CN103757889B - Finishing agent of a kind of resisted shrinkage ANTIPILLING and preparation method thereof - Google Patents

Finishing agent of a kind of resisted shrinkage ANTIPILLING and preparation method thereof Download PDF

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Publication number
CN103757889B
CN103757889B CN201310750885.2A CN201310750885A CN103757889B CN 103757889 B CN103757889 B CN 103757889B CN 201310750885 A CN201310750885 A CN 201310750885A CN 103757889 B CN103757889 B CN 103757889B
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parts
finishing agent
antipilling
preparation
resisted shrinkage
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CN103757889A (en
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张德轩
左冬华
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Wujiang Dingneng textile finishing Co., Ltd
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SUZHOU XUANDE TEXTILE SCIENCE & TECHNOLOGY Co Ltd
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Abstract

Finishing agent of a kind of resisted shrinkage ANTIPILLING and preparation method thereof, the finishing agent of resisted shrinkage ANTIPILLING is made up of according to weight ratio following composition: petroleum sodium sulfonate is 4 ~ 6 parts, polypropylene glycol diglycidyl ether is 1 ~ 2 part, alanine is 3 ~ 5 parts, dioctadecyl dimethyl ammonium chloride is 2 ~ 3 parts, amylalcohol is 7 ~ 8 parts, potassium phosphate is 2 ~ 3 parts, sodium sulphate is 1 ~ 2 part, water is 230 ~ 240 parts.Carried out by the compositing formula of finishing agent of the present invention mixing, the step such as stirring obtains finishing agent, the finishing agent prepared can be used for arranging cotton clothes, and cotton clothes can be made to possess good resisted shrinkage and the performance of ANTIPILLING.

Description

Finishing agent of a kind of resisted shrinkage ANTIPILLING and preparation method thereof
Technical field
The present invention relates to a kind of finishing agent of clothing and the preparation method of finishing agent thereof, particularly relate to and a kind of there is resisted shrinkage, the clothing finishing agent of anti-pilling property and the preparation method of finishing agent.
Background technology
Conventional clothing, after repeatedly being cleaned, all can have the shrink phenomenon of part to produce.The reason causing clothing to shrink has a variety of, and the fiber of such as clothing own wrapping phenomena can occur after repeatedly cleaning, and also has certain metaboly simultaneously.Some clothing arranges without the finishing agent of special resisted shrinkage, therefore has certain shrink phenomenon and occurs.If cotton dress is in the process of dress, too much rubs with the external world, after the time is long, also can produce very serious pilling effect.Pilling effect affects the attractive in appearance of fabric very much, reduces the pilling effect of fabric after repeatedly rubbing, also extremely important.In sum, the performance improving the resisted shrinkage of clothing and ANTIPILLING is very necessary.
Summary of the invention
The technical problem solved: common clothing does not have the performance of good resisted shrinkage and ANTIPILLING, the problem that clothing can significantly shrink after repeatedly cleaning, pilling effect is serious.
Technical scheme: the finishing agent that the invention discloses a kind of resisted shrinkage ANTIPILLING, the finishing agent of resisted shrinkage ANTIPILLING is made up of according to weight ratio following composition: petroleum sodium sulfonate is 4 ~ 6 parts, polypropylene glycol diglycidyl ether is 1 ~ 2 part, alanine is 3 ~ 5 parts, dioctadecyl dimethyl ammonium chloride is 2 ~ 3 parts, amylalcohol is 7 ~ 8 parts, potassium phosphate is 2 ~ 3 parts, sodium sulphate is 1 ~ 2 part, water is 230 ~ 240 parts.
A kind of preparation method of finishing agent of resisted shrinkage ANTIPILLING, preparation method comprises the following steps: (1) gets that petroleum sodium sulfonate is 4 ~ 6 parts, polypropylene glycol diglycidyl ether is 1 ~ 2 part, dioctadecyl dimethyl ammonium chloride is 2 ~ 3 parts, undertaken mixing and stirring by after three kinds of composition heating, mix rear for subsequent use; (2) water intaking is 230 ~ 240 parts, then adds that alanine is 3 ~ 5 parts, amylalcohol is 7 ~ 8 parts, potassium phosphate is 2 ~ 3 parts, sodium sulphate is 1 ~ 2 part, alanine, amylalcohol, potassium sulfate, sodium sulphate water is uniformly dissolved; (3) added in the aqueous solution in step (2) by the mixed liquor prepared in step (1), stir with mechanical agitation oar, speed of agitator is 200 ~ 250rpm, stirs; (4) finally finishing agent is loaded in hermetically sealed can, preserve.
Beneficial effect: after being arranged with dressing liquid of the present invention by cotton clothes, cotton clothes only has 0.2% to 0.5% at washing 20 post-shrinkage ratios, and the ANTIPILLING grade of cotton clothes is 4 to 5 grades, has good resisted shrinkage and the performance of ANTIPILLING.
Detailed description of the invention
Embodiment 1
(1) get that petroleum sodium sulfonate is 4kg, polypropylene glycol diglycidyl ether is 2kg, dioctadecyl dimethyl ammonium chloride is 3kg, undertaken mixing and stirring by after three kinds of compositions heating, mix rear for subsequent use; (2) water intaking is for 230kg, then adds that alanine is 3kg, amylalcohol is 8kg, potassium phosphate is 2kg, sodium sulphate is 2kg, alanine, amylalcohol, potassium sulfate, sodium sulphate water is uniformly dissolved; (3) added in the aqueous solution in step (2) by the mixed liquor prepared in step (1), stir with mechanical agitation oar, speed of agitator is 200rpm, stirs; (4) finally finishing agent is loaded in hermetically sealed can, preserve.
Embodiment 2
(1) get that petroleum sodium sulfonate is 6kg, polypropylene glycol diglycidyl ether is 1kg, dioctadecyl dimethyl ammonium chloride is 2kg, undertaken mixing and stirring by after three kinds of compositions heating, mix rear for subsequent use; (2) water intaking is for 235kg, then adds that alanine is 5kg, amylalcohol is 7kg, potassium phosphate is 3kg, sodium sulphate is 1kg, alanine, amylalcohol, potassium sulfate, sodium sulphate water is uniformly dissolved; (3) added in the aqueous solution in step (2) by the mixed liquor prepared in step (1), stir with mechanical agitation oar, speed of agitator is 250rpm, stirs; (4) finally finishing agent is loaded in hermetically sealed can, preserve.
Embodiment 3
(1) get that petroleum sodium sulfonate is 5kg, polypropylene glycol diglycidyl ether is 2kg, dioctadecyl dimethyl ammonium chloride is 2kg, undertaken mixing and stirring by after three kinds of compositions heating, mix rear for subsequent use; (2) water intaking is for 240kg, then adds that alanine is 4kg, amylalcohol is 8kg, potassium phosphate is 2kg, sodium sulphate is 1kg, alanine, amylalcohol, potassium sulfate, sodium sulphate water is uniformly dissolved; (3) added in the aqueous solution in step (2) by the mixed liquor prepared in step (1), stir with mechanical agitation oar, speed of agitator is 230rpm, stirs; (4) finally finishing agent is loaded in hermetically sealed can, preserve.
By textile clothes, dry after soaking 50min under the finishing agent room temperature by embodiment 1, embodiment 2, embodiment 3.Dry rear washing machine and clean 20 times.Measure the shrinkage factor before and after cotton clothes arrangement and ANTIPILLING grade, pilling grade bioassay standard is GB/T4802.2-1997.Test result is as following table.
Reference examples Embodiment 1 Embodiment 2 Embodiment 3
Shrinkage factor 13% 0.2% 0.4% 0.5%
ANTIPILLING grade 1 grade 5 grades 4 grades 5 grades
Cotton clothes, after finishing agent arranges, has possessed the performance of excellent resisted shrinkage and ANTIPILLING.

Claims (2)

1. a finishing agent for resisted shrinkage ANTIPILLING, is characterized in that the finishing agent of resisted shrinkage ANTIPILLING is made up of according to weight ratio following composition: petroleum sodium sulfonate is 4 ~ 6 parts, polypropylene glycol diglycidyl ether is 1 ~ 2 part, alanine is 3 ~ 5 parts, dioctadecyl dimethyl ammonium chloride is 2 ~ 3 parts, amylalcohol is 7 ~ 8 parts, potassium phosphate is 2 ~ 3 parts, sodium sulphate is 1 ~ 2 part, water is 230 ~ 240 parts.
2. the preparation method of the finishing agent of a kind of resisted shrinkage ANTIPILLING according to claim 1, it is characterized in that preparation method comprises the following steps: (1) gets that petroleum sodium sulfonate is 4 ~ 6 parts, polypropylene glycol diglycidyl ether is 1 ~ 2 part, dioctadecyl dimethyl ammonium chloride is 2 ~ 3 parts, undertaken mixing and stirring by after three kinds of composition heating, mix rear for subsequent use; (2) water intaking is 230 ~ 240 parts, then adds that alanine is 3 ~ 5 parts, amylalcohol is 7 ~ 8 parts, potassium phosphate is 2 ~ 3 parts, sodium sulphate is 1 ~ 2 part, alanine, amylalcohol, potassium phosphate, sodium sulphate water is uniformly dissolved; (3) added in the aqueous solution in step (2) by the mixed liquor prepared in step (1), stir with mechanical agitation oar, speed of agitator is 200 ~ 250rpm, stirs; (4) finally finishing agent is loaded in hermetically sealed can, preserve.
3. the preparation method of the finishing agent of a kind of resisted shrinkage ANTIPILLING according to claim 2, is characterized in that the polypropylene glycol diglycidyl ether added is 2 parts.
4. the preparation method of the finishing agent of a kind of resisted shrinkage ANTIPILLING according to claim 2, is characterized in that adding alanine is 3 parts.
5. the preparation method of the finishing agent of a kind of resisted shrinkage ANTIPILLING according to claim 2, is characterized in that speed of agitator is 250rpm.
CN201310750885.2A 2013-12-31 2013-12-31 Finishing agent of a kind of resisted shrinkage ANTIPILLING and preparation method thereof Active CN103757889B (en)

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Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105220496A (en) * 2015-09-29 2016-01-06 江苏金太阳纺织科技有限公司 A kind ofly improve the composition of all-cotton fabric anti-fuzz balls performance and anti-fuzz balls finishing technique
CN105484030B (en) * 2015-12-29 2017-09-29 绍兴海神印染制衣有限公司 A kind of aftertreatment technology of all-cotton fabric
CN106319952A (en) * 2016-08-19 2017-01-11 常熟市鑫博伟针纺织有限公司 After-finishing process of brushed fabric
CN106958144A (en) * 2017-05-24 2017-07-18 东台市联翔纺织有限公司 It is a kind of to prevent the textile material of balling-up
CN107893329A (en) * 2017-11-30 2018-04-10 苏州绣艳天下刺绣工艺有限公司 A kind of preparation method embroidered with anti-shrink finishing agent

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CN1172053C (en) * 2001-02-09 2004-10-20 广东溢达纺织有限公司 Technology for knitting washing-resistant cotton fabric without ironing
CN100519921C (en) * 2005-03-08 2009-07-29 张家港市国泰华荣化工新材料有限公司 Synthesis method for anti-napping and anti-pilling conditioning agent for fabric
CN1306106C (en) * 2005-03-29 2007-03-21 东华大学 Method for fabricating wool keratin clad acrylon, polypropylene, capron and textiles
CN101302276B (en) * 2008-06-16 2012-10-03 宁波润禾化学工业有限公司 Preparation technology of soft highly-elastic fabric anti-fluffing anti-pilling finishing agent
CN102154828B (en) * 2011-03-22 2014-08-27 互太(番禺)纺织印染有限公司 Fluff resistant and pilling resistant cotton and elastic cotton knitted fabric and production method thereof

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Inventor after: Zhang Dexuan

Inventor after: Zuo Donghua

Inventor before: Zhang Dexuan

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Effective date of registration: 20191223

Address after: 215200 Da Xie village, Shengze Town, Wujiang District, Suzhou, Jiangsu

Patentee after: Wujiang Dingneng textile finishing Co., Ltd

Address before: 7 groups of friendship village Songling town of Wujiang District of Suzhou City, Jiangsu province 215200 split eight community

Patentee before: SUZHOU XUANDE TEXTILE SCIENCE & TECHNOLOGY CO., LTD.