CN104119717A - Nanometer-based waterproof coating - Google Patents
Nanometer-based waterproof coating Download PDFInfo
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- CN104119717A CN104119717A CN201410293839.9A CN201410293839A CN104119717A CN 104119717 A CN104119717 A CN 104119717A CN 201410293839 A CN201410293839 A CN 201410293839A CN 104119717 A CN104119717 A CN 104119717A
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- 239000011248 coating agent Substances 0.000 title abstract description 6
- 238000000576 coating method Methods 0.000 title abstract description 6
- 239000002994 raw material Substances 0.000 claims abstract description 18
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000008367 deionised water Substances 0.000 claims abstract description 13
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 13
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 10
- 239000011734 sodium Substances 0.000 claims abstract description 10
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 10
- 239000001506 calcium phosphate Substances 0.000 claims abstract description 9
- 229910000389 calcium phosphate Inorganic materials 0.000 claims abstract description 9
- 150000001261 hydroxy acids Chemical class 0.000 claims abstract description 7
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000391 magnesium silicate Substances 0.000 claims abstract description 7
- 229910052919 magnesium silicate Inorganic materials 0.000 claims abstract description 7
- 235000019792 magnesium silicate Nutrition 0.000 claims abstract description 7
- HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 claims abstract description 7
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims abstract description 7
- KGIGUEBEKRSTEW-UHFFFAOYSA-N 2-vinylpyridine Chemical compound C=CC1=CC=CC=N1 KGIGUEBEKRSTEW-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 4
- IMUDHTPIFIBORV-UHFFFAOYSA-N aminoethylpiperazine Chemical compound NCCN1CCNCC1 IMUDHTPIFIBORV-UHFFFAOYSA-N 0.000 claims abstract description 4
- -1 monoalkyl ether phosphate Chemical class 0.000 claims abstract description 4
- 229920000570 polyether Polymers 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 18
- 239000003973 paint Substances 0.000 claims description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000002253 acid Substances 0.000 claims description 12
- 239000004816 latex Substances 0.000 claims description 12
- 229920000126 latex Polymers 0.000 claims description 12
- 238000004581 coalescence Methods 0.000 claims description 9
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 7
- XISFOXBYRQWDNK-UHFFFAOYSA-N 2-(2-methylphenyl)propan-2-amine;hydrochloride Chemical compound [Cl-].CC1=CC=CC=C1C(C)(C)[NH3+] XISFOXBYRQWDNK-UHFFFAOYSA-N 0.000 claims description 6
- 241001116389 Aloe Species 0.000 claims description 6
- 235000003935 Hippophae Nutrition 0.000 claims description 6
- 241000229143 Hippophae Species 0.000 claims description 6
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 6
- 235000011399 aloe vera Nutrition 0.000 claims description 6
- 239000006185 dispersion Substances 0.000 claims description 6
- ILRSCQWREDREME-UHFFFAOYSA-N dodecanamide Chemical compound CCCCCCCCCCCC(N)=O ILRSCQWREDREME-UHFFFAOYSA-N 0.000 claims description 6
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 claims description 6
- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 claims description 6
- 229940043351 ethyl-p-hydroxybenzoate Drugs 0.000 claims description 6
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 claims description 6
- 229940059574 pentaerithrityl Drugs 0.000 claims description 6
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 6
- 239000000741 silica gel Substances 0.000 claims description 6
- 229910002027 silica gel Inorganic materials 0.000 claims description 6
- 108050008598 Phosphoesterases Proteins 0.000 claims description 3
- 150000001346 alkyl aryl ethers Chemical class 0.000 claims description 3
- 150000002334 glycols Chemical class 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 238000005299 abrasion Methods 0.000 abstract description 2
- 239000012752 auxiliary agent Substances 0.000 abstract description 2
- 238000005336 cracking Methods 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 2
- 235000011010 calcium phosphates Nutrition 0.000 abstract 2
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 abstract 2
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 abstract 1
- 150000001408 amides Chemical class 0.000 abstract 1
- 238000013329 compounding Methods 0.000 abstract 1
- 235000014113 dietary fatty acids Nutrition 0.000 abstract 1
- 230000000694 effects Effects 0.000 abstract 1
- 239000000839 emulsion Substances 0.000 abstract 1
- 239000000194 fatty acid Substances 0.000 abstract 1
- 229930195729 fatty acid Natural products 0.000 abstract 1
- 150000004665 fatty acids Chemical class 0.000 abstract 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 abstract 1
- 239000010452 phosphate Substances 0.000 abstract 1
- 229920001296 polysiloxane Polymers 0.000 abstract 1
- 239000000463 material Substances 0.000 description 5
- 230000032683 aging Effects 0.000 description 2
- 239000004568 cement Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000004078 waterproofing Methods 0.000 description 2
- 239000002131 composite material Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
The invention discloses a nanometer-based waterproof coating which comprises the following raw materials in parts by weight: 63-70 parts of silicone acrylic emulsions, 1.3-2 parts of pyrrolidone hydroxy acid sodium, 0.1-0.2 part of aminoethyl piperazine, 0.1-0.2 part of monoalkyl ether phosphate, 0.6-1 part of sea buckthron oil, 0.5-1 part of ammonium tungstate, 0.2-0.5 part of coco fatty acid diethanol amide, 2-3 parts of magnesium silicate, 0.6-1 part of 2-vinylpyridine, 5-7 part of nanometer calcium phosphate, 2-3 parts of polyether glycol, 5-8 parts of nanometer diatomite, 5-8 parts of film-forming auxiliary agents and 10-17 parts of deionized water. Since nanometer diatomite and nanometer calcium phosphate are added to the nanometer-based waterproof coating disclosed by the invention, the cracking resistant property and abrasion resistant property of a coated film can be enhanced effectively; and the nanometer-based waterproof coating has the advantages of reasonable raw material compounding, good environmental friendliness, excellent frost resistance and low-temperature flexibility, good constructability, no blistering, good film-forming effect and high water resistance.
Description
Technical field
The present invention relates generally to a kind of coating, relates in particular to a kind of nano based waterproof paint.
Background technology
Traditional water-proof material mainly contains the flexible waterproof materials such as waterproof roll, waterproof paint, sealing cement, and taking cement matrix as main, adds the rigidity water-proofing material of liquid medicine agent and other auxiliary agent.The most of waterproofing work of China all adopts conventional waterproof material, conventional waterproof material exist loss of properties on aging, tensile strength low, to shortcomings such as temperature sensitives.Conventional waterproof coating is used for roof waterproof, easily cause aging, dry and cracked, be out of shape, fracture, the phenomenon such as layering, for indoor waterproof, for complex-shaped place, constructional difficulties, and to Seepage, quality is more difficult to ensure, people will spend a large amount of funds every several years and labor force reprocesses, and have not only confused people's orthobiosis, work and the production order, and affect the work-ing life of whole building nano based thing.In order to meet the requirement of every profession and trade to waterproof paint, production high-performance, widely used waterproof paint is necessary.
Summary of the invention
The object of the invention is just to provide a kind of nano based waterproof paint.
The present invention is achieved by the following technical solutions:
A kind of nano based waterproof paint, it is made up of the raw material of following weight parts:
Organosilicon crylic acid latex 63-70, pyrrolidone hydroxy acid sodium 1.3-2, aminoethyl piperazine 0.1-0.2, monoalky lether phosphoesterase 30 .1-0.2, Oleum Hippophae 0.6-1, ammonium tungstate 0.5-1, lauric acid amide of ethanol 0.2-0.5, Magnesium Silicate q-agent 2-3,2-vinyl pyridine 0.6-1, nano-calcium phosphate 5-7, polyether Glycols 2-3, nano diatomite 5-8, film coalescence aid 5-8, deionized water 10-17;
Described film coalescence aid is made up of the raw material of following weight parts:
Organosilicon crylic acid latex 30-35, extract solution from aloe 0.3-2, ethyl p-hydroxybenzoate 1-2, Sodium Silicofluoride 0.8-1, tetramethylolmethane 2-3, dibutyl tin laurate 0.1-0.2, micropowder silica gel 2-4, trimethyl benzyl ammonia chloride 0.8-2, deionized water 70-75;
Micropowder silica gel is mixed with tetramethylolmethane, at 65-70 DEG C, be uniformly mixed 2-4 minute, add 30-40%, the trimethyl benzyl ammonia chloride of above-mentioned deionized water weight, 100-200 rev/min of dispersed with stirring 6-12 minute, obtains dispersion liquid;
Ethyl p-hydroxybenzoate is mixed with extract solution from aloe, after stirring, join in organosilicon crylic acid latex, insulated and stirred 10-15 minute at 35-40 DEG C, add above-mentioned dispersion liquid, dibutyl tin laurate, be stirred to normal temperature, add the each raw material of residue, 300-400 rev/min of dispersed with stirring 7-10 minute, obtains described film coalescence aid.
A preparation method for nano based waterproof paint, comprises the following steps:
Nano-calcium phosphate, Magnesium Silicate q-agent, nano diatomite are mixed, join in deionized water, after stirring, add lauric acid amide of ethanol, ammonium tungstate, at 70-76 DEG C, be uniformly mixed 4-5 minute;
Pyrrolidone hydroxy acid sodium is mixed with Oleum Hippophae, join in organosilicon crylic acid latex, 100-120 rev/min is uniformly mixed 3-5 minute, adds monoalky lether phosphoric acid ester, stirs;
Above-mentioned each raw material after treatment is mixed with the each raw material of residue, and 500-600 rev/min of dispersed with stirring 20-30 minute, obtains described nano based waterproof paint.
Advantage of the present invention is:
Nano diatomite, nano-calcium phosphate that waterproof paint of the present invention adds, can effectively improve cracking resistance, the abrasion resistance of film, and each raw material is composite rationally, the feature of environmental protection is good, also has good frost resistance and low temperature flexibility, and application property is good, non-foaming, film-formation result good, water-repellancy is strong.
Embodiment
Embodiment 1
A kind of nano based waterproof paint, it by following weight parts (kilogram) raw material form:
Organosilicon crylic acid latex 70, pyrrolidone hydroxy acid sodium 1.3, aminoethyl piperazine 0.2, monoalky lether phosphoesterase 30 .2, Oleum Hippophae 0.6, ammonium tungstate 0.5, lauric acid amide of ethanol 0.5, Magnesium Silicate q-agent 3,2-vinyl pyridine 0.6, nano-calcium phosphate 5, polyether Glycols 2-3, nano diatomite 5, film coalescence aid 8, deionized water 17;
Described film coalescence aid is made up of the raw material of following weight parts:
Organosilicon crylic acid latex 35, extract solution from aloe 0.3, ethyl p-hydroxybenzoate 2, Sodium Silicofluoride 0.8, tetramethylolmethane 2, dibutyl tin laurate 0.1, micropowder silica gel 2, trimethyl benzyl ammonia chloride 0.8-2, deionized water 75;
Micropowder silica gel is mixed with tetramethylolmethane, at 70 DEG C, is uniformly mixed 4 minutes, add above-mentioned deionized water weight 40%, trimethyl benzyl ammonia chloride, 100 revs/min of dispersed with stirring 12 minutes, obtain dispersion liquid;
Ethyl p-hydroxybenzoate is mixed with extract solution from aloe, after stirring, join in organosilicon crylic acid latex, insulated and stirred 15 minutes at 40 DEG C, add above-mentioned dispersion liquid, dibutyl tin laurate, be stirred to normal temperature, add the each raw material of residue, 400 revs/min of dispersed with stirring 10 minutes, obtain described film coalescence aid.
A preparation method for nano based waterproof paint, comprises the following steps:
Nano-calcium phosphate, Magnesium Silicate q-agent, nano diatomite are mixed, join in deionized water, after stirring, add lauric acid amide of ethanol, ammonium tungstate, at 76 DEG C, be uniformly mixed 4 minutes;
Pyrrolidone hydroxy acid sodium is mixed with Oleum Hippophae, join in organosilicon crylic acid latex, 120 revs/min are uniformly mixed 3 minutes, add monoalky lether phosphoric acid ester, stir;
Above-mentioned each raw material after treatment is mixed with the each raw material of residue, and 600 revs/min of dispersed with stirring 30 minutes, obtain described nano based waterproof paint.
Performance test:
Unit elongation: >=300%;
Watertightness: 0.3MPa (one hour waterproof).
Claims (2)
1. a nano based waterproof paint, is characterized in that what it was made up of the raw material of following weight parts:
Organosilicon crylic acid latex 63-70, pyrrolidone hydroxy acid sodium 1.3-2, aminoethyl piperazine 0.1-0.2, monoalky lether phosphoesterase 30 .1-0.2, Oleum Hippophae 0.6-1, ammonium tungstate 0.5-1, lauric acid amide of ethanol 0.2-0.5, Magnesium Silicate q-agent 2-3,2-vinyl pyridine 0.6-1, nano-calcium phosphate 5-7, polyether Glycols 2-3, nano diatomite 5-8, film coalescence aid 5-8, deionized water 10-17;
Described film coalescence aid is made up of the raw material of following weight parts:
Organosilicon crylic acid latex 30-35, extract solution from aloe 0.3-2, ethyl p-hydroxybenzoate 1-2, Sodium Silicofluoride 0.8-1, tetramethylolmethane 2-3, dibutyl tin laurate 0.1-0.2, micropowder silica gel 2-4, trimethyl benzyl ammonia chloride 0.8-2, deionized water 70-75;
Micropowder silica gel is mixed with tetramethylolmethane, at 65-70 DEG C, be uniformly mixed 2-4 minute, add 30-40%, the trimethyl benzyl ammonia chloride of above-mentioned deionized water weight, 100-200 rev/min of dispersed with stirring 6-12 minute, obtains dispersion liquid;
Ethyl p-hydroxybenzoate is mixed with extract solution from aloe, after stirring, join in organosilicon crylic acid latex, insulated and stirred 10-15 minute at 35-40 DEG C, add above-mentioned dispersion liquid, dibutyl tin laurate, be stirred to normal temperature, add the each raw material of residue, 300-400 rev/min of dispersed with stirring 7-10 minute, obtains described film coalescence aid.
2. a preparation method for nano based waterproof paint as claimed in claim 1, is characterized in that comprising the following steps:
Nano-calcium phosphate, Magnesium Silicate q-agent, nano diatomite are mixed, join in deionized water, after stirring, add lauric acid amide of ethanol, ammonium tungstate, at 70-76 DEG C, be uniformly mixed 4-5 minute;
Pyrrolidone hydroxy acid sodium is mixed with Oleum Hippophae, join in organosilicon crylic acid latex, 100-120 rev/min is uniformly mixed 3-5 minute, adds monoalky lether phosphoric acid ester, stirs;
Above-mentioned each raw material after treatment is mixed with the each raw material of residue, and 500-600 rev/min of dispersed with stirring 20-30 minute, obtains described nano based waterproof paint.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410293839.9A CN104119717B (en) | 2014-06-26 | 2014-06-26 | A kind of nanometer base waterproof coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410293839.9A CN104119717B (en) | 2014-06-26 | 2014-06-26 | A kind of nanometer base waterproof coating |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104119717A true CN104119717A (en) | 2014-10-29 |
| CN104119717B CN104119717B (en) | 2016-08-24 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410293839.9A Active CN104119717B (en) | 2014-06-26 | 2014-06-26 | A kind of nanometer base waterproof coating |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104119717B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106905793A (en) * | 2017-04-06 | 2017-06-30 | 合肥欧克斯新型建材有限公司 | A kind of imitation porcelain coating and preparation method thereof |
| CN116285532A (en) * | 2023-04-04 | 2023-06-23 | 四川亿胜建设集团有限公司 | Waterproof building coating and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1083084A (en) * | 1993-05-31 | 1994-03-02 | 大连市风彩涂料厂 | Waterproof paint |
| CN103614039A (en) * | 2013-10-28 | 2014-03-05 | 蚌埠市高华电子有限公司 | Waterproof silicone acrylic emulsion coating |
| CN103614038A (en) * | 2013-10-28 | 2014-03-05 | 蚌埠市高华电子有限公司 | Environmentally-friendly composite waterproof coating |
-
2014
- 2014-06-26 CN CN201410293839.9A patent/CN104119717B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1083084A (en) * | 1993-05-31 | 1994-03-02 | 大连市风彩涂料厂 | Waterproof paint |
| CN103614039A (en) * | 2013-10-28 | 2014-03-05 | 蚌埠市高华电子有限公司 | Waterproof silicone acrylic emulsion coating |
| CN103614038A (en) * | 2013-10-28 | 2014-03-05 | 蚌埠市高华电子有限公司 | Environmentally-friendly composite waterproof coating |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106905793A (en) * | 2017-04-06 | 2017-06-30 | 合肥欧克斯新型建材有限公司 | A kind of imitation porcelain coating and preparation method thereof |
| CN116285532A (en) * | 2023-04-04 | 2023-06-23 | 四川亿胜建设集团有限公司 | Waterproof building coating and preparation method thereof |
| CN116285532B (en) * | 2023-04-04 | 2024-08-16 | 四川亿胜建设集团有限公司 | Waterproof building coating and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104119717B (en) | 2016-08-24 |
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Effective date of registration: 20240320 Address after: 261000 Datuo Village, Taitou Town, Shouguang City, Weifang City, Shandong Province Patentee after: Weifang Yinhong waterproof material Co.,Ltd. Country or region after: Zhong Guo Address before: No.18, Shaoji Ershi Road, Banta Town, Laian County, Chuzhou City, Anhui Province Patentee before: ANHUI KUAILAI WATERPROOFING & ANTI-CORROSION Co.,Ltd. Country or region before: Zhong Guo |