CN104119717B - A kind of nanometer base waterproof coating - Google Patents
A kind of nanometer base waterproof coating Download PDFInfo
- Publication number
- CN104119717B CN104119717B CN201410293839.9A CN201410293839A CN104119717B CN 104119717 B CN104119717 B CN 104119717B CN 201410293839 A CN201410293839 A CN 201410293839A CN 104119717 B CN104119717 B CN 104119717B
- Authority
- CN
- China
- Prior art keywords
- raw material
- minutes
- nano
- stirring
- waterproof coating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000011248 coating agent Substances 0.000 title claims abstract description 16
- 238000000576 coating method Methods 0.000 title claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 18
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000008367 deionised water Substances 0.000 claims abstract description 13
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 13
- 239000000839 emulsion Substances 0.000 claims abstract description 13
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000001506 calcium phosphate Substances 0.000 claims abstract description 9
- 229910000389 calcium phosphate Inorganic materials 0.000 claims abstract description 9
- 235000003935 Hippophae Nutrition 0.000 claims abstract description 7
- 241000229143 Hippophae Species 0.000 claims abstract description 7
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 7
- ILRSCQWREDREME-UHFFFAOYSA-N dodecanamide Chemical compound CCCCCCCCCCCC(N)=O ILRSCQWREDREME-UHFFFAOYSA-N 0.000 claims abstract description 7
- 150000001261 hydroxy acids Chemical class 0.000 claims abstract description 7
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000391 magnesium silicate Substances 0.000 claims abstract description 7
- 229910052919 magnesium silicate Inorganic materials 0.000 claims abstract description 7
- 235000019792 magnesium silicate Nutrition 0.000 claims abstract description 7
- 239000011734 sodium Substances 0.000 claims abstract description 7
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 7
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims abstract description 7
- KGIGUEBEKRSTEW-UHFFFAOYSA-N 2-vinylpyridine Chemical class C=CC1=CC=CC=N1 KGIGUEBEKRSTEW-UHFFFAOYSA-N 0.000 claims abstract description 4
- 108050008598 Phosphoesterases Proteins 0.000 claims abstract description 4
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 4
- 150000001346 alkyl aryl ethers Chemical class 0.000 claims abstract description 4
- IMUDHTPIFIBORV-UHFFFAOYSA-N aminoethylpiperazine Chemical compound NCCN1CCNCC1 IMUDHTPIFIBORV-UHFFFAOYSA-N 0.000 claims abstract description 4
- 150000002334 glycols Chemical class 0.000 claims abstract description 4
- 229920000570 polyether Polymers 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 30
- 238000002156 mixing Methods 0.000 claims description 9
- 239000007788 liquid Substances 0.000 claims description 7
- XISFOXBYRQWDNK-UHFFFAOYSA-N 2-(2-methylphenyl)propan-2-amine;hydrochloride Chemical compound [Cl-].CC1=CC=CC=C1C(C)(C)[NH3+] XISFOXBYRQWDNK-UHFFFAOYSA-N 0.000 claims description 6
- 241001116389 Aloe Species 0.000 claims description 6
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 6
- 235000011399 aloe vera Nutrition 0.000 claims description 6
- 239000006185 dispersion Substances 0.000 claims description 6
- 229960001617 ethyl hydroxybenzoate Drugs 0.000 claims description 6
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 6
- GYCKQBWUSACYIF-UHFFFAOYSA-N o-hydroxybenzoic acid ethyl ester Natural products CCOC(=O)C1=CC=CC=C1O GYCKQBWUSACYIF-UHFFFAOYSA-N 0.000 claims description 6
- 229940059574 pentaerithrityl Drugs 0.000 claims description 6
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 6
- HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 claims description 6
- 239000000741 silica gel Substances 0.000 claims description 6
- 229910002027 silica gel Inorganic materials 0.000 claims description 6
- MPPQGYCZBNURDG-UHFFFAOYSA-N 2-propionyl-6-dimethylaminonaphthalene Chemical compound C1=C(N(C)C)C=CC2=CC(C(=O)CC)=CC=C21 MPPQGYCZBNURDG-UHFFFAOYSA-N 0.000 claims description 3
- 229910019142 PO4 Inorganic materials 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- -1 monoalky lether phosphate ester Chemical class 0.000 claims description 3
- 239000010452 phosphate Substances 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 2
- 239000003973 paint Substances 0.000 abstract description 5
- 239000005871 repellent Substances 0.000 abstract description 5
- 238000004078 waterproofing Methods 0.000 abstract description 4
- 238000005299 abrasion Methods 0.000 abstract description 2
- 238000013329 compounding Methods 0.000 abstract description 2
- 238000005336 cracking Methods 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 238000005187 foaming Methods 0.000 abstract description 2
- 239000000463 material Substances 0.000 description 5
- 230000032683 aging Effects 0.000 description 2
- 239000004568 cement Substances 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
nullThe invention discloses a kind of nanometer base waterproof coating，It is made up of the raw material of following weight parts: silicone acrylic emulsion 63 70、Ketopyrrolidine hydroxy acid sodium 1.3 2、Aminoethyl piperazine 0.1 0.2、Monoalky lether phosphoesterase 30 .1 0.2、Oleum Hippophae 0.6 1、Ammonium tungstate 0.5 1、Lauric acid amide of ethanol 0.2 0.5、Magnesium silicate 23、2 vinylpyridines 0.6 1、Nano-calcium phosphate 57、Polyether Glycols 23、Nano diatomite 58、Coalescents 58、Deionized water 10 17，The nano diatomite that the water-repellent paint of the present invention adds、Nano-calcium phosphate，Can effectively improve the cracking resistance of film、Abrasion resistance,Each raw material is compounding rationally，The feature of environmental protection is good，Also there is excellent frost resistance and low temperature flexibility，Application property is good，Non-foaming、Film-formation result is good，Water proofing property is strong.
Description
Technical field
The invention mainly relates to a kind of coating, particularly relate to a kind of nanometer base waterproof coating.
Background technology
Traditional waterproof material mainly has the flexible waterproof materials such as waterproof roll, water-repellent paint, sealing cement, and based on cement matrix, adds liquid medicine agent and the rigidity water-proofing material of other auxiliary agent.China's major part waterproofing work shortcoming such as loss of properties on aging, hot strength be low, temperature sensitive that all uses conventional waterproof material, conventional waterproof material to also exist.Conventional waterproof coating is used for roof waterproof, easily cause aging, dry and cracked, deform, fracture, the phenomenon such as layering, waterproof for indoor, for complex-shaped place, constructional difficulties, and to Seepage, quality is more difficult to ensure, people's every few years will spend substantial amounts of fund and labour force to reprocess, and not only confuse the orthobiosis of people, work and the production order, and affect the service life of whole building nanometer substrates.In order to meet the every profession and trade requirement to water-repellent paint, producing high-performance, widely used water-repellent paint is necessary.
Summary of the invention
The object of the invention is just to provide a kind of nanometer base waterproof coating.
The present invention is achieved by the following technical solutions:
A kind of nanometer base waterproof coating, it is made up of the raw material of following weight parts:
Silicone acrylic emulsion 63-70, ketopyrrolidine hydroxy acid sodium 1.3-2, aminoethyl piperazine 0.1-0.2, monoalky lether phosphoesterase 30 .1-0.2, Oleum Hippophae 0.6-1, ammonium tungstate 0.5-1, lauric acid amide of ethanol 0.2-0.5, magnesium silicate 2-3,2-vinylpyridine 0.6-1, nano-calcium phosphate 5-7, polyether Glycols 2-3, nano diatomite 5-8, coalescents 5-8, deionized water 10-17；
Described coalescents is made up of the raw material of following weight parts:
Silicone acrylic emulsion 30-35, Aloe extraction solution 0.3-2, ethyl hydroxybenzoate 1-2, prodan 0.8-1, tetramethylolmethane 2-3, dibutyl tin laurate 0.1-0.2, micropowder silica gel 2-4, trimethyl benzyl ammonia chloride 0.8-2, deionized water 70-75；
Micropowder silica gel being mixed with tetramethylolmethane, at 65-70 DEG C, stirring mixing 2-4 minute, adds the 30-40% of above-mentioned deionized water weight, trimethyl benzyl ammonia chloride, 100-200 rev/min of dispersed with stirring 6-12 minute, obtains dispersion liquid；
Ethyl hydroxybenzoate is mixed with Aloe extraction solution, it is stirring evenly and then adding in silicone acrylic emulsion, insulated and stirred 10-15 minute at 35-40 DEG C, add above-mentioned dispersion liquid, dibutyl tin laurate, stirring is to room temperature, add and remain each raw material, 300-400 rev/min of dispersed with stirring 7-10 minute, obtain described coalescents.
The preparation method of a kind of nanometer base waterproof coating, comprises the following steps:
By nano-calcium phosphate, magnesium silicate, nano diatomite mixing, join in deionized water, be stirring evenly and then adding into lauric acid amide of ethanol, ammonium tungstate, stirring mixing 4-5 minute at 70-76 DEG C；
Being mixed with Oleum Hippophae by ketopyrrolidine hydroxy acid sodium, join in silicone acrylic emulsion, 100-120 rev/min of stirring mixes 3-5 minute, adds monoalky lether phosphate ester, stirs；
Each raw material after above-mentioned process is mixed with remaining each raw material, 500-600 rev/min of dispersed with stirring 20-30 minute, obtain described nanometer base waterproof coating.
The invention have the advantage that
The nano diatomite of water-repellent paint addition of the present invention, nano-calcium phosphate, can effectively improve the cracking resistance of film, abrasion resistance, and each raw material is compounding rationally, the feature of environmental protection is good, also has excellent frost resistance and low temperature flexibility, and application property is good, non-foaming, film-formation result good, water proofing property is strong.
Detailed description of the invention
Embodiment 1
A kind of nanometer base waterproof coating, it is made up of the raw material of following weight parts (kilogram):
Silicone acrylic emulsion 70, ketopyrrolidine hydroxy acid sodium 1.3, aminoethyl piperazine 0.2, monoalky lether phosphoesterase 30 .2, Oleum Hippophae 0.6, ammonium tungstate 0.5, lauric acid amide of ethanol 0.5, magnesium silicate 3,2-vinylpyridine 0.6, nano-calcium phosphate 5, polyether Glycols 2-3, nano diatomite 5, coalescents 8, deionized water 17；
Described coalescents is made up of the raw material of following weight parts:
Silicone acrylic emulsion 35, Aloe extraction solution 0.3, ethyl hydroxybenzoate 2, prodan 0.8, tetramethylolmethane 2, dibutyl tin laurate 0.1, micropowder silica gel 2, trimethyl benzyl ammonia chloride 0.8-2, deionized water 75；
Micropowder silica gel is mixed with tetramethylolmethane, stirring mixing 4 minutes at 70 DEG C, add the 40% of above-mentioned deionized water weight, trimethyl benzyl ammonia chloride, 100 revs/min of dispersed with stirring 12 minutes, obtain dispersion liquid；
Ethyl hydroxybenzoate is mixed with Aloe extraction solution, is stirring evenly and then adding in silicone acrylic emulsion, insulated and stirred 15 minutes at 40 DEG C, add above-mentioned dispersion liquid, dibutyl tin laurate, stir to room temperature, add and remain each raw material, 400 revs/min of dispersed with stirring 10 minutes, obtain described coalescents.
The preparation method of a kind of nanometer base waterproof coating, comprises the following steps:
By nano-calcium phosphate, magnesium silicate, nano diatomite mixing, join in deionized water, be stirring evenly and then adding into lauric acid amide of ethanol, ammonium tungstate, stirring mixing 4 minutes at 76 DEG C；
Being mixed with Oleum Hippophae by ketopyrrolidine hydroxy acid sodium, join in silicone acrylic emulsion, 120 revs/min of stirrings mix 3 minutes, add monoalky lether phosphate ester, stir；
Each raw material after above-mentioned process is mixed with remaining each raw material, 600 revs/min of dispersed with stirring 30 minutes, obtain described nanometer base waterproof coating.
Performance test:
Elongation percentage: >=300%；
Impermeability: 0.3MPa (one hour waterproof).
Claims (2)
1. a nanometer base waterproof coating, it is characterised in that it is made up of the raw material of following weight parts: silicone acrylic emulsion 70, ketopyrrolidine hydroxy acid sodium 1.3, aminoethyl piperazine 0.2, monoalky lether phosphoesterase 30 .2, Oleum Hippophae 0.6, ammonium tungstate 0.5, lauric acid amide of ethanol 0.5, magnesium silicate 3,2-vinylpyridine 0.6, nano-calcium phosphate 5, polyether Glycols 2-3, nano diatomite 5, coalescents 8, deionized water 17；
Described coalescents is made up of the raw material of following weight parts:
Silicone acrylic emulsion 35, Aloe extraction solution 0.3, ethyl hydroxybenzoate 2, prodan 0.8, tetramethylolmethane 2, dibutyl tin laurate 0.1, micropowder silica gel 2, trimethyl benzyl ammonia chloride 0.8-2, deionized water 75；
Micropowder silica gel is mixed with tetramethylolmethane, stirring mixing 4 minutes at 70 DEG C, add the 40% of above-mentioned deionized water weight, trimethyl benzyl ammonia chloride, 100 revs/min of dispersed with stirring 12 minutes, obtain dispersion liquid；
Ethyl hydroxybenzoate is mixed with Aloe extraction solution, is stirring evenly and then adding in silicone acrylic emulsion, insulated and stirred 15 minutes at 40 DEG C, add above-mentioned dispersion liquid, dibutyl tin laurate, stir to room temperature, add and remain each raw material, 400 revs/min of dispersed with stirring 10 minutes, obtain described coalescents.
2. the preparation method of a nanometer base waterproof coating as claimed in claim 1, it is characterized in that comprising the following steps: by nano-calcium phosphate, magnesium silicate, nano diatomite mixing, join in deionized water, it is stirring evenly and then adding into lauric acid amide of ethanol, ammonium tungstate, stirring mixing 4 minutes at 76 DEG C；
Being mixed with Oleum Hippophae by ketopyrrolidine hydroxy acid sodium, join in silicone acrylic emulsion, 120 revs/min of stirrings mix 3 minutes, add monoalky lether phosphate ester, stir；
Each raw material after above-mentioned process is mixed with remaining each raw material, 600 revs/min of dispersed with stirring 30 minutes, obtain described nanometer base waterproof coating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410293839.9A CN104119717B (en) | 2014-06-26 | 2014-06-26 | A kind of nanometer base waterproof coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410293839.9A CN104119717B (en) | 2014-06-26 | 2014-06-26 | A kind of nanometer base waterproof coating |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104119717A CN104119717A (en) | 2014-10-29 |
| CN104119717B true CN104119717B (en) | 2016-08-24 |
Family
ID=51765364
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410293839.9A Active CN104119717B (en) | 2014-06-26 | 2014-06-26 | A kind of nanometer base waterproof coating |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104119717B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106905793A (en) * | 2017-04-06 | 2017-06-30 | 合肥欧克斯新型建材有限公司 | A kind of imitation porcelain coating and preparation method thereof |
| CN116285532A (en) * | 2023-04-04 | 2023-06-23 | 四川亿胜建设集团有限公司 | Waterproof building coating and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1038761C (en) * | 1993-05-31 | 1998-06-17 | 大连市风彩涂料厂 | Water-proof paint |
| CN103614038B (en) * | 2013-10-28 | 2016-04-13 | 蚌埠市高华电子有限公司 | A kind of environmental-friendly composite water-proof paint |
| CN103614039B (en) * | 2013-10-28 | 2016-05-18 | 蚌埠市高华电子有限公司 | A kind of Silicone acrylic emulsion water-repellent paint |
-
2014
- 2014-06-26 CN CN201410293839.9A patent/CN104119717B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN104119717A (en) | 2014-10-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104119712B (en) | A kind of heat-insulating waterproof coating | |
| CN104130647B (en) | A kind of anti-corrosive and waterproof paint | |
| CN107619224B (en) | Anti-cracking heat-preserving recycled aggregate mortar and preparation method thereof | |
| CN104250459A (en) | High-temperature-resistant anticorrosion waterproof paint | |
| CN104119734B (en) | A kind of environment-friendly waterproof paint | |
| CN104650720A (en) | Low-temperature-resistant anti-leakage waterproof paint and preparation method thereof | |
| CN104119717B (en) | A kind of nanometer base waterproof coating | |
| CN104119711B (en) | A kind of asphalt waterproofing paint | |
| CN104119716B (en) | A kind of automatically cleaning water-repellent paint | |
| CN104673087A (en) | Anti-flaking waterproof coating material for buildings and preparation method thereof | |
| CN103468136B (en) | A kind of Environmental-protecwaterproof waterproof paint | |
| CN104650721A (en) | Waterproof paint with high corrosion resistance and adhesive property and preparation method of waterproof paint | |
| CN108531026A (en) | A kind of polymer eakleite cementitious composite water-proof heat-insulating paint | |
| CN104650719A (en) | Sterilizing freezing-tolerance waterproof paint and preparation method thereof | |
| CN109233364A (en) | A kind of feature of environmental protection conch meal water-repellent paint | |
| CN103614017A (en) | Waterproof coating containing rosin water | |
| CN104672965A (en) | Waterproof paint with high adhesive force and crack resistance and preparation method of waterproof paint | |
| CN104119750B (en) | A kind of indoor decoration type water-repellent paint | |
| CN104119757B (en) | A kind of exterior wall waterproofing coating | |
| CN104119756B (en) | A kind of anti-low temperature water-repellent paint | |
| CN106634418B (en) | A kind of new-energy automobile epoxy graft grapheme finishing coat and preparation method thereof | |
| CN104119713B (en) | A kind of Hesperidin water-repellent paint | |
| CN104119755B (en) | A kind of anticracking waterproof coating | |
| CN105950062A (en) | Efficient waterproof binder and production method thereof | |
| CN104119758A (en) | Dense anti-leakage waterproof coating |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20240320 Address after: 261000 Datuo Village, Taitou Town, Shouguang City, Weifang City, Shandong Province Patentee after: Weifang Yinhong waterproof material Co.,Ltd. Country or region after: Zhong Guo Address before: No.18, Shaoji Ershi Road, Banta Town, Laian County, Chuzhou City, Anhui Province Patentee before: ANHUI KUAILAI WATERPROOFING & ANTI-CORROSION Co.,Ltd. Country or region before: Zhong Guo |
|
| TR01 | Transfer of patent right |