CN104082653A - Preparation method of intelligence promoting solid honey rich in DHA and product thereof - Google Patents

Preparation method of intelligence promoting solid honey rich in DHA and product thereof Download PDF

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Publication number
CN104082653A
CN104082653A CN201410369619.XA CN201410369619A CN104082653A CN 104082653 A CN104082653 A CN 104082653A CN 201410369619 A CN201410369619 A CN 201410369619A CN 104082653 A CN104082653 A CN 104082653A
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honey
dha
preheating
condition
under
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罗文华
殷素会
戴荣国
王瑞生
姬聪慧
程尚
高丽娇
杨金龙
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Chongqing Academy of Animal Sciences
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Chongqing Academy of Animal Sciences
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/115—Fatty acids or derivatives thereof; Fats or oils
    • A23L33/12—Fatty acids or derivatives thereof
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
    • A23L21/20—Products from apiculture, e.g. royal jelly or pollen; Substitutes therefor
    • A23L21/25—Honey; Honey substitutes
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Mycology (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Jellies, Jams, And Syrups (AREA)

Abstract

The invention discloses a preparation method of intelligence promoting solid honey rich in DHA and a product thereof. The preparation method comprises the following steps: firstly, blending and mixing honey of different sources uniformly, then preheating at 15 DEG C-35 DEG C, weighing DHA 20-100 microgram for each kilogram of preheated honey, then adding into the preheated honey with the weight equivalent to 5-9 times of that of DHA, stirring and heating after adding so as to enable the honey to reach 45 DEG C-60 DEG C, then carrying out ultrasonic wave emulsification by adopting a method of progressively increasing with equal quantity, carrying out vacuum filtration, refrigerating a mixture under the condition of minus 20 DEG C-minus 25 DEG C, then cryopreserving for 0.5-1.5 hours under the condition of vacuum degree of minus 0.6 MPa-minus 1.0 MPa, then heating under the vacuum condition of 30-40 DEG C until the weight percentage of moisture in the mixture is 1%-3%, cooling and crushing so as to obtain the intelligence promoting solid honey. The method disclosed by the invention is simple, is low in production energy consumption and cost, can ensure purity of the honey rich in DHA, and has intelligence promoting function.

Description

Be rich in preparation method of the intelligence development solid bee honey of DHA and products thereof
Technical field
The invention belongs to health products manufacture field, be specifically related to preparation method of the intelligence development solid bee honey that is rich in DHA and products thereof.
Background technology
Along with the progressively raising of people's living standard, people more and more pay attention to health care and beauty treatment.Therefore studying a kind of food anticancer, health-care effect of improving looks that has, realize edible food in people's life and can reach the anticancer object of beauty treatment, realize integration of drinking and medicinal herbs, is the direction of Developing.
Honey be translucent, with gloss, dense thick liquid, white, to faint yellow or crocus to yellowish-brown, is put for a long time or meets cold gradually adularescent crystalline particulate and separate out.The main component of honey is fructose and glucose, and both content add up to approximately 70%; Still containing a small amount of sucrose (content is quite high sometimes), maltose, dextrin, natural gum, and nitrogen-containing compound, organic acid, volatile oil, pigment, wax, plant relic (particularly pollen grain), yeast, enzyme, inorganic salts etc.; But general only containing mcg vitamin, as vitamin A, vitamin C, vitamin D, choline, vitamin B2, niacin, pantothenic acid, biotin, folic acid, Cobastab and vitamin K etc.Honey, due to containing abundant nutrition composition, is extensively liked by people as a kind of health food.But the shortcoming of honey is fluid, the edible inconvenience of carrying.In order to be convenient for carrying, honey is processed into solid bee honey, its main method is to add appropriate auxiliary material, and honey is processed into powdery, graininess and bulk.But, in production engineering, mostly need temperature higher than 100 DEG C of processing, honey active ingredient is destroyed, affect the original local flavor of honey and effect.
Since the nineties in 20th century, unrighted acid DHA (DHA) is a large focal spot of child nutrition product always.Brain nutrient research institute of Britain croft professor and Japanese famous nutritionist Austria are by the secret that accounts for beautiful professor and disclosed the earliest DHA, and their result of study shows: DHA is one of people's brain development, important substance of growth.DHA accounts for 25% of its fat content in nerve fiber, and cynapse is the key position that control information is transmitted, and is made up of synaptic membrane and gap, and DHA contributes to its structural integrity, Function.In the time of the medium-term and long-term shortage of meals DHA, in synaptic membrane, will lack the PL containing DHA, structure will be destroyed, and then information transmission, thinking ability are produced to harmful effect.Therefore studying a kind of honey food with nootropic effect, realize the object that in people's life, edible honey can reach intelligence development, realize integration of drinking and medicinal herbs, is a direction of Developing.
Summary of the invention
In view of this, one of object of the present invention is to provide the preparation method of the solid bee honey with effect of benefiting intelligence; Two of object of the present invention is to provide the product being made by said method.
For achieving the above object, the invention provides following technical scheme:
1, the preparation method who is rich in the intelligence development solid bee honey of DHA, comprises the steps:
(1) by honey blending and mixings different source, then, by honey preheating under 15 DEG C of-35 DEG C of conditions, obtain preheating honey;
(2) take DHA20-100 μ g by every kilogram of preheating honey, then DHA is added and be equivalent to, in DHA weight 5-9 preheating honey doubly, add rear stirring to make honey temperature reach 45 DEG C～60 DEG C, obtain premix;
(3) step (2) gained premix is carried out to ultrasonic emulsification, the preheating honey of weight such as then add, continue ultrasonic emulsification, and then the preheating honey of weight such as add, continue ultrasonic emulsification, so repeatedly until step (1) gained preheating honey ultrasonic emulsification is complete; The condition of described ultrasonic emulsification is that proportion is 30～45kHz under 15 DEG C～60 DEG C conditions, and the ultrasonic emulsification that voltage is 30～40V is processed 20～30 minutes;
(4) by step (3), the mixture after ultrasonic emulsification makes the granularity of honey reach 80～200 orders with vacuum filtration;
(5) by the mixture of step (4) vacuum filtration first under the condition of-20 DEG C～-25 DEG C freezing 12～48 hours, then move in vacuum drier, at-20 DEG C～-25 DEG C, vacuum be-preserve 0.5～1.5 hour under the condition of 0.6MPa～-1.0MPa, at 30～40 DEG C, vacuum be after this-be heated to mixture under 0.6MPa～-1.0MPa condition in the percentage by weight of moisture content be 1%-3%;
(6) mixture of processing through step (5) is pulverized and be get final product under 20-25 DEG C of condition.
Preferably, in described step (1), described preheating is by honey preheating under 30 DEG C of conditions.
Preferably, described step (2), for to take DHA100 μ g by every kilogram of preheating honey, then adds DHA in the preheating honey that is equivalent to 9 times of DHA weight, adds rear stirring to make honey temperature reach 45 DEG C, obtains premix.
Preferred, in described step (2), described stirring is to stir 10-20 minute with the rotating speed of 2000 revs/min.
Preferably, in described step (3), the condition of described ultrasonic emulsification is under 15 DEG C of conditions, and proportion is 45kHz, and the ultrasonic emulsification that voltage is 40V is processed 25 minutes.
Preferred, described step (4) is that the mixture by step (3) after ultrasonic emulsification makes the granularity of honey reach 200 orders with vacuum filtration, described suction filtration adopts the filter type of 3 grades, the first order 80 orders, the second level 100 orders, the third level 200 orders.
Preferred, described step (5) is by the mixture of step (4) suction filtration first under the condition of-25 DEG C freezing 48 hours, then move in vacuum drier, at-25 DEG C, vacuum be-preserve 1.5 hours under the condition of 0.8MPa, at 35 DEG C, vacuum be after this-be heated to mixture under 0.8MPa condition in the percentage by weight of moisture content be 2%.
2, the intelligence development solid bee honey that is rich in DHA being made by described preparation method.
Beneficial effect of the present invention is: the preparation method who the invention discloses the solid bee honey that is rich in DHA, the method preparation technology is simple, process time is short, and processing temperature is controlled at below 60 DEG C, can ensure original local flavor and the quality of honey, obtain solid bee honey solubility good, add appropriate water can obtain conventional honey, and the present invention has added DHA in solid bee honey simultaneously, after honey and DHA combination, its puzzle effect is strengthened, can play effect of spleen-benefiting mind-tranquilizing, blood yiqi simultaneously.
Detailed description of the invention
Below in conjunction with preferred embodiment, the present invention is described in detail.The experimental technique of unreceipted actual conditions in embodiment, the condition of conventionally advising according to normal condition or according to manufacturer.
EXAMPLE l
The preparation method who is rich in the intelligence development solid bee honey of DHA, comprises the steps:
(1) by honey blending and mixings different source, then, by honey preheating under 30 DEG C of conditions, obtain preheating honey; Preheating ensures the mobility of honey, facilitates following process;
(2) take DHA20 μ g by every kilogram of preheating honey, then DHA is added in the preheating honey that is equivalent to 5 times of DHA weight, rotating speed with 2000 revs/min after adding stirs 15 minutes with hand-held mixer, makes honey temperature reach 50 DEG C, obtains premix;
(3) step (2) gained premix is carried out to ultrasonic emulsification, the preheating honey of weight such as then add, continue ultrasonic emulsification, and then the preheating honey of weight such as add, continue ultrasonic emulsification, so repeatedly until step (1) gained preheating honey ultrasonic emulsification is complete; The condition of described ultrasonic emulsification is under 30 DEG C of conditions, and proportion is 30kHz, and the ultrasonic emulsification that voltage is 30V is processed 20 minutes;
(4) by step (3), the mixture after ultrasonic emulsification makes the granularity of honey reach 80 orders with vacuum filtration;
(5) by the mixture of step (4) suction filtration first under the condition of-20 DEG C freezing 12 hours, then move in vacuum drier, at-20 DEG C, vacuum be-preserve 0.5 hour under the condition of 0.6MPa, at 30 DEG C, vacuum be after this-heat under 0.6MPa condition 0.5 hour to the percentage by weight of moisture content in mixture be 3%;
(6) the intelligence development solid bee honey that is rich in DHA is pulverized and obtained to the mixture of processing through step (5) under room temperature (20 DEG C) condition.
The intelligence development solid bee honey that is rich in DHA making is randomly drawed to 1g, then detect by " GB26400-2011: the assay method of National Standard of the People's Republic of China's food additives DHA ", result shows in every kilogram of solid bee honey product containing DHA20 μ g, meet product requirement, and after processing, free from extraneous odour produces.
Comparative example 1
Prepare solid bee honey according to the method identical with embodiment 1, difference is not add DHA in preparation process.
Then solid bee honey embodiment 1 and comparative example 1 being made carries out puzzle effect experiment, specific as follows: 153 of children that choose 9-10 year, be divided at random 3 groups, every group each 51, the experimental group intelligence development solid bee honey 10g that is rich in DHA that every day, edible embodiment 1 made, the solid bee honey that the edible comparative example 1 of control group 1 makes, the edible 200 μ g DHA of control group 2, record respectively 30 days and 60 days memory quotients, result is as shown in table 1:
Table 1. embodiment 1 makes the memory quotient of solid bee honey
Number of days Experimental group Control group 1 Control group 2
30 104.81 91.89 102.52
60 106.52 91.90 101.33
As shown in Table 1, the solid bee honey that edible embodiment 1 makes can improve memory quotient, improves memory, has nootropic effect.
Embodiment 2
The preparation method who is rich in the intelligence development solid bee honey of DHA, comprises the steps:
(1) by honey blending and mixings different source, then, by honey preheating under 35 DEG C of conditions, obtain preheating honey; Preheating ensures the mobility of honey, facilitates following process;
(2) take DHA60 μ g by every kilogram of preheating honey, then DHA is added in the preheating honey that is equivalent to 9 times of DHA weight, rotating speed with 2000 revs/min after adding stirs 20 minutes with hand-held mixer, makes honey temperature reach 60 DEG C, obtains premix;
(3) step (2) gained premix is carried out to ultrasonic emulsification, the preheating honey of weight such as then add, continue ultrasonic emulsification, and then the preheating honey of weight such as add, continue ultrasonic emulsification, so repeatedly until step (1) gained preheating honey ultrasonic emulsification is complete; The condition of described ultrasonic emulsification is at 60 DEG C, and proportion is 40kHz, and the ultrasonic emulsification that voltage is 40V is processed 30 minutes;
(4) by step (3), the mixture after ultrasonic emulsification makes the granularity of honey reach 120 orders with vacuum filtration; When suction filtration, adopt the filter type of 3 grades, the first order 80 orders, the second level 100 orders, the third level 120 orders;
(5) by the mixture of step (4) suction filtration first under the condition of-25 DEG C freezing 24 hours, then move in vacuum drier, at-25 DEG C, vacuum be-preserve 1 hour under the condition of 1.0MPa, at 40 DEG C, vacuum be after this-heat under 1.0MPa condition 1 hour to the percentage by weight of moisture content in mixture be 1%;
(6) the intelligence development solid bee honey that is rich in DHA is pulverized and obtained to the mixture of processing through step (5) under room temperature (22 DEG C) condition.
The intelligence development solid bee honey that is rich in DHA making is randomly drawed to 1g, then detect by " GB26400-2011: the assay method of National Standard of the People's Republic of China's food additives DHA ", result shows in every kilogram of solid bee honey product containing DHA60 μ g, meet product requirement, and after processing, free from extraneous odour produces.
Comparative example 2
Prepare solid bee honey according to the method identical with embodiment 2, difference is not add DHA in preparation process.
Then solid bee honey embodiment 1 and comparative example 1 being made carries out puzzle effect experiment, specific as follows: 153 of children that choose 9-10 year, be divided at random 3 groups, every group each 51, experimental group edible embodiment 2 every day makes the intelligence development solid bee honey 10g that is rich in DHA, the solid bee honey that the edible comparative example 2 of control group makes, the edible 600 μ g DHA of control group 2, record respectively 30 days and 60 days memory quotients, result is as shown in table 2:
Table 2. embodiment 2 makes the memory quotient of solid bee honey
Number of days Experimental group Control group 1 Control group 2
30 104.92 91.89 102.65
60 106.93 91.90 104.33
As shown in Table 2, the solid bee honey that edible embodiment 2 makes can improve memory quotient, improves memory, has nootropic effect.
Embodiment 3
The preparation method who is rich in the intelligence development solid bee honey of DHA, comprises the steps:
(1) by honey blending and mixings different source, then, by honey preheating under 15 DEG C of conditions, obtain preheating honey; Preheating ensures the mobility of honey, facilitates following process;
(2) take DHA100 μ g by every kilogram of preheating honey, then DHA is added in the preheating honey that is equivalent to 9 times of DHA weight, rotating speed with 2000 revs/min after adding stirs 10 minutes with hand-held mixer, makes honey temperature reach 45 DEG C, obtains premix;
(3) step (2) gained premix is carried out to ultrasonic emulsification, the preheating honey of weight such as then add, continue ultrasonic emulsification, and then the preheating honey of weight such as add, continue ultrasonic emulsification, so repeatedly until step (1) gained preheating honey ultrasonic emulsification is complete; The condition of described ultrasonic emulsification is under 15 DEG C of conditions, and proportion is 45kHz, and the ultrasonic emulsification that voltage is 40V is processed 25 minutes;
(4) by step (3), the mixture after ultrasonic emulsification makes the granularity of honey reach 200 orders with vacuum filtration; When suction filtration, adopt the filter type of 3 grades, the first order 80 orders, the second level 100 orders, the third level 200 orders;
(5) by the mixture of step (4) suction filtration first under the condition of-25 DEG C freezing 48 hours, then move in vacuum drier, at-25 DEG C, vacuum be-preserve 1.5 hours under the condition of 0.8MPa, at 35 DEG C, vacuum be after this-heat under 0.8MPa condition 1.5 hours to the percentage by weight of moisture content in mixture be 2%;
(6) the intelligence development solid bee honey that is rich in DHA is pulverized and obtained to the mixture of processing through step (5) under room temperature (25 DEG C) condition.
The intelligence development solid bee honey that is rich in DHA making is randomly drawed to 1g, then detect by " GB26400-2011: the assay method of National Standard of the People's Republic of China's food additives DHA ", result shows in every kilogram of solid bee honey product containing DHA100 μ g, meet product requirement, and after processing, free from extraneous odour produces.
Comparative example 3
Prepare solid bee honey according to the method identical with embodiment 3, difference is not add DHA in preparation process.
Then solid bee honey embodiment 3 and comparative example 3 being made carries out puzzle effect experiment, specific as follows: 153 of children that choose 9-10 year, be divided at random 3 groups, every group each 51, experimental group edible embodiment 3 every day makes the intelligence development solid bee honey 10g that is rich in DHA, the solid bee honey that the edible comparative example 3 of control group makes, the edible 1000 μ g DHA of control group 2, record respectively 30 days and 60 days memory quotients, result is as shown in table 3:
Table 3, embodiment 3 and comparative example 3 make the memory quotient of solid bee honey
Number of days Experimental group Control group 1 Control group 2
30 105.21 91.89 102.62
60 107.31 91.90 105.78
As shown in Table 3, the solid bee honey that edible embodiment 3 makes can improve memory quotient, improves memory, has nootropic effect.
Finally explanation is, above preferred embodiment is only unrestricted in order to technical scheme of the present invention to be described, although the present invention is described in detail by above preferred embodiment, but those skilled in the art are to be understood that, can make various changes to it in the form and details, and not depart from the claims in the present invention book limited range.

Claims (8)

1. the preparation method who is rich in the intelligence development solid bee honey of DHA, is characterized in that, comprises the steps:
(1) by honey blending and mixings different source, then, by honey preheating under 15 DEG C of-35 DEG C of conditions, obtain preheating honey;
(2) take DHA20-100 μ g by every kilogram of preheating honey, then DHA is added and be equivalent to, in DHA weight 5-9 preheating honey doubly, add rear stirring to make honey temperature reach 45 DEG C～60 DEG C, obtain premix;
(3) step (2) gained premix is carried out to ultrasonic emulsification, the preheating honey of weight such as then add, continue ultrasonic emulsification, and then the preheating honey of weight such as add, continue ultrasonic emulsification, so repeatedly until step (1) gained preheating honey ultrasonic emulsification is complete; The condition of described ultrasonic emulsification is that proportion is 30～45kHz under 15 DEG C～60 DEG C conditions, and the ultrasonic emulsification that voltage is 30～40V is processed 20～30 minutes;
(4) by step (3), the mixture after ultrasonic emulsification makes the granularity of honey reach 80～200 orders with vacuum filtration;
(5) by the mixture of step (4) vacuum filtration first under the condition of-20 DEG C～-25 DEG C freezing 12～48 hours, then move in vacuum drier, at-20 DEG C～-25 DEG C, vacuum be-preserve 0.5～1.5 hour under the condition of 0.6MPa～-1.0MPa, at 30～40 DEG C, vacuum be after this-be heated to mixture under 0.6MPa～-1.0MPa condition in the percentage by weight of moisture content be 1%-3%; (6) mixture of processing through step (5) is pulverized and be get final product under 20-25 DEG C of condition.
2. preparation method according to claim 1, is characterized in that: in described step (1), described preheating is by honey preheating under 30 DEG C of conditions.
3. according to the preparation method described in claim 1-2 any one, it is characterized in that: described step (2) is for to take DHA100 μ g by every kilogram of preheating honey, then DHA is added in the preheating honey that is equivalent to 9 times of DHA weight, add rear stirring to make honey temperature reach 45 DEG C, obtain premix.
4. preparation method according to claim 3, is characterized in that: in described step (2), described stirring is to stir 10-20 minute with the rotating speed of 2000 revs/min.
5. preparation method according to claim 1, is characterized in that: in described step (3), the condition of described ultrasonic emulsification is under 15 DEG C of conditions, and proportion is 45kHz, and the ultrasonic emulsification that voltage is 40V is processed 25 minutes.
6. preparation method according to claim 1, it is characterized in that: described step (4) is, mixture by step (3) after ultrasonic emulsification makes the granularity of honey reach 200 orders with vacuum filtration, described suction filtration adopts the filter type of 3 grades, the first order 80 orders, the second level 100 orders, the third level 200 orders.
7. preparation method according to claim 1, it is characterized in that: described step (5) is by the mixture of step (4) suction filtration first under the condition of-25 DEG C freezing 48 hours, then move in vacuum drier, at-25 DEG C, vacuum be-preserve 1.5 hours under the condition of 0.8MPa, at 35 DEG C, vacuum be after this-be heated to mixture under 0.8MPa condition in the percentage by weight of moisture content be 2%.
8. the intelligence development solid bee honey that is rich in DHA being made by preparation method described in claim 1-7 any one.
CN201410369619.XA 2014-07-30 2014-07-30 Preparation method of intelligence promoting solid honey rich in DHA and product thereof Pending CN104082653A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6131048A (en) * 1984-07-23 1986-02-13 Gifu Youhou Kk Preparation of honey containing pollen powder
CN1200884A (en) * 1997-06-03 1998-12-09 胡兴中 Phosphatidyl honey and preparation method therefor
CN1265840A (en) * 2000-01-12 2000-09-13 黄玲 Method for making solid honey
WO2005120174A2 (en) * 2004-05-24 2005-12-22 Interactive Research Institute For Health Affairs Omega-3 fatty acid compositions with honey
CN1820629A (en) * 2006-03-02 2006-08-23 陈西喆 Method for producing solid honey

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6131048A (en) * 1984-07-23 1986-02-13 Gifu Youhou Kk Preparation of honey containing pollen powder
CN1200884A (en) * 1997-06-03 1998-12-09 胡兴中 Phosphatidyl honey and preparation method therefor
CN1265840A (en) * 2000-01-12 2000-09-13 黄玲 Method for making solid honey
WO2005120174A2 (en) * 2004-05-24 2005-12-22 Interactive Research Institute For Health Affairs Omega-3 fatty acid compositions with honey
CN1820629A (en) * 2006-03-02 2006-08-23 陈西喆 Method for producing solid honey

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Application publication date: 20141008