CN103933917B - 一种反应装置 - Google Patents

一种反应装置 Download PDF

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CN103933917B
CN103933917B CN201410139086.6A CN201410139086A CN103933917B CN 103933917 B CN103933917 B CN 103933917B CN 201410139086 A CN201410139086 A CN 201410139086A CN 103933917 B CN103933917 B CN 103933917B
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reaction unit
support
fixed
air inlet
inlet pipe
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CN103933917A (zh
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蔡荣盛
李祥福
傅哲龙
林鸿志
陆曹生
陆璐
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NANTONG XIEXIN HOT MELT ADHESIVE CO., LTD.
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林鸿志
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Priority to CN201610081572.6A priority Critical patent/CN105561908B/zh
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Priority to CN201610081575.XA priority patent/CN105709677B/zh
Priority to CN201410139086.6A priority patent/CN103933917B/zh
Priority to CN201610081571.1A priority patent/CN105664821B/zh
Priority to CN201610081569.4A priority patent/CN105561829B/zh
Priority to CN201610081574.5A priority patent/CN105688777B/zh
Priority to CN201610081570.7A priority patent/CN105688734B/zh
Priority to CN201610081573.0A priority patent/CN105597648B/zh
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    • B01J2219/00135—Electric resistance heaters

Abstract

本发明涉及反应装置，其罐盖中央的圆孔上方固定有支架，支架内设置有密封球面轴承，密封球面轴承的球体连接搅拌轴，圆孔与球体之间固定有密封膜，密封膜与支架之间形成密封腔，密封腔内注水，反应装置还包括气体加热装置和从底部插入的进气管，以及带辅助加热的水循环系统。由于密封膜上方的密封腔内注有水，因此当罐内压力变化时，密封腔能够对密封膜起到良好的支撑作用，密封膜不会鼓起或塌陷，也就不会受到额外的张力，因此不易破损，使用寿命更长。进气管输入的气体快速向上运动的特性，加上带辅助加热的水循环系统，有助于将物料产生对流，使电加热管的热量更快更均匀的传递给物料。

Description

一种反应装置
技术领域
本发明涉及一种反应装置。
背景技术
现在市面上大多数用于制备印染助剂的反应装置没有设置搅拌装置，使得反应的物料搅拌不充分和不均匀，这就直接导致反应速度慢，且反应不完全，浪费了资源，提高了生产成本，且反应后罐内残留下的一些反应介质容易腐蚀，影响了反应设备，不能提高经济效益。
为了解决上述问题，中国实用新型专利CN203123964U，公开了一种用于制备印染助剂的反应装置，其在罐盖上安装有伸入于罐身内的搅拌轴，搅拌轴底端安装有锚形桨叶，实现对物料的搅拌，加快反应速度。
然而某些印染助剂在制备过程中有有害物质挥发出，因此需要在密闭环境中进行搅拌。传统带搅拌反应装置大多采用填料密封或机械密封，填料密封的密封性能差且阻力大、易损耗；而机械密封则价格高，使用一段时间后密封性能下降，维护更换成本高昂。
此外，有时反应需要一定的加热环境，传统只能通过对罐体加热来实现对物料的加热，加热速度缓慢且罐内物料温度不均匀，不利于反应的顺利进行。
发明内容
本发明的目的在于：克服上述现有技术的缺陷，提出一种反应装置。
为了达到上述目的，本发明提出的反应装置，组成包括罐身、罐盖、搅拌电机、搅拌轴、搅拌桨，所述罐身上设有投料口、出料口，其特征在于：所述罐盖中央开设圆孔，圆孔上方固定有支架，所述支架内设置有密封球面轴承，所述密封球面轴承的球体连接搅拌轴，密封球面轴承的轴承箱与支架固定，所述圆孔与球体之间固定有柔性密封膜，所述柔性密封膜与支架之间形成密封腔，该密封腔内注满纯水；所述罐身底部安装有主电加热管，所述主电加热管上方的罐身内壁固定有朝斜下方向喷射的喷嘴，所述主电加热管下方的罐身底部固定有抽水口，所述罐身外设置有将抽水口与喷嘴连接的管路，管路上安装有水泵，管路内设置有辅助电加热管；反应装置还包括气体加热装置和从底部插入罐身的数根进气管，所述进气管与气体加热装置的出气端相连，所述气体加热装置的进气端通过管道连接惰性气体气源，插入罐身的进气管端部安装有散气盘，所述散气盘位于主电加热管下方，所述罐盖上安装有排气管，所述排气管上装有泄压阀。
本发明反应装置，进一步的改进在于：
1、所述罐身外壁设有冷却腔，冷却腔的上部具有冷却水入口，冷却腔的下部具有冷却水出口。
2、所述罐盖上安装有观察口和插入罐身内的温度计。
3、所述柔性密封膜呈环形，内外侧分别通过法兰与球体、罐盖圆孔密封连接。
4、所述罐盖与罐身的接口处卡装接合。
5、所述喷嘴的喷射方向与搅拌轴转动方向相反。
本发明反应装置使用球轴承实现搅拌桨全方位的搅动，不留死角；选用柔性密封膜密封，使得内部罐内气体不泄露，有效保护操作人员且不会对环境造成污染；由于密封膜上方的密封腔内注有水，因此当罐内压力变化时，特别是压力大幅增加时或压力急剧降低时，密封腔能够对密封膜起到良好的支撑作用，这是因为当外界压力变化时液体的体积随几乎不发生变化，因此密封膜不会鼓起或塌陷，也就不会受到额外的张力，因此不易破损，使用寿命更长。
故，本发明所用的密封结构成本低廉，且能够承受罐内不同的压力变化，具有更强的适应性。
本发明设备的罐身内设置有主电加热管，并且在水循环的管道内设置辅助电加热管，能够对物料进行加热。水循环促进了物料的混合，提高搅拌效果，通过电加热管可以对物料进行加热，实现对物料加热的目的。电加热设置于循环管道内可以使被加热物料更均匀与罐内物料混合，使物料更均匀的被加热，提高物料的反应速度和平稳性，进一步提高生产效率。并且罐身底部通入有进气管，利用该进气管向罐身内部输送经过加热的惰性气体，能够迅速将热量传递给罐身内的物料；由于进气管输入的气体快速向上运动的特性，有助于将物料产生对流，使电加热管的热量更快更均匀的传递给物料。气流与水流共同作用，互相促进，使物料能够充分混合，能够平稳均匀的提高物料温度，提高反映效率。
附图说明
下面结合附图对本发明作进一步的说明。
图1是本发明反应装置结构示意图。
图2是本发明反应装置的喷嘴喷射水流示意图。
图中标号示意如下：
1-罐身，1＇-罐盖，2-电机，3-搅拌轴，4-搅拌桨，5-投料口，6-出料口，7-观察口，8-支架，9-轴承箱，10-球体，11-柔性密封膜，12-密封腔，13-喷嘴，14-电加热管，15-温度计，16-水泵，17-管路，18-排气管，19-泄压阀，20-抽水口，21-进气管，22-散气盘，23-管道，24-气体加热装置，25-冷却腔，26-冷却水入口，27-冷却水出口。
具体实施方式
下面结合附图和具体实施例对本发明做进一步说明。
如图1所示，为本发明反应装置，组成包括罐身1和设置于罐身1上方的罐盖1＇，罐盖1＇与罐身1的接口处卡装接合，罐盖1＇上安装有排气管18，排气管18上装有泄压阀19，罐盖1＇上还安装有观察口7、插入罐身1内的温度计15，罐身1上设有投料口5、出料口6，所述罐盖1＇安装有伸入于罐身1内由电机2驱动的搅拌轴3，搅拌轴3底部固定有搅拌桨4，罐盖1＇中央开设圆孔，圆孔上方固定有支架8，支架8内设置有密封球面轴承（由轴承箱9和球体10），密封球面轴承的球体10连接搅拌轴3，密封球面轴承的轴承箱9与支架8固定，圆孔与球体10之间固定有环形柔性密封膜11，环形柔性密封膜11内外侧分别通过法兰与球体10、罐盖圆孔密封连接；柔性密封膜11与支架8之间形成密封腔12，该密封腔12内注满纯水；罐身1底部安装有螺旋形主电加热管14，主电加热管14上方的罐身1内壁固定有朝斜下方向喷射的喷嘴13，主电加热管14下方的罐身底部固定有抽水口20，罐身外设置有将抽水口20与喷嘴13连接的管路17，管路17上安装有水泵16，管路内设置有辅助电加热管（图中未画出）。可利用水泵将物料从罐身底部抽出，并从喷嘴喷出，一方面提高搅拌效果，另一方便可提高加热均匀性。
如图1所示，本例的反应装置还具有气体加热装置24和从底部插入罐身一根进气管21，进气管21与气体加热装置24的出气端相连，气体加热装置24的进气端通过管道23连接惰性气体气源，插入罐身1的进气管21端部安装有散气盘22，散气盘22位于主电加热管14下方。
本例中罐身1外壁设有冷却腔25，冷却腔25的上部具有冷却水入口26，冷却腔25的下部具有冷却水出口27。
本设备一方面利用进气管向罐身内部输送经过加热的惰性气体，能够迅速将热量传递给罐身内的物料，实现对物料加热的目的，同时进气管喷出的气体向上运动，有助于将物料产生对流，提高电加热管的加热效率；另一方面，本设备可利用水泵将物料从罐身底部抽出，并从喷嘴喷出，并进行辅助加热，提高搅拌效果、加热均匀性的同时，更快的对物料进行加热。
如图2所示，本例中，喷嘴13的喷射方向C与搅拌轴转动方向A相反。本例中，搅拌桨除了进行公转外，还进行自传，图中，B为搅拌桨自转转动方向。图中，1为罐身。
除上述实施例外，本发明还可以有其他实施方式。凡采用等同替换或等效变换形成的技术方案，均落在本发明要求的保护范围。

Claims (4)

1.一种反应装置，组成包括罐身、罐盖、搅拌电机、搅拌轴、搅拌桨，所述罐身上设有投料口、出料口，其特征在于：所述罐盖中央开设圆孔，圆孔上方固定有支架，所述支架内设置有密封球面轴承，所述密封球面轴承的球体连接搅拌轴，密封球面轴承的轴承箱与支架固定，所述圆孔与球体之间固定有柔性密封膜，所述柔性密封膜与支架之间形成密封腔，该密封腔内注满纯水；所述罐身底部安装有主电加热管，所述主电加热管上方的罐身内壁固定有朝斜下方向喷射的喷嘴，所述主电加热管下方的罐身底部固定有抽水口，所述罐身外设置有将抽水口与喷嘴连接的管路，管路上安装有水泵，管路内设置有辅助电加热管；反应装置还包括气体加热装置和从底部插入罐身的数根进气管，所述进气管与气体加热装置的出气端相连，所述气体加热装置的进气端通过管道连接惰性气体气源，插入罐身的进气管端部安装有散气盘，所述散气盘位于主电加热管下方，所述罐盖上安装有排气管，所述排气管上装有泄压阀。
2.根据权利要求1所述的反应装置，其特征在于：所述罐身外壁设有冷却腔，冷却腔的上部具有冷却水入口，冷却腔的下部具有冷却水出口。
3.根据权利要求1所述的反应装置，其特征在于：所述罐盖上安装有观察口和插入罐身内的温度计。
4.根据权利要求1所述的反应装置，其特征在于：所述罐盖与罐身的接口处卡装接合。
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