CN104178747B - Split type gas shower assembly and metal organic chemical vapor deposition device - Google Patents

Split type gas shower assembly and metal organic chemical vapor deposition device Download PDF

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Publication number
CN104178747B
CN104178747B CN201310198956.2A CN201310198956A CN104178747B CN 104178747 B CN104178747 B CN 104178747B CN 201310198956 A CN201310198956 A CN 201310198956A CN 104178747 B CN104178747 B CN 104178747B
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type
gas
plate parts
gas distribution
distribution member
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CN104178747A (en
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马悦
奚明
萨尔瓦多
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Ideal Semiconductor Equipment Shanghai Co ltd
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Ideal Semiconductor Equipment (shanghai) Co Ltd
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Abstract

The present invention relates to a kind of split type gas shower assembly and metal organic chemical vapor deposition device, described gas shower assembly includes the first air inlet pipeline, second air inlet pipeline, if gas distribution member and dry plate parts, described gas distribution member includes A type and Type B gas distribution chamber, described A type, Type B gas distribution chamber interval is arranged, it is respectively used to distribute first, second gas, A type is installed in described gas distribution member, Type B plate parts, described A type, Type B plate parts respectively with described A type, Type B gas distribution chamber is oppositely arranged, described A type, Type B plate parts mutually splice, and described gas distribution member is separated with described pedestal.Gas shower modular construction provided by the present invention is simple, gas distribution member handling ease, and have only to safeguard described A type, Type B plate parts during using, decrease dismounting or the installation of whole gas shower assembly, decrease the maintenance time of described metal organic vapor phase deposition device, improve utilization rate.

Description

Split type gas shower assembly and metal organic chemical vapor deposition device
Technical field
The present invention relates to semiconductor Preparation equipment field, particularly relate to a kind of split type gas shower assembly and gold Belong to organic chemical vapor deposition device.
Background technology
Chemical gaseous phase deposition (Chemical vapor deposition is called for short CVD) is that reactive material is at gaseous state bar Part issues biochemical reaction, generates solid matter and is deposited on the solid matrix surface of heating, and then prepares solid The technology of body material, it is achieved by chemical vapor deposition unit.Specifically, CVD device By inlet duct, reacting gas is passed through in reative cell, and controls the reactions such as the pressure of reative cell, temperature Condition so that reacting gas reacts, thus complete deposition process step.Chemical gaseous phase deposition comprises Many types, as plasma gas phase deposition (Plasma Enhanced Chemical Vapor Deposition, PECVD), low-pressure chemical vapor deposition (Low Pressure Chemical Vapor Deposition, LPCVD) and metal organic chemical vapor deposition (Metal Organic Chemical Vapor Deposition, MOCVD) etc., each CVD method is respectively suitable for the preparation of different types of thin film solid material.
MOCVD be mainly used in the Group III-V compound semiconductor such as gallium nitride, GaAs, indium phosphide and The preparation of the thin layer monocrystalline functional structure material of alloy, along with above-mentioned functions structural material range of application not Disconnected expansion, one of MOCVD device important device having become as chemical vapor deposition unit.MOCVD General using III metal organic source and V race hydride source etc. as reacting gas, with hydrogen or nitrogen conduct Carrier gas, carries out vapor phase epitaxial growth on substrate in pyrolysis mode, thus grows various iii-v The thin layer monocrystal material of compound semiconductor and their multivariate solid solution.MOCVD of the prior art Device generally comprises:
Reaction chamber, is arranged at the glove box outside described reaction chamber and air-spy's gas surge chamber;
Being positioned at the gas shower assembly at described reaction chamber top, described gas shower assembly includes two air inlets Pipeline and gas distribution member, III metal organic source and V race are hydrogenated by said two air inlet pipeline respectively Thing source is transmitted to gas distribution member, and described gas distribution member has deflation area, and described deflation area has There is steam vent, be used for discharging described III metal organic source and V race hydride source;
The pedestal being oppositely arranged with described gas shower assembly, described pedestal has heating unit, described base Seat be used for supporting and heating substrate, by described gas shower assembly discharge described III metal organic source and V race hydride source reacts after arriving described substrate, generates Group III-V compound semiconductor.
Generally, being provided with glove box in the outside of MOCVD reaction chamber, the atmosphere in described glove box is High pure nitrogen.Described III metal organic source and V race hydride source in MOCVD reaction chamber easily exist Reaction intracavity contact generation parasitic reaction, and then, reaction chamber inwall or gas shower assembly temperature relatively Low position forms loose film, when described loose film reaches to a certain degree, can produce the most micro- Grain, and drop to film surface when deposited semiconductor device film, in causing film, defect concentration increases, Affect film quality so that the yield of product reduces.Additionally, described microparticle adsorbs at described steam vent Sidewall on this may reduce described steam vent discharge gas speed.When described deflation area is by described loose When film portion covers, the heat-radiating properties of described deflation area, as its thermal emissivity also can change, This thermal balance can broken in described reaction chamber, causes the change of described reaction cavity temperature, final shadow Ring the stability of technical process.
The described deflation area of the most described gas shower assembly must periodically clean, in order to remove on it because of Parasitic reaction and the described loose film that deposits or the described microparticle of absorption, just can carry out normal technique Course of reaction.For gas shower assembly of the prior art, due to the row of a kind of reacting gas Pore is on integrated with described gas distribution member, and the most described deflation area has with described The integrated structure of gas distribution member, and this part can not be processed by individually removing, therefore Need to take out described gas shower assembly entirety from reaction chamber, and put in baking box and toast, Or be carried out by other means.But owing to described gas shower assembly yardstick is big, and comprise substantial amounts of Parts, carry out integral demounting and are again fixed on described reaction chamber top and relate to described gas shower assembly And operation extremely complex, substantial amounts of time and cost can be wasted;And at described gas shower assembly Dismounting and installation process can make described reaction chamber be in open state for a long time, destroy it internal high-purity The nitrogen atmosphere of degree, needs again to be passed through above-mentioned gas and could recover to carry out the atmosphere needed for deposition reaction, This can make device systems need the longer time just can return to carry out the state needed for technological reaction.
The gas shower assembly of the most existing multiple gases distribution cavity is sandwich construction, is processed as multi-point welding, Generally want thousands of pads, such as the Shen by Aix-en-Provence spy bright (Aixtron) the company application of Germany Please be number for the gas shower comprising multiple structuring dish disclosed in the Chinese patent of CN200880019034 Assembly, or the gas shower assembly disclosed in Publication No. US20110186228 United States Patent (USP).Its processing Extremely complex, expensive, and follow-up maintenance cost is high.
It is thus desirable to it is a kind of simple, low cost but the gas shower of multiple gases distribution cavity can be realized Assembly, described gas shower assembly has complete dismountable deflation area so that can facilitate timely to institute State deflation area to dismantle and clean, reduce the maintenance cost of equipment.
Summary of the invention
It is an object of the invention to provide a kind of simple in construction, be prone to processing split type gas shower assembly And metal organic vapor phase deposition device.
The present invention provide metal organic chemical vapor deposition device, including reaction chamber, be arranged at described instead Answer the glove box outside chamber and air-spy's gas surge chamber, be positioned at the gas shower assembly at described reaction chamber top with And the pedestal being oppositely arranged with described gas shower assembly, described pedestal can the most described gas shower group Part rotates, and described gas shower assembly includes that the distribution of the first air inlet pipeline, the second air inlet pipeline, gas is single If unit and dry plate parts, described first, second air inlet pipeline is respectively used to the first gas and the second gas Transmission is to described gas distribution member, and described gas shower assembly has deflation area, and the distribution of described gas is single The single layer structure that unit is formed in one, described gas distribution member includes A type gas distribution chamber and Type B gas Body distribution cavity, described A type gas distribution chamber and Type B gas distribution chamber interval are arranged, and are respectively used to distribution Described first gas and the second gas, be provided with described plate parts, described plate in described gas distribution member Parts include A template parts and Type B plate parts, described A template parts and described A type gas distribution chamber Being oppositely arranged, described Type B plate parts are oppositely arranged with described Type B gas distribution chamber, described A template portion Part and Type B plate parts have steam vent, are respectively used to discharge described first gas and the second gas, described A template parts and Type B plate parts mutually splice, and described gas distribution member are separated with described pedestal.
The metal organic chemical vapor deposition device that the present invention provides provides the benefit that: described gas shower The single layer structure that described gas distribution member in assembly is formed in one, not existing substantial amounts of needs multiple spot The parts welded together, it is easy to be processed manufacturing and simple in construction.Described gas shower assembly Described deflation area is by the described A template parts being installed in described gas distribution member and Type B plate parts structure Becoming, described A type, Type B plate parts have steam vent, are respectively used to discharge described first, second gas. Owing to described A template parts and Type B plate parts all can remove from described gas distribution member, when When needing to remove the described microparticle of the described loose film of deposition on described deflation area or absorption, only need by Than gas shower assembly, overall much smaller A type, Type B plate parts remove, and are buffered by air-spy's gas Room transmits out in nitrogen atmosphere, puts in baking box or is carried out otherwise, and changing one Overlap new A type, Type B plate parts, it is simply installed in described gas distribution member, without Described gas shower assembly entirety is disassembled from described reaction chamber and processes, save described metal The time that organic vapor phase deposition device is shut down, also will not destroy the height in the glove box outside reaction chamber simultaneously Purity nitrogen gas atmosphere.Therefore, gas shower modular construction provided by the present invention is simple, and gas distribution is single Unit's handling ease, and there are easy-to-dismount A type, Type B plate parts, have only to during use safeguard Described A type, Type B plate parts, decrease dismounting or the installation of whole gas shower assembly, decrease institute State the maintenance time of metal organic vapor phase deposition device, improve utilization rate.Additionally, when described reaction chamber When internal airflow field needs regulation, it is only necessary to change the described steam vent on described A type, Type B plate parts Distribution, it is not necessary to change described gas shower assembly.
Preferably, described gas distribution member has the space bar of the upper surface being perpendicular to described pedestal, uses Described A type gas distribution chamber and Type B gas distribution chamber to be separated, described space bar is provided with groove, Described A type, Type B plate parts two sides parallel with described space bar are provided with and described groove fit Buckle teeth portion, in order to install described A type, Type B plate parts.
Preferably, described space bar is provided with the first groove towards the side of described A type gas distribution chamber, Described space bar is provided with the second groove, described first groove towards the side of described Type B gas distribution chamber It is respectively used to install described A template parts and Type B plate parts, described first groove and with the second groove Two grooves mutually stagger along the direction of the upper surface being perpendicular to described pedestal.Described space bar is due to described recessed The existence of groove and its thickness can be made to diminish, reduce its mechanical strength, if described first groove and the second groove Being arranged at described pedestal upper surface sustained height, described space bar will become there is described groove Thinner, in order to reduce the impact on space bar mechanical strength of the described groove, it is desirable to described first groove and Second groove is mutually staggering along the direction of the upper surface being perpendicular to described pedestal.
Preferably, described A template parts two sides parallel with described space bar are additionally provided with groove, Described Type B plate parts two sides parallel with described space bar are provided with and the institute of described A template parts State the buckle teeth portion of groove fit, in order to described Type B plate parts to be installed on two the described A being adjacent On template parts.Have an advantage in that and need not lengthen described space bar two kinds of described plate parts are installed, Only described A template parts need to be installed on described space bar, and described Type B plate parts are by its buckle teeth Portion was i.e. securable in described gas distribution member, jointly with coordinating of the groove on described A template parts It is spliced into a complete deflation area.
Preferably, described plate parts have end on the cross section being parallel to described pedestal upper surface, described End is near the edge of described gas distribution member, and described plate parts are respectively provided with in the both sides of described end Nip portion and auxiliary section, the described auxiliary section that described nip portion is adjacent cooperates, in order to prevent State plate parts along described gas distribution member radial direction produce displacement, in described plate parts at least one with Lock mode is fixed in described gas distribution member.Gas in described A type, Type B gas distribution chamber When described end quickly flows, described A type, Type B plate parts can there be is active force, it is often more important that, When described gas shower assembly is being heated and is cooling down in cyclic process, and described A type, Type B plate parts are subject to The compression that described gas distribution member body causes due to thermal deformation, causes described A type, Type B plate parts There is the trend of radial outward movement along described gas distribution member, by described A type, Type B plate portion The described end of part arranges described nip portion and auxiliary section, and described A type, Type B plate parts can be hindered to produce Raw actual displacement, can facilitate simultaneously and timely described A type, Type B plate parts are dismantled or pacified Dress.
It is further preferred that the protuberance on the right side that described nip portion is described end, described protuberance to The adjacent described plate parts on right side extend, and described auxiliary section is the notch part in the left side of described end, institute The described notch part stating protuberance adjacent with on the right side of it cooperates, in order to prevent described plate parts along institute The radial direction stating gas distribution member produces displacement.Described plate parts at least one be scheduled on described with screwed lock In gas distribution member.
Preferably, described gas distribution member is provided with nesting part near the face of described pedestal in its edge, In order to described plate parts are more firmly fixed in described gas distribution member.It is further preferred that Described nesting part is an annulus contacted with the described end of described plate parts, and the center of circle of described annulus is institute State the center of gas distribution member.
Preferably, described gas shower assembly also includes the connecting plate parts being disposed therein the heart, described A Type, Type B plate parts are connected with described connecting plate parts near the one end at described gas distribution member center, In order to more firm, described A type, Type B plate parts are installed.
Preferably, described gas distribution member has circular depressions, described circular depressions away from the mask of pedestal Connect with described first air inlet pipeline, in order to transmit described first gas to described A type gas distribution chamber.
Preferably, there are an annular channel, described annular channel and described B in the center of described gas distribution member Type gas distribution chamber connects, and connects with described second air inlet pipeline, in order to transmit described second gas extremely Described Type B gas distribution chamber.
Preferably, described gas distribution member and described A type, the material of Type B plate parts include following material One or more in matter: graphite, stainless steel, aluminium, aluminium nitride, carborundum, molybdenum, boron nitride, carbon Change boron, tungsten.
Preferably, described first gas is III metal organic source, and described second gas is V race hydride Source;Preferably, described first gas is V race hydride source, and described second gas is that III metal is organic Source.Preferably, described III metal organic source includes Ga (CH3)3、In(CH3)3、Al(CH3)3、 Ga(C2H5)3、Zn(C2H5)2Deng one or more in gas;Preferably, described V race hydride source bag Include NH3、PH3、AsH3Deng one or more in gas.
Present invention also offers the spray of a kind of gas being arranged in described metal organic chemical vapor deposition device Drenching assembly, described gas shower assembly includes that the distribution of the first air inlet pipeline, the second air inlet pipeline, gas is single If unit and dry plate parts, described first, second air inlet pipeline is respectively used to the first gas and the second gas Transmission is to described gas distribution member, and described gas distribution member has deflation area, and the distribution of described gas is single The single layer structure that unit is formed in one, described gas distribution member includes A type gas distribution chamber and Type B gas Body distribution cavity, described A type gas distribution chamber and Type B gas distribution chamber interval are arranged, and are respectively used to distribution Described first gas and the second gas, be provided with described plate parts, described plate in described gas distribution member Parts include A template parts and Type B plate parts, described A template parts and described A type gas distribution chamber Being oppositely arranged, described Type B plate parts are oppositely arranged with described Type B gas distribution chamber, described A template portion Part and Type B plate parts have steam vent, are respectively used to discharge described first gas and the second gas, described A template parts and Type B plate parts mutually splice, and described gas distribution member are separated with described pedestal.
Preferably, described gas distribution member and described A type, the material of Type B plate parts include following material One or more in matter: graphite, stainless steel, aluminium, aluminium nitride, carborundum, molybdenum, boron nitride, carbon Change boron, tungsten.
Accompanying drawing explanation
Fig. 1 is the structural representation of metal organic chemical vapor deposition device provided by the present invention;
Fig. 2 A is the structural representation of a kind of described gas shower assembly in the preferred embodiment of the invention;
Fig. 2 B is the structural representation of another kind of described gas shower assembly in the preferred embodiment of the invention;
Fig. 3 is the described gas distribution member structural representation away from the cross section of pedestal;
Fig. 4 is in the preferred embodiment of the invention, and a kind of described gas distribution member is along the cross section of A-A ' line Schematic diagram;
Fig. 5 is in the preferred embodiment of the invention, another kind of described gas distribution member cutting along A-A ' line Face schematic diagram;
Fig. 6 is that in a kind of preferred embodiment of the present invention, described gas distribution member is near described pedestal Face on the schematic diagram of adjacent two described plate parts.
Fig. 7 is in the preferred embodiment of the invention, the structural representation of another described gas shower assembly.
Detailed description of the invention
Understandable, below in conjunction with the accompanying drawings for enabling the above-mentioned purpose of the present invention, feature and advantage to become apparent from The detailed description of the invention of the present invention is described in detail.
Elaborate a lot of detail in the following description so that fully understanding the present invention, but this Bright other can also be used to be different from alternate manner described here implement, therefore the present invention is not by following The restriction of disclosed specific embodiment.
Fig. 1 is the structural representation of metal organic chemical vapor deposition device provided by the present invention.Reference Fig. 1, described metal organic chemical vapor deposition device 10 includes reaction chamber 11, is arranged at described reaction chamber Glove box 50 outside 11 and air-spy's gas surge chamber 40, and it is arranged at the gas in described reaction chamber 11 Spray assemblies 12 and pedestal 13;Described gas shower assembly 12 is fixedly installed on the top of reaction chamber 11, Described pedestal 13 is arranged at the bottom of described reaction chamber 11, and described pedestal has heating unit 131.Described Gas shower assembly 12 is oppositely arranged with described pedestal 13.Described gas shower assembly 12 and described pedestal Reaction zone is formed between 13.Reacting gas is incorporated into described reaction zone from described gas shower assembly 12.
Described pedestal 13 includes one towards the substrate seating surface of described gas shower assembly 12, described substrate Supporting surface is used for supporting one or more pending substrate 14.During carrying out chemical gaseous phase deposition, Pending substrate 14 is sent in reaction chamber 11 by air-spy's gas surge chamber 40, and is arranged on described base On sheet supporting surface, the substrate 14 processed is transmitted from reaction chamber 11 by described air-spy's gas surge chamber 40 Out;Described pedestal 13 is supported in a rotating shaft 132, described rotating shaft 132 make described pedestal 13 around The axis in one vertical described substrate support face rotates.Owing to described spray assemblies 12 is fixed on reaction chamber 11 On, therefore, described pedestal 13 also rotates relative to described gas shower assembly 12 simultaneously.
Fig. 2 A is the structural representation of a kind of described gas shower assembly in the preferred embodiment of the invention.Ginseng According to Fig. 2 A, described gas shower assembly 12 include first air inlet pipeline the 111, second air inlet pipeline 112, If being positioned at the gas distribution member 122 below described reaction chamber top board 110 and dry plate parts;Described first Air inlet pipeline 111 and the second air inlet pipeline 112 are single to the distribution of described gas respectively through reaction chamber top board 110 Unit 122 conveying the first gas and the second gas, the individual layer that described gas distribution member 122 is formed in one Structure, described gas distribution member 122 includes A type gas distribution chamber 210 and Type B gas distribution chamber 220, Described A type gas distribution chamber 210 and Type B gas distribution chamber 220 interval are arranged, and described A type gas divides Join chamber 210 and basis that Type B gas distribution chamber 220 is described plate parts and described gas distribution member 210 The cavity that body surrounds, is respectively used to distribute described first gas and the second gas.
Being provided with described plate parts in described gas distribution member 122, described plate parts include A template portion Part 123 and Type B plate parts 124, described A template parts 123 and described A type gas distribution chamber 210 Being oppositely arranged, described Type B plate parts 124 are oppositely arranged with described Type B gas distribution chamber 220, described A template parts 123 and Type B plate parts 124 have steam vent (not shown), are respectively used to discharge institute Stating the first gas and the second gas, described A template parts 123 and Type B plate parts 124 mutually splice, And described gas distribution member is separated with described pedestal.
The individual layer being formed in one due to the described gas distribution member 122 in described gas shower assembly 12 Structure, is not related to parts and the multi-point welding technique of complexity during processing and manufacturing.Due to described A template portion Part 123 and Type B plate parts 124 all can remove from described gas distribution member 122, work as needs When removing on described deflation area 125 the described microparticle of the described loose film of deposition or absorption, only need by Than gas shower assembly 12, overall much smaller described A type, Type B plate parts 123/124 remove, logical Cross air-spy's gas surge chamber 40 to transmit out in nitrogen atmosphere, put in baking box or enter otherwise Row cleans, and does without described gas shower assembly 12 entirety being disassembled from described reaction chamber 11 Process, save the time that described metal organic vapor phase deposition device 10 is shut down, also will not destroy anti-simultaneously Answer the high-purity nitrogen atmosphere in the glove box 50 outside chamber.Therefore, gas shower provided by the present invention Modular construction is simple, gas distribution member handling ease, and has easy-to-dismount A type, Type B plate portion Part 123/124, has only to during use safeguard described A type, Type B plate parts 123/124, decreases The dismounting of whole gas shower assembly 12 or installation, decrease the dimension of described metal organic vapor phase deposition device Protect the time, improve utilization rate.Additionally, when the airflow field in described reaction chamber 11 body needs regulation, Have only to the described steam vent distribution changing on described A type, Type B plate parts 123/124, it is not necessary to more Change described gas shower assembly 12.
Fig. 3 is the described gas distribution member 122 structural representation away from the cross section of pedestal 13.Join simultaneously According to Fig. 2 A and Fig. 3, described gas distribution member 122 has circular depressions 211 away from the cross section of pedestal, Described circular depressions 211 connects with described first air inlet pipeline 111, in order to transmit described first gas to institute State A type gas distribution chamber 210.Described first gas is arranged by the steam vent on described A template parts 123 Go out.
There are an annular channel 221, described annular channel 221 and institute in the center of described gas distribution member 122 State Type B gas distribution chamber 220 to connect, and connect, in order to transmit with described second air inlet pipeline 112 State the second gas to described Type B gas distribution chamber 220, described annular channel 221 and described A type gas There is a dividing plate 212 distribution cavity 210 junction, enters described A type gas in order to completely cut off described second gas Distribution cavity 210, described second gas is discharged by the steam vent on described Type B plate parts 124.
Described gas distribution member 122 has the space bar of the upper surface being perpendicular to described pedestal 13, in order to Described A type gas distribution chamber 210 and Type B gas distribution chamber 220 are separated, described space bar is arranged Fluted, described A template parts 123 and Type B plate parts 124 two sides parallel with described space bar It is provided with the buckle teeth portion with described groove fit, in order to install described A template parts 123 and Type B plate Parts 124.
Fig. 4 is that in one preferred embodiment of the present invention, gas distribution member 122 is along the cross section of A-A ' line Schematic diagram.With reference to Fig. 4, described groove includes the first groove 1261 and the second groove 1262, described interval On plate 126, side towards described A type gas distribution chamber 210 is provided with the first groove 1261, described between On dividing plate 126, the side towards described Type B gas distribution chamber 220 is provided with the second groove 1262, described First groove 1261 cooperates with the buckle teeth portion 1230 on A template parts 123, described second groove 1262 and Type B plate parts 124 on buckle teeth portion 1240 cooperate, be respectively used to described A type is installed Plate parts 123 and Type B plate parts 124.On described A template parts 123, there is steam vent 1231, use In discharging described first gas, described Type B plate parts 124 has steam vent 1241, for described the Two gases.Described first groove 1261 and the second groove 1262 are along the upper surface being perpendicular to described pedestal 13 Direction mutually stagger, i.e. the height apart from the upper surface of described pedestal 13 is different.Its reason is, institute Stating space bar 126 can make its thickness diminish owing to there is described groove 1261/1262, reduces its machinery strong Degree, if described first groove 1261 and the second groove 1262 are arranged at the upper surface away from described pedestal 13 together At one height, the most described space bar 126 will become thinner, in order to reduce there is described groove State the groove 1261/1262 impact on space bar mechanical strength, it is desirable to described first groove 1261 and second Groove 1262 is mutually staggering along the direction of the upper surface being perpendicular to described pedestal.
Refer to shown in Fig. 2 B, in some embodiment being more highly preferred to of the present invention, described gas sprays Drenching assembly and also include the connecting plate parts 2111 that are disposed therein the heart, described A template parts 123 are near institute The one end stating gas distribution member 122 center is connected with described connecting plate parts 2111, specifically, and institute State connecting plate parts and there is slot (not shown), for housing a part for described A template parts 123. Equally, described Type B plate parts 124 and described connecting plate parts 2111 are near described gas distribution member 122 The one end at center is connected, and specifically, a part for described Type B plate parts 124 is housed in described slot In.Described connecting plate parts 2111 install described A type, Type B plate parts 123/124 in order to more firm.
Fig. 5 is in another kind preferred embodiment of the present invention, gas distribution member 122 cutting along A-A ' line Face schematic diagram.With reference to Fig. 5, described A template parts 210 are by its buckle teeth portion 1230 and described space bar The cooperation of the described groove 1261 on 126 is installed in described gas distribution member 122.Additionally, it is described A template 210 two sides parallel with described space bar 126 are additionally provided with groove 1232, described Type B Plate parts 124 two sides parallel with described space bar 126 are provided with and the institute of described A template parts State the buckle teeth portion 1242 that groove 1232 coordinates, in order to be installed on and its phase by described Type B plate parts 124 On two adjacent described A template parts 123.Its beneficial functional is, it is not necessary to by described space bar 126 Lengthen and described plate parts are installed, only described A template parts 123 need to be installed on described space bar 126 On, and described Type B plate parts 124 are by described buckle teeth portion 1242 and described A template parts 123 The cooperation of groove 1232 is i.e. securable in described gas distribution member 122, be jointly spliced into one complete Face 125.
Fig. 6 is in a kind of preferred embodiment of the present invention, two plate parts adjacent on described deflation area Schematic diagram.With reference to Fig. 6, described plate parts 140 and plate parts 150 are in adjacent position, described plate portion There is on part 140/150 steam vent 1400/1500, be used for discharging described first gas or the second gas.Institute State plate parts 140/150, on the cross section of upper surface being parallel to described pedestal 13, there is end 141/151, Described end 141/151 is near the edge of described gas distribution member 122, and described plate parts 140/150 exist The both sides of described end are respectively provided with nip portion 142/152 and auxiliary section 143/153, the institute of plate parts 140 The described auxiliary section 153 stating the plate parts 150 that nip portion 142 is adjacent cooperates, in order to prevent Described plate parts produce displacement along the radial direction of described gas distribution member 122.In the preferred embodiment, Described nip portion 142/152 is the protuberance on the right side of described end 141/151, and described protuberance is right to it The adjacent described plate parts of side extend, and described auxiliary section 142/152 is the left side of described end 141/151 Notch part, the described notch part that described protuberance is adjacent with on the right side of it cooperates, in order to prevent State the plate parts 140/150 radial direction generation displacement along described gas distribution member 122, described plate parts 140 Being fixed in described gas distribution member with lock mode, as shown in Figure 6, described lock mode is for using spiral shell Silk 144 locking.
Gas in described A type, Type B gas distribution chamber, can be right when described end 141 quickly flows Described A type, Type B plate parts have active force, it is often more important that, when described gas shower assembly 12 is being subject to Heat and cooling cyclic process in, described plate parts 140/150 by described gas distribution member 12 body by In the compression that thermal deformation causes, described plate parts 140/150 are caused to have the footpath along described gas distribution member To the trend moved out, described by arranging at the described end 141/151 of described plate parts 140/150 Pressing 142/152 and auxiliary section 143/153, it is possible to hinder described plate parts 140/150 to produce reality Displacement
Additionally, arrange the nip portion that cooperates and auxiliary section fixes described plate parts, it is only necessary to use Screw 144 locks described plate parts 140, thus can facilitate and tear described plate parts open timely Unload or install.Needs dismantle described plate parts do cleaning treatment time, only need to will lock with screw 144 Described plate parts 140 disassemble in advance, the direction that other plate parts just can extend along described nip portion The most sequentially disassemble, described air-spy's gas surge chamber 40 transmit out described reaction chamber 11;Install Can take during new cage plate parts same method by described air-spy gas surge chamber 40 transmit into described in Reaction chamber 11 is also sequentially installed, thus considerably simplify dismounting and the erector of described plate parts Sequence, improves the utilization rate of described metal organic vapor phase deposition device.
Described gas distribution member is provided with nesting part near the face of described pedestal in its edge, in order to incite somebody to action Described A template parts 123 and Type B plate parts 124 are more firmly fixed to described gas distribution member On.Described nesting part is an annulus contacted with the described end of described plate parts, the center of circle of described annulus Center for described gas distribution member.
Fig. 7 is in the preferred embodiment of the present invention, the structural representation of another described gas shower assembly Figure.With reference to Fig. 7, described nesting part 60 has two cross sections, left and right, the most respectively with described A template parts The cross section that the described end of 123 contacts with the described end of Type B plate parts 124, in described A template portion The described end of part 123, described nesting part 60 has upper and lower two external members separated, at described Type B plate The described end of parts 124, described nesting part 60 is continuously one, in order to by described A template parts 123 and Type B plate parts 124 be more firmly fixed in described gas distribution member.
In the preferred embodiment of the invention, described gas distribution member and described A type, Type B plate parts Material include one or more in following material: graphite, stainless steel, aluminium, aluminium nitride, carborundum, Molybdenum, boron nitride and tungsten.
In the preferred embodiment of the invention, described first gas is for including III metal organic source, described Second gas is one or more in V race hydride source and carrier gas;In the present invention, other are the most real Executing in example, described first gas is V race hydride source, and described second gas is organic for including III metal Source.
Described III metal organic source includes Ga (CH3)3、In(CH3)3、Al(CH3)3、Ga(C2H5)3、 Zn(C2H5)2One or more in gas;Described V race hydride source includes NH3、PH3、AsH3Gas One or more in body;Described carrier gas includes N2、H2, one or more in Ar gas.
Although the present invention discloses as above with preferred embodiment, but the present invention is not limited to this.Any Skilled person, without departing from the spirit and scope of the present invention, all can make various changes or modifications, Therefore protection scope of the present invention should be as the criterion with claim limited range.

Claims (18)

1. a metal organic chemical vapor deposition device, including reaction chamber, is arranged at the hand outside described reaction chamber Casing and air-spy's gas surge chamber, be positioned at the gas shower assembly at described reaction chamber top and with described The pedestal that gas shower assembly is oppositely arranged, described pedestal can rotate relative to described gas shower assembly, If described gas shower assembly include the first air inlet pipeline, the second air inlet pipeline, gas distribution member and Dry plate parts, described first, second air inlet pipeline is respectively used to the first gas and the second gas transport To described gas distribution member, described gas distribution member has deflation area, it is characterised in that described The single layer structure that gas distribution member is formed in one, described gas distribution member includes that A type gas divides Join chamber and Type B gas distribution chamber, described A type gas distribution chamber and Type B gas distribution chamber interval to arrange, Being respectively used to distribute described first gas and the second gas, described gas distribution member bottom has been installed Stating plate parts, described plate parts include A template parts and Type B plate parts, described A template parts with Described A type gas distribution chamber is oppositely arranged, described Type B plate parts and described Type B gas distribution chamber phase To setting, described A template parts and Type B plate parts have steam vent, are respectively used to discharge described One gas and the second gas, described A template parts and Type B plate parts mutually splice, and by described gas Body allocation unit separates with described pedestal.
2. metal organic chemical vapor deposition device as claimed in claim 1, it is characterised in that described gas Allocation unit has the space bar of the upper surface being perpendicular to described pedestal, in order to be divided by described A type gas Join chamber and Type B gas distribution chamber separates, described space bar is provided with groove, described A type, Type B Plate parts two sides parallel with described space bar are provided with the buckle teeth portion with described groove fit, use To install described A type, Type B plate parts.
3. metal organic chemical vapor deposition device as claimed in claim 2, it is characterised in that described interval Plate is provided with the first groove towards the side of described A type gas distribution chamber, and described space bar is towards described The side of Type B gas distribution chamber is provided with the second groove, and described first groove and the second groove are used respectively In installing described A template parts and Type B plate parts, described first groove and the second groove along being perpendicular to Mutually stagger in the direction of the upper surface of described pedestal.
4. metal organic chemical vapor deposition device as claimed in claim 2, it is characterised in that described A type Plate parts two sides parallel with described space bar are additionally provided with groove, described Type B plate parts and institute State two parallel sides of space bar and be provided with the buckle teeth of the described groove fit with described A template parts Portion, in order to be installed on described Type B plate parts on two be adjacent described A template parts.
5. metal organic chemical vapor deposition device as claimed in claim 2, it is characterised in that described plate portion Part has end on the cross section being parallel to described pedestal upper surface, and described end divides near described gas Joining the edge of unit, described plate parts are respectively provided with nip portion and auxiliary section in the both sides of described end, The described auxiliary section that described nip portion is adjacent cooperates, in order to prevent described plate parts along described The radial direction of gas distribution member produces displacement, in described plate parts at least one fix with lock mode In described gas distribution member.
6. metal organic chemical vapor deposition device as claimed in claim 5, it is characterised in that described pressing Portion is the protuberance on the right side of described end, and described protuberance adjacent described plate parts to the right prolong Stretching, described auxiliary section is the notch part in the left side of described end, and described protuberance is adjacent with on the right side of it Described notch part cooperate, in order to prevent described plate parts along the radial direction of described gas distribution member Produce displacement, in described plate parts at least one be scheduled in described gas distribution member with screwed lock.
7. metal organic chemical vapor deposition device as claimed in claim 6, it is characterised in that described gas Allocation unit is provided with nesting part near the face of described pedestal in its edge, in order to by described plate parts More it is firmly fixed to described gas distribution member exist.
8. metal organic chemical vapor deposition device as claimed in claim 7, it is characterised in that described nesting Portion is an annulus contacted with the described end of described plate parts, and the center of circle of described annulus is described gas The center of allocation unit.
9. metal organic chemical vapor deposition device as claimed in claim 8, described gas shower assembly also wraps Include the connecting plate parts being disposed therein the heart, described connecting plate parts and described A type, Type B plate parts Be connected near the one end at described gas distribution member center, in order to more firm install described A type, Type B plate parts.
10. metal organic chemical vapor deposition device as claimed in claim 8, it is characterised in that described gas Allocation unit has circular depressions, described circular depressions and described first air inlet pipeline away from the mask of pedestal Connection, in order to transmit described first gas to described A type gas distribution chamber.
11. metal organic chemical vapor deposition devices as claimed in claim 9, it is characterised in that described gas The center of allocation unit has an annular channel, described annular channel to connect with described Type B gas distribution chamber, And connect with described second air inlet pipeline, distribute to described Type B gas in order to transmit described second gas Chamber.
12. metal organic chemical vapor deposition devices as claimed in claim 1, it is characterised in that described gas Allocation unit and described A type, the material of Type B plate parts include one or more in following material: Graphite, stainless steel, aluminium, aluminium nitride, carborundum, molybdenum, boron nitride, boron carbide, tungsten.
13. metal organic chemical vapor deposition devices as claimed in claim 1, it is characterised in that described first Gas is III metal organic source, and described second gas is V race hydride source.
14. metal organic chemical vapor deposition devices as claimed in claim 1, it is characterised in that described first Gas is V race hydride source, and described second gas is III metal organic source.
The 15. metal organic chemical vapor deposition devices as according to any one of claim 13 or 14, its feature Being, described III metal organic source includes Ga (CH3)3、In(CH3)3、Al(CH3)3、Ga(C2H5)3、Zn(C2H5)2One or more in gas.
The 16. metal organic chemical vapor deposition devices as according to any one of claim 13 or 14, its feature Being, described V race hydride source includes NH3、PH3、AsH3One or more in gas.
17. 1 kinds of gas shower groups being arranged in metal organic chemical vapor deposition device as claimed in claim 1 Part, described gas shower assembly includes the first air inlet pipeline, the second air inlet pipeline, gas distribution member If with dry plate parts, described first, second air inlet pipeline is respectively used to the first gas and the second gas Transmission is to described gas distribution member, and described gas distribution member has deflation area, it is characterised in that The single layer structure that described gas distribution member is formed in one, described gas distribution member includes A type gas Body distribution cavity and Type B gas distribution chamber, described A type gas distribution chamber and Type B gas distribution chamber interval Arrange, be respectively used to distribute described first gas and the second gas, install in described gas distribution member Described plate parts, described plate parts are had to include A template parts and Type B plate parts, described A template portion Part is oppositely arranged with described A type gas distribution chamber, and described Type B plate parts distribute with described Type B gas Chamber is oppositely arranged, and described A template parts and Type B plate parts have steam vent, is respectively used to discharge institute Stating the first gas and the second gas, described A template parts and Type B plate parts mutually splice, and by institute State gas distribution member to separate with described pedestal.
18. gas shower assemblies as claimed in claim 17, it is characterised in that described gas distribution member and institute State A type, the material of Type B plate parts includes one or more in following material: graphite, stainless steel, Aluminium, aluminium nitride, carborundum, molybdenum, boron nitride, boron carbide, tungsten.
CN201310198956.2A 2013-05-24 2013-05-24 Split type gas shower assembly and metal organic chemical vapor deposition device Active CN104178747B (en)

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CN101545103A (en) * 2008-03-25 2009-09-30 东捷科技股份有限公司 Device for distributing gas
CN101760728A (en) * 2008-12-24 2010-06-30 鸿富锦精密工业(深圳)有限公司 Chemical vapor deposition system
CN102373440A (en) * 2010-08-12 2012-03-14 Snt能源技术有限公司 Chemical vapor deposition device
CN202688435U (en) * 2012-05-11 2013-01-23 中微半导体设备(上海)有限公司 Gas distributing device for metal organic chemical gas phase deposition reaction device and reaction device

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101545103A (en) * 2008-03-25 2009-09-30 东捷科技股份有限公司 Device for distributing gas
CN101760728A (en) * 2008-12-24 2010-06-30 鸿富锦精密工业(深圳)有限公司 Chemical vapor deposition system
CN102373440A (en) * 2010-08-12 2012-03-14 Snt能源技术有限公司 Chemical vapor deposition device
CN202688435U (en) * 2012-05-11 2013-01-23 中微半导体设备(上海)有限公司 Gas distributing device for metal organic chemical gas phase deposition reaction device and reaction device

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Denomination of invention: Split gas spray assembly and metal-organic chemical vapor deposition device

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