 7th day.If IR does not appear in 72h, get final product termination test.If find to involve cornea or not recuperator arranged in other stimulations 7d, be reversibility or the irreversibility of confirming this infringement, need to prolong observing time, generally be no more than 21d, and the 7th, 14,21 day visual report is provided.Except corneal, iris, conjunctiva were observed, other detrimental effects were all noted down and are reported.All write down the integration of eye IR in each inspection by the standards of grading of eye infringement.Use handheld slit lamp to carry out an IR inspection.After 24h observation and record end; With fluorescein sodium the eyes of all animals are done further inspection, with give tried animal corneal behind the thing, iris or conjunctiva 24,48h or 72h the top and recovery time of observing the IR of time point estimate, judge the stimulation degree of thing to eye of being tried.
Test result shows: no matter be acute skin irritation property test or repeatedly the skin irritation test does not see that all zest and corrosivity reacts, integration is 0.Explain that product of the present invention to the skin nonirritant, can not damage skin.In the test of acute eye irritation, only there is 1 rabbit conjunctiva when 1h observes that slight hyperemia is arranged, slight temporary transient zest is described, but recover normal during the 24h observation; All the other do not observe any IR in 72h, integration is 0, explain that product of the present invention to the eyes nonirritant, can not damage eyes, but will avoid pleasing to the eye when using, and prevent to cause of short duration zest.
Compared with prior art; The present invention adopts simple process and equipment; To the deficiency of existing anophelifuge method, prepare a kind of disposable bath gel of function of driving mosquitoes, the present invention not only uses the active component anophelifuge of pure Chinese herbal and crude drugs preparations; Also adopted the form of disposable bath gel to make the effective ingredient of medicine can be attached to skin surface for a long time; Chinese herbal medicine effective ingredients is slowly volatilized and play the effect that anophelifuge is kept away worm in a long time, play skin moisturizing and the effect of preserving moisture again, also solved chemicals to the pollution of environment and to the side effect of human body.
The specific embodiment
Embodiment 1: drug extract preparation: calculate by weight; Accurately take by weighing 30 parts of Radix Sophorae Flavescentiss, 20 parts of Radix Aconiti Kusnezoffii, 10 parts of Herba Senecionis Scandentiss, 10 parts of Radixs Stemonae, 10 portions of Oleum menthae, 10 portions of Oleum Caryophyllis, 5 parts of Borneolum Syntheticums, decocte with water 3 times adds 6 times of water gagings for the first time; Second and third time respectively adds 5 times of water gagings; The each decoction 1 hour filters, and merging filtrate gets drug extract.
Disposable bath gel method for preparing with function of driving mosquitoes:
(1) gets 10 parts of alkyl glyceryl ether sulfonates and 5 parts of alanine derivatives are dissolved in 30 parts of water, stir, add 8 parts of aforesaid drug extracts then, continue to stir and make its mix homogeneously;
(2) 0.3 part of P-hydroxybenzoic acid fat is joined in 3 parts of propylene glycol, fully stir and make its dissolving;
(3) (1) and (2) two parts solution being mixed, and regulate pH=6 with citric acid, is to stir 45 minutes under the 6000rmp in homogenizing speed, promptly gets.
Embodiment 2: drug extract preparation: calculate by weight; Accurately take by weighing 25 parts of Radix Sophorae Flavescentiss, 15 parts of Radix Aconiti Kusnezoffii, 5 parts of Herba Senecionis Scandentiss, 5 parts of Radixs Stemonae, 5 portions of Oleum menthae, 5 portions of Oleum Caryophyllis, 3 parts of Borneolum Syntheticums, decocte with water 3 times decocted 1 hour at every turn; Filter, merging filtrate gets drug extract.
Disposable bath gel method for preparing with function of driving mosquitoes:
(1) gets 2 portions of polyoxyethylene alkyl ether sulfate salt and 1 part of imidazolidine derivatives is dissolved in 10 parts of water, stir, add 5 parts of aforesaid drug extracts then, continue to stir and make its mix homogeneously;
(2) 0.005 part of benzoic acid is joined in 1 part of hyaluronic acid, fully stir and make its dissolving;
(3) (1) and (2) two parts solution is mixed, and the stirring that homogenizes promptly gets.
Embodiment 3: drug extract preparation: calculate by weight; Accurately take by weighing 35 parts of Radix Sophorae Flavescentiss, 25 parts of Radix Aconiti Kusnezoffii, 15 parts of Herba Senecionis Scandentiss, 15 parts of Radixs Stemonae, 15 portions of Oleum menthae, 15 portions of Oleum Caryophyllis, 8 parts of Borneolum Syntheticums, decocte with water 3 times adds 6 times of water gagings for the first time; Second and third time respectively adds 5 times of water gagings; The each decoction 1 hour filters, and merging filtrate gets drug extract.
Disposable bath gel method for preparing with function of driving mosquitoes:
(1) sulfuric acid and 10 parts of betanin derivative of getting 15 parts of derivative of fatty acid are dissolved in 50 parts of water, stir, and add 10 parts of aforesaid drug extracts then, continue to stir to make its mix homogeneously;
(2) 0.5 part of sorbic acid, 6 parts of stearic acid and 0.6 part of hydroxyethyl-cellulose are joined in 5 parts of chitosans, fully stir and make its dissolving;
(3) (1) and (2) two parts solution being mixed, and regulate pH=7 with citric acid, is to stir 60 minutes under the 10000rmp in homogenizing speed, promptly gets.
Embodiment 4: drug extract preparation: calculate by weight; Accurately take by weighing 28 parts of Radix Sophorae Flavescentiss, 18 parts of Radix Aconiti Kusnezoffii, 12 parts of Herba Senecionis Scandentiss, 12 parts of Radixs Stemonae, 12 portions of Oleum menthae, 12 portions of Oleum Caryophyllis, 7 parts of Borneolum Syntheticums, decocte with water 3 times adds 6 times of water gagings for the first time; Second and third time respectively adds 5 times of water gagings; The each decoction 1 hour filters, and merging filtrate gets drug extract.
Disposable bath gel method for preparing with function of driving mosquitoes:
(1) gets 8 parts of lignosulfonates and 8 parts of betanin derivative are dissolved in 40 parts of water, stir, add 6 parts of aforesaid drug extracts then, continue to stir and make its mix homogeneously;
(2) 0.1 part of benzoate, 5 parts of vaseline and 0.5 part of polyvinylpyrrolidone are joined in 4 parts of Aloe glues, fully stir and make its dissolving;
(3) (1) and (2) two parts solution being mixed, and regulate pH=7 with citric acid, is to stir 40 minutes under the 8000rmp in homogenizing speed, promptly gets.
The method for using of above product is: extrude an amount of shower and be exposed on the centre of the palm or the moistening bubble cottonrose hibiscus, evenly wipe and rub whole body.
Claims (10)
1. the disposable bathing with function of driving mosquitoes is revealed; It is characterized in that: calculate by weight, it is to be prepared from 2～15 portions of anion surfactants, 1～10 part of amphoteric surfactant, 5～10 parts of drug extracts, 1～5 part of wetting agent and 0.005～0.5 portion of antiseptic.
2. a kind of disposable bathing with function of driving mosquitoes according to claim 1 is revealed, and it is characterized in that: it is to be prepared from 10 portions of anion surfactants, 5 parts of amphoteric surfactantes, 8 parts of drug extracts, 3 parts of wetting agents and 0.3 portion of antiseptic.
3. a kind of disposable bathing with function of driving mosquitoes according to claim 1 and 2 is revealed; It is characterized in that: described drug extract prepares according to following method: calculate by weight; Accurately take by weighing 25～35 parts of Radix Sophorae Flavescentiss, 15～25 parts of Radix Aconiti Kusnezoffii, 5～15 parts of Herba Senecionis Scandentiss, 5～15 parts of Radixs Stemonae, 5～15 portions of Oleum menthae, 5～15 portions of Oleum Caryophyllis, 3～8 parts of Borneolum Syntheticums, decocte with water 3 times decocted 1 hour at every turn; Filter, merging filtrate gets drug extract.
4. a kind of disposable bathing with function of driving mosquitoes according to claim 3 is revealed, and it is characterized in that: described drug extract prepares according to following method: calculate by weight, accurately take by weighing 30 parts of Radix Sophorae Flavescentiss, 20 parts of Radix Aconiti Kusnezoffii, 10 parts of Herba Senecionis Scandentiss, 10 parts of Radixs Stemonae, 10 portions of Oleum menthae, 10 portions of Oleum Caryophyllis, 5 parts of Borneolum Syntheticums; Decocte with water 3 times; For the first time add 6 times of water gagings, second and third time respectively adds 5 times of water gagings, decocts 1 hour at every turn; Filter, merging filtrate gets drug extract.
5. a kind of disposable bathing with function of driving mosquitoes according to claim 1 and 2 is revealed, and it is characterized in that: described anion surfactant is one or more in sulfuric acid, lignosulfonates and the alkyl glyceryl ether sulfonate of polyoxyethylene alkyl ether sulfate salt, derivative of fatty acid; Described amphoteric surfactant is one or more in imidazolidine derivatives, betanin derivative and the alanine derivatives; Described wetting agent be in hyaluronic acid, chitosan, Aloe glue, glycerol and the propylene glycol one or more; Described antiseptic is one or more in benzoic acid and sodium benzoate, sorbic acid and its esters and the P-hydroxybenzoic acid lipid.
6. the method for preparing that arbitrary described disposable bathing with function of driving mosquitoes is revealed like claim 1～5, it is characterized in that: said method comprises following steps:
(1) gets anion surfactant according to aforementioned weight and amphoteric surfactant is soluble in water, stir, add drug extract then, continue to stir and make its mix homogeneously;
(2) according to aforementioned weight antiseptic is joined in the wetting agent, fully stir and make its dissolving; (3) (1) and (2) two parts solution is mixed, and the stirring that homogenizes promptly gets.
7. the method for preparing that arbitrary described disposable bathing with function of driving mosquitoes is revealed according to claim 6, it is characterized in that: said method comprises following steps:
(1) gets anion surfactant and amphoteric surfactant according to aforementioned weight, and be dissolved in 10～50 parts of water, stir, add drug extract then, continue stirring and make its mix homogeneously;
(2) according to aforementioned weight antiseptic is joined in the wetting agent, fully stir and make its dissolving;
(3) (1) and (2) two parts solution being mixed, and regulate pH=5～7 with citric acid, is to stir 30～60 minutes under 3000～10000rmp in homogenizing speed.
8. the method for preparinies of revealing according to claim 6 or 7 described disposable bathings with function of driving mosquitoes is characterized in that: one or both in said preparation process (2) in 4～6 portions of skin protectant of adding and 0.3～0.6 part of viscosifier.
9. the method for preparing that the said according to Claim 8 disposable bathing with function of driving mosquitoes is revealed, it is characterized in that: described skin protectant is one or more in stearic acid, olive oil, vaseline, lecithin and the liquid paraffin.
10. the method for preparing that the disposable bathing with function of driving mosquitoes according to claim 8 is revealed, it is characterized in that: described viscosifier are one or more in hydroxyethyl-cellulose, methylcellulose, sodium carboxymethyl cellulose and the polyvinylpyrrolidone.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010105280354A CN102451132A (en) | 2010-11-01 | 2010-11-01 | Leave-in shower gel with mosquito repelling function and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2010105280354A CN102451132A (en) | 2010-11-01 | 2010-11-01 | Leave-in shower gel with mosquito repelling function and preparation method thereof |
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| CN102451132A true CN102451132A (en) | 2012-05-16 |
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| CN2010105280354A Pending CN102451132A (en) | 2010-11-01 | 2010-11-01 | Leave-in shower gel with mosquito repelling function and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104264473A (en) * | 2014-10-08 | 2015-01-07 | 苏州印丝特纺织数码科技有限公司 | Environmentally-friendly mosquito-repelling finishing agent |
| CN105878104A (en) * | 2016-04-08 | 2016-08-24 | 哈尔滨工业大学 | Washing-free low-foam bathing product for space or diving environment and preparation method thereof |
| CN106389272A (en) * | 2016-08-16 | 2017-02-15 | 南通蛇类治疗研究所 | Natural plant effective bath lotion |
| CN107236627A (en) * | 2017-06-05 | 2017-10-10 | 丁惠良 | Mosquito proof liquid detergent |
-
2010
- 2010-11-01 CN CN2010105280354A patent/CN102451132A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104264473A (en) * | 2014-10-08 | 2015-01-07 | 苏州印丝特纺织数码科技有限公司 | Environmentally-friendly mosquito-repelling finishing agent |
| CN105878104A (en) * | 2016-04-08 | 2016-08-24 | 哈尔滨工业大学 | Washing-free low-foam bathing product for space or diving environment and preparation method thereof |
| CN105878104B (en) * | 2016-04-08 | 2018-09-11 | 哈尔滨工业大学 | A kind of disposable low bubble bath product and preparation method thereof being used for space or submersible environment |
| CN106389272A (en) * | 2016-08-16 | 2017-02-15 | 南通蛇类治疗研究所 | Natural plant effective bath lotion |
| CN107236627A (en) * | 2017-06-05 | 2017-10-10 | 丁惠良 | Mosquito proof liquid detergent |
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Application publication date: 20120516 |