CN103783228B - Production method for folium viticis negundo caffeine - Google Patents
Production method for folium viticis negundo caffeine Download PDFInfo
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- CN103783228B CN103783228B CN201410062390.5A CN201410062390A CN103783228B CN 103783228 B CN103783228 B CN 103783228B CN 201410062390 A CN201410062390 A CN 201410062390A CN 103783228 B CN103783228 B CN 103783228B
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Abstract
The invention discloses a production method for folium viticis negundo caffeine. The folium viticis negundo caffeine is produced by the following steps: adopting folium viticis negundo as a raw material, preparing the raw material, carrying out color protection treatment, carrying out heat extraction, carrying out ultrasonic extraction, crushing, mixing, lyophilizing and drying, classifying and packaging and the like. The folium viticis negundo caffeine produced by the method takes the widely-existing folium viticis negundo as the raw material and the production cost is reduced; the heat extraction treatment and the ultrasonic extraction treatment are carried out so that active matters of the raw material can be sufficiently kept; a lyophilizing and drying method is adopted so that the loss of nutrient substances is reduced and the utilization rate of the raw material is reduced; the finished-product caffeine has the health-care effects of relieving exterior syndrome and clearing heat, draining dampness and detoxifying and the like.
Description
Technical field
The present invention relates to a kind of preparation method of caffein, especially relate to a kind of preparation method of Negundo Chastetree Leaf caffein.
Background technology
Negundo Chastetree Leaf is the leaf of Verenaceae Vitex five-leaved chaste tree, containing casticin, cyanidenon-7-glycoside, tetrahydroxy-methoxy flavone alpha-D-glucose glucoside, 5-hydroxyl-3,6,7,3', 4'-pentamethoxyl flavones, P-hydroxybenzoic acid, 5-hydroxyl iso-phthalic acid, PCA etc., also containing nishindine and vitamin C etc." south of the Five Ridges gather medicinal herbs record " is recorded: " control children's five infantile malnutrition due to digestive disturbances or intestinalparasites.Decoct soup bath body, heat radiation, the sore that disappears swells and ache, and rice stir-fry hardening drinks it, and antiemetic rushes down." there is heat-clearing of inducing sweat, eliminating damp, detoxifying, cure cold, heatstroke, vomits and diarrhoea, dysentery, malaria, jaundice, rheumatism, treating swelling and pain by traumatic injury, the effect of sore carbuncle mange.At present, the processing and utilization of Negundo Chastetree Leaf is also in gather as maturation and is used as medicine the stage, and Negundo Chastetree Leaf is processed into caffein, has no relevant report and Related product listing.
Summary of the invention
For vacancy and the consumption demand of existing market, the technical problem to be solved in the present invention is to provide a kind of preparation method of Negundo Chastetree Leaf caffein, this method process stabilizing, simple to operate, be easy to grasp, free of contamination Negundo Chastetree Leaf natural resources is processed into and drinks drink easily, not only enrich drink kind, and improve the economic worth of Negundo Chastetree Leaf.
The present invention solves the technical scheme that its technical problem takes: a kind of preparation method of Negundo Chastetree Leaf caffein, is characterized in that: adopt following steps:
A, raw material prepare: pluck fresh, leaf age at the Negundo Chastetree Leaf of 15-20 days, clean water tender leaf surface, is filtered dry moisture, the bar of growth 1-2cm, wide 0.4-0.6cm, for subsequent use;
B, color retention: Negundo Chastetree Leaf bar is put into the citric acid solution that concentration is 0.06-0.1%, soak 2-3 hour, soaks and terminate rear clear water rinsing, drain away the water, by color retention, original color and luster of tender leaf can not only be kept, the active component in sampling tea can also be improved into;
C, extraction heat: be placed in weight 3-4 water doubly decoct protecting the Negundo Chastetree Leaf bar after look, and add the sodium ascorbate of Negundo Chastetree Leaf bar weight 0.1-0.3%, extraction temperature controls as 80-90 DEG C, time controling is 20-30min, repeat to decoct 3-4 time, decoction liquor is mixed, filters obtained extraction heat liquid and Negundo Chastetree Leaf first slag;
D, ultrasonic wave extract: send in ultrasonic extraction kettle by the Negundo Chastetree Leaf first slag after being filtered dry, and add Negundo Chastetree Leaf first slag weight 2-3 pure water doubly, setting ultrasonic frequency 40-50kHz, keep extracting pot constant temperature 60-70 DEG C, through extracting 30-40min, releasing and extract juice and with centrifugal filtration, obtain extract and Negundo Chastetree Leaf slag, extracted twice, fully can retain the nutritional labeling in raw material;
E, pulverizing: the Negundo Chastetree Leaf slag after being filtered dry is carried out ultra-fine grinding process, granularity is 180-200 μm, obtained Negundo Chastetree Leaf powder;
F, mixing: heat-obtaining extract 55-70 weight portion, extract 20-30 weight portion, Negundo Chastetree Leaf powder 10-15 weight portion, fully mix, obtained mixed liquor;
G, lyophilization: by mixed liquor under-20 ~-15 DEG C of conditions, freezing 4-6 hour, presses 6-8kg/m by the mixed liquor after freezing in useful load
2, operating pressure 40-60Pa, resolve pressure 20-30Pa, temperature 35-40 DEG C condition under dry, obtained Negundo Chastetree Leaf caffein, lyophilization can reduce the infringement to raw material nutriment, reduces the loss of nutriment;
H, packaging: Negundo Chastetree Leaf caffein food-grade packaging material are packed, enters in aeration-drying environment and store.
Beneficial effect: this method make Negundo Chastetree Leaf caffein with the Negundo Chastetree Leaf extensively existed for raw material, reduce production cost, by extraction heat and ultrasonic wave extraction process, fully can retain the active material of raw material, adopt the method for lyophilization, decrease the loss of nutriment, improve the utilization rate of raw material, finished product caffein has heat-clearing of inducing sweat, the health-care efficacies such as eliminating damp, detoxifying.
Detailed description of the invention
Embodiment 1: a kind of preparation method of Negundo Chastetree Leaf caffein, is characterized in that: adopt following steps:
A, raw material prepare: pluck fresh, leaf age at the Negundo Chastetree Leaf of 15 days, clean water tender leaf surface, is filtered dry moisture, the bar of growth 1cm, wide 0.4cm, for subsequent use;
B, color retention: Negundo Chastetree Leaf bar is put into the citric acid solution that concentration is 0.06%, soak 3 hours, soaks and terminate rear clear water rinsing, drain away the water, by color retention, original color and luster of tender leaf can not only be kept, the active component in sampling tea can also be improved into;
C, extraction heat: 5kg is protected the Negundo Chastetree Leaf bar after look and be placed in the water of 15kg and decoct, and add the sodium ascorbate of 0.005kg, it is 80 DEG C that extraction temperature controls, time controling is 30min, repeat decoction 4 times, decoction liquor is mixed, filter obtained extraction heat liquid and Negundo Chastetree Leaf first slag;
D, ultrasonic wave extract: the Negundo Chastetree Leaf first slag after being filtered dry by 2kg is sent in ultrasonic extraction kettle, and add the pure water of 4kg, setting ultrasonic frequency 40kHz, keep extracting pot constant temperature 70 DEG C, through extracting 30min, releasing and extract juice and with centrifugal filtration, obtain extract and Negundo Chastetree Leaf slag, extracted twice, fully can retain the nutritional labeling in raw material;
E, pulverizing: the Negundo Chastetree Leaf slag after being filtered dry is carried out ultra-fine grinding process, granularity is 180 μm, obtained Negundo Chastetree Leaf powder;
F, mixing: heat-obtaining extract 6kg, extract 3kg, Negundo Chastetree Leaf powder 1kg, fully mix, obtained mixed liquor;
G, lyophilization: by mixed liquor under-20 DEG C of conditions, freezing 4 hours, press 6kg/m by the mixed liquor after freezing in useful load
2, operating pressure 40Pa, resolve pressure 20Pa, temperature 40 DEG C condition under dry, obtained Negundo Chastetree Leaf caffein, lyophilization can reduce the infringement to raw material nutriment, reduces the loss of nutriment;
H, packaging: Negundo Chastetree Leaf caffein food-grade packaging material are packed, enters in aeration-drying environment and store.
Embodiment 2: a kind of preparation method of Negundo Chastetree Leaf caffein, is characterized in that: adopt following steps:
A, raw material prepare: pluck fresh, leaf age at Negundo Chastetree Leaf, buckwheat leaf, the feed with paper-mulberry leaf of 18 days, clean water tender leaf surface, is filtered dry moisture, the bar of growth 1.5cm, wide 0.5cm, for subsequent use;
B, color retention: after 4kg Negundo Chastetree Leaf bar, 1kg buckwheat leaf bar, 1kg feed with paper-mulberry leaf bar are mixed, obtained raw material leaf, put into the citric acid solution that concentration is 0.08%, soak 2.5 hours, immersion terminates rear clear water rinsing, drains away the water, passes through color retention, original color and luster of tender leaf can not only be kept, the active component in sampling tea can also be improved into;
C, extraction heat: 4kg is protected the raw material leaf bar after look and be placed in the water of 14kg and decoct, and add the sodium ascorbate of 0.008kg, it is 85 DEG C that extraction temperature controls, time controling is 25min, repeat decoction 4 times, decoction liquor is mixed, filter obtained extraction heat liquid and raw material leaf first slag;
D, ultrasonic wave extract: the raw material leaf first slag after being filtered dry by 2kg is sent in ultrasonic extraction kettle, and add the pure water of 5kg, setting ultrasonic frequency 45kHz, keep extracting pot constant temperature 65 DEG C, through extracting 35min, releasing and extract juice and with centrifugal filtration, obtain extract and raw material leaf slag, extracted twice, fully can retain the nutritional labeling in raw material;
E, pulverizing: the raw material leaf slag after being filtered dry is carried out ultra-fine grinding process, and granularity is 190 μm, obtained raw material leaf powder;
F, mixing: heat-obtaining extract 5.5kg, extract 3kg, Negundo Chastetree Leaf powder 1.2kg, HFCS 0.3kg, fully mix, obtained mixed liquor;
G, lyophilization: by mixed liquor under-18 DEG C of conditions, freezing 5 hours, press 7kg/m by the mixed liquor after freezing in useful load
2, operating pressure 50Pa, resolve pressure 25Pa, temperature 38 DEG C condition under dry, obtained Negundo Chastetree Leaf caffein, lyophilization can reduce the infringement to raw material nutriment, reduces the loss of nutriment;
H, packaging: Negundo Chastetree Leaf caffein food-grade packaging material are packed, enters in aeration-drying environment and store.
Embodiment 3: a kind of preparation method of Negundo Chastetree Leaf caffein, is characterized in that: adopt following steps:
A, raw material prepare: pluck fresh, leaf age 20 days Negundo Chastetree Leaf, loguat leaf, mulberry leaves, honeysuckle, clean water tender leaf surface, is filtered dry moisture, the bar of growth 2cm, wide 0.6cm, for subsequent use;
B, color retention: after the honeysuckle of 5kg Negundo Chastetree Leaf bar, 0.5kg loguat leaf bar, 1kg mulberry leaves bar, 0.5kg is mixed, obtained raw material leaf, put into the vitamin c solution that concentration is 0.1%, soak 2 hours, immersion terminates rear clear water rinsing, drains away the water, passes through color retention, original color and luster of tender leaf can not only be kept, the active component in sampling tea can also be improved into;
C, extraction heat: 5kg is protected the raw material leaf bar after look and be placed in the water of 20kg and decoct, and add the sodium ascorbate of 0.015kg, it is 90 DEG C that extraction temperature controls, time controling is 20min, repeat decoction 3 times, decoction liquor is mixed, filter obtained extraction heat liquid and raw material leaf first slag;
D, ultrasonic wave extract: the raw material leaf first slag after being filtered dry by 2kg is sent in ultrasonic extraction kettle, and add the pure water of 6kg, setting ultrasonic frequency 50kHz, keep extracting pot constant temperature 70 DEG C, through extracting 30min, releasing and extract juice and with centrifugal filtration, obtain extract and raw material leaf slag, extracted twice, fully can retain the nutritional labeling in raw material;
E, pulverizing: the raw material leaf slag after being filtered dry is carried out ultra-fine grinding process, and granularity is 200 μm, obtained Negundo Chastetree Leaf powder;
F, mixing: heat-obtaining extract 5.5kg, extract 2kg, Negundo Chastetree Leaf powder 1kg, kudzuvine root juice 0.5kg, honey 0.5kg, Sucus Phyllanthi 0.3kg, Snakegourd Fruit juice 0.2kg, fully mix, obtained mixed liquor;
G, lyophilization: by mixed liquor under-15 DEG C of conditions, freezing 6 hours, press 8kg/m by the mixed liquor after freezing in useful load
2, operating pressure 60Pa, resolve pressure 30Pa, temperature 35 DEG C condition under dry, obtained Negundo Chastetree Leaf caffein, lyophilization can reduce the infringement to raw material nutriment, reduces the loss of nutriment;
H, packaging: Negundo Chastetree Leaf caffein food-grade packaging material are packed, enters in aeration-drying environment and store.
The part that the present invention does not relate to prior art that maybe can adopt all same as the prior art is realized.
Claims (1)
1. a preparation method for Negundo Chastetree Leaf caffein, is characterized in that: adopt following steps:
A, raw material prepare: pluck fresh, leaf age at the Negundo Chastetree Leaf of 15-20 days, clean water tender leaf surface, is filtered dry moisture, the bar of growth 1-2cm, wide 0.4-0.6cm, for subsequent use;
B, color retention: Negundo Chastetree Leaf bar is put into the citric acid solution that concentration is 0.06-0.1%, soak 2-3 hour, soaks and terminate rear clear water rinsing, drain away the water;
C, extraction heat: be placed in weight 3-4 water doubly decoct protecting the Negundo Chastetree Leaf bar after look, and add the sodium ascorbate of Negundo Chastetree Leaf bar weight 0.1-0.3%, extraction temperature controls as 80-90 DEG C, time controling is 20-30min, repeat to decoct 3-4 time, decoction liquor is mixed, filters obtained extraction heat liquid and Negundo Chastetree Leaf first slag;
D, ultrasonic wave extract: send in ultrasonic extraction kettle by the Negundo Chastetree Leaf first slag after being filtered dry, and add Negundo Chastetree Leaf first slag weight 2-3 pure water doubly, setting ultrasonic frequency 40-50kHz, keep extracting pot constant temperature 60-70 DEG C, through extracting 30-40min, release and extract juice and with centrifugal filtration, obtain extract and Negundo Chastetree Leaf slag;
E, pulverizing: the Negundo Chastetree Leaf slag after being filtered dry is carried out ultra-fine grinding process, granularity is 180-200 μm, obtained Negundo Chastetree Leaf powder;
F, mixing: heat-obtaining extract 55-70 weight portion, extract 20-30 weight portion, Negundo Chastetree Leaf powder 10-15 weight portion, fully mix, obtained mixed liquor;
G, lyophilization: by mixed liquor under-20 ~-15 DEG C of conditions, freezing 4-6 hour, presses 6-8kg/m by the mixed liquor after freezing in useful load
2, operating pressure 40-60Pa, resolve pressure 20-30Pa, temperature 35-40 DEG C condition under dry, obtained Negundo Chastetree Leaf caffein;
H, packaging: Negundo Chastetree Leaf caffein food-grade packaging material are packed, enters in aeration-drying environment and store.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410762195.3A CN104365951B (en) | 2014-02-22 | 2014-02-22 | A kind of preparation method of Negundo Chastetree Leaf caffein |
| CN201410062390.5A CN103783228B (en) | 2014-02-22 | 2014-02-22 | Production method for folium viticis negundo caffeine |
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| CN201410062390.5A CN103783228B (en) | 2014-02-22 | 2014-02-22 | Production method for folium viticis negundo caffeine |
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| CN201410762195.3A Division CN104365951B (en) | 2014-02-22 | 2014-02-22 | A kind of preparation method of Negundo Chastetree Leaf caffein |
| CN201410762194.9A Division CN104381548A (en) | 2014-02-22 | 2014-02-22 | Preparation method of vitex negundo leaf caffeine |
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| CN104605110A (en) * | 2015-02-22 | 2015-05-13 | 彭常安 | Preparation method of mulgedium sibiricum solid tea tablets |
| CN105326049A (en) * | 2015-09-24 | 2016-02-17 | 李琪 | Processing method of rubus rosaefolius smith-pomegranate seed nutritional powder |
| CN105533005A (en) * | 2015-12-13 | 2016-05-04 | 李春生 | Moringa oleifera and chili double-leaf tea essence production technology |
| CN105815703A (en) * | 2016-03-21 | 2016-08-03 | 张俊辉 | Method for processing trichosanthes peel, cortex albiziae and hawthorn fruit healthcare powder |
| CN106070862A (en) * | 2016-06-08 | 2016-11-09 | 彭常安 | A kind of preparation method of the celestial close illiteracy caffein of phoenix |
| CN105994846A (en) * | 2016-06-30 | 2016-10-12 | 余林岚 | Processing method of Chinese holly leaf compound tea powder |
| CN105994845A (en) * | 2016-06-30 | 2016-10-12 | 程龙凤 | Production method of matrimony vine health tea powder |
| CN108967615A (en) * | 2018-08-09 | 2018-12-11 | 陈建辉 | A kind of herbal tea product and its preparation method and application |
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| CN102228565B (en) * | 2011-05-13 | 2013-05-15 | 潮州市泽润制药有限公司 | Preparation method and application of Vitex agnuscastus extract |
| CN103571613A (en) * | 2012-08-06 | 2014-02-12 | 湖北大自然农业实业有限公司 | Preparation method of vitex negundo linn volatile oil |
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Address after: 214000 Jiangsu Province, Wuxi City Lake Ehu town Xishan District Road No. 6 Patentee after: Peng Changan Address before: Kangfulu Jinghu District 241000 Anhui city of Wuhu province No. 111 7-106 Patentee before: Peng Changan |
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Effective date of registration: 20220106 Address after: 518000 room 704, building 5, Fulian garden, 5011 Hongli Road, Futian District, Shenzhen City, Guangdong Province Patentee after: Ruan Shaoping Address before: 214000 No. 6, e Hu Road, Xishan, Wuxi, Jiangsu Patentee before: Peng Changan |