CN1038037A - 浸有毒物滤饼的处理 - Google Patents
浸有毒物滤饼的处理 Download PDFInfo
- Publication number
- CN1038037A CN1038037A CN88108742A CN88108742A CN1038037A CN 1038037 A CN1038037 A CN 1038037A CN 88108742 A CN88108742 A CN 88108742A CN 88108742 A CN88108742 A CN 88108742A CN 1038037 A CN1038037 A CN 1038037A
- Authority
- CN
- China
- Prior art keywords
- filter cake
- poisonous substance
- glass
- matrix material
- glass matrix
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000012065 filter cake Substances 0.000 title claims abstract description 29
- 239000000126 substance Substances 0.000 title claims abstract description 25
- 231100000614 poison Toxicity 0.000 title claims abstract description 21
- 230000007096 poisonous effect Effects 0.000 title claims abstract description 21
- 239000011521 glass Substances 0.000 claims abstract description 31
- 238000000034 method Methods 0.000 claims abstract description 19
- 239000000203 mixture Substances 0.000 claims abstract description 18
- 239000011159 matrix material Substances 0.000 claims abstract description 16
- 239000012633 leachable Substances 0.000 claims abstract description 8
- AYRZLUSHOXJGKY-UHFFFAOYSA-N [bis(sulfanylidene)-$l^{5}-arsanyl]sulfanyl-bis(sulfanylidene)-$l^{5}-arsane Chemical compound S=[As](=S)S[As](=S)=S AYRZLUSHOXJGKY-UHFFFAOYSA-N 0.000 claims abstract description 7
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000001816 cooling Methods 0.000 claims abstract description 6
- 238000002386 leaching Methods 0.000 claims abstract description 5
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 3
- 239000000463 material Substances 0.000 claims description 13
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 7
- 239000000155 melt Substances 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 6
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 231100000331 toxic Toxicity 0.000 claims description 2
- 230000002588 toxic effect Effects 0.000 claims description 2
- 235000012839 cake mixes Nutrition 0.000 claims 3
- 235000013305 food Nutrition 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 6
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 6
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 3
- 235000011941 Tilia x europaea Nutrition 0.000 description 3
- 239000004571 lime Substances 0.000 description 3
- 238000007789 sealing Methods 0.000 description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 description 3
- 235000017550 sodium carbonate Nutrition 0.000 description 3
- 235000010344 sodium nitrate Nutrition 0.000 description 3
- 239000004317 sodium nitrate Substances 0.000 description 3
- 229910052785 arsenic Inorganic materials 0.000 description 2
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 238000005755 formation reaction Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 231100000481 chemical toxicant Toxicity 0.000 description 1
- 238000004710 electron pair approximation Methods 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229910000403 monosodium phosphate Inorganic materials 0.000 description 1
- 235000019799 monosodium phosphate Nutrition 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 description 1
- HUAUNKAZQWMVFY-UHFFFAOYSA-M sodium;oxocalcium;hydroxide Chemical compound [OH-].[Na+].[Ca]=O HUAUNKAZQWMVFY-UHFFFAOYSA-M 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/002—Use of waste materials, e.g. slags
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
- B09B3/00—Destroying solid waste or transforming solid waste into something useful or harmless
- B09B3/20—Agglomeration, binding or encapsulation of solid waste
- B09B3/25—Agglomeration, binding or encapsulation of solid waste using mineral binders or matrix
- B09B3/29—Agglomeration, binding or encapsulation of solid waste using mineral binders or matrix involving a melting or softening step
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S422/00—Chemical apparatus and process disinfecting, deodorizing, preserving, or sterilizing
- Y10S422/90—Decreasing pollution or environmental impact
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Processing Of Solid Wastes (AREA)
- Glass Compositions (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
一种由玻璃母体物质构成，并浸渍有一般可沥滤
的毒物的滤饼，可以最好与至少另一种玻璃母体物质
一起，加热到足够的高温，以形成一种熔融组合物，冷
却后，固化而成玻璃。一般可沥滤的毒物固定在玻璃
中，使其基本上难以沥滤，从而可符合环境标准而排
放，如通过填埋技术排入。该方法可用来处理从制备
食品级磷酸过程中所得到浸有五硫化二砷的滤饼。
Description
本发明涉及的是浸有化学毒物的滤饼的处理方法，以把毒物固定或密封在滤饼中。
现有多种化工过程采用滤饼材料，如硅藻土，从液态化学物流中过滤不需要的物质，如毒物。当过滤操作完成后，过滤的固体残渣构成了滤饼，它浸渍有从滤液中除去的物质。当在滤饼中含有可沥滤的毒物时，倾倒浸过的滤饼(如，填埋)将因毒物的沥滤而带来环境(污染)问题。
本发明的方法是关于将一般可沥滤的毒物有效地固定在由玻璃母体物质构成的滤饼材料中。它包括将含有一般可沥滤的毒物的滤饼，最好同至少一种其它玻璃母体物质一起加热，从而形成一含有毒物的熔融物质。得到的熔融物质固化形成玻璃，将毒物密封或固定在内，使之基本难以从中沥滤出来。本文所用的术语“玻璃母体”是指一种或多种这样的物质，在它加热(最好同至少一种其它“玻璃母体”物质一起)到足够的高温后，会形成一熔融组合物，一旦冷却，就变成一种玻璃组合物。
本发明可广泛地适用于固定或密封在特定一类滤饼介质中(即滤饼由一般可沥滤的毒物。玻璃母体物质，如硅质材料象硅藻土等构成)它特别适用于在热法制食品级磷酸工艺过程中，用过滤除去五硫化二砷。
根据本发明，最好将由玻璃母体物质如硅藻土构成的滤饼，与一种或几种相容的玻璃母体物质混合(如，这些物质与含氧化硅的物质一起加热时形成玻璃)，以形成一熔融组合物，冷却后形成玻璃从而密封毒物。可与硅质滤饼一起使用的相容的玻璃母体物质如纯碱，石灰和氧化铝。当然，对由玻璃母体物质构成的滤饼，若在没有任何其他物质存在下加热，仍将形成一熔融组合物，它一旦冷却，即形成玻璃组合物，这种情形，也包括在本发明的范围之内。玻璃母体物质的相对含量，以及加热温度，均可在较大的范围内变动，对于玻璃加工工艺，只要形成的熔融组合物一旦冷却，固化而成玻状物质，从而密封或固定一般可沥滤的毒物，使其基本上难以沥滤即可。根据需要，所加热的混合物中可添加一些助剂，以帮助在形成的最终玻璃物质中完成密封毒物的过程。例如，业已发现，若滤饼中的毒物是五硫化二砷，则添加约1％的硝酸钠，使硫化物氧化到其难挥发的+5价氧化态(As2S5)，将是有益的。
以下的实施例进一步说明本发明的方法。
实施例1
将水洗后，烘干后，浸有五硫化二砷的硅藻土滤饼(37g)与纯碱(24g)，熟石灰(13g)，脱水氧化铝(2g)，以及硝酸钠(1g)混合。再加入足够的水使混合物湿化，并控制可能的起尘。然后使湿混合物彻底混合。将一部分形成的混合物放入一坩锅，插入一熔化炉，将炉温升高到1450°-1500℃，保持10分钟。将坩锅中的熔融物倒入一不锈钢皿中，使其固化成一玻璃组合物：玻璃呈透明的浅绿色。
将固体玻璃破碎进行特定的分析试验：毒性特性沥滤过程(TCLP)以及EP毒性测试。TCLP测试可见联邦注册登记，86年11月7日。第40643-40654页描述。 EP毒性测试EPA方法1310，40CFR261.24。TCLP和EP测试的沥滤液中均未发现可检测到的砷。
实施例2
将硅藻土助滤剂(35g)，五硫化二砷(2g)，磷酸二氢钠(6.09)，碳酸钠(9.5g)，熟石灰(6.5g)，脱水氧化铝(3g)，硝酸钠(1g)，和活性炭(0.5g)混合。加入足够量的水使混合物湿化并控制其起尘，使形成的混合物彻底混合。再把得到的混合物倒入一坩锅中，按实施1所述方法加热。形成的玻状组合物呈黑色，不透明。TCLP测试其沥滤液中未发现有可检测到的砷。
前述的实施例仅用来说明本发明的某些实施方案，但不能理解为是对本发明的限制。本发明的保护范围应依下述权利要求而定。
Claims (9)
1.一种将一般可沥滤的毒物固定在由玻璃母体物质构成的滤饼中，从而使毒物基本上难以从中沥滤的方法，其特征在于将含有毒物的滤饼加热，形成一熔融组合物，冷却后，形成一含毒物的玻璃。
2.根据权利要求1的方法，其特征在于滤饼由硅质材料构成。
3.根据权利要求2的方法，其特征在于滤饼由硅藻土构成。
4.根据权利要求1的方法，其特征在于滤饼由硅质材料构成，毒物是五硫化二砷。
5.根据权利要求4的方法，其特征在于滤饼由硅藻土构成。
6.根据权利要求4的方法，其特征在于滤饼和毒物是在过滤含所述的五硫化二砷的磷酸过程中得到的。
7.根据权利要求1的方法，其特征在于加热之前，滤饼与至少另一种玻璃母体物质混合。
8.根据权利要求2的方法，其特征在于加热之前，滤饼与至少一种其它玻璃母体物质混合。
9.根据权利要求6的方法，其特征在于在加热之前，滤饼与至少另一种玻璃母体物质混合。
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US07/111,828 US4820325A (en) | 1987-10-22 | 1987-10-22 | Treatment of toxicant-impregnated filter cake |
| US07/111,828 | 1987-10-22 | ||
| US111,828 | 1987-10-22 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1038037A true CN1038037A (zh) | 1989-12-20 |
| CN1017503B CN1017503B (zh) | 1992-07-22 |
Family
ID=22340653
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN88108742A Expired CN1017503B (zh) | 1987-10-22 | 1988-10-22 | 浸有五硫化二砷毒物的滤饼的处理方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US4820325A (zh) |
| EP (1) | EP0313321B1 (zh) |
| CN (1) | CN1017503B (zh) |
| DE (1) | DE3886344T2 (zh) |
| DK (1) | DK589688A (zh) |
| MA (1) | MA21419A1 (zh) |
| MX (1) | MX165650B (zh) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102349685A (zh) * | 2011-07-26 | 2012-02-15 | 许盛英 | 球形茶叶防潮脱氧保鲜剂 |
| CN103691314A (zh) * | 2013-12-30 | 2014-04-02 | 广州优克日用品有限公司 | 一种除味组合物及其应用 |
| CN104792778A (zh) * | 2015-03-25 | 2015-07-22 | 广东广益科技实业有限公司 | 一种氧指示剂制备方法 |
| CN105561744A (zh) * | 2016-01-26 | 2016-05-11 | 张云 | 长效脱氧组合干燥剂配方片材及其制造方法 |
| CN106508977A (zh) * | 2016-09-07 | 2017-03-22 | 马鞍山纽盟知识产权管理服务有限公司 | 一种高效防潮除味剂 |
| CN106616201A (zh) * | 2016-11-22 | 2017-05-10 | 南京航天天宁新材料科技有限公司 | 一种无水抑氢型除氧剂 |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4988376A (en) * | 1989-08-02 | 1991-01-29 | Western Research Institute | Glassification of lead and silica solid waste |
| US5067978A (en) * | 1989-08-24 | 1991-11-26 | Fowler Benjamin P | Method for the removal of lead from waste products |
| EP0448174A1 (en) * | 1990-03-21 | 1991-09-25 | Van Eggelen, Cornelis Theodorus Petrus | Method of processing waste materials |
| US5340372A (en) * | 1991-08-07 | 1994-08-23 | Pedro Buarque de Macedo | Process for vitrifying asbestos containing waste, infectious waste, toxic materials and radioactive waste |
| US5245120A (en) * | 1991-12-27 | 1993-09-14 | Physical Sciences, Inc. | Process for treating metal-contaminated materials |
| US5434333A (en) * | 1992-09-18 | 1995-07-18 | The United States Of America As Represented By The United States Department Of Energy | Method for treating materials for solidification |
| US5369062A (en) * | 1993-08-20 | 1994-11-29 | The Research Foundation Of State University Of Ny | Process for producing ceramic glass composition |
| US5508236A (en) * | 1993-08-20 | 1996-04-16 | The Research Foundation Of State University Of New York | Ceramic glass composition |
| US5556447A (en) * | 1995-01-23 | 1996-09-17 | Physical Sciences, Inc. | Process for treating metal-contaminated materials |
| US5678236A (en) * | 1996-01-23 | 1997-10-14 | Pedro Buarque De Macedo | Method and apparatus for eliminating volatiles or airborne entrainments when vitrifying radioactive and/or hazardous waste |
| US6145343A (en) * | 1998-05-02 | 2000-11-14 | Westinghouse Savannah River Company | Low melting high lithia glass compositions and methods |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3007882A (en) * | 1957-12-12 | 1961-11-07 | Lach Vladimir | Method of producing shaped bodies of ceramic material protective against ionising radiation |
| DE2244085A1 (de) * | 1972-09-08 | 1974-03-14 | Kuehn Martin Prof Dr Phil Nat | Verfahren zur verwertung und unschaedlichmachung von als haertesalze gebrauchten rueckstaenden von alkalicyaniden |
| JPS49115986A (zh) * | 1973-03-10 | 1974-11-06 | ||
| US4020004A (en) * | 1975-11-21 | 1977-04-26 | The United States Of America As Represented By The United States Energy Research And Development Administration | Conversion of radioactive ferrocyanide compounds to immobile glasses |
| DE2830897A1 (de) * | 1977-07-22 | 1979-02-01 | Pelt & Hooykaas | Verfahren fuer die behandlung von aus mehreren stoffen zusammengesetzten, nassen filterrueckstaenden |
| DE2845916C2 (de) * | 1978-10-21 | 1980-06-12 | Riedel-De Haen Ag, 3016 Seelze | Umweltentlastende Verwertung von verbrauchten wäßrigen Kobalt/Manganacetat-Katalysatorlösungen |
| FR2490113B1 (fr) * | 1980-09-16 | 1986-04-25 | Cernesson Martine | Utilisation des rejets des usines de traitement de surface par electrolyse des metaux, comme matieres premieres dans les industries des produits vitrifies |
| GB8331031D0 (en) * | 1983-11-21 | 1983-12-29 | Roberts D | Vitrification of asbestos waste |
| NL8403501A (nl) * | 1984-11-15 | 1986-06-02 | Pelt & Hooykaas | Werkwijze voor het omzetten in onschadelijke vorm van bij chemische of fysische werkwijzen vrijkomende deeltjes door mengen met een gesmolten silicaathoudend materiaal alsmede gevormd materiaal. |
-
1987
- 1987-10-22 US US07/111,828 patent/US4820325A/en not_active Expired - Lifetime
-
1988
- 1988-10-19 DE DE88309790T patent/DE3886344T2/de not_active Expired - Fee Related
- 1988-10-19 EP EP88309790A patent/EP0313321B1/en not_active Expired - Lifetime
- 1988-10-21 MX MX013502A patent/MX165650B/es unknown
- 1988-10-21 DK DK589688A patent/DK589688A/da not_active Application Discontinuation
- 1988-10-22 CN CN88108742A patent/CN1017503B/zh not_active Expired
- 1988-10-26 MA MA21660A patent/MA21419A1/fr unknown
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102349685A (zh) * | 2011-07-26 | 2012-02-15 | 许盛英 | 球形茶叶防潮脱氧保鲜剂 |
| CN103691314A (zh) * | 2013-12-30 | 2014-04-02 | 广州优克日用品有限公司 | 一种除味组合物及其应用 |
| CN103691314B (zh) * | 2013-12-30 | 2016-11-23 | 广州优克日用品有限公司 | 一种除味组合物及其应用 |
| CN104792778A (zh) * | 2015-03-25 | 2015-07-22 | 广东广益科技实业有限公司 | 一种氧指示剂制备方法 |
| CN104792778B (zh) * | 2015-03-25 | 2018-02-27 | 广东广益科技实业有限公司 | 一种氧指示剂制备方法 |
| CN105561744A (zh) * | 2016-01-26 | 2016-05-11 | 张云 | 长效脱氧组合干燥剂配方片材及其制造方法 |
| CN105561744B (zh) * | 2016-01-26 | 2018-01-23 | 张云 | 长效脱氧组合干燥剂配方片材及其制造方法 |
| CN106508977A (zh) * | 2016-09-07 | 2017-03-22 | 马鞍山纽盟知识产权管理服务有限公司 | 一种高效防潮除味剂 |
| CN106616201A (zh) * | 2016-11-22 | 2017-05-10 | 南京航天天宁新材料科技有限公司 | 一种无水抑氢型除氧剂 |
Also Published As
| Publication number | Publication date |
|---|---|
| US4820325A (en) | 1989-04-11 |
| MA21419A1 (fr) | 1989-07-01 |
| CN1017503B (zh) | 1992-07-22 |
| DE3886344T2 (de) | 1994-05-05 |
| EP0313321A1 (en) | 1989-04-26 |
| DE3886344D1 (de) | 1994-01-27 |
| MX165650B (es) | 1992-11-26 |
| DK589688D0 (da) | 1988-10-21 |
| EP0313321B1 (en) | 1993-12-15 |
| DK589688A (da) | 1989-04-23 |
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