CN104004588B - A kind of method of comprehensive utilization of peppermint - Google Patents

A kind of method of comprehensive utilization of peppermint Download PDF

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Publication number
CN104004588B
CN104004588B CN201410251521.4A CN201410251521A CN104004588B CN 104004588 B CN104004588 B CN 104004588B CN 201410251521 A CN201410251521 A CN 201410251521A CN 104004588 B CN104004588 B CN 104004588B
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peppermint
essential oil
comprehensive utilization
residue
distilled water
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CN104004588A (en
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赵忠娟
魏艳丽
李纪顺
杨合同
李哲
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ECOLOGY INSTITUTE OF SHANDONG ACADEMY OF SCIENCES (THE SINO-JAPANESE FRIENDSHIP BIOTECHNOLOGY RESEARCH CENTER, SHANDONG ACADEMY OF SCIENCES)
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/10Biofuels, e.g. bio-diesel
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/30Fuel from waste, e.g. synthetic alcohol or diesel
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P60/00Technologies relating to agriculture, livestock or agroalimentary industries
    • Y02P60/80Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
    • Y02P60/87Re-use of by-products of food processing for fodder production

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  • Cosmetics (AREA)
  • Fats And Perfumes (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The invention discloses a kind of method of comprehensive utilization of peppermint.Relate to the integrated application of Peppermint essential oil in peppermint, water soluble component, non-volatile component and extraction of essential oil residue.Present method can utilize Peppermint essential oil, peppermint distilled water and the composition such as peppermint water vat liquor and peppermint residue simultaneously, realize production process to produce without waste, significantly improve the comprehensive utilization value of peppermint, for the utilization of peppermint water-soluble components and residue provides new way.

Description

A kind of method of comprehensive utilization of peppermint
Technical field
The present invention relates to the method for comprehensive utilization of a kind of plant, be specifically related to a kind of method of comprehensive utilization of peppermint, relate to the integrated application of Peppermint essential oil in peppermint, water soluble component, non-volatile component and extraction of essential oil residue.
Background technology
Peppermint is Labiatae Mentha per nnial herb, calls European peppermint, Mentha arvensis L. syn.M.haplocalyxBrig, black peppermint, originates in the U.S., and 20th century of China introduce.Peppermint is natural perfume, and leading product are Peppermint essential oil, is widely used in food, makeup and medicine trade.Main in peppermint essential oil about have 230 compounds containing piperitone, menthol, menthyl acetate etc., the content of most compound is very micro-, wherein topmost effective constituent is menthol, and it is the one of lopps monoterpene, plays a leading role to the quality of Peppermint essential oil and aroma quality.
In peppermint except volatile Peppermint essential oil, also containing the abundant main component such as carbohydrate, lipid, protein and a large amount of nonvolatile phenolic compound, amino acid, trace element etc.Phenolic compound refers to the compound generated after the hydrogen atom on aromatic ring is replaced by hydroxyl or functional deriv, the phenols in peppermint mainly flavones, anthraquinone and organic acid.Containing than more rich amino acid in peppermint, mainly comprise glycine, aspartic acid, α-amino-isovaleric acid, methionine(Met), L-glutamic acid, Serine, Threonine, Methionin, L-Ala, aspartic acid, leucine, Isoleucine, phenylalanine, tyrosine, Histidine and arginine totally 16 kinds.That the trace element in peppermint has detected is Al, B, Ba, Ca, Cu, Fe, K, Mg, Mn, Na, Ni, P, Pb, Sr, V, Zn etc. 16 kinds.These non-volatile substances have the antitumor and oxidation resistant effect of hepatic cholagogic.Also containing the acidic polysaccharose material that a class and protein be combined with each other in peppermint, there is hypoglycemic, hypotensive, enhancing body immunizing power, anti-inflammatory, the multiple efficacies such as anticancer.In common process, all the other materials extracted after Peppermint essential oil abandon as waste, in peppermint, a large amount of carbohydrate, protein, lipid, aldehydes matter, amino acid, trace element are not fully used, therefore to the utilization of composition various in peppermint, improving the comprehensive utilization ratio of peppermint, is a major issue needing to solve.
Summary of the invention
Object of the present invention is exactly defect for above-mentioned existence and provides a kind of method of comprehensive utilization of peppermint.Relate to the integrated application of Peppermint essential oil in peppermint, water soluble component, non-volatile component and extraction of essential oil residue.
The method of comprehensive utilization technical scheme of a kind of peppermint of the present invention is comprise the following steps:
(1) Peppermint essential oil in extraction by steam distillation peppermint is utilized;
(2) distilled water formed after collecting water vapor condensation while collecting Peppermint essential oil; Containing the Peppermint essential oil of about 0.01% and other water-soluble volatile components in the peppermint distilled water collected.
(3) the peppermint distilled water of collection is added the mint beverage that auxiliary material is processed into the cooling of energy relieving summer-heat;
(4) the peppermint distilled water of collection is mixed with toner; There is skin care, anti-oxidant and eliminate blackhead and be of value to the effect of oiliness skin quality.
(5) the peppermint water vat liquor of collection is mixed with foot-soaking liquid; There is antiperspirant, sterilization, smelly effect of dispelling, being applicable to pin has peculiar smell and suffers from the crowd of beriberi.
(6) using the additive of peppermint residue as domestic animal, poultry feed; The growth of domestic animal, poultry can be promoted, strengthen carcass immunizing power.
(7) peppermint residue is made into briquette-fuel, replace coal as the fuel of coal firing boiler, the remaining ash content that burns can reclaim as potash fertilizer; Achieve the Efficient Cycle of " peppermint residue-fuel-fertilizer ".
Step (1) is specially: the peppermint of gathering is dried, pulverized, and puts in volatile oil extractor, and add water distillation, and after extracting 2h, collect Peppermint essential oil, the extraction yield of Peppermint essential oil is 96.12% after measured.
Step (3) is specially: pump in carbonated-water generator according to the ratio of 90.8:9.0:0.2 respectively by peppermint distilled water, white sugar and citric acid, cool after carrying out quantitatively mixing, add after carbonic acid gas makes mixture carbonating and load container, be produced into the peppermint drinks of energy relieving summer-heat cooling.This mint beverage has the refrigerant of peppermint, has good stimulating effect, containing Peppermint essential oil have anti-to cure cold, clearing heat and detoxicating effect, again containing carbonic acid gas, there is the taste of popular " cola ".
Step (4) is specially: collect peppermint distilled water, be then by weight: peppermint distilled water 69.8%, EDTA-Na20.10%, wallantoin 0.20%, glycerine 15.0%, propylene glycol 3.50%, 1,3 butylene glycol 8.0%, amino acid humectant 3.40 prepares toner.The toner of preparation has skin care, anti-oxidant and eliminate blackhead and be of value to the effect of oiliness skin quality.
In step (4), the preparation steps of toner is:
1. the material except amino acid humectant is mixed in proportion, stirs and be heated to 85 ~ 90 DEG C;
2. within 20 minutes, with sterilizing, then slow cooling, adds amino acid humectant to temperature lower than when 60 DEG C, stirs in standing insulation;
3. packing after cooling.
Step (5) is specially: after Peppermint essential oil is extracted and terminated, pulp water mixed solution in container is filtered, collect peppermint vat liquor, add a small amount of antioperspirant, tensio-active agent, skin conditioning agent and sanitas etc., be mixed with foot-soaking liquid, each composition is by weight as follows: H2O73.5%, peppermint water vat liquor 15.0%, phenol p-sulfonic acid zinc 4.0%, propylene glycol 3.5%, aliphatic acid polyethenoxy ether sodium sulfate 2.5%, thickening material 1.5%.This foot-soaking liquid is by natural plant extracts and compounded a kind of thick liquid such as antioperspirant and tensio-active agent, directly adds 45 DEG C of warm bubbly water pin, need not rinse in addition when foot bath.Both there is antiperspirant, sterilization, smelly effect of dispelling, can also prevention and therapy beriberi, be applicable to the crowd that pin has peculiar smell and suffers from beriberi.
Step (6) is specially: dried by the peppermint residue after filtering, pulverize, add in feed preparation as additive, after at least one mixing in same corn, dregs of beans, rice bran, wheat bran, produces cattle food.
Step (7) is specially: after being dried by peppermint residue, pulverizes, utilizes stalk block making machine to be pressed into solid fuel, the briquette-fuel density be pressed into: 700-1400 kilograms per cubic meter; Ash content: 1-20%; Moisture≤15%, calorific value is 3000-5000 kilocalorie.
The invention provides the peppermint method of comprehensive utilization of Saline-alkaline Soils of Yellow River Delta district plantation, present method can utilize Peppermint essential oil, peppermint distilled water and the composition such as peppermint water vat liquor and peppermint residue simultaneously, realize production process to produce without waste, significantly improve the comprehensive utilization value of peppermint, for the utilization of peppermint water-soluble components and residue provides new way.
embodiment:
In order to understand the present invention better, describe technical scheme of the present invention in detail with specific examples below, but the present invention is not limited thereto.
" No. 1, institute of section " peppermint new variety that following examples peppermint used is Shandong Province academy sciences Biology Research Institute screening and cultivates, this kind can tolerate the salt stress of 0.8%, the Delta Region of The Yellow River growth conditions higher in soil salinization degree is good, and Peppermint essential oil content is higher.After measured in its cured leaf oleaginousness 4.7% of peppermint of Delta Region of The Yellow River growth.
Embodiment 1
(1) the present invention utilizes the Peppermint essential oil in extraction by steam distillation peppermint, and the peppermint of gathering is dried, pulverized, and puts in volatile oil extractor, and add water distillation, and after extracting 2h, collect Peppermint essential oil, the extraction yield of Peppermint essential oil is 96.12% after measured.
(2) peppermint distilled water is collected while collecting Peppermint essential oil, peppermint distilled water, white sugar and citric acid are pumped in carbonated-water generator according to the ratio of 90.8:9.0:0.2 respectively, cool after carrying out quantitatively mixing, add after carbonic acid gas makes mixture carbonating and load container, be produced into the peppermint drinks of a kind of energy relieving summer-heat cooling.This mint beverage has the refrigerant of peppermint, has good stimulating effect, containing Peppermint essential oil have anti-to cure cold, clearing heat and detoxicating effect, again containing carbonic acid gas, there is the taste of popular " cola ".Its Production Flow Chart is as follows:
Peppermint distilled water-add white sugar and citric acid mixing-cooling-carbonating-filling-sealing-inspection-finished beverage-container-cleaning-inspection.
(3), after peppermint residue being dried, pulverize according to briquetting press mould pore size, utilize stalk block making machine to be pressed into solid fuel.The briquette-fuel density be pressed into: 700-1400 kilograms per cubic meter; Ash content: 1-20%; Moisture≤15%, calorific value is about 3000-5000 kilocalorie.
Embodiment 2
(1) the present invention utilizes the Peppermint essential oil in extraction by steam distillation peppermint, and the peppermint of gathering is dried, pulverized, and puts in volatile oil extractor, and add water distillation, and after extracting 2h, collect Peppermint essential oil, the extraction yield of Peppermint essential oil is 96.12% after measured.
(2) collect peppermint distilled water, then press the toner of formulated shown in table 1, the toner of preparation has skin care, anti-oxidant and eliminate blackhead and be of value to the effect of oiliness skin quality.
Table 1
1. the material except amino acid humectant in formula is mixed in proportion, stirs and be heated to 85 ~ 90 DEG C;
2. within 20 minutes, with sterilizing, then slow cooling, adds amino acid humectant to temperature lower than when 60 DEG C, stirs in standing insulation;
3. packing after cooling.
(3) after Peppermint essential oil is extracted and terminated, the pulp water mixed solution in container is filtered, collect peppermint vat liquor, add a small amount of antioperspirant, tensio-active agent, skin conditioning agent and sanitas etc., be mixed with foot-soaking liquid.Fill a prescription as shown in table 2:
Table 2
This foot-soaking liquid is by natural plant extracts and compounded a kind of thick liquid such as antioperspirant and tensio-active agent, directly adds 45 DEG C of warm bubbly water pin, need not rinse in addition when foot bath.Both there is antiperspirant, sterilization, smelly effect of dispelling, can also prevention and therapy beriberi, be applicable to the crowd that pin has peculiar smell and suffers from beriberi.
(4) by remaining, peppermint residue is dried, pulverize, add as fodder additives in feed preparation, after the raw materials such as same corn, dregs of beans, rice bran, wheat bran mix by a certain percentage, produce cattle food.Production Flow Chart is as follows:
Raw material reception-pulverize-batching and stirring-flow scheme design-granulation-discharging.
More than invention provides peppermint method of comprehensive utilization, Peppermint essential oil, peppermint distilled water and the composition such as peppermint water vat liquor and peppermint residue can be utilized simultaneously, realize production process to produce without waste, significantly improve the comprehensive utilization value of peppermint, for the utilization of peppermint water-soluble components and residue provides new way.

Claims (7)

1. a method of comprehensive utilization for peppermint, is characterized in that, comprises the following steps:
(1) Peppermint essential oil in extraction by steam distillation peppermint is utilized;
(2) distilled water formed after collecting water vapor condensation while collecting Peppermint essential oil;
(3) the peppermint distilled water of collection is added auxiliary material be processed into can relieving summer-heat cooling mint beverage maybe the peppermint distilled water of collection is mixed with toner:
Collect peppermint distilled water, be then by weight: peppermint distilled water 69.8%, EDTA-Na 20.10%, wallantoin 0.20%, glycerine 15.0%, propylene glycol 3.50%, 1,3 butylene glycol 8.0%, amino acid humectant 3.40% prepares toner;
(4) after Peppermint essential oil is extracted and terminated, filtered by the pulp water mixed solution in container, collect peppermint vat liquor, the peppermint vat liquor of collection is mixed with foot-soaking liquid;
(5) using peppermint residue as the additive of domestic animal, poultry feed or peppermint residue is made into briquette-fuel, replace coal as the fuel of coal firing boiler, the remaining ash content that burns reclaims as potash fertilizer.
2. the method for comprehensive utilization of a kind of peppermint according to claim 1, is characterized in that, step (1) is specially: the peppermint of gathering is dried, pulverized, and puts in volatile oil extractor, and add water distillation, after extracting 2h, collects Peppermint essential oil.
3. the method for comprehensive utilization of a kind of peppermint according to claim 1, it is characterized in that, in step (3), the peppermint distilled water of collection is added auxiliary material be processed into can relieving summer-heat cooling mint beverage be specially: peppermint distilled water, white sugar and citric acid are pumped in carbonated-water generator according to the ratio of 90.8:9.0:0.2 respectively, cool after carrying out quantitatively mixing, add after carbonic acid gas makes mixture carbonating and load container, be produced into the mint beverage of energy relieving summer-heat cooling.
4. the method for comprehensive utilization of a kind of peppermint according to claim 1, is characterized in that, in step (3), the preparation steps of toner is:
1. the material except amino acid humectant is mixed in proportion, stirs and be heated to 85 ~ 90 DEG C;
2. within 20 minutes, with sterilizing, then slow cooling, adds amino acid humectant to temperature lower than when 60 DEG C, stirs in standing insulation;
3. packing after cooling.
5. the method for comprehensive utilization of a kind of peppermint according to claim 1, is characterized in that, step (4) is specially: after Peppermint essential oil is extracted and terminated, pulp water mixed solution in container is filtered, collect peppermint vat liquor, be mixed with foot-soaking liquid, each composition is by weight as follows: H 2o73.5%, peppermint vat liquor 15.0%, phenol p-sulfonic acid zinc 4.0%, propylene glycol 3.5%, aliphatic acid polyethenoxy ether sodium sulfate 2.5%, thickening material 1.5%.
6. the method for comprehensive utilization of a kind of peppermint according to claim 1, it is characterized in that, the additive of peppermint residue as domestic animal, poultry feed is specially by step (5): dried remaining by peppermint residue, pulverize, add as fodder additives in feed preparation, after at least one mixing in same corn, dregs of beans, rice bran, wheat bran, produce cattle food.
7. the method for comprehensive utilization of a kind of peppermint according to claim 1, it is characterized in that, peppermint residue is made into briquette-fuel and is specially by step (5): after being dried by peppermint residue, pulverize, stalk block making machine is utilized to be pressed into solid fuel, the briquette-fuel density be pressed into: 700-1400 kilograms per cubic meter; Ash content: 1-20%; Moisture≤15%, calorific value is 3000-5000 kilocalorie.
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CN104560400A (en) * 2014-12-26 2015-04-29 江苏省中国科学院植物研究所 Method for extracting peppermint oil
CN105969527A (en) * 2016-05-23 2016-09-28 铜陵薇吉特生物科技有限公司 Comprehensive utilization method of ginger leaves

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CN1186612A (en) * 1996-12-28 1998-07-08 洛阳春都集团股份有限公司 Peppermint cool tea drink dand producing method
CN100348167C (en) * 2005-11-17 2007-11-14 上海交通大学 Natural aromatic plant distillate type gargle
CN101157880A (en) * 2007-10-11 2008-04-09 上海交通大学 Aromatic plant essential oil ecological processing method
CN102250689A (en) * 2011-05-30 2011-11-23 新疆大学 Equipment and method for extracting perfume plant essential oil by reduced pressure steam distillation

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