CN104003762A - Bone matte glaze and method for manufacturing bone china product by using same - Google Patents
Bone matte glaze and method for manufacturing bone china product by using same Download PDFInfo
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- CN104003762A CN104003762A CN201410263524.XA CN201410263524A CN104003762A CN 104003762 A CN104003762 A CN 104003762A CN 201410263524 A CN201410263524 A CN 201410263524A CN 104003762 A CN104003762 A CN 104003762A
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- 210000000988 bone and bone Anatomy 0.000 title claims abstract description 21
- 238000000034 method Methods 0.000 title claims abstract description 16
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 30
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000011787 zinc oxide Substances 0.000 claims abstract description 15
- 238000010304 firing Methods 0.000 claims abstract description 7
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims abstract description 7
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 7
- 229910021532 Calcite Inorganic materials 0.000 claims abstract description 6
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000004327 boric acid Substances 0.000 claims abstract description 6
- BDAGIHXWWSANSR-NJFSPNSNSA-N hydroxyformaldehyde Chemical compound O[14CH]=O BDAGIHXWWSANSR-NJFSPNSNSA-N 0.000 claims abstract description 6
- 229910000018 strontium carbonate Inorganic materials 0.000 claims abstract description 6
- 239000000454 talc Substances 0.000 claims abstract description 6
- 229910052623 talc Inorganic materials 0.000 claims abstract description 6
- 235000012222 talc Nutrition 0.000 claims abstract description 6
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 claims abstract description 6
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 claims abstract description 3
- -1 6~15 parts Chemical compound 0.000 claims description 17
- 108010048734 sclerotin Proteins 0.000 claims description 13
- 239000002994 raw material Substances 0.000 claims description 11
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 7
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 5
- 230000003647 oxidation Effects 0.000 claims description 5
- 238000007254 oxidation reaction Methods 0.000 claims description 5
- 229910052700 potassium Inorganic materials 0.000 claims description 5
- 239000011591 potassium Substances 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 238000005507 spraying Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000005034 decoration Methods 0.000 abstract description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract description 4
- 239000002253 acid Substances 0.000 abstract description 2
- 229910021538 borax Inorganic materials 0.000 abstract description 2
- 239000004927 clay Substances 0.000 abstract description 2
- 239000010433 feldspar Substances 0.000 abstract description 2
- 239000010453 quartz Substances 0.000 abstract description 2
- 239000004328 sodium tetraborate Substances 0.000 abstract description 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 abstract 1
- 229910052808 lithium carbonate Inorganic materials 0.000 abstract 1
- 229940072033 potash Drugs 0.000 abstract 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 abstract 1
- 235000015320 potassium carbonate Nutrition 0.000 abstract 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 229910052573 porcelain Inorganic materials 0.000 description 9
- 229910052810 boron oxide Inorganic materials 0.000 description 3
- 238000002425 crystallisation Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 3
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000000155 melt Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 239000010456 wollastonite Substances 0.000 description 2
- 229910052882 wollastonite Inorganic materials 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000001506 calcium phosphate Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 239000004579 marble Substances 0.000 description 1
- LGZXYFMMLRYXLK-UHFFFAOYSA-N mercury(2+);sulfide Chemical compound [S-2].[Hg+2] LGZXYFMMLRYXLK-UHFFFAOYSA-N 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
- 229940078499 tricalcium phosphate Drugs 0.000 description 1
- 229910000391 tricalcium phosphate Inorganic materials 0.000 description 1
- 235000019731 tricalcium phosphate Nutrition 0.000 description 1
Abstract
The invention relates to bone matte glaze. The bone matte glaze comprises, by weight, 100 parts of frits, 3-8 parts of clay, 2-12 parts of aedelforsite, 3-6 parts of aluminum oxide, 6-15 parts of zinc oxide and 6 parts of stannic oxide. The frits comprise, by weight, 16-24 parts of quartz, 28-38 parts of potash feldspar, 12-18 parts of borax, 0-7 parts of boric acid, 0-5 parts of strontium carbonate, 0-8 parts of lithium carbonate, 0-10 parts of zinc oxide, 0-3 parts of talcum, 0-12 parts of calcite and 0-0.5 part of zirconium silicate. The glaze surface of a product using the glaze is fine, smooth, resistant to pollution, resistant to acid and alkali, easy to wash and suitable for the decoration means such as decal. The invention further provides a method for manufacturing the bone china product by using the bone matte glaze. The method is simple in firing process, stable in production and good in benefit.
Description
Technical field
A kind of method that the present invention relates to sclerotin matt glaze and make Bone China product of this glaze.
Background technology
Bone China is called for short china, formal name used at school bone china, that to take bone carbon, clay, feldspar and the quartz of animal be main raw material, through high temperature biscuiting and low temperature sinter, fire a kind of porcelain forming for twice, according to the set china standard of Britain, contain more than 30% from the tricalcium phosphate in animal skeleton, and finished product has light transmission, side must become china, and the standard of the U.S. is minimum will reaching more than 25%.
Bone China appearance looks elegant, porcelain exquisiteness is penetrating, and structured shape degree is high, elegant attractive in appearance, and the moist light of glaze can be ornamental strong, and flower face is colourful, and porcelain physical strength is high, and impact resistance is good, can make thin tire product.Bone China begins to originate in Britain, is Britain imperial family and noble's special-purpose porcelain for a long time, is the high-grade porcelain kind of generally acknowledging in the world at present, it has practical and artistic dual value concurrently, being right and status symbol, is also the embodiment of life grade, is known as " king of porcelain ".
Bone China good decorative property, is the natural characteristics that other porcelain cannot be comparable, and high-grade bone china faience is that the trailing that is posted in-glaze decoration marble paper on white quality china goods is made at present, and its technological principle is that colorant is molten in glaze layer in roast process; Chinese red, the yellow low temperature color glaze of emperor are decorated and have been widely used in sclerotin porcelain, and decoration technology complexity is various.Due to technological reason, the reason such as low-temp exists hardness of glaze surface low, and anti-pollution characteristic is poor, acid-alkali-corrosive-resisting ability, is never being used matt glaze aspect china product decoration.
Summary of the invention
In order to realize the making of above-mentioned sclerotin matt glaze, a kind of method that the invention provides sclerotin matt glaze and make Bone China product of this glaze.
For achieving the above object, the present invention by the following technical solutions:
A sclerotin matt glaze, comprises following component and weight proportion umber: 100 parts of frits, 3～8 parts of clays, 2～12 parts of wollastonites, 3～6 parts, aluminum oxide, 6～15 parts, zinc oxide, 6 parts, stannic oxide; Wherein, described frit comprises following component and weight proportion umber: quartzy 16～24 parts, and 28～38 parts of potassium felspar sands, 12～18 parts of boraxs, 0～7 part of boric acid, 0～5 part of Strontium carbonate powder, 0～8 part of Quilonum Retard, 0～10 part, zinc oxide, 0～3 part, talcum, calcite 0～12,0～0.5 part of zirconium silicate.
The method that use sclerotin matt glaze claimed in claim 1 is made Bone China product, method steps is:
S1: the raw material stirring in described frit formula is even, at 1300-1330 ℃ of temperature, melt, make frit standby;
S2: get the frit obtaining in S1, the raw material in described glaze formula is entered to mill, take total mass as benchmark, adding mass percent is the water of 30-32%, grinds 48-55 hour, fineness 325 mesh sieve residue≤0.1% are crossed 200-250 mesh sieve, standby;
S3: the glaze obtaining in S2 glaze spraying in bique is dried, and glaze layer thickness scope is 6 grams/100 cm
2, entering kiln oxidation and fire, firing condition is: normal temperature heating, speed with 3 ~ 5 ℃/min is warmed up to 360 ℃, and then the speed with 2 ~ 4 ℃/min is warmed up to 900 ℃, then is warmed up to 1150 ~ 1180 ℃ with the speed of 1 ~ 2 ℃/min, insulation 20 ~ 30min, naturally cools to room temperature.Can burn till with common china light glaze, firing process is simple simultaneously.
Borax is in sclerotin matte glaze product, and mainly with boron oxide generation effect, in glaze, zinc oxide, wollastonite play a decisive role to separating out crystallite, and silica alumina ratio is controlled at the scope of 10:1 and boron oxide 8% left and right, is conducive to crystallization; Stannic oxide has good milkiness effect, is conducive to crystallization simultaneously, improves porcelain glaze whiteness, and the difference of wollastonite and zinc oxide is arranged in pairs or groups, and can adjust the glaze of different maturing temperatures.Zinc oxide, boron oxide, aluminum oxide, stannic oxide acting in conjunction, be both conducive to crystallization, prevents that again crystal from growing up.
Compared with prior art, the present invention has following beneficial effect: glaze is fine and smooth, and hardness is good, and durability against pollution is good, and acid and alkali-resistance ability is good, does not affect the secondary decoration technology requirements such as applique.
Embodiment
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
A kind of method that the present embodiment discloses sclerotin matt glaze and made Bone China product of this glaze.
Get following component and weight proportion umber: quartzy 16 parts, 28 parts of potassium felspar sands, 16 parts of boraxs, 6 parts of boric acid, 1 part of Strontium carbonate powder, 5 parts of Quilonum Retards, 2 parts, zinc oxide, 3 parts, talcum, 10 parts, calcite, 0.5 part of zirconium silicate, stirs above-mentioned raw materials, at 1310 ℃ of temperature, melts, and makes frit standby;
Get 100 parts of above-mentioned frits, 5 parts of clays, 10 parts of wollastonites, 6 parts, aluminum oxide, 10 parts, zinc oxide, 6 parts, stannic oxide, enters mill by above-mentioned raw materials, take total mass as benchmark, and adding mass percent is 30% water, grind 50 hours, fineness 325 mesh sieve residues 0.09%, cross 200 mesh sieves, standby;
Glaze obtained above glaze spraying in bique is dried, and glaze layer thickness is 6 grams/100 cm
2, entering kiln oxidation and fire, firing condition is: normal temperature heating, with the speed of 3 ℃/min, be warmed up to 360 ℃, then the speed with 2 ℃/min is warmed up to 900 ℃, then is warmed up to 1150 ℃ with the speed of 1 ℃/min, and insulation 20min, naturally cools to room temperature.
Matt glaze china product prepared by the present embodiment does not once split by 180-20 ℃ of hydrothermal exchange; By 200 tests of dishwasher, glaze does not significantly change, and with 5% acetum and 5% sodium hydroxide solution, soaks respectively 4 hours, and glaze is without the considerable change on observing.
Embodiment 2
A kind of method that the present embodiment discloses sclerotin matt glaze and made Bone China product of this glaze.
Get following component and weight proportion umber: quartzy 20 parts, 32 parts of potassium felspar sands, 13 parts of boraxs, 6 parts of boric acid, 4 parts of Strontium carbonate powders, 7 parts of Quilonum Retards, 10 parts, zinc oxide, 1 part, talcum, 5 parts, calcite, 0.2 part of zirconium silicate, stirs above-mentioned raw materials, at 1330 ℃ of temperature, melts, and makes frit standby;
Get 100 parts of above-mentioned frits, 7 parts of clays, 6 parts of wollastonites, 5 parts, aluminum oxide, 8 parts, zinc oxide, 6 parts, stannic oxide, enters mill by above-mentioned raw materials, take total mass as benchmark, and adding mass percent is 32% water, grind 55 hours, fineness 325 mesh sieve residues 0.08%, cross 220 mesh sieves, standby;
Glaze obtained above glaze spraying in bique is dried, and glaze layer thickness scope is 6 grams/100 cm
2, entering kiln oxidation and fire, firing condition is: normal temperature heating, with the speed of 5 ℃/min, be warmed up to 360 ℃, then the speed with 4 ℃/min is warmed up to 900 ℃, then is warmed up to 1180 ℃ with the speed of 2 ℃/min, and insulation 30min, naturally cools to room temperature.
Matt glaze china product prepared by the present embodiment does not once split by 180-20 ℃ of hydrothermal exchange; By 180 tests of dishwasher, glaze does not significantly change, and with 5% acetum and 5% sodium hydroxide solution, soaks respectively 4 hours, and glaze is without the considerable change on observing.
Embodiment 3
A kind of method that the present embodiment discloses sclerotin matt glaze and made Bone China product of this glaze.
Get following component and weight proportion umber: quartzy 24 parts, 38 parts of potassium felspar sands, 12 parts of boraxs, 3 parts of boric acid, 5 parts of Strontium carbonate powders, 9 parts, zinc oxide, 1 part, talcum, 12 parts, calcite, 0.5 part of zirconium silicate, stirs above-mentioned raw materials, at 1300 ℃ of temperature, melts, and makes frit standby;
Get 100 parts of above-mentioned frits, 8 parts of clays, 9 parts of wollastonites, 6 parts, aluminum oxide, 6 parts, zinc oxide, 6 parts, stannic oxide, enters mill by above-mentioned raw materials, take total mass as benchmark, and adding mass percent is 30% water, grind 52 hours, fineness 325 mesh sieve residues 0.05%, cross 250 mesh sieves, standby;
Glaze obtained above glaze spraying in bique is dried, and glaze layer thickness scope is 6 grams/100 cm
2, entering kiln oxidation and fire, firing condition is: normal temperature heating, with the speed of 4 ℃/min, be warmed up to 360 ℃, then the speed with 3 ℃/min is warmed up to 900 ℃, then is warmed up to 1160 ℃ with the speed of 1 ℃/min, and insulation 25min, naturally cools to room temperature.
Matt glaze china product prepared by the present embodiment does not once split by 180-20 ℃ of hydrothermal exchange; By 220 tests of dishwasher, glaze does not significantly change, and with 5% acetum and 5% sodium hydroxide solution, soaks respectively 4 hours, and glaze is without the considerable change on observing.
Claims (2)
1. a sclerotin matt glaze, is characterized in that, comprises following component and weight proportion umber: 100 parts of frits, 3～8 parts of clays, 2～12 parts of wollastonites, 3～6 parts, aluminum oxide, 6～15 parts, zinc oxide, 6 parts, stannic oxide; Wherein, described frit comprises following component and weight proportion umber: quartzy 16～24 parts, and 28～38 parts of potassium felspar sands, 12～18 parts of boraxs, 0～7 part of boric acid, 0～5 part of Strontium carbonate powder, 0～8 part of Quilonum Retard, 0～10 part, zinc oxide, 0～3 part, talcum, 0～12 part, calcite, 0～0.5 part of zirconium silicate.
2. of sclerotin matt glaze claimed in claim 1, make a method for Bone China product, it is characterized in that, method steps is:
S1: the raw material stirring in described frit formula is even, at 1300-1330 ℃ of temperature, melt, make frit standby;
S2: get the frit obtaining in S1, the raw material in described glaze formula is entered to mill, take total mass as benchmark, adding mass percent is the water of 30-32%, grinds 48-55 hour, fineness 325 mesh sieve residue≤0.1% are crossed 200-250 mesh sieve, standby;
S3: the glaze obtaining in S2 glaze spraying in bique is dried, and glaze layer thickness is 6 grams/100 cm
2, entering kiln oxidation and fire, firing condition is: normal temperature heating, speed with 3 ~ 5 ℃/min is warmed up to 360 ℃, and then the speed with 2 ~ 4 ℃/min is warmed up to 900 ℃, then is warmed up to 1150 ~ 1180 ℃ with the speed of 1 ~ 2 ℃/min, insulation 20 ~ 30min, naturally cools to room temperature.
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| CN201410263524.XA CN104003762B (en) | 2014-06-13 | 2014-06-13 | A kind of sclerotin matt glaze and the method with this glaze making Bone China product |
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| CN201410263524.XA CN104003762B (en) | 2014-06-13 | 2014-06-13 | A kind of sclerotin matt glaze and the method with this glaze making Bone China product |
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| CN105753326A (en) * | 2015-12-27 | 2016-07-13 | 襄阳高铭矿业有限公司 | Diamond glaze for ceramic tiles |
| CN106587631A (en) * | 2016-12-29 | 2017-04-26 | 湖南泰鑫瓷业有限公司 | Mat glaze similar to denim and manufacturing method thereof |
| CN106747660A (en) * | 2015-11-20 | 2017-05-31 | 广东顺祥陶瓷有限公司 | A kind of zinc boron fritted glaze high |
| CN106810075A (en) * | 2017-02-20 | 2017-06-09 | 湖南丰德利瓷业有限公司 | Bone china furnace transmutation glaze and preparation method thereof |
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| CN108975705A (en) * | 2018-10-31 | 2018-12-11 | 江苏拜富科技有限公司 | Marble paper flux and preparation method thereof in leadless glaze |
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| CN111548016B (en) * | 2020-05-20 | 2022-02-11 | 蒙娜丽莎集团股份有限公司 | Matt protection glaze with glossiness of below 3 degrees for thin ceramic tile, thin ceramic tile and preparation method thereof |
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| CN113248149B (en) * | 2021-07-12 | 2021-10-12 | 佛山市东鹏陶瓷发展有限公司 | Glaze slip with auspicious cloud effect, preparation method, ceramic tile and application in preparing ceramic tile |
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