CN104026145B - A kind of composite insecticide - Google Patents
A kind of composite insecticide Download PDFInfo
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- CN104026145B CN104026145B CN201410304952.2A CN201410304952A CN104026145B CN 104026145 B CN104026145 B CN 104026145B CN 201410304952 A CN201410304952 A CN 201410304952A CN 104026145 B CN104026145 B CN 104026145B
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- 239000002917 insecticide Substances 0.000 title claims abstract description 25
- 239000002131 composite material Substances 0.000 title claims abstract description 18
- 239000004615 ingredient Substances 0.000 claims abstract description 27
- 239000000203 mixture Substances 0.000 claims abstract description 27
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical group OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 21
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000013530 defoamer Substances 0.000 claims abstract description 19
- 239000002270 dispersing agent Substances 0.000 claims abstract description 19
- 239000002562 thickening agent Substances 0.000 claims abstract description 19
- 239000000080 wetting agent Substances 0.000 claims abstract description 19
- ZSBXGIUJOOQZMP-UHFFFAOYSA-N Isomatrine Natural products C1CCC2CN3C(=O)CCCC3C3C2N1CCC3 ZSBXGIUJOOQZMP-UHFFFAOYSA-N 0.000 claims abstract description 15
- ZSBXGIUJOOQZMP-JLNYLFASSA-N Matrine Chemical compound C1CC[C@H]2CN3C(=O)CCC[C@@H]3[C@@H]3[C@H]2N1CCC3 ZSBXGIUJOOQZMP-JLNYLFASSA-N 0.000 claims abstract description 14
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical group [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 14
- 229930014456 matrine Natural products 0.000 claims abstract description 14
- BUHNCQOJJZAOMJ-UHFFFAOYSA-N ZXI 8901 Chemical compound C=1C=C(OC(F)F)C=CC=1C(C(C)C)C(=O)OC(C#N)C(C=1)=CC=CC=1OC1=CC=C(Br)C=C1 BUHNCQOJJZAOMJ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229930192734 Avilamycin Natural products 0.000 claims abstract description 12
- 239000004190 Avilamycin Substances 0.000 claims abstract description 12
- 239000005906 Imidacloprid Substances 0.000 claims abstract description 12
- XIRGHRXBGGPPKY-OTPQUNEMSA-N [(2r,3s,4r,6s)-6-[(2'r,3's,3ar,4r,4'r,6s,7ar)-6-[(2s,3r,4r,5s,6r)-2-[(2r,3s,4s,5s,6s)-6-[(2r,3as,3'ar,6'r,7r,7's,7ar,7'ar)-7'-acetyl-7'-hydroxy-6'-methyl-7-(2-methylpropanoyloxy)spiro[4,6,7,7a-tetrahydro-3ah-[1,3]dioxolo[4,5-c]pyran-2,4'-6,7a-dihydro-3ah- Chemical compound O([C@H]1[C@H](O)C[C@@H](O[C@@H]1C)O[C@H]1[C@H](O)CC2(O[C@]3(C)C[C@@H](O[C@H](C)[C@H]3O2)O[C@H]2[C@@H](OC)[C@@H](C)O[C@H]([C@@H]2O)O[C@H]2[C@H](O)[C@H](OC)[C@H](OC3[C@@H]([C@@H]4O[C@]5(O[C@H]4CO3)[C@@H]3OCO[C@H]3[C@@](O)([C@@H](C)O5)C(C)=O)OC(=O)C(C)C)O[C@@H]2COC)O[C@@H]1C)C(=O)C1=C(C)C(Cl)=C(O)C(Cl)=C1OC XIRGHRXBGGPPKY-OTPQUNEMSA-N 0.000 claims abstract description 12
- 229960005185 avilamycin Drugs 0.000 claims abstract description 12
- 235000019379 avilamycin Nutrition 0.000 claims abstract description 12
- YWTYJOPNNQFBPC-UHFFFAOYSA-N imidacloprid Chemical compound [O-][N+](=O)\N=C1/NCCN1CC1=CC=C(Cl)N=C1 YWTYJOPNNQFBPC-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229940056881 imidacloprid Drugs 0.000 claims abstract description 12
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 8
- 239000004141 Sodium laurylsulphate Substances 0.000 claims abstract description 7
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical group [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 claims abstract description 7
- 229920005646 polycarboxylate Polymers 0.000 claims abstract description 7
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims abstract description 7
- 239000000230 xanthan gum Substances 0.000 claims abstract description 7
- 229920001285 xanthan gum Polymers 0.000 claims abstract description 7
- 229940082509 xanthan gum Drugs 0.000 claims abstract description 7
- 235000010493 xanthan gum Nutrition 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 239000002994 raw material Substances 0.000 claims description 10
- 230000000749 insecticidal effect Effects 0.000 abstract description 4
- 239000000463 material Substances 0.000 abstract description 2
- 239000000575 pesticide Substances 0.000 abstract description 2
- 239000003814 drug Substances 0.000 description 9
- 241000196324 Embryophyta Species 0.000 description 7
- 230000003449 preventive effect Effects 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 239000000375 suspending agent Substances 0.000 description 5
- 241000607479 Yersinia pestis Species 0.000 description 4
- 241001465754 Metazoa Species 0.000 description 3
- 229930013930 alkaloid Natural products 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 3
- 210000000582 semen Anatomy 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 2
- 206010059866 Drug resistance Diseases 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 241000238631 Hexapoda Species 0.000 description 2
- 235000013339 cereals Nutrition 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000001804 emulsifying effect Effects 0.000 description 2
- ZSBXGIUJOOQZMP-BHPKHCPMSA-N sophoridine Chemical compound C1CC[C@@H]2CN3C(=O)CCC[C@@H]3[C@@H]3[C@H]2N1CCC3 ZSBXGIUJOOQZMP-BHPKHCPMSA-N 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 210000002784 stomach Anatomy 0.000 description 2
- 231100000419 toxicity Toxicity 0.000 description 2
- 230000001988 toxicity Effects 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- XVPBINOPNYFXID-JARXUMMXSA-N 85u4c366qs Chemical compound C([C@@H]1CCC[N@+]2(CCC[C@H]3[C@@H]21)[O-])N1[C@@H]3CCCC1=O XVPBINOPNYFXID-JARXUMMXSA-N 0.000 description 1
- 240000001592 Amaranthus caudatus Species 0.000 description 1
- 235000009328 Amaranthus caudatus Nutrition 0.000 description 1
- 235000005637 Brassica campestris Nutrition 0.000 description 1
- 241001301148 Brassica rapa subsp. oleifera Species 0.000 description 1
- 244000052707 Camellia sinensis Species 0.000 description 1
- 244000052363 Cynodon dactylon Species 0.000 description 1
- 244000058871 Echinochloa crus-galli Species 0.000 description 1
- 235000007351 Eleusine Nutrition 0.000 description 1
- 241000209215 Eleusine Species 0.000 description 1
- 241000258937 Hemiptera Species 0.000 description 1
- 241000255777 Lepidoptera Species 0.000 description 1
- 241000238814 Orthoptera Species 0.000 description 1
- 206010033799 Paralysis Diseases 0.000 description 1
- 241000125167 Rhopalosiphum padi Species 0.000 description 1
- AAGFPTSOPGCENQ-UHFFFAOYSA-N Sophocarpin I Natural products C1CCC2CN3C(=O)C=CCC3C3C2N1CCC3 AAGFPTSOPGCENQ-UHFFFAOYSA-N 0.000 description 1
- IGXQFUGORDJEST-UHFFFAOYSA-N Sophocarpine Natural products O=C1C=CCC2C3CCCC4CCCC(CN12)C34 IGXQFUGORDJEST-UHFFFAOYSA-N 0.000 description 1
- 241001468227 Streptomyces avermitilis Species 0.000 description 1
- 241001655322 Streptomycetales Species 0.000 description 1
- 235000006468 Thea sinensis Nutrition 0.000 description 1
- 150000003797 alkaloid derivatives Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- -1 lactone compounds Chemical class 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- QMGGMESMCJCABO-UHFFFAOYSA-N n-oxysophocarpine Chemical compound C12C3CCC[N+]2([O-])CCCC1CN1C3CC=CC1=O QMGGMESMCJCABO-UHFFFAOYSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229930015582 oxymatrine Natural products 0.000 description 1
- 244000045947 parasite Species 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002728 pyrethroid Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- AAGFPTSOPGCENQ-JLNYLFASSA-N sophocarpine Chemical compound C1CC[C@H]2CN3C(=O)C=CC[C@@H]3[C@@H]3[C@H]2N1CCC3 AAGFPTSOPGCENQ-JLNYLFASSA-N 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of composite insecticide, belong to technical field of pesticide.Including effective ingredient and auxiliary agent, described auxiliary agent is wetting agent, dispersant, thickening agent and defoamer, and described effective ingredient includes following components: brofluthrinate, avilamycin, matrine and imidacloprid.Described wetting agent is sodium lauryl sulphate, the mixture of dodecyl sodium sulfate weight ratio 1:1:1；Described dispersant is sodium lignin sulfonate and the mixture of polycarboxylate weight ratio 1:1；Described thickening agent is xanthan gum；Described defoamer is ethylene glycol and the mixture of propylene glycol 1:1 by weight.Above-mentioned several insecticidal materials are compounded by the present invention in proportion, the problem that on the one hand can solve to be easily generated resistance when being used alone, on the one hand, can increase again the insecticidal properties of composite insecticide.
Description
Technical field
The present invention relates to a kind of composite insecticide, belong to technical field of pesticide.
Background technology
Brofluthrinate has tags and stomach poison function, it it is efficient, wide spectrum, a pyrethroid insecticides for longevity of residure length, brofluthrinate can be used for various pests and the demodicid mite classes such as Cotton Gossypii, fruit tree, vegetable, Camellia sinensis, cereal crops, preventing and treating Lepidoptera, Semiptera, Homoptera, Orthoptera.Avilamycin is the ten hexa-atomic Macrocyclic lactone compounds that the class first developed by Japan's North university big village intelligence etc. and Merck company of the U.S. has parasite killing, mite killing, eelworm-killing activity, Avid kyowamycin Streptomyces avermitilis fermentation in streptomycete produce.Matrine is made up through organic solvent extraction such as ethanol of the dry root of leguminous plant Radix Sophorae Flavescentis, plant, fruit, is alkaloid.Generally Radix Sophorae Flavescentis total alkaloids, its main component has the multiple alkaloids such as matrine, sophocarpine, N-oxysophocarpine, sophoridine, the highest with matrine, oxymatrine concentration.Other sources are Radix Sophorae Tonkinensis and Radix Sophorae Tonkinensis aerial parts, and sterling outward appearance is white powder.Imidacloprid is nicotinoids ultra high efficiency insecticide, have wide spectrum, efficiently, low toxicity, low-residual, insect is not likely to produce resistance, to features such as people, animal, plant and natural enemies securities, and have tag, the multiple action such as stomach toxicity and interior suction.After contacting pests medicament, nervus centralis normal conduction is obstructed so that it is paralysis death.Product quick-acting is good, within after medicine 1 day, i.e. has higher preventive effect, and residual period is up to about 25 days.Drug effect and temperature are proportionate, and temperature is high, good disinsection effect.It is mainly used in preventing and treating sucking pest.Annual gramineous weed and the perennial grassy weeds such as Bermuda grass, Herba Imperatae such as Herba Digitariae, amur foxtail, Herba Eleusines Indicae, barnyard grass, Herba Setariae Viridis, Semen Euphorbiae is prevented and kill off for the multiple broad leaf crop such as Semen sojae atricolor, Cotton Gossypii, Semen arachidis hypogaeae, Brassica campestris L, nursery, Caulis et Folium Lini, invalid to broadleaved herb and dried tuber.Plant is due to life-time service chemical insecticide, the drug resistance of worm is more and more stronger, in addition to developing new insecticide, will escalated dose in order to kill insect pest, use the plant fruit of this insecticide, vegetable and grain that human and animal all can produce toxicity, the growth of infringement animal and the health of the mankind.Accordingly, it would be desirable to develop a kind of medicine, the resistance problem that above-mentioned several drugs is used alone can be solved.
Summary of the invention
Instant invention overcomes the deficiencies in the prior art, it is provided that a kind of composite insecticide.
Technical scheme is as follows:
A kind of composite insecticide, is characterized in that, including effective ingredient and auxiliary agent,
Described effective ingredient includes following components: brofluthrinate, avilamycin, matrine and imidacloprid.
Preferably, described effective ingredient is brofluthrinate, avilamycin, matrine and the imidacloprid mixture by weight 1:1:1:1.
Preferably, it is made up of the raw material of following weight portion: effective ingredient 10-40 part, wetting agent 2-5 part, dispersant 2-5 part, thickening agent 0.2-0.5 part, defoamer 0.1-0.3 part, water 30-70 part.
Preferably, it is made up of the raw material of following weight portion: effective ingredient 15-30 part, wetting agent 3-4 part, dispersant 3-4 part, thickening agent 0.3-0.4 part, defoamer 0.2 part, water 40-60 part.
Preferably, it is made up of the raw material of following weight portion: effective ingredient 30 parts, wetting agent 4 parts, dispersant 4 parts, thickening agent 0.4 part, defoamer 0.2 part, 60 parts of water.
Preferably, described wetting agent is sodium lauryl sulphate, the mixture of dodecyl sodium sulfate weight ratio 1:1；
Described dispersant is sodium lignin sulfonate and the mixture of polycarboxylate weight ratio 1:1；
Described thickening agent is xanthan gum；
Described defoamer is ethylene glycol and the mixture of propylene glycol 1:1 by weight.
The present invention compared with prior art, has a following outstanding feature:
Brofluthrinate, avilamycin, matrine and imidacloprid are existing conventional insecticide, but, on crop during application, due to life-time service chemical insecticide, the drug resistance of worm is increasingly stronger, and above-mentioned several insecticidal materials are compounded by the present invention in proportion, the problem that on the one hand can solve to be easily generated resistance when being used alone, on the one hand, the insecticidal properties of composite insecticide can be increased again.
Detailed description of the invention
The present invention is only described further by embodiment, but is not limited only to this, and those skilled in the art obtains other embodiments on the premise of not paying creative work, belongs to the scope of protection of the invention.
Embodiment 1
A kind of composite insecticide, including effective ingredient and auxiliary agent, is made up of the raw material of following weight portion: effective ingredient 30 parts, wetting agent 4 parts, dispersant 4 parts, thickening agent 0.4 part, defoamer 0.2 part, 60 parts of water.Described effective ingredient is brofluthrinate, avilamycin, matrine and the imidacloprid mixture by weight 1:1:1:1.Described wetting agent is sodium lauryl sulphate, the mixture of dodecyl sodium sulfate weight ratio 1:1；Described dispersant is sodium lignin sulfonate and the mixture of polycarboxylate weight ratio 1:1；Described thickening agent is xanthan gum；Described defoamer is ethylene glycol and the mixture of propylene glycol 1:1 by weight.
Effective ingredient, wetting agent, dispersant, thickening agent, defoamer, water etc. conventionally (are added grinder to grind, be subsequently adding territory emulsifying kettle emulsifying, obtain suspending agent) by above-mentioned substance makes suspending agent.
This embodiment is used for preventing and treating wheat aphid, and the composite insecticide 3000 of the present embodiment is watered dilution spraying again, and after medicine, the preventive effect of 7 days and 15 days is respectively 92.6% and 97.9%.And the preventive effect of 7 days and 15 days is respectively 73.8% and 80.9% after the imidacloprid medicine of same concentration；After the brofluthrinate medicine of same concentration, the preventive effect of 7 days and 15 days is respectively 69.8% and 76.9%；After the avilamycin medicine of same concentration, the preventive effect of 7 days and 15 days is respectively 74.2% and 81.3%；After the matrine medicine of same concentration, the preventive effect of 7 days and 15 days is respectively 64.1% and 72.2%.
Embodiment 2
A kind of composite insecticide, including effective ingredient and auxiliary agent, is made up of the raw material of following weight portion: effective ingredient 20 parts, wetting agent 3 parts, dispersant 3 parts, thickening agent 0.3 part, defoamer 0.3 part, 70 parts of water.Described effective ingredient is brofluthrinate, avilamycin, matrine and the imidacloprid mixture by weight 1:1:1:1.Described wetting agent is sodium lauryl sulphate, the mixture of dodecyl sodium sulfate weight ratio 1:1；Described dispersant is sodium lignin sulfonate and the mixture of polycarboxylate weight ratio 1:1；Described thickening agent is xanthan gum；Described defoamer is ethylene glycol and the mixture of propylene glycol 1:1 by weight.
Above-mentioned substance conventionally makes suspending agent, it is possible to embodiment 1.
Embodiment 3
A kind of composite insecticide, including effective ingredient and auxiliary agent, is made up of the raw material of following weight portion: effective ingredient 25 parts, wetting agent 4 parts, dispersant 4 parts, thickening agent 0.4 part, defoamer 0.2 part, 70 parts of water.Described effective ingredient is brofluthrinate, avilamycin, matrine and the imidacloprid mixture by weight 1:1:1:1.Described wetting agent is sodium lauryl sulphate, the mixture of dodecyl sodium sulfate weight ratio 1:1；Described dispersant is sodium lignin sulfonate and the mixture of polycarboxylate weight ratio 1:1；Described thickening agent is xanthan gum；Described defoamer is ethylene glycol and the mixture of propylene glycol 1:1 by weight.
Above-mentioned substance conventionally makes suspending agent, it is possible to embodiment 1.
Embodiment 4
A kind of composite insecticide, including effective ingredient and auxiliary agent, is made up of the raw material of following weight portion: effective ingredient 15 parts, wetting agent 2.5 parts, dispersant 2.5 parts, thickening agent 0.25 part, defoamer 0.25 part, 60 parts of water.Described effective ingredient is brofluthrinate, avilamycin, matrine and the imidacloprid mixture by weight 1:1:1:1.Described wetting agent is sodium lauryl sulphate, the mixture of dodecyl sodium sulfate weight ratio 1:1；Described dispersant is sodium lignin sulfonate and the mixture of polycarboxylate weight ratio 1:1；Described thickening agent is xanthan gum；Described defoamer is ethylene glycol and the mixture of propylene glycol 1:1 by weight.
Above-mentioned substance conventionally makes suspending agent, it is possible to embodiment 1.
Claims (5)
1. a composite insecticide, is characterized in that, including effective ingredient and auxiliary agent,
Described effective ingredient includes following components: brofluthrinate, avilamycin, matrine and imidacloprid；Institute
Stating effective ingredient is that brofluthrinate, avilamycin, matrine and imidacloprid are by weight 1:1:1:1
Mixture.
Composite insecticide the most according to claim 1, is characterized in that, by the raw material system of following weight portion
Become: effective ingredient 10-40 part, wetting agent 2-5 part, dispersant 2-5 part, thickening agent 0.2-0.5 part, defoamer 0.1-0.3
Part, water 30-70 part.
Composite insecticide the most according to claim 2, is characterized in that, by the raw material system of following weight portion
Become: effective ingredient 15-30 part, wetting agent 3-4 part, dispersant 3-4 part, thickening agent 0.3-0.4 part, defoamer 0.2
Part, water 40-60 part.
Composite insecticide the most according to claim 3, is characterized in that, by the raw material system of following weight portion
Become: effective ingredient 30 parts, wetting agent 4 parts, dispersant 4 parts, thickening agent 0.4 part, defoamer 0.2 part, water 60
Part.
5., according to the arbitrary described composite insecticide of claim 2-4, it is characterized in that,
Described wetting agent is sodium lauryl sulphate, the mixture of dodecyl sodium sulfate weight ratio 1:1；
Described dispersant is sodium lignin sulfonate and the mixture of polycarboxylate weight ratio 1:1；
Described thickening agent is xanthan gum；
Described defoamer is ethylene glycol and the mixture of propylene glycol 1:1 by weight.
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| CN201410304952.2A CN104026145B (en) | 2014-06-30 | 2014-06-30 | A kind of composite insecticide |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410304952.2A CN104026145B (en) | 2014-06-30 | 2014-06-30 | A kind of composite insecticide |
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| CN104026145A CN104026145A (en) | 2014-09-10 |
| CN104026145B true CN104026145B (en) | 2016-09-28 |
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| CN104351220B (en) * | 2014-11-14 | 2016-04-13 | 济南新起点医药科技有限公司 | A kind of composition and application containing brofluthrinate |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1437846A (en) * | 2002-11-29 | 2003-08-27 | 金中北 | Aqueous farm chemical with various insecticidal activity |
| CN1792153A (en) * | 2005-12-21 | 2006-06-28 | 金中北 | Mineral oil micro-emulsion insecticide |
| CN1839695A (en) * | 2005-03-28 | 2006-10-04 | 北京华京五方实用纳米科技开发有限公司 | Aqueous pesticide and preparation method thereof |
| CN101243791A (en) * | 2008-03-20 | 2008-08-20 | 宁波中北生物科技发展股份有限公司 | Ricinus oil groups insecticide |
-
2014
- 2014-06-30 CN CN201410304952.2A patent/CN104026145B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1437846A (en) * | 2002-11-29 | 2003-08-27 | 金中北 | Aqueous farm chemical with various insecticidal activity |
| CN1839695A (en) * | 2005-03-28 | 2006-10-04 | 北京华京五方实用纳米科技开发有限公司 | Aqueous pesticide and preparation method thereof |
| CN1792153A (en) * | 2005-12-21 | 2006-06-28 | 金中北 | Mineral oil micro-emulsion insecticide |
| CN101243791A (en) * | 2008-03-20 | 2008-08-20 | 宁波中北生物科技发展股份有限公司 | Ricinus oil groups insecticide |
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