CN103919706B - A kind of precious Rogor lightening compositions and preparation method thereof - Google Patents

A kind of precious Rogor lightening compositions and preparation method thereof Download PDF

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CN103919706B
CN103919706B CN201410188496.XA CN201410188496A CN103919706B CN 103919706 B CN103919706 B CN 103919706B CN 201410188496 A CN201410188496 A CN 201410188496A CN 103919706 B CN103919706 B CN 103919706B
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precious rogor
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raw material
polydimethylsiloxane
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CN103919706A (en
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刘山
向文浩
焦红
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Guangzhou Bese Clean Cosmetics Manufacturer Co., Ltd.
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GUANGZHOU BESE CLEAN COSMETICS MANUFACTURER CO Ltd
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Abstract

The invention discloses a kind of precious Rogor lightening compositions and preparation method thereof, precious Rogor compositions is made up of the component of following percetage by weight: 3-o-ethylascorbyl 0.2-1.0%, and precious Rogor powder 0.5-1.5%, surplus is auxiliary agent.The present invention is by carrying out composite by 3-o-ethylascorbyl and precious Rogor powder in the ratio limited, under this ratio, precious Rogor powder can suppress the activity of tryrosinase to the full extent, TYR hydroxylating can be effectively stoped to be changed into DOPA quinone, internal melanin is formed be obstructed, thus reaching the effect of best whitening.

Description

A kind of precious Rogor lightening compositions and preparation method thereof
Technical field
The present invention relates to skin care field, specifically, relate to a kind of precious Rogor lightening compositions and preparation method thereof.
Background technology
Precious Rogor (Borojo) is a kind of fruit being grown in South America Tropical rain forest, and unique adaptation Ecuador weather, fruit belongs to Rubiaceae woods.Borojo fruit diameter reaches 7-12 centimetre, green during immaturity, transfers dark brown after maturation to, weight 700-1000 gram/only, and sarcocarp is soft, sour in the mouth and thickness, and after removing seed, sarcocarp weight accounts for 88%.Fresh Borojo is the fruit of extremely acid (pH2.74), low moisture (69.22%), high carbohydrate (28.02%), low sugar (9.72%), high protein (1.22%), high dietary-fiber (2.98%).The content of B1 in vitamin B group, B2, nicotinic acid, folic acid and vitamin E is far above most fruits.Free amino acid total content is 1.35%, 25 kinds;Containing 19 seed amino acid materials after hydrolysis, total amount reaches 2.51%, and wherein containing the necessary aminoacid of 5 kinds of human bodies, 2 kinds of conditions must aminoacid.Borojo medium trace element enriches, containing potassium 3500mg/kg, magnesium 280mg/kg, ferrum 160mg/kg and zinc 0.64mg/kg;Containing micro elements needed by human zinc, copper, cobalt, ferrum, it may be necessary to trace element manganese, silicon, nickel, boron, and rare trivalent chromium and nickel in vegetable and fruit.Total amount of rare earth and 16 kinds of rare earth element content are all within normal range, to human health without potential hazard.Harmful heavy metal lead is 24 μ g/kg, and hydrargyrum, arsenic, cadmium are below lowest detectable limit.Borojo contains abundant needed by human linoleic acid (9.91%) and linolenic acid (0.89%), and total flavones reaches 335.2mg/kg, and 8,9-iridoid glycosides reach 1.92g/100g, and polyphenol reaches 270mg/kg.
Borojo is the fruit that a kind of nutritive value is significantly high, but does not have at present and be used for manufacturing whitening cosmetic compound with other combination of components by Borojo.
Summary of the invention
It is an object of the invention to overcome the deficiencies in the prior art, it is provided that a kind of precious Rogor compositions for whitening.
For achieving the above object, the technical scheme that the present invention takes is:
A kind of precious Rogor lightening compositions, is made up of the component of following percetage by weight:
3-o-ethylascorbyl 0.2-1.0%,
Precious Rogor powder 0.5-1.5%,
Surplus is auxiliary agent.
nullIn above-mentioned precious Rogor lightening compositions,Preferred formula is: 3-o-ethylascorbyl 0.2-1.0%,Precious Rogor powder 0.5-1.5%,Component X1.0-3.0%,PEG-100 stearate 1.0-3.0%,Isopropyl palmitate 1.0-3.0%,IPIS 1.0-3.0%,Polydimethylsiloxane 1.0-4.0%,Ring five polydimethylsiloxane 0.1-1.0%,Caprylic/capric triglyceride 1.0-4.0%,Jojoba seed oil 1.0-3.0%,Cetearyl alcohol 1.0-3.0%,Squalane 0.1-3.0%,Cera alba 0.1-3.0%,Tocopherol acetas 0.1-1.0%,Methyl hydroxybenzoate 0.01-0.3%,Propyl hydroxybenzoate 0.01-0.3%,Glycerol 1.0-6.0%,Butanediol 1.0-6.0%,Xanthan gum 0.01-0.3%,Hyaluronate sodium 0.001-0.3%,Trehalose 1.0-6.0%,EDETATE SODIUM 0.01-0.1%,Component Y0.1-1.5%,Component Z0.01-0.12%,Surplus is water;Described component X is made up of cetearyl alcohol and C12-20 alkyl androstanediol, its percetage by weight respectively 20-40% and 60-80%;Described component Y is made up of polyacrylic acid, polyisobutylene and polysorbate-20, its percetage by weight respectively 5-10%, 20-55% and 40-70%;Described component Z is made up of Methylisothiazolinone and Sensiva SC50, its percetage by weight respectively 3-8% and 92-97%.
Compared with prior art, there is advantages that the present invention is by carrying out composite by 3-o-ethylascorbyl and precious Rogor powder in the ratio limited, under this ratio, precious Rogor powder can suppress the activity of tryrosinase to the full extent, TYR hydroxylating can be effectively stoped to be changed into DOPA quinone, internal melanin is formed be obstructed, thus reaching the effect of best whitening.
Detailed description of the invention
The preparation of precious Rogor powder:
(1) take precious Rogor (Borojo) fresh fruit, clean peeling, fruit, core are separated;
(2) in sarcocarp, add the water of 10% sarcocarp weight, grind, be subsequently adding the pectase of 1 ‰ sarcocarp weight, at 30~40 DEG C, make sarcocarp enzymolysis, digestion 1.5 hours;
(3) by the sarcocarp filter pressing remove impurity after enzymolysis, digestion, heat to 80 DEG C of maintenance 5min, kill enzyme;
(4) sodium carbonate adding 5 ‰ sarcocarp weight regulates pH, is then concentrated into BRIX in-65 DEG C of vacuum and reaches 20%;
(5) add the cycloheptaamylose of 1% sarcocarp weight, then spray drying, obtain precious Rogor (Borojo) powder.
Precious Rogor preparation method of composition:
(1) various raw materials in precise formula, hold with vessel that are clean and that disinfect;
(2) adding in vacuum emulsification pot by A phase raw material (water, glycerol, butanediol, xanthan gum, hyaluronate sodium, trehalose, EDETATE SODIUM), stirring stirs, is incubated standby after being warming up to 80~85 DEG C;
(3) B phase raw material (cetearyl alcohol and C12-20 alkyl androstanediol, PEG-100 stearate, isopropyl palmitate, IPIS, polydimethylsiloxane, propyl hydroxybenzoate, caprylic/capric triglyceride, Jojoba (SIMMONDSIACHINENSIS) seed oil, cetearyl alcohol, squalane, cera alba, tocopherol acetas, methyl hydroxybenzoate, ring five polydimethylsiloxane) is added in oil cauldron, stirring is warming up to 80~85 DEG C, stir, be incubated standby;
(4) by B phase raw material suction vacuum emulsification pot, C phase raw material (polyacrylic acid, polyisobutylene and polysorbate-20) is added after mixing and stirring, after emulsifying 5-8 minute, stirring, constant temperature stirring froth breaking was lowered the temperature after 10 minutes;
(5), below when being cooled to 45 DEG C, add D phase raw material (precious Rogor, 3-o-ethylascorbyl, Methylisothiazolinone and Sensiva SC50), stir rear discharging, standing;
(6) after the assay was approved, fill, packaging, coding;
(7) after the assay was approved, warehouse-in.
Embodiment 1: formula is table 1 such as.
Table 1
In form, each component sum is 100%.
Embodiment 2: formula is table 2 such as.
Table 2
In form, each component sum is 100%.
Comparative example 1: formula is table 3 (contrast sample 1) such as
Table 3
In form, each component sum is 100%.
Comparative example 2: formula is table 4 (contrast sample 2) such as
Table 4
In form, each component sum is 100%.
Whitening effect contrast experiment:
Embodiment 1 and 2 is to the addition of precious Rogor and the 3-o-ethylascorbyl of different proportion.Comparative example 1 is contrast sample 1, only with the addition of 3-o-ethylascorbyl.Comparative example 2 is contrast sample 2, only with the addition of precious Rogor.As shown in table 5, the data of each test group are the meansigma methodss being respectively directed to the test data that 10 people make, the crowd of described test group 1-5 corresponding dry skin, neutral skin, oily skin, mixed type skin, sensitive skin respectively;From test result: use comparative example 1 (contrast sample 1) and comparative example 2 (contrasting sample 2) from melanin value downward trend after instrument test data analysis, but downward trend is inconspicuous.Using embodiment 1 and 2 is after instrument test data analysis, and after using 4 weeks, melanin value declines substantially, and uses front and after 4 weeks melanin value to differ greatly, and illustrates that the collaborative whitening effect of precious Rogor collocation 3-o-ethylascorbyl product is notable.
Table 5

Claims (1)

1. the precious Rogor compositions for whitening, it is characterised in that be made up of the component of following percetage by weight:
null3-o-ethylascorbyl 0.2-1.0%,Precious Rogor 0.5-1.5%,Component X1.0-3.0%,PEG-100 stearate 1.0-3.0%,Isopropyl palmitate 1.0-3.0%,IPIS 1.0-3.0%,Polydimethylsiloxane 1.0-4.0%,Ring five polydimethylsiloxane 0.1-1.0%,Caprylic/capric triglyceride 1.0-4.0%,Jojoba seed oil 1.0-3.0%,Cetearyl alcohol 1.0-3.0%,Squalane 0.1-3.0%,Cera alba 0.1-3.0%,Tocopherol acetas 0.1-1.0%,Methyl hydroxybenzoate 0.01-0.3%,Propyl hydroxybenzoate 0.01-0.3%,Glycerol 1.0-6.0%,Butanediol 1.0-6.0%,Xanthan gum 0.01-0.3%,Hyaluronate sodium 0.001-0.3%,Trehalose 1.0-6.0%,EDETATE SODIUM 0.01-0.1%,Component Y0.1-1.5%,Component Z0.01-0.12%,Surplus is water;Described component X is made up of cetearyl alcohol and C12-20 alkyl androstanediol, its percetage by weight respectively 20-40% and 60-80%;Described component Y is made up of polyacrylic acid, polyisobutylene and polysorbate-20, its percetage by weight respectively 5-10%, 20-55% and 40-70%;Described component Z is made up of Methylisothiazolinone and Sensiva SC50, its percetage by weight respectively 3-8% and 92-97%;
Preparation method comprises the steps:
(1) various raw materials in precise formula, hold with vessel that are clean and that disinfect;
(2) by A phase raw material, water, glycerol, butanediol, xanthan gum, hyaluronate sodium, trehalose, EDETATE SODIUM, add in vacuum emulsification pot, stirring stirs, is incubated standby after being warming up to 80~85 DEG C;
(3) by B phase raw material, cetearyl alcohol and C12-20 alkyl androstanediol, PEG-100 stearate, isopropyl palmitate, IPIS, polydimethylsiloxane, propyl hydroxybenzoate, caprylic/capric triglyceride, Jojoba seed oil, cetearyl alcohol, squalane, cera alba, tocopherol acetas, methyl hydroxybenzoate, ring five polydimethylsiloxane, add in oil cauldron, stirring is warming up to 80~85 DEG C, stir, be incubated standby;
(4) by B phase raw material suction vacuum emulsification pot, C phase raw material after mixing and stirring, is added, polyacrylic acid, polyisobutylene and polysorbate-20, after emulsifying 5-8 minute, stir, constant temperature stirring froth breaking was lowered the temperature after 10 minutes;
(5), below when being cooled to 45 DEG C, add D phase raw material, precious Rogor, 3-o-ethylascorbyl, Methylisothiazolinone and Sensiva SC50, stir rear discharging, standing;
(6) after the assay was approved, fill, packaging, coding;
(7) after the assay was approved, warehouse-in.
CN201410188496.XA 2014-05-06 2014-05-06 A kind of precious Rogor lightening compositions and preparation method thereof Active CN103919706B (en)

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CN106109277A (en) * 2016-07-28 2016-11-16 广州赛莱拉干细胞科技股份有限公司 A kind of moisture-keeping composition and a kind of skin nursing products
CN106265365A (en) * 2016-09-29 2017-01-04 广州赛莱拉干细胞科技股份有限公司 A kind of lightening compositions and a kind of skin nursing products
CN108158881A (en) * 2017-12-30 2018-06-15 广州雅纯化妆品制造有限公司 A kind of skin care item comprising precious Rogor powder and preparation method and application
CN108815014A (en) * 2018-08-15 2018-11-16 白东跃 Skin care item and preparation method thereof containing swan-mussel polysaccharide and precious Rogor

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US20090246231A1 (en) * 2008-03-25 2009-10-01 Giovanni Valencia Formulations containing borojo
US20100136064A1 (en) * 2008-12-03 2010-06-03 Rufina Shatkina Nutraceutical composition
CN102351927A (en) * 2011-08-17 2012-02-15 梁公壁 Borojo active extract and preparation method and antibacterial and anti-oxidation application thereof
CN103585037A (en) * 2013-11-04 2014-02-19 苏州冉新生物技术有限公司 Whitening patch-lightening cosmetic

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US20090246231A1 (en) * 2008-03-25 2009-10-01 Giovanni Valencia Formulations containing borojo
US20100136064A1 (en) * 2008-12-03 2010-06-03 Rufina Shatkina Nutraceutical composition
CN102351927A (en) * 2011-08-17 2012-02-15 梁公壁 Borojo active extract and preparation method and antibacterial and anti-oxidation application thereof
CN103585037A (en) * 2013-11-04 2014-02-19 苏州冉新生物技术有限公司 Whitening patch-lightening cosmetic

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Effective date of registration: 20161024

Address after: 510470, Baiyun District, Guangdong, Guangzhou province and Xiushui Rice Industrial Park, No. 2

Patentee after: Guangzhou Bese Clean Cosmetics Manufacturer Co., Ltd.

Patentee after: Jiao Hong

Address before: 510470, Baiyun District, Guangdong, Guangzhou province and Xiushui Rice Industrial Park, No. 2

Patentee before: Guangzhou Bese Clean Cosmetics Manufacturer Co., Ltd.