CN104263224A - Cold-resistant and water-proof damping coating - Google Patents
Cold-resistant and water-proof damping coating Download PDFInfo
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- CN104263224A CN104263224A CN201410592421.8A CN201410592421A CN104263224A CN 104263224 A CN104263224 A CN 104263224A CN 201410592421 A CN201410592421 A CN 201410592421A CN 104263224 A CN104263224 A CN 104263224A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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Abstract
The invention discloses a cold-resistant and water-proof damping coating which is characterized in that raw materials comprise the following components in parts by weight: 40-60 parts of waterborne polyurethane/polyacrylate latex, 5-16 parts of sericite modified by a coupling agent, 5-15 parts of talcum powder, 3-10 parts of hollow glass beads, 3-8 parts of mica powder, 5-12 parts of perlite, 5-17 parts of kieselguhr, 4-10 parts of nanometer acrylate rubber powder, 0.3-0.9 parts ofphosphate modified amine compound, 3-6 parts of magnesium hydroxide, 5-12 parts of aluminium hydroxide, 3-10 parts of glass fibre, 1-3 parts of boron-containing phenolic resin, 2-5 parts of organic solvent, 2-7 parts of a film coalescing aid, 2-5 parts of aids, and 20-30 parts of deionized water. The cold-resistant and water-proof damping coating provided by the invention has good damping performance, cold resistance and water-proof property.
Description
Technical field
The present invention relates to technical field of coatings, particularly relate to a kind of cold-resistant water-fast polymer damping paint.
Background technology
Polymer damping paint take high molecular polymer as the speciality coating with damping, sound insulation and certain stopping property that binder resin obtains, because of easy construction, especially more can embody its superiority to baroque surface, be widely used in the noise reduction of the damping of aircraft, boats and ships, vehicle and various machinery at present.Raising along with people's living standard and the attention to environmental factors, the requirement of people to sound insulation, noise-reducing coating is also more and more higher, and the damping capacity of existing damping paint, winter hardiness and water tolerance can not meet the requirement of society.Therefore, how to develop a kind of cold-resistant, water-fast high damping coating, become task extremely urgent at present.
Summary of the invention
The present invention proposes a kind of cold-resistant water-fast polymer damping paint, its damping capacity, cold-resistant and water-tolerant.
The present invention proposes a kind of cold-resistant water-fast polymer damping paint, its raw material comprises following component by weight: aqueous polyurethane/polyacrylate dispersion 40-60 part, coupling agent modified sericite 5-16 part, talcum powder 5-15 part, hollow glass micropearl 3-10 part, mica powder 3-8 part, perlite 5-12 part, diatomite 5-17 part, nano acrylic ester rubber powder 4-10 part, phosphate modified amine compound 0.3-0.9 part, magnesium hydroxide 3-6 part, aluminium hydroxide 5-12 part, glass fibre 3-10 part, boron bakelite resin 1-3 part, organic solvent 2-5 part, film coalescence aid 2-7 part, auxiliary agent 2-5 part, deionized water 20-35 part,
Wherein, described phosphate modified amine compound is prepared according to following technique: join in flask by 20-40 part phosphoric acid and 10-20 part quadrol by weight, stirring reaction 20-35min, stirring is warming up to 45-55 DEG C, and reaction 20-28min, is warming up to 82-90 DEG C, reaction 20-28min, add 10-18 part hexamethylenetetramine, stirring reaction 40-60min, after cooling, drying obtains described phosphate modified amine compound.
Preferably, its raw material comprises following component by weight: aqueous polyurethane/polyacrylate dispersion 50-56 part, coupling agent modified sericite 9-14 part, talcum powder 7-13 part, hollow glass micropearl 7-8.5 part, mica powder 5-6.8 part, perlite 9-11 part, diatomite 9-13 part, nano acrylic ester rubber powder 7-8.9 part, phosphate modified amine compound 0.5-0.79 part, magnesium hydroxide 5-5.6 part, aluminium hydroxide 7-10 part, glass fibre 6-9 part, boron bakelite resin 1.7-2.3 part, organic solvent 2.9-4.5 part, film coalescence aid 5-6.7 part, auxiliary agent 3-4.5 part, deionized water 26-32 part.
Preferably, its raw material comprises following component by weight: aqueous polyurethane/polyacrylate dispersion 54 parts, coupling agent modified sericite 13 parts, talcum powder 11 parts, hollow glass micropearl 8.3 parts, mica powder 6.5 parts, perlite 10 parts, 12 parts, diatomite, nano acrylic ester rubber powder 8.6 parts, phosphate modified amine compound 0.63 part, magnesium hydroxide 5.3 parts, 8.3 parts, aluminium hydroxide, 7.6 parts, glass fibre, boron bakelite resin 2.1 parts, organic solvent 3.4 parts, film coalescence aid 5.9 parts, auxiliary agent 4.2 parts, deionized water 31 parts.
Preferably, described organic solvent is one or more the combination in ethanol, Virahol, methyl alcohol, propyl alcohol, propyl carbinol, ethylene glycol, Diethylene Glycol, 1,2-PD, 1,3-PD, dipropylene glycol, BDO, pentanediol, glycerol.
Preferably, described film coalescence aid is one or more the combination in polyoxyethylene glycol, propylene glycol phenylate, alcohol ester 12, butyl glycol ether.
Preferably, described auxiliary agent is one or more the combination in defoamer, thickening material, flow agent, dispersion agent, wetting agent.
Preferably, described thickening material is one or more the combination in carboxymethyl cellulose, Walocel MT 20.000PV, sodium polyacrylate, polyvinyl alcohol, Natvosol, o-phthalic acid dibutyl ester, Tritolyl Phosphate, dibutyl phthalate.
Preferably, described phosphate modified amine compound is prepared according to following technique: join in flask by 29-33 part phosphoric acid and 14-18 part quadrol by weight, stirring reaction 29-32min, stirring is warming up to 49-53 DEG C, and reaction 24-26min, is warming up to 84-87 DEG C, reaction 25-27min, add 12-16 part hexamethylenetetramine, stirring reaction 49-54min, after cooling, drying obtains described phosphate modified amine compound.
Preferably, described phosphate modified amine compound is prepared according to following technique: join in flask by 32 parts of phosphoric acid and 15 parts of quadrols by weight, stirring reaction 31min, stirring is warming up to 52 DEG C, and reaction 25min, is warming up to 85 DEG C, reaction 26min, add 14 parts of hexamethylenetetramines, stirring reaction 53min, after cooling, drying obtains described phosphate modified amine compound.
Urethane has good winter hardiness, elasticity, organic solvent resistance etc., but its poor water resistance, polyacrylic ester has good water tolerance, chemicals-resistant and weathering resistance, aqueous polyurethane/the polyacrylate dispersion selected in the present invention achieves the combination of urethane and polyacrylic ester, as the filmogen of coating, make the coating obtained not only have the original winter hardiness of urethane, elasticity, organic solvent resistance, have the water tolerance of acrylate, chemical-resistant and weathering resistance simultaneously concurrently, sericite is sheet structure, specific surface area is large, there is good elasticity and toughness, the contact area between filler and emulsion can be improved in coating, when running into external shock, can oriented sliding, increase the friction internal loss of coating, simultaneously, sericite particle diameter is little, the surface density of coating can be improved, increase the decay to sound wave, there is good dissipation factor and sound insulation property, improve the damping capacity of coating, but the surface properties of sericite and emulsion difference very large, both poor compatibility, the group be effectively combined with organism is contained on coupling agent modified sericite surface, change its original surface properties, better can be combined with polymer emulsion, good with the covering property of emulsion, in conjunction with tight, coating has better properties, talcum powder can give the brush of coating excellence, levelling property and gloss retention, mica powder provides snappiness, and hardness is higher, coating has good shock-resistance, effectively can also improve solidity to corrosion and the dryness of coating simultaneously, perlite can improve sound absorbing and the anti-freezing property of coating, it is large that diatomite has voidage, absorptivity is strong, stable chemical nature, wear-resisting, the feature such as heat-resisting, excellent surface property can be provided for coating, increase-volume, thickening and raising sticking power, owing to having larger pore volume, film can be made to shorten time of drying, the consumption of resin can also be reduced, reduce costs, the various fillers added cooperatively interact, not only occupy polymer segment in system and pile up space, and can with the mutual friction of polymer macromolecule interchain phase, add the internal loss of coating, improve the damping capacity of coating, by adding nanometer acrylic rubber powder and regulating its content, under the prerequisite preventing system viscosity from increasing, further improve the damping capacity of coating, boron bakelite resin has the distinguishing features such as resistance toheat is good, charring rate is high, in the present invention, it is coordinated as fire retardant with phosphate modified amine compound, improve the flame retardant resistance of coating, decrease inflammable emulsion to burn the infringement brought, improve the performance of coating.
The various raw materials selected in the present invention cooperatively interact, there are good chemical compatibility and stability, the advantage of each raw material is collaborative to be promoted, the coating damping temp field width obtained, can sound insulation damping, flame-proof environmental protection, have larger sticking power to base material, raw material is sufficient, good economy performance, can be applicable to the field such as automobile, boats and ships.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in detail; should understand; embodiment is only for illustration of the present invention, instead of for limiting the present invention, any amendment, equivalent replacement etc. made on basis of the present invention is all in protection scope of the present invention.
In a particular embodiment, cold-resistant water-fast polymer damping paint of the present invention, in its raw material, the parts by weight of aqueous polyurethane/polyacrylate dispersion can be 40.3, 41, 41.5, 42, 42.3, 43, 43.4, 44, 44.5, 45, 45.6, 46, 46.7, 47, 47.5, 48, 48.3, 49, 49.5, 50.3, 51, 51.2, 52, 52.6, 53, 53.4, 54.6, 55, 55.7, 56.8, 57, 57.4, 58, 58.6, 59, 59.3 parts, the parts by weight of coupling agent modified sericite can be 5.6, 6, 6.3, 7, 7.4, 8, 8.5, 9.3, 10, 10.3, 11, 11.5, 12, 12.4, 13.6, 14.5, 15, 15.7 parts, talcous parts by weight can be 5.3, 6, 6.7, 7.4, 8, 8.2, 9, 9.6, 10, 10.3, 11.5, 12, 12.4, 13.5, 14, 14.8 parts, the parts by weight of hollow glass micropearl can be 3.2, 3.9, 4, 4.5, 4.9, 5, 5.3, 5.8, 6, 6.4, 6.8, 7.5, 7.9, 8, 9, 9.4, 9.8 parts, the parts by weight of mica powder can be 3.2, 3.8, 4, 4.5, 5.6, 6, 6.4, 7, 7.8 parts, perlitic parts by weight can be 5.6, 6, 6.3, 7, 7.5, 8, 8.4, 9.5, 10.3, 10.8, 11.2, 11.8 parts, diatomaceous parts by weight can be 5.3, 5.8, 6, 6.3, 6.7, 7, 7.8, 8, 8.5, 9.6, 10, 10.3, 11, 11.5, 12.4, 13.6, 14, 14.5, 15, 15.8, 16, 16.7 parts, the parts by weight of nano acrylic ester rubber powder can be 4.2, 4.9, 5, 5.3, 5.8, 6, 6.4, 7.4, 7.9, 8, 8.2, 8.7, 9, 9.6 parts, the parts by weight of phosphate modified amine compound can be 0.36, 0.4, 0.45, 0.56, 0.6, 0.68, 0.7, 0.72, 0.8, 0.83, 0.89 part, the parts by weight of magnesium hydroxide can be 3.2, 3.8, 4, 4.2, 4.5, 4.7, 5.2, 5.8, 6 parts, the parts by weight of aluminium hydroxide can be 5.2, 5.8, 6, 6.4, 6.8, 7.2, 7.8, 8, 8.6, 9, 9.4, 10.2, 10.8, 11, 11.3, 11.5 parts, the parts by weight of glass fibre can be 3.2, 4, 5, 5.6, 6.8, 7, 7.5, 8, 8.9, 9.3 parts, the parts by weight of boron bakelite resin can be 1.2, 1.5, 1.8, 2, 2.6, 2.72, 2.9 parts, the parts by weight of organic solvent can be 2.3, 2.6, 2.8, 3, 3.8, 4, 4.9 parts, the parts by weight of film coalescence aid can be 2.3, 2.6, 2.9, 3, 3.4, 3.8, 4, 4.3, 4.9, 5.3, 5.8, 6, 6.2, 6.9 parts, the parts by weight of auxiliary agent can be 2.3, 2.9, 3.4, 3.8, 4, 4.8 parts, the parts by weight of deionized water can be 20.3, 21, 21.6, 22, 22.3, 23, 23.4, 24.5, 25, 25.6, 26.3, 27, 27.5, 28, 28.4, 29, 29.3, 30, 30.5, 31.6, 32.4, 33, 33.5, 34 parts.
Embodiment 1
Cold-resistant water-fast polymer damping paint of the present invention, its raw material comprises following component by weight: aqueous polyurethane/polyacrylate dispersion 40 parts, coupling agent modified sericite 16 parts, talcum powder 5 parts, hollow glass micropearl 10 parts, mica powder 3 parts, perlite 12 parts, 5 parts, diatomite, nano acrylic ester rubber powder 10 parts, phosphate modified amine compound 0.3 part, magnesium hydroxide 6 parts, 5 parts, aluminium hydroxide, 10 parts, glass fibre, boron bakelite resin 1 part, organic solvent 5 parts, film coalescence aid 2 parts, auxiliary agent 5 parts, deionized water 20 parts;
Wherein, described phosphate modified amine compound is prepared according to following technique: join in flask by 20 parts of phosphoric acid and 20 parts of quadrols by weight, stirring reaction 20min, stirring is warming up to 55 DEG C, and reaction 20min, is warming up to 90 DEG C, reaction 20min, add 18 parts of hexamethylenetetramines, stirring reaction 40min, after cooling, drying obtains described phosphate modified amine compound.
Performance Detection is carried out to water-fast polymer damping paint cold-resistant described in the present embodiment, its detected result and technical indicator as shown in table 1:
Cold-resistant water-fast polymer damping paint performance test results and technical indicator described in table 1 embodiment 1
Embodiment 2
Cold-resistant water-fast polymer damping paint of the present invention, its raw material comprises following component by weight: aqueous polyurethane/polyacrylate dispersion 60 parts, coupling agent modified sericite 5 parts, talcum powder 15 parts, hollow glass micropearl 3 parts, mica powder 8 parts, perlite 5 parts, 17 parts, diatomite, nano acrylic ester rubber powder 4 parts, phosphate modified amine compound 0.9 part, magnesium hydroxide 3 parts, 12 parts, aluminium hydroxide, 3 parts, glass fibre, boron bakelite resin 3 parts, dipropylene glycol 2 parts, propylene glycol phenylate 3 parts, alcohol ester 12 parts, auxiliary agent 2 parts, deionized water 35 parts;
Wherein, described auxiliary agent is that defoamer, thickening material, flow agent, dispersion agent, wetting agent are by the combination of any weight ratio;
Described phosphate modified amine compound is prepared according to following technique: join in flask by 40 parts of phosphoric acid and 10 parts of quadrols by weight, stirring reaction 35min, stirring is warming up to 45 DEG C, reaction 28min, be warming up to 82 DEG C, reaction 28min, adds 10 parts of hexamethylenetetramines, stirring reaction 60min, after cooling, drying obtains described phosphate modified amine compound.
Performance Detection is carried out to water-fast polymer damping paint cold-resistant described in the present embodiment, its detected result and technical indicator as shown in table 2:
Cold-resistant water-fast polymer damping paint performance test results and technical indicator described in table 2 embodiment 2
Embodiment 3
Cold-resistant water-fast polymer damping paint of the present invention, its raw material comprises following component by weight: aqueous polyurethane/polyacrylate dispersion 51.2 parts, coupling agent modified sericite 10 parts, talcum powder 13.5 parts, hollow glass micropearl 6.4 parts, mica powder 7.8 parts, perlite 11.2 parts, 11.5 parts, diatomite, nano acrylic ester rubber powder 8.7 parts, phosphate modified amine compound 0.83 part, magnesium hydroxide 5.8 parts, 10.8 parts, aluminium hydroxide, 7 parts, glass fibre, boron bakelite resin 2.6 parts, 1, 4-butyleneglycol 1.5 parts, pentanediol 2.3 parts, film coalescence aid 5.8 parts, thickening material 3.8 parts, deionized water 30 parts,
Wherein, described film coalescence aid is that polyoxyethylene glycol, propylene glycol phenylate, alcohol ester 12, butyl glycol ether are by the combination of any weight ratio; Described thickening material is that carboxymethyl cellulose, Walocel MT 20.000PV, sodium polyacrylate, polyvinyl alcohol, Natvosol, o-phthalic acid dibutyl ester, Tritolyl Phosphate, dibutyl phthalate are by the combination of any weight ratio;
Described phosphate modified amine compound is prepared according to following technique: join in flask by 26 parts of phosphoric acid and 17 parts of quadrols by weight, stirring reaction 29min, stirring is warming up to 49 DEG C, reaction 25min, be warming up to 87 DEG C, reaction 26min, adds 17 parts of hexamethylenetetramines, stirring reaction 53min, after cooling, drying obtains described phosphate modified amine compound.
Performance Detection is carried out to water-fast polymer damping paint cold-resistant described in the present embodiment, its detected result and technical indicator as shown in table 3:
Cold-resistant water-fast polymer damping paint performance test results and technical indicator described in table 3 embodiment 3
Embodiment 4
Cold-resistant water-fast polymer damping paint of the present invention, its raw material comprises following component by weight: aqueous polyurethane/polyacrylate dispersion 54 parts, coupling agent modified sericite 13 parts, talcum powder 11 parts, hollow glass micropearl 8.3 parts, mica powder 6.5 parts, perlite 10 parts, 12 parts, diatomite, nano acrylic ester rubber powder 8.6 parts, phosphate modified amine compound 0.63 part, magnesium hydroxide 5.3 parts, 8.3 parts, aluminium hydroxide, 7.6 parts, glass fibre, boron bakelite resin 2.1 parts, organic solvent 3.4 parts, propylene glycol phenylate 5.9 parts, Walocel MT 20.000PV 2 parts, wetting agent 2.2 parts, deionized water 31 parts,
Wherein, described organic solvent is that ethanol, Virahol, methyl alcohol, propyl alcohol, propyl carbinol, ethylene glycol, Diethylene Glycol, 1,2-PD, 1,3-PD, dipropylene glycol, BDO, pentanediol, glycerol are by the combination of any weight ratio;
Described phosphate modified amine compound is prepared according to following technique: join in flask by 32 parts of phosphoric acid and 15 parts of quadrols by weight, stirring reaction 31min, stirring is warming up to 52 DEG C, reaction 25min, be warming up to 85 DEG C, reaction 26min, adds 14 parts of hexamethylenetetramines, stirring reaction 53min, after cooling, drying obtains described phosphate modified amine compound.
Performance Detection is carried out to water-fast polymer damping paint cold-resistant described in the present embodiment, its detected result and technical indicator as shown in table 4:
Cold-resistant water-fast polymer damping paint performance test results and technical indicator described in table 4 embodiment 4
The above; be only the present invention's preferably embodiment; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (9)
1. a cold-resistant water-fast polymer damping paint, it is characterized in that, its raw material comprises following component by weight: aqueous polyurethane/polyacrylate dispersion 40-60 part, coupling agent modified sericite 5-16 part, talcum powder 5-15 part, hollow glass micropearl 3-10 part, mica powder 3-8 part, perlite 5-12 part, diatomite 5-17 part, nano acrylic ester rubber powder 4-10 part, phosphate modified amine compound 0.3-0.9 part, magnesium hydroxide 3-6 part, aluminium hydroxide 5-12 part, glass fibre 3-10 part, boron bakelite resin 1-3 part, organic solvent 2-5 part, film coalescence aid 2-7 part, auxiliary agent 2-5 part, deionized water 20-35 part,
Wherein, described phosphate modified amine compound is prepared according to following technique: join in flask by 20-40 part phosphoric acid and 10-20 part quadrol by weight, stirring reaction 20-35min, stirring is warming up to 45-55 DEG C, and reaction 20-28min, is warming up to 82-90 DEG C, reaction 20-28min, add 10-18 part hexamethylenetetramine, stirring reaction 40-60min, after cooling, drying obtains described phosphate modified amine compound.
2. resist cold water-fast polymer damping paint according to claim 1, it is characterized in that, its raw material comprises following component by weight: aqueous polyurethane/polyacrylate dispersion 50-56 part, coupling agent modified sericite 9-14 part, talcum powder 7-13 part, hollow glass micropearl 7-8.5 part, mica powder 5-6.8 part, perlite 9-11 part, diatomite 9-13 part, nano acrylic ester rubber powder 7-8.9 part, phosphate modified amine compound 0.5-0.79 part, magnesium hydroxide 5-5.6 part, aluminium hydroxide 7-10 part, glass fibre 6-9 part, boron bakelite resin 1.7-2.3 part, organic solvent 2.9-4.5 part, film coalescence aid 5-6.7 part, auxiliary agent 3-4.5 part, deionized water 26-32 part.
3. cold-resistant water-fast polymer damping paint according to claim 1 or 2, it is characterized in that, its raw material comprises following component by weight: aqueous polyurethane/polyacrylate dispersion 54 parts, coupling agent modified sericite 13 parts, talcum powder 11 parts, hollow glass micropearl 8.3 parts, mica powder 6.5 parts, perlite 10 parts, 12 parts, diatomite, nano acrylic ester rubber powder 8.6 parts, phosphate modified amine compound 0.63 part, magnesium hydroxide 5.3 parts, 8.3 parts, aluminium hydroxide, 7.6 parts, glass fibre, boron bakelite resin 2.1 parts, organic solvent 3.4 parts, film coalescence aid 5.9 parts, auxiliary agent 4.2 parts, deionized water 31 parts.
4. cold-resistant water-fast polymer damping paint according to any one of claim 1-3, it is characterized in that, described organic solvent is ethanol, Virahol, methyl alcohol, propyl alcohol, propyl carbinol, ethylene glycol, Diethylene Glycol, 1,2-propylene glycol, 1, one or more combination in ammediol, dipropylene glycol, BDO, pentanediol, glycerol.
5. cold-resistant water-fast polymer damping paint according to any one of claim 1-4, it is characterized in that, described film coalescence aid is one or more the combination in polyoxyethylene glycol, propylene glycol phenylate, alcohol ester 12, butyl glycol ether.
6. cold-resistant water-fast polymer damping paint according to any one of claim 1-5, it is characterized in that, described auxiliary agent is one or more the combination in defoamer, thickening material, flow agent, dispersion agent, wetting agent.
7. resist cold water-fast polymer damping paint according to claim 6, it is characterized in that, described thickening material is one or more the combination in carboxymethyl cellulose, Walocel MT 20.000PV, sodium polyacrylate, polyvinyl alcohol, Natvosol, o-phthalic acid dibutyl ester, Tritolyl Phosphate, dibutyl phthalate.
8. cold-resistant water-fast polymer damping paint according to any one of claim 1-7, it is characterized in that, described phosphate modified amine compound is prepared according to following technique: join in flask by 29-33 part phosphoric acid and 14-18 part quadrol by weight, stirring reaction 29-32min, stirring is warming up to 49-53 DEG C, reaction 24-26min, be warming up to 84-87 DEG C, reaction 25-27min, add 12-16 part hexamethylenetetramine, stirring reaction 49-54min, after cooling, drying obtains described phosphate modified amine compound.
9. resist cold water-fast polymer damping paint according to claim 8, it is characterized in that, described phosphate modified amine compound is prepared according to following technique: join in flask by 32 parts of phosphoric acid and 15 parts of quadrols by weight, stirring reaction 31min, stirs and is warming up to 52 DEG C, reaction 25min, be warming up to 85 DEG C, reaction 26min, adds 14 parts of hexamethylenetetramines, stirring reaction 53min, after cooling, drying obtains described phosphate modified amine compound.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410592421.8A CN104263224A (en) | 2014-10-29 | 2014-10-29 | Cold-resistant and water-proof damping coating |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410592421.8A CN104263224A (en) | 2014-10-29 | 2014-10-29 | Cold-resistant and water-proof damping coating |
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| Publication Number | Publication Date |
|---|---|
| CN104263224A true CN104263224A (en) | 2015-01-07 |
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| CN201410592421.8A Pending CN104263224A (en) | 2014-10-29 | 2014-10-29 | Cold-resistant and water-proof damping coating |
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Cited By (12)
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| CN105440643A (en) * | 2015-12-28 | 2016-03-30 | 张桂华 | Shock-absorption synthetic rubber and preparation method thereof |
| CN105860719A (en) * | 2016-06-06 | 2016-08-17 | 青岛爱尔家佳新材料有限公司 | Sprayable baking type water soluble damping coating and preparation method thereof |
| CN106009980A (en) * | 2016-07-11 | 2016-10-12 | 潘明华 | Cold-resistant damping coating and preparation method thereof |
| CN106280778A (en) * | 2016-08-30 | 2017-01-04 | 广东东方雨虹防水工程有限公司 | A kind of aqueous sound insulation sound-absorbing, waterproof integrated coating and preparation method thereof |
| CN106957601A (en) * | 2017-03-28 | 2017-07-18 | 北京东方雨虹防水技术股份有限公司 | The preparation method and modified waterproof asphalt material and its application method of a kind of modified waterproof asphalt material |
| CN107384074A (en) * | 2017-08-03 | 2017-11-24 | 合肥泓定科技有限公司 | Cold-resistant damping paint |
| CN107722766A (en) * | 2017-11-05 | 2018-02-23 | 陈兴 | A kind of environmental protection coating material of multi-blade flue mouth |
| CN108546482A (en) * | 2018-05-14 | 2018-09-18 | 徐慧 | A kind of polymer cement waterproof paint and preparation method thereof using modified sericite in powder |
| US10472293B2 (en) | 2016-04-29 | 2019-11-12 | Certainteed Gypsum, Inc. | Building assembly containing a water barrier coating film and method of making the building assembly |
| CN113667368A (en) * | 2021-09-14 | 2021-11-19 | 惠州市汉惠河环境科技有限公司 | Reinforced concrete floor impact sound insulation coating and preparation method thereof |
| CN114700243A (en) * | 2022-03-29 | 2022-07-05 | 中船桂江造船有限公司 | Construction method for laying deck dressing on improved damping coating surface |
| CN114854156A (en) * | 2022-06-09 | 2022-08-05 | 四川三棵树涂料有限公司 | Light high-strength waterproof breathable decoration panel material and preparation method thereof |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105440643A (en) * | 2015-12-28 | 2016-03-30 | 张桂华 | Shock-absorption synthetic rubber and preparation method thereof |
| US10472293B2 (en) | 2016-04-29 | 2019-11-12 | Certainteed Gypsum, Inc. | Building assembly containing a water barrier coating film and method of making the building assembly |
| CN105860719B (en) * | 2016-06-06 | 2018-07-27 | 青岛爱尔家佳新材料股份有限公司 | A kind of sprayable baking-type aqueous damping coating and preparation method thereof |
| CN105860719A (en) * | 2016-06-06 | 2016-08-17 | 青岛爱尔家佳新材料有限公司 | Sprayable baking type water soluble damping coating and preparation method thereof |
| CN106009980A (en) * | 2016-07-11 | 2016-10-12 | 潘明华 | Cold-resistant damping coating and preparation method thereof |
| CN106280778A (en) * | 2016-08-30 | 2017-01-04 | 广东东方雨虹防水工程有限公司 | A kind of aqueous sound insulation sound-absorbing, waterproof integrated coating and preparation method thereof |
| CN106957601A (en) * | 2017-03-28 | 2017-07-18 | 北京东方雨虹防水技术股份有限公司 | The preparation method and modified waterproof asphalt material and its application method of a kind of modified waterproof asphalt material |
| CN107384074A (en) * | 2017-08-03 | 2017-11-24 | 合肥泓定科技有限公司 | Cold-resistant damping paint |
| CN107722766A (en) * | 2017-11-05 | 2018-02-23 | 陈兴 | A kind of environmental protection coating material of multi-blade flue mouth |
| CN108546482A (en) * | 2018-05-14 | 2018-09-18 | 徐慧 | A kind of polymer cement waterproof paint and preparation method thereof using modified sericite in powder |
| CN113667368A (en) * | 2021-09-14 | 2021-11-19 | 惠州市汉惠河环境科技有限公司 | Reinforced concrete floor impact sound insulation coating and preparation method thereof |
| CN114700243A (en) * | 2022-03-29 | 2022-07-05 | 中船桂江造船有限公司 | Construction method for laying deck dressing on improved damping coating surface |
| CN114854156A (en) * | 2022-06-09 | 2022-08-05 | 四川三棵树涂料有限公司 | Light high-strength waterproof breathable decoration panel material and preparation method thereof |
| CN114854156B (en) * | 2022-06-09 | 2023-09-26 | 四川三棵树涂料有限公司 | Light high-strength waterproof breathable decoration panel and preparation method thereof |
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