CN104027707A - Digestion-helping and qi-stagnation-eliminating lozenge and preparation method thereof - Google Patents
Digestion-helping and qi-stagnation-eliminating lozenge and preparation method thereof Download PDFInfo
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses a digestion-helping and qi-stagnation-eliminating lozenge and a preparation method thereof. The digestion-helping and qi-stagnation-eliminating lozenge is characterized by being prepared from the following raw materials by weight: 30 to 50 parts of pawpaw, 20 to 30 parts of dried orange peel, 10 to 15 parts of tsaoko fruit, 10 to 15 parts of emblic leafflower fruit, 10 to 15 parts of olive and 5 to 8 parts of mint. The lozenge has the advantages of digestion-helping, toxin-expelling, qi-stagnation-eliminating, bowel-relaxing and vomiting-arresting effects, no toxic and side effects, short healing time and especially, a substantial effect on diseases like dyspepsia, gastrectasia, gastric acid, regurgitation, vomiting and dysentery.
Description
Technical field
The present invention relates to Chinese herbal and crude drugs preparations technical field, be specially a kind of stagnant buccal tablet and preparation method thereof that helps digestion.
Background technology
Along with improving constantly of society economy, people's living standard is also improving constantly, and people's work is more and more busier, and operating pressure is also increasing, and it is irregular that the catering trade becomes, and the kind of diet kind also becomes more and more abundanter simultaneously.If the frequent eating and drinking too much at one meal of diet, has the beer more at ordinary times, do not focus on individual dietetic hygiene, the food such as greasy, raw and cold, Broiled Dishes often consume oil, will cause dyspepsia, gastrointestinal function dies down, and often occurs flatulence, gastric acid, stomachache, diarrhoea, constipation, feels sick, the symptom such as regurgitation.
At present, treat dyspepsia on market, the medicine of the gastrointestinal dysfunctions such as flatulence, gastric acid is also more, and as stomachic tablet, yeast tablet, lenitive pill etc., its therapeutic effect is also sure.But treatment cycle is long, help digestion residual effect fruit slowly, patient has the demand for the treatment of as early as possible conventionally ill, so that releasing is ailing, recovers normal work and lives.Therefore, develop and a kind ofly have and help digestion fast and effectively, cheaply, remove stagnant gas, relieving constipation, preventing or arresting vomiting, the stagnant buccal tablet that helps digestion of the effect of the diaphragm gas that disappears is just necessary.
Summary of the invention
The object of the invention is for above-mentioned prior art not enough and propose a kind of fast and effectively, cheaply, have and help digestion, toxin expelling, remove stagnant gas, relieving constipation, the effect of preventing or arresting vomiting, have no side effect, healing time is short, particularly the diseases such as dyspepsia, flatulence gastric acid, regurgitation, vomiting, dysentery had the stagnant buccal tablet and preparation method thereof that helps digestion of significant curative effect.
The present invention realizes by the following technical solutions:
The present invention's stagnant buccal tablet that helps digestion, by the raw material of following parts by weight, made:
Fructus Chaenomelis 30-50 part, Pericarpium Citri Reticulatae 20-30 part, Fructus Tsaoko 10-15 part, Fructus Phyllanthi 10-15 part, Fructus Canarii albi 10-15 part, Herba Menthae 5-8 part.
The above-described stagnant buccal tablet that helps digestion, is made by the raw material of following parts by weight: Fructus Chaenomelis 40-45 part, Pericarpium Citri Reticulatae 25-30 part, Fructus Tsaoko 12-15 part, Fructus Phyllanthi 12-15 part, Fructus Canarii albi 12-15 part, Herba Menthae 6-8 part.
The present invention is comprised of Chinese medicinal materials such as Fructus Chaenomelis, Pericarpium Citri Reticulatae, Fructus Tsaoko, Fructus Phyllanthi, Fructus Canarii albi, Herba Menthaes, has and helps digestion, toxin expelling, remove stagnant gas, relieving constipation, preventing or arresting vomiting, the disappear effect of diaphragm gas, thereby treatment dyspepsia, gastral cavity abdomen, regurgitation, vomiting, dysentery are had to significant curative effect.
Each medicine active ingredient of the above-described stagnant buccal tablet Chinese medicine formula that helps digestion is analyzed:
Fructus Chaenomelis, [Latin] (Carica papaya L.) claim again Fructus Caricae, newborn melon, papaw, is the torrid zone, the large-scale herbaceos perennial of subtropical evergreen soft wood, evergreen soft wood dungarunga, up to 8-10 rice, tool milk; Stem is branch or sometimes in injury region branch not, the stipule trace of tool helical arrangement.It is upper that fruit is longer than tree, outer image melon, therefore named Fructus Chaenomelis.Function: sweet, flat.Help digestion, anthelmintic, subduing swelling and detoxicating, lactogenesis, blood pressure lowering.For dyspepsia, taeniasis, enterobiasis, carbuncle furuncle and phyma poison, treating swelling and pain by traumatic injury, eczema, centipete bite, Peptic Ulcers, puerpera's breast is few, dysentery, vascular hypertension, two is not just smooth.
Pericarpium Citri Reticulatae, [another name] Pericarpium Citri tangerinae, expensive old, Folium Styracis Suberifoliae, Fructus Citri tangerinae skin, wide Pericarpium Citri tangerinae, Pericarpium Citri tangerinae, Citrus chachiensis Hort. C. Suavissima Tanaka, Pericarpium citri reticuatae chachiensis; [English name] Citrus reticulata Blanco.[Latin] Pericarpium Citri Reticulatae, the young fruit of rutaceae orange and variety thereof or the peel of immature fruit; [nature and flavor] 1. < < Chinese Pharmacopoeia > > gas are fragrant, acrid in the mouth, hardship; [function cures mainly] regulating qi-flowing for strengthening spleen, drying dampness to eliminate phlegm, the distension and fullness in the abdomen of stagnation of QI in spleen and stomach or pain, dyspepsia.1. < < medicine origin > >: Pericarpium Citri tangerinae energy QI invigorating, add Pericarpium Citri Reticulatae Viride and reduce by half, remove stagnant gas, push away Chen Zhixin.2. < < day is with herbal > >: Pericarpium Citri tangerinae, and can fall apart and can rush down, can temperature can mend, the diaphragm gas that can disappear, the saliva that reduces phlegm, and spleen antitussive, lead to five types of stranguria.3. < < medicine origin > >: go cold-evil in the heart, broken stagnant gas, strengthening the spleen stomach.
Fructus Tsaoko, [another name] Fructus Tsaoko, SEMEN TSAOKO; [Latin] Amomum tsao-ko. Zingiberaceae; Fructus Tsaoko grows in the broad-leaf forest of the torrid zone, the damp and hot concealment in subtropical zone, the ground such as distribution Yunnan, Guangxi, Guizhou.Flavor efficacy: acrid in the mouth, warm in nature, nontoxic.[function cures mainly] malaria, phlegm retention feeling of fullness, coldness and pain in the epigastrium, regurgitation, vomiting, dysentery, food stagnation etc.1. < < herbal classic is met former > >: except cold, and dampness, dissipating depression of QI, relieving dyspepsia, expectorant on sharp diaphragm, separates wheaten food, fish, all poison of meat.2. < < Yin Shan Zhengyao, Principles of Correct Diet > >: control cardiac and abdominal pain, preventing or arresting vomiting, mends stomach, the therapeutic method to keep the adverse QI flowing downwards.3. < < Bencao Beiyao > >: coldness and pain in the epigastrium, accumulation of food in the stomach and intes tine due to indigestion, or diet is not fragrant, vomiting regurgitation person should eat.
Fructus Phyllanthi, [another name] emblic leafflower fruit, rice contain, hope fruit, wooden ripple, seven to examine sorrow happiness, Lu public affairs fat, Phyllanthus emblica L.; [Latin] Phyllanthus emblica; Euphorbiaceae, is born in height above sea level 200-2300 rice mountain region sparse woods, shrubbery, wasteland or gully area without shade.The ground such as distribution Jiangxi, Fujian, Guangdong, Hainan, Guangxi, Sichuan.[nature and flavor] are sweet, micro-puckery, cool.1. < < Chinese Pharmacopoeia > >--really: clearing away heat and cooling blood, promoting digestion and invigorating the stomach, the cough-relieving of promoting the production of body fluid.2. < < whole nation Chinese herbal medicine compilation > > root: for hypertension, stomachache, enteritis, tuberculous lymphadenitis.[function cures mainly] heat in blood blood stasis, dyspepsia, abdominal distention, cough, laryngalgia, xerostomia and vitamin C deficiency disease.
Fructus Canarii albi, [another name] yellow olive, Fructus Canarii, black apple, white olive, red olive, blue or green son, the fruit of remonstrating with, loyal fruit; [English name] Chinese White Olive[Latin] Canavium album Raeuseh, Burseraceae; Distribution Fujian, Guangdong, Guangxi, Taiwan, Sichuan, zhejiang and other places district; [nature and flavor] sour in the mouth, puckery, sweet, warm in nature, nontoxic; [function cures mainly] removing heat from the lung and relieving sorethroat; Promoting the production of body fluid to quench thirst; Removing toxic substances etc.1. < < the southern regions of the Yunnan Province book on Chinese herbal medicine > >: control on all larynx fire scorching, epidemic infection with swollen head disease.Can separate damp and hot, spring-warm syndrome, promoting the production of body fluid to quench thirst, sharp expectorant, separates ichthyotoxin, wine, stagnant.2. < < book on Chinese herbal medicine new > > again: suppressing the hyperactive liver appetizing, lung moistening YIN nourishing, expectorant is regulated the flow of vital energy, and cough-relieving is coughed, and controls haematemesis.3. < < detailed outline > >: control throat pain, chew pharynx juice, can separate all fish Trionyx sinensis Wiegmanns poison.
Herba Menthae, [another name] HERBA MENTHAE, water mint, core Adiantum monochlamys Eaton., luxuriant lotus dish, Herba Menthae Rotundifoliae; [English name] Wild Mint, Herb of Wild Mint, Peppermint, [Latin] Mentha haplocalyx Briq, Burseraceae; Be distributed in North China, East China, Central China, south China and southwestern various places.[nature and flavor] are pungent, cool, [function cures mainly] wind heat of faling apart; Refresh oneself; Throat; Rash; Resolving depression.1. < < detailed outline > >: throat, all diseases of ability to speak.Control scrofula, skin ulcer scabies, wind scabies addiction.2. < < doctor will compile and want > >: more toothache, cough due to heat, resolving depression summer-heat, excessive thirst only, the dysentery of stopping blooding, diuresis.< < medicineization justice > >: Herba Menthae, acrid in the mouth can fall apart, cool in nature and clear.
The above-described stagnant buccal tablet that helps digestion is tentatively on probation in the projects such as clinical treatment dyspepsia, flatulence gastric acid, and reflection is good, without obvious toxic-side effects.
Above-mentioned each component medicine is made the help digestion preparation method of stagnant buccal tablet of the present invention:
(1) by weight dry Fructus Chaenomelis, Pericarpium Citri Reticulatae, Fructus Tsaoko, Fructus Phyllanthi, Fructus Canarii albi and Herba Menthae powder are broken into l00-120 object fine powder; Medicated powder is poured in pithos and is soaked 40 minutes, add the water yield be medicine gross weight 8-10 doubly, boil 1-2 hour, when fluid temperature is down to 30 ℃-60 ℃, filter, obtain extracting solution;
(2) medicinal residues after filtering in step 1 are added the water yield be medicine gross weight 3-5 doubly, boil 0.5-1 hour, when fluid temperature is down to 30 ℃-60 ℃, filter, obtain extracting solution;
(3) extracting solution step 1 and step 2 being obtained mixes, and is condensed into thick paste, adds wet and slippery dose of mix homogeneously to make soft material;
(4) soft material is crossed to 18 orders, then dry under 50-60 ℃ of condition, gained granule carries out tabletting, makes Traditional Chinese medicine lozenge.
Above-described wet and slippery dose is one or more in stearate, Pulvis Talci, hydride vegetable oil, Polyethylene Glycol.
Above-mentioned Chinese medicine of the present invention, according to different situations and pharmaceutical factory condition, can also make other external preparation.
The invention has the beneficial effects as follows:
1, the present invention plays and helps digestion, and toxin expelling removes stagnant gas, relieving constipation, and preventing or arresting vomiting, the effect of the diaphragm gas that disappears, has significant curative effect to treatment dyspepsia, flatulence gastric acid, regurgitation, vomiting, dysentery.
2, use the present invention to treat and all can alleviate for dyspepsia 1-3 days, within 4-7 days, can fully recover, cure rate reaches more than 85%, and effective percentage can reach more than 90%, and human body is had no side effect, easy to use, and cost is low.
The specific embodiment
Embodiment 1:
(1) get by weight 8 parts of 50 parts of dry Fructus Chaenomeliss, 30 parts of Pericarpium Citri Reticulataes, 15 parts of Fructus Tsaokos, 15 parts of Fructus Phyllanthis, 15 parts of Fructus Canarii albis and Herba Menthaes and be cut into segment, be crushed to 120 orders; Medicated powder is poured in pithos and soaked 40 minutes, and adding the water yield is 10 times of medicine gross weight, boils 2 hours, when fluid temperature is down to 30 ℃-60 ℃, filters, and obtains extracting solution;
(2) medicinal residues after filtering in step 1 being added to the water yield is 5 times of medicine gross weight, boils 1 hour, when fluid temperature is down to 30 ℃-60 ℃, filters, and obtains extracting solution;
(3) extracting solution step 1 and step 2 being obtained mixes, and is condensed into thick paste, adds hydride vegetable oil mix homogeneously to make soft material;
(4) soft material is crossed to 18 orders, then dry under 60 ℃ of conditions, gained granule carries out tabletting, makes Traditional Chinese medicine lozenge.
Embodiment 2:
(1) get by weight 7 parts of 45 parts of dry Fructus Chaenomeliss, 25 parts of Pericarpium Citri Reticulataes, 14 parts of Fructus Tsaokos, 14 parts of Fructus Phyllanthis, 14 parts of Fructus Canarii albis and Herba Menthaes and be cut into segment, be crushed to 120 orders; Medicated powder is poured in pithos and soaked 40 minutes, and adding the water yield is 10 times of medicine gross weight, boils 2 hours, when fluid temperature is down to 30 ℃-60 ℃, filters, and obtains extracting solution;
(2) medicinal residues after filtering in step 1 being added to the water yield is 5 times of medicine gross weight, boils 1 hour, when fluid temperature is down to 30 ℃-60 ℃, filters, and obtains extracting solution;
(3) extracting solution step 1 and step 2 being obtained mixes, and is condensed into thick paste, adds stearate mix homogeneously to make soft material;
(4) soft material is crossed to 18 orders, then dry under 55 ℃ of conditions, gained granule carries out tabletting, makes Traditional Chinese medicine lozenge.
Embodiment 3:
(1) get by weight 6 parts of 40 parts of dry Fructus Chaenomeliss, 22 parts of Pericarpium Citri Reticulataes, 13 parts of Fructus Tsaokos, 13 parts of Fructus Phyllanthis, 12 parts of Fructus Canarii albis and Herba Menthaes and be cut into segment, be crushed to 110 orders; Medicated powder is poured in pithos and soaked 40 minutes, and adding the water yield is 10 times of medicine gross weight, boils 1.5 hours, when fluid temperature is down to 30 ℃-60 ℃, filters, and obtains extracting solution;
(2) medicinal residues after filtering in step 1 being added to the water yield is 5 times of medicine gross weight, boils 0.5 hour, when fluid temperature is down to 30 ℃-60 ℃, filters, and obtains extracting solution;
(3) extracting solution step 1 and step 2 being obtained mixes, and is condensed into thick paste, adds Pulvis Talci mix homogeneously to make soft material;
(4) soft material is crossed to 18 orders, then dry under 52 ℃ of conditions, gained granule carries out tabletting, makes Traditional Chinese medicine lozenge.
Embodiment 4:
(1) get by weight 5 parts of 30 parts of dry Fructus Chaenomeliss, 20 parts of Pericarpium Citri Reticulataes, 10 parts of Fructus Tsaokos, 10 parts of Fructus Phyllanthis, 10 parts of Fructus Canarii albis and Herba Menthaes and be cut into segment, be crushed to 100 orders; Medicated powder is poured in pithos and soaked 40 minutes, and adding the water yield is 10 times of medicine gross weight, boils 1 hour, when fluid temperature is down to 30 ℃-60 ℃, filters, and obtains extracting solution;
(2) medicinal residues after filtering in step 1 being added to the water yield is 5 times of medicine gross weight, boils 0.5 hour, when fluid temperature is down to 30 ℃-60 ℃, filters, and obtains extracting solution;
(3) extracting solution step 1 and step 2 being obtained mixes, and is condensed into thick paste, adds hydride vegetable oil and Polyethylene Glycol mix homogeneously to make soft material;
(4) soft material is crossed to 18 orders, then dry under 50 ℃ of conditions, gained granule carries out tabletting, makes Traditional Chinese medicine lozenge.
clinical therapeutic efficacy:
For show medicine of the present invention to dyspepsia, flatulence gastric acid, vomit and rush down therapeutic effect, carried out following clinical experiment, since 2012, treat altogether dyspepsia patient 187 examples, cure and reach 168 person-times, transfer well 13 person-times to, invalid is 6 people, and cure rate can reach 89.8%, and effective percentage can reach 96.8%; Treatment flatulence gastric acid 146 cases, cures and reaches 124 person-times, effectively can reach 18 person-times, and invalid is 4 person-times, and cure rate is 84.9%, and effective percentage can reach 97.2%; 135 person-times for the treatment of nausea and vomiting patients, cure and reach 118 person-times, and effective percentage is 10 person-times, and invalid is 7 person-times, and cure rate is 87.4%, and effective percentage can reach 94.8%; Its total cure rate is 87.6%, and total effective rate is 96.3%.
According to the practice of traditional Chinese medical science pharmacology and clinical treatment, can draw: the Traditional Chinese medicine lozenge that nourishing the stomach disappears is to treatment dyspepsia, weakness of the spleen and stomach, distension and fullness of the chest and abdomen, uncomfortable in chest, the diseases such as vomiting have significant effect, can be widely used in clinical treatment use.
Model case:
Case 1: Zheng, man, 56 years old, people from Nanning, certain Listed Company, because operating pressure is large, add frequent dinner party, diet is irregular, cause often having dyspepsia, the symptom such as gastric acid flatulence occurs, often takes multiple invigorating the stomach and promoting digestion Chinese medicine and also has no and be clearly better, and the state of an illness is outbreak repeatedly easily.Taking buccal tablet of the present invention, three times on the one, one time after four,, digestion is normal, the transference cures such as flatulence stomachache, and later daily taking, the state of an illness is again without recurring.
Case 2: Lee, female, 4 years old, the new village people of Tang in Guigang, Guangxi province, vomiting, what is eaten and all can tell major part, cause malnutrition, become thin, took plurality of Chinese as children's indigestion tablet after, symptom is still not improved.Take Traditional Chinese medicine lozenge of the present invention after 2 days, beginning diet is normal, continues to take 1 week, and appetite increases, and body weight is slowly recovered.
Case 3: Lee, man, 48 years old, Baisha Zhen Shawan, Guigang, Guangxi villager, build in lower Guangdong, and often overtime work causes diet irregular, adds the normal time and is engaged in high strength physical work, and health often occurs that stomach rises, gastric acid, appetite are poor.Through taking the present invention's stagnant buccal tablet that helps digestion, every day three times, each 4, after 5 days, flatulence gastric acid transference cure, appetite improves.
Case 4: Tang so-and-so, man, 16 years old, Guangxi college student, due to the health that is not careful in one's diet at ordinary times, often ate roadside stands and barbecue, causes health often to be suffered from diarrhoea, the symptoms such as vomiting.Take the present invention and help digestion stagnant buccal tablet after 1 day, diarrhoea, symptoms of emesis is alleviated to some extent, continues to take after 3 days, diarrhoea, symptoms of emesis disappears.
Case 5: deep so-and-so, man, 33 years old, Guigang, Guangxi celebrating Fengzhen Dendrobium denneanum Kerr. ridge people from village, is engaged in truck man in Nanning City, because the three meals in a day of driving at ordinary times can not be taken food on time, add out that long-distance truck need be seated for a long time, cause the symptoms such as frequent dyspepsia, stomachache, appetite be poor.Through taking the present invention, help digestion stagnant buccal tablet after 3 days, digestion is normal, takes after one week stomachache transference cure.
Case 6: Wu so-and-so, man, 45 years old, Guigang, Guangxi, is engaged in building materials business, due to working principle, need often dinner party client, eating and drinking too much at one meal, smokes and drink, cause often feeling dyspepsia, abdominal distention, constipation and the symptom such as weak, through taking the present invention, help digestion stagnant buccal tablet after 5 days, digestion is normal, abdominal distention, constipation and the transference cure such as weak.
Claims (4)
1. the stagnant buccal tablet that helps digestion, is made by the raw material of following parts by weight: Fructus Chaenomelis 30-50 part, Pericarpium Citri Reticulatae 20-30 part, Fructus Tsaoko 10-15 part, Fructus Phyllanthi 10-15 part, Fructus Canarii albi 10-15 part, Herba Menthae 5-8 part.
2. the stagnant buccal tablet that helps digestion according to claim 1, is characterized in that: the raw material by following parts by weight is made: Fructus Chaenomelis 40-45 part, Pericarpium Citri Reticulatae 25-30 part, Fructus Tsaoko 12-15 part, Fructus Phyllanthi 12-15 part, Fructus Canarii albi 12-15 part, Herba Menthae 6-8 part.
3. the help digestion preparation method of stagnant buccal tablet, is characterized in that:
(1) by weight dry Fructus Chaenomelis, Pericarpium Citri Reticulatae, Fructus Tsaoko, Fructus Phyllanthi, Fructus Canarii albi and Herba Menthae powder are broken into 100-120 object fine powder; Medicated powder is poured in pithos and is soaked 40 minutes, add the water yield be medicine gross weight 8-10 doubly, boil 1-2 hour, when fluid temperature is down to 30 ℃-60 ℃, filter, obtain extracting solution;
(2) medicinal residues after filtering in step 1 are added the water yield be medicine gross weight 3-5 doubly, boil 0.5-1 hour, when fluid temperature is down to 30 ℃-60 ℃, filter, obtain extracting solution;
(3) extracting solution step 1 and step 2 being obtained mixes, and is condensed into thick paste, adds wet and slippery dose of mix homogeneously to make soft material;
(4) soft material is crossed to 18 orders, then dry under 50-60 ℃ of condition, gained granule carries out tabletting, makes Traditional Chinese medicine lozenge.
4. the preparation method of the stagnant buccal tablet that helps digestion according to claim 3, is characterized in that: described wet and slippery dose is one or more in stearate, Pulvis Talci, hydride vegetable oil, Polyethylene Glycol.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105533534A (en) * | 2015-12-16 | 2016-05-04 | 广西宏美农业科技有限公司 | Papaya-tea chewable tablet and preparation method thereof |
| CN105558062A (en) * | 2015-12-16 | 2016-05-11 | 广西宏美农业科技有限公司 | Pawpaw and milk chewable tablets and preparation method thereof |
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2014
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| 《中华茶饮养生大全》编写组编: "《中华茶饮养生大全》", 31 July 2009, 广东世界图书出版公司 * |
| 周建龙: "止呕中药简介", 《现代中医药》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105533534A (en) * | 2015-12-16 | 2016-05-04 | 广西宏美农业科技有限公司 | Papaya-tea chewable tablet and preparation method thereof |
| CN105558062A (en) * | 2015-12-16 | 2016-05-11 | 广西宏美农业科技有限公司 | Pawpaw and milk chewable tablets and preparation method thereof |
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