CN103936877B - 一种从乌贼墨囊中提取粘多糖的方法 - Google Patents
一种从乌贼墨囊中提取粘多糖的方法 Download PDFInfo
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- CN103936877B CN103936877B CN201410167302.8A CN201410167302A CN103936877B CN 103936877 B CN103936877 B CN 103936877B CN 201410167302 A CN201410167302 A CN 201410167302A CN 103936877 B CN103936877 B CN 103936877B
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- Prior art keywords
- ink sac
- sepiellae seu
- seu sepiae
- mucopolysaccharide
- precipitate
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- 229920002683 Glycosaminoglycan Polymers 0.000 title claims abstract description 27
- 238000000034 method Methods 0.000 title claims abstract description 25
- 229940098363 cuttle fish ink Drugs 0.000 title abstract 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000000843 powder Substances 0.000 claims abstract description 32
- 230000000694 effects Effects 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 238000001556 precipitation Methods 0.000 claims abstract description 4
- 238000000498 ball milling Methods 0.000 claims description 21
- 239000002244 precipitate Substances 0.000 claims description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 16
- 230000001413 cellular effect Effects 0.000 claims description 14
- 239000006228 supernatant Substances 0.000 claims description 13
- 150000004676 glycans Chemical class 0.000 claims description 10
- 229920001282 polysaccharide Polymers 0.000 claims description 10
- 239000005017 polysaccharide Substances 0.000 claims description 10
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 6
- SCVFZCLFOSHCOH-UHFFFAOYSA-M potassium acetate Chemical compound [K+].CC([O-])=O SCVFZCLFOSHCOH-UHFFFAOYSA-M 0.000 claims description 6
- 238000004062 sedimentation Methods 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 102000004169 proteins and genes Human genes 0.000 claims description 5
- 108090000623 proteins and genes Proteins 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 4
- 230000007062 hydrolysis Effects 0.000 claims description 4
- 238000006460 hydrolysis reaction Methods 0.000 claims description 4
- 230000001954 sterilising effect Effects 0.000 claims description 4
- 108090000145 Bacillolysin Proteins 0.000 claims description 3
- 108090000790 Enzymes Proteins 0.000 claims description 3
- 102000004190 Enzymes Human genes 0.000 claims description 3
- 102000035092 Neutral proteases Human genes 0.000 claims description 3
- 108091005507 Neutral proteases Proteins 0.000 claims description 3
- -1 centrifugal Substances 0.000 claims description 3
- 238000005119 centrifugation Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 235000011056 potassium acetate Nutrition 0.000 claims description 3
- 238000004064 recycling Methods 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 238000001291 vacuum drying Methods 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 238000004061 bleaching Methods 0.000 claims description 2
- 239000000047 product Substances 0.000 abstract description 9
- 239000004615 ingredient Substances 0.000 abstract description 5
- 206010028980 Neoplasm Diseases 0.000 abstract description 4
- 238000012545 processing Methods 0.000 abstract description 4
- 230000000975 bioactive effect Effects 0.000 abstract description 3
- 230000006378 damage Effects 0.000 abstract description 3
- 238000004090 dissolution Methods 0.000 abstract description 3
- 230000036039 immunity Effects 0.000 abstract description 3
- 235000015097 nutrients Nutrition 0.000 abstract description 3
- 230000002255 enzymatic effect Effects 0.000 abstract 1
- 239000000413 hydrolysate Substances 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 230000002401 inhibitory effect Effects 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 230000000717 retained effect Effects 0.000 abstract 1
- 201000011510 cancer Diseases 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- 241000238366 Cephalopoda Species 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 1
- 241000251468 Actinopterygii Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 241000699670 Mus sp. Species 0.000 description 1
- 241000238413 Octopus Species 0.000 description 1
- 208000008469 Peptic Ulcer Diseases 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 241000472272 Sepiida Species 0.000 description 1
- 241000238371 Sepiidae Species 0.000 description 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
- 229930003270 Vitamin B Chemical group 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical group OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 239000001506 calcium phosphate Substances 0.000 description 1
- 229910000389 calcium phosphate Inorganic materials 0.000 description 1
- 235000011010 calcium phosphates Nutrition 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 108010006161 conchiolin Proteins 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 235000004213 low-fat Nutrition 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 230000014860 sensory perception of taste Effects 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 235000019156 vitamin B Nutrition 0.000 description 1
- 239000011720 vitamin B Chemical group 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
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- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
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CN201410167302.8A CN103936877B (zh) | 2014-04-24 | 2014-04-24 | 一种从乌贼墨囊中提取粘多糖的方法 |
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CN201410167302.8A CN103936877B (zh) | 2014-04-24 | 2014-04-24 | 一种从乌贼墨囊中提取粘多糖的方法 |
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CN103936877A CN103936877A (zh) | 2014-07-23 |
CN103936877B true CN103936877B (zh) | 2017-01-11 |
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CN201410167302.8A Expired - Fee Related CN103936877B (zh) | 2014-04-24 | 2014-04-24 | 一种从乌贼墨囊中提取粘多糖的方法 |
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Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
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TWI565419B (zh) * | 2015-02-11 | 2017-01-11 | The method of deodorizing the oocysts | |
CN106832033B (zh) * | 2017-01-23 | 2019-03-26 | 石狮市华宝海洋生物医药有限公司 | 分段复合酶解提取乌贼墨小分子硫酸粘多糖的工艺 |
CN107793491A (zh) * | 2017-09-22 | 2018-03-13 | 浙江海洋大学 | 一种鱿鱼墨多糖寡糖的制备方法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1288169C (zh) * | 2002-08-30 | 2006-12-06 | 大连轻工业学院 | 海参粘多糖的制备方法 |
CN101451157B (zh) * | 2008-12-25 | 2012-09-05 | 大连海晏堂生物有限公司 | 一种低分子量海参多糖的制备方法 |
CN102008528B (zh) * | 2010-12-14 | 2012-01-25 | 大连海晏堂生物有限公司 | 复方海参制剂及其制备方法 |
CN102718879B (zh) * | 2012-06-16 | 2013-12-25 | 山东绿洲醇食品有限公司 | 海参粘多糖提取工艺及其功能性保健饮料 |
CN103585252A (zh) * | 2013-11-13 | 2014-02-19 | 苏州鹰皇药业有限公司 | 一种直接口服中药饮片的超微复合破壁方法 |
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