CN103834504B - A kind of ginseng polypeptide Transparent handmade soap and preparation method thereof - Google Patents
A kind of ginseng polypeptide Transparent handmade soap and preparation method thereof Download PDFInfo
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- CN103834504B CN103834504B CN201310745073.9A CN201310745073A CN103834504B CN 103834504 B CN103834504 B CN 103834504B CN 201310745073 A CN201310745073 A CN 201310745073A CN 103834504 B CN103834504 B CN 103834504B
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Abstract
The invention belongs to cosmetics and cleaning supplies field, be specifically related to a kind of ginseng polypeptide Transparent handmade soap and preparation method thereof.Product of the present invention contains ginseng polypeptide, it is possible to promote fibroblastic growth, resist UV-induced cell injury, there is wrinkle reduction and prevent skin ageing effect, playing skin care effect.Ginseng polypeptide Transparent handmade soap takes the compositions such as natural vegetable oil, and such as Petiolus Trachycarpi oil, Oleum Cocois, Oleum Ricini and olive oil etc., and soap base made by the caustic alkali such as sodium hydroxide or potassium hydroxide, adds composite natral clarifier and ginseng polypeptide prepares.Not only there is good cleaning and supplementary moisture of skin effect, the metabolism of skin can be promoted simultaneously, repair damaged cell, resist the multiple efficacies such as UV-induced cell injury, keep skin smooth submissive, have significant skin effect.
Description
Technical field
The invention belongs to cosmetics and cleaning supplies field, be specifically related to a kind of ginseng polypeptide Transparent handmade soap and preparation method thereof.
Background technology
In recent years, along with people are to quality of the life and able-bodied pursuit of rationality, pure natural, avirulent vegetalization cosmetic have become the leading of international cosmetic market, and wherein handmade soap becomes one of product enjoying consumers welcomed.It, with multiple pure natural plant oils and fatss such as Petiolus Trachycarpi oil, Oleum Cocois, olive oil as raw material, uses cold method processed to make by hand, does not removes natural moisture preserving agent glycerol, and remain a large number of nutrients in vegetable oil, non-stimulated, foaming abundancy, there is well cleaning, skin care effect.
It is known that " whitening and skin-protecting " is one of primary efficacy of Radix Ginseng for thousands of years, and it is widely recognized as by the whole world.The ginseng polypeptide added in the present invention, it is possible to promote fibroblastic growth, resist UV-induced cell injury, has wrinkle reduction and prevents skin ageing effect, and then playing skin care effect.The handmade soap that the present invention provides, not only remain vegetable oil Middle nutrition composition, and with the addition of ginseng polypeptide, not only there is good cleaning and supplementary moisture of skin effect, the metabolism of skin can be promoted simultaneously, repair damaged cell, resist the multiple efficacies such as UV-induced cell injury, keep skin smooth submissive, have significant skin effect.
Summary of the invention
It is an object of the invention to provide a kind of ginseng polypeptide Transparent handmade soap, it is possible to while cleaning skin, effectively protection and skin care, reach anti-skin ageing effect.
For achieving the above object, the technical solution used in the present invention is: ginseng polypeptide Transparent handmade soap, it is characterised in that: mainly comprise: ginseng polypeptide, vegetable oil, alkali etc..
Ginseng polypeptide preparation method proposed by the invention, it is characterised in that specifically comprise the following steps that
(1) fresh ginseng 20g is taken, extract 12-48 hour under the conditions of pH5-9 with 1:5-1:20 ratio with 0.01mol/lPBS, take supernatant adding volume ratio is the pre-cold acetone precipitation of 1:1.0-3.0 ice, fully stand overnight after mixing, 5000r/min, takes precipitation pH5-9 after centrifugal 10min, after 0.01mol/l PBS dissolves, lyophilizing, obtains Radix Ginseng crude protein.
(2), after the crude protein that obtained by acetone precipitation dissolves, filter through the defecator of 0.45 μm, be that 30 KDa are concentrated by ultrafiltration through membrane aperture, collect filter liquor, then the ultrafiltration through 10 KDa, collect molecular weight less than 10KDa effluent, lyophilizing, i.e. obtains highly purified ginseng polypeptide.
Transparent handmade soap preparation method proposed by the invention, it is characterised in that concrete preparation process is as follows:
(1) formula components becomes to be grouped into each of percentage by weight: Petiolus Trachycarpi oil 15-25%；Oleum Cocois 5-15%；Oleum Ricini 10-15%；Alkali 3-8%；Distilled water 21-28%；Ethanol 10-16%；Glycerol 6-15%；Sucrose 5-10%；Ginseng polypeptide 0.1-1%, each component sum is 100%.
(2) according to the proportioning of step (1) by vegetable oil heated and stirred to 60 DEG C, it is slowly added to alkali, stir and within 20-30 minute, complete saponification, add glycerol and stir 20-30 minute, to gluey, add ethanol stirring 10-30 clock, sucrose stirs 10-30 minute, continues stirring and treats that temperature drops to less than 37 DEG C and adds ginseng polypeptide, treats that bubble is wholly absent and pour mould into, put into 4--20 DEG C freezing 4-24 hour, put into 20-40 DEG C of maturation after taking-up and get final product.
Detailed description of the invention
Below in conjunction with embodiment, technical scheme is described further.
The preparation of ginseng polypeptide
Embodiment 1:
(1) fresh ginseng 20g is taken, extract under the conditions of pH8.0 24 hours with 1:10 ratio with 0.01mol/lPBS, take supernatant adding volume ratio is the pre-cold acetone precipitation of 1:1.5 ice, fully stand overnight after mixing, 5000r/min, after taking the dissolving of precipitation pH8.0PBS after centrifugal 10min, lyophilizing, obtain Radix Ginseng crude protein.
(2), after the crude protein that obtained by acetone precipitation dissolves, filter through the defecator of 0.45 μm, be that 30 Kda are concentrated by ultrafiltration through membrane aperture, collect filter liquor, then the ultrafiltration through 10 KDa, collect molecular weight less than 10KDa effluent, lyophilizing, i.e. obtains highly purified ginseng polypeptide.
Embodiment 2:
(1) fresh ginseng 20g is taken, extract under the conditions of pH6.0 48 hours with 1:15 ratio with 0.01mol/lPBS, take supernatant adding volume ratio is the pre-cold acetone precipitation of 1:2.5 ice, fully stand overnight after mixing, 5000r/min, after taking the dissolving of precipitation pH6.0PBS after centrifugal 10min, lyophilizing, obtain Radix Ginseng crude protein.
(2) other operations are same as in Example 1.
Embodiment 1 compares with embodiment 2 ginseng polypeptide extract protein content, as shown in table 1 below:
Table 1
| Embodiment 1 | Embodiment 2 | |
| Protein content (%) | 35% | 42% |
Ginseng polypeptide Transparent handmade soap preparation method
Embodiment 3:
(1) formula components becomes to be grouped into each of percentage by weight: Petiolus Trachycarpi oil 20%；Oleum Cocois 10%；Oleum Ricini 12%；Sodium hydroxide 6%；Distilled water 24%；Ethanol 16%；Glycerol 9%；Sucrose 7%；Ginseng polypeptide 0.1%.
(2) according to the proportioning of step (1) by vegetable oil heated and stirred to 60 DEG C, it is slowly added to alkali, stir and within 25 minutes, complete saponification, add glycerol and stir 20 minutes, to gluey, add ethanol and stir 20 clocks, sucrose stirs 20 minutes, continues stirring and treats that temperature drops to less than 37 DEG C and adds ginseng polypeptide, and band bubble is wholly absent pours mould into, put into-20 DEG C of freezings 16 hours, put into 25 DEG C of maturations after taking-up and get final product.
Embodiment 4:
(1) formula components becomes to be grouped into each of percentage by weight: Petiolus Trachycarpi oil 16%；Oleum Cocois 13%；Oleum Ricini 10%；Sodium hydroxide 4%；Distilled water 24%；Ethanol 20%；Glycerol 11%；Sucrose 5%；Ginseng polypeptide 0.3%.
(2) according to the proportioning of step (1) by vegetable oil heated and stirred to 60 DEG C, it is slowly added to alkali, stir and within 25 minutes, complete saponification, add glycerol and stir 20 minutes, to gluey, add ethanol and stir 20 clocks, sucrose stirs 20 minutes, continues stirring and treats that temperature drops to less than 37 DEG C and adds ginseng polypeptide, and band bubble is wholly absent pours mould into, put into-20 DEG C of freezings 10 hours, put into 37 DEG C of maturations after taking-up and get final product.
Ginseng polypeptide Transparent handmade soap efficacy assessments
(1) the ginseng polypeptide Transparent handmade soap example moisture-keeping efficacy that embodiment 3 is prepared with embodiment 4 compares
Choose 50 volunteers, age is in 25-30 year, it is divided into two groups according to skin dryness, often organize 25 people, use embodiment 1 ginseng polypeptide Transparent handmade soap and embodiment 2 ginseng polypeptide Transparent handmade soap respectively, use 1 time the most respectively every day, use skinanalysis apparatus tracking and testing moisture of skin, after using 60 days, using effect is added up, and result is as shown in table 2:
Table 2
| Embodiment 1 | Embodiment 2 | |
| Good result | 46 | 47 |
| To no effect | 4 | 3 |
(2) the ginseng polypeptide Transparent handmade soap example that embodiment 3 is prepared with embodiment 4 is moistened effect and is compared
Choose 50 volunteers, age is in 30-35 year, it is divided into two groups according to collagen fiber degree contained in skin, often organize 25 people, use embodiment 1 ginseng polypeptide Transparent handmade soap and embodiment 2 ginseng polypeptide Transparent handmade soap respectively, use 1 time the most respectively every day, use skinanalysis apparatus tracking and testing collagen fibers of skin content, after using 60 days, using effect is added up, and result is as shown in table 3:
Table 3
| Embodiment 1 | Embodiment 2 | |
| Good result | 47 | 49 |
| To no effect | 3 | 1 |
Claims (2)
1. the preparation method of a ginseng polypeptide Transparent handmade soap, it is characterised in that specifically comprise the following steps that
(1) fresh ginseng 20g is taken, extract 12-48 hour under the conditions of pH5-9 with 1:5-1:20 ratio with 0.01mol/L PBS, take supernatant adding volume ratio is the pre-cold acetone precipitation of 1:1.0-3.0 ice, fully stands overnight after mixing, takes precipitation pH5-9,0.01mol/L after being centrifuged
After PBS dissolves, lyophilizing, obtain Radix Ginseng crude protein；
(2) after the crude protein obtained by acetone precipitation dissolves, filter through defecator, be that 30 KDa are concentrated by ultrafiltration through membrane aperture, collect filter liquor, then the ultrafiltration through 10 KDa, collect molecular weight and be less than 10KDa effluent, lyophilizing, i.e. obtain highly purified ginseng polypeptide；
(3) formula becomes to be grouped into each of percentage by weight: Petiolus Trachycarpi oil 15-25%；Oleum Cocois 5-15%；Oleum Ricini 10-15%；Alkali 3-8%；Distilled water 21-28%；Ethanol 10-16%；Glycerol 6-15%；Sucrose 5-10%；Ginseng polypeptide 0.1-1%, each component sum is 100%, by above proportioning by vegetable oil heated and stirred to 60 DEG C, it is slowly added to alkali, stir and complete saponification in 20-30 minute, add glycerol to stir 20-30 minute, to gluey, adding ethanol to stir 10-30 minute, sucrose stirs 10-30 minute, continues stirring and treats that temperature drops to less than 37 DEG C and adds ginseng polypeptide, treat that bubble is wholly absent and pour mould into, put into 4--20 DEG C freezing 4-24 hour, after taking-up, put into 20-40 DEG C, after taking-up, both obtain ginseng polypeptide Transparent handmade soap.
2. the ginseng polypeptide Transparent handmade soap prepared according to the preparation method of claim 1, it is characterised in that be mainly composed of ginseng polypeptide, vegetable oil, caustic alkali.
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| CN105002016A (en) * | 2015-06-29 | 2015-10-28 | 广西健宝石斛有限责任公司 | Production method of Dendrobium officinale polysaccharide handmade soap |
| CN107760493A (en) * | 2016-08-18 | 2018-03-06 | 广东中澔柏画健康药业有限公司 | It is a kind of to contribute to anti-oxidant, anti-aging soap of Chinese medicine preparation method |
| CN108285836A (en) * | 2017-01-07 | 2018-07-17 | 潮州市龙植馨生物科技实业有限公司 | A kind of plant polypeptide low molecule glue protein perfumed soap manufacturing method |
| CN107099406A (en) * | 2017-06-21 | 2017-08-29 | 广州市博真电子科技有限公司 | A kind of panax ginseng extractum oil soap and preparation method thereof |
| CN108277112B (en) * | 2018-03-23 | 2020-05-19 | 上海应用技术大学 | Acne-removing and beautifying handmade soap containing salicylic acid microcapsules and preparation method thereof |
| CN114569483A (en) * | 2022-02-23 | 2022-06-03 | 孙万亮 | Ginseng polypeptide extract, preparation method thereof and anti-ultraviolet whitening essence |
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| CN1057267A (en) * | 1990-06-12 | 1991-12-25 | 吉林大学 | The coproduction technique of ginseng polypeptide, polysaccharide, saponin |
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