CN103741478B - A kind of resisted shrinkage curtain dressing liquid and preparation method thereof - Google Patents
A kind of resisted shrinkage curtain dressing liquid and preparation method thereof Download PDFInfo
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- CN103741478B CN103741478B CN201310687560.4A CN201310687560A CN103741478B CN 103741478 B CN103741478 B CN 103741478B CN 201310687560 A CN201310687560 A CN 201310687560A CN 103741478 B CN103741478 B CN 103741478B
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- resisted shrinkage
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- 239000007788 liquid Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 238000003756 stirring Methods 0.000 claims abstract description 21
- -1 poly(tributoxy titanium) Polymers 0.000 claims abstract description 19
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 claims abstract description 9
- OOCMUZJPDXYRFD-UHFFFAOYSA-L calcium;2-dodecylbenzenesulfonate Chemical compound [Ca+2].CCCCCCCCCCCCC1=CC=CC=C1S([O-])(=O)=O.CCCCCCCCCCCCC1=CC=CC=C1S([O-])(=O)=O OOCMUZJPDXYRFD-UHFFFAOYSA-L 0.000 claims abstract description 8
- 239000012153 distilled water Substances 0.000 claims abstract description 8
- 229920001230 polyarylate Polymers 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229920000742 Cotton Polymers 0.000 claims description 15
- 238000002156 mixing Methods 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 3
- 238000010028 chemical finishing Methods 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 102000000429 Factor XII Human genes 0.000 description 1
- 108010080865 Factor XII Proteins 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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Abstract
A kind of resisted shrinkage curtain dressing liquid and preparation method thereof, resisted shrinkage curtain dressing liquid consisting of according to weight ratio: polyarylate is 3 ~ 5 parts, butyl acrylate is 2 ~ 4 parts, poly(tributoxy titanium) is 2 ~ 3 parts, silester is 5 ~ 8 parts, calcium dodecyl benzene sulfonate is 6 ~ 9 parts, distilled water is 145 ~ 165 parts.The curtain dressing liquid preparation of resisted shrinkage comprises the steps such as mixing, heating, stirring, and the curtain dressing liquid prepared has the excellent function preventing curtain from shrinking.
Description
Technical field
The present invention relates to a kind of dressing liquid and preparation method thereof, particularly relate to a kind of resisted shrinkage curtain dressing liquid and preparation method thereof.
Background technology
The material of curtain is more, has the material such as cotton, silk, fiber, blending.Wherein cotton curtain has certain shrink phenomenon after cleaning.This have impact on the attractive in appearance of curtain greatly.By arranging curtain, giving the resisted shrinkage ability that curtain is certain, the shrinkage factor of curtain may be reduced, extend the service time of curtain.Common finishing agent is generally the mixture of resin and some other chemical composition, after curtain is arranged with common chemical finishing agent, the resisted shrinkage ability of curtain improves and not obvious, needs the one-tenth changing conventional chemical finishing agent to be grouped into, to improve the performance of finishing agent.
Summary of the invention
The technical problem solved: cotton curtain repeatedly cleans the higher problem of post-shrinkage ratio.
Technical scheme: the invention discloses a kind of resisted shrinkage curtain dressing liquid and preparation method thereof, resisted shrinkage curtain dressing liquid consisting of according to weight ratio: polyarylate is 3 ~ 5 parts, butyl acrylate is 2 ~ 4 parts, poly(tributoxy titanium) is 2 ~ 3 parts, silester is 5 ~ 8 parts, calcium dodecyl benzene sulfonate is 6 ~ 9 parts, distilled water is 145 ~ 165 parts.
A preparation method for resisted shrinkage curtain dressing liquid, preparation method comprises the following steps: (1) gets distilled water is 145 ~ 165 parts, is transferred in reactor, capping still after being heated to 50 DEG C ~ 55 DEG C; (2) open reactor, in reactor, add that silester is 5 ~ 8 parts, calcium dodecyl benzene sulfonate is 6 ~ 9 parts, carry out closing with dasher and stir, stir; (3) temperature of reaction kettle is risen to 80 DEG C, then open reactor, add that polyarylate is 3 ~ 5 parts, butyl acrylate is 2 ~ 4 parts, poly(tributoxy titanium) is 2 ~ 3 parts wherein again, reuse dasher and carry out closing and stir, stir; (4) after dressing liquid being incubated 2h ~ 3h at 80 DEG C, naturally cool to room temperature, be prepared into curtain dressing liquid.
By dressing liquid is incubated 2h ~ 3h at 80 DEG C, mutual dissolving and the reaction of composition wherein can be promoted, and then improve the resisted shrinkage performance of curtain when arranging.
Beneficial effect: common cotton curtain is after cleaning 10 times, and shrinkage factor is 12%, the curtain after dressing liquid of the present invention arranges, after it cleans 10 times, shrinkage factor only has 1.7% to 2.1%.
Detailed description of the invention
Embodiment 1
(1) getting distilled water is 145kg, is transferred in reactor after being heated to 55 DEG C, capping still; (2) open reactor, in reactor, add that silester is 8kg, calcium dodecyl benzene sulfonate is 9kg, carry out closing with dasher and stir, stir; (3) temperature of reaction kettle is risen to 80 DEG C, then open reactor, add that polyarylate is 3kg, butyl acrylate is 4kg, poly(tributoxy titanium) is 3kg wherein again, reuse dasher and carry out closing and stir, stir; (4) after dressing liquid being incubated 3h at 80 DEG C, naturally cool to room temperature, be prepared into curtain dressing liquid.
Embodiment 2
(1) getting distilled water is 155kg, is transferred in reactor after being heated to 50 DEG C, capping still; (2) open reactor, in reactor, add that silester is 5kg, calcium dodecyl benzene sulfonate is 6kg, carry out closing with dasher and stir, stir; (3) temperature of reaction kettle is risen to 80 DEG C, then open reactor, add that polyarylate is 5kg, butyl acrylate is 3kg, poly(tributoxy titanium) is 2kg wherein again, reuse dasher and carry out closing and stir, stir; (4) after dressing liquid being incubated 2h at 80 DEG C, naturally cool to room temperature, be prepared into curtain dressing liquid.
Embodiment 3
(1) getting distilled water is 165kg, is transferred in reactor after being heated to 55 DEG C, capping still; (2) open reactor, in reactor, add that silester is 7kg, calcium dodecyl benzene sulfonate is 7kg, carry out closing with dasher and stir, stir; (3) temperature of reaction kettle is risen to 80 DEG C, then open reactor, add that polyarylate is 4kg, butyl acrylate is 2kg, poly(tributoxy titanium) is 3kg wherein again, reuse dasher and carry out closing and stir, stir; (4) after dressing liquid being incubated 2h at 80 DEG C, naturally cool to room temperature, be prepared into curtain dressing liquid.
Get identical pure cotton curtain two pieces, get wherein one piece immerse and soak 2h in the curtain dressing liquid of embodiment 1, embodiment 2, embodiment 3 after, preliminary drying 40min at 80 DEG C, more thoroughly dry at 105 DEG C.After untrimmed cotton curtain and treated cotton curtain routine are cleaned 10 times, measure their shrinkage factor, result is as follows.
| Reference examples | Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Shrinkage factor | 12% | 1.9% | 2.1% | 1.7% |
Cotton curtain after dressing liquid arranges, its repeatedly clean after shrinkage factor significantly reduce, effectively avoid curtain and repeatedly clean the too much problem of after-contraction and occur, improve utilization rate and the service time of curtain.
Claims (5)
1. a resisted shrinkage cotton curtain dressing liquid, is characterized in that resisted shrinkage cotton curtain dressing liquid consisting of according to weight ratio: polyarylate is 3 ~ 5 parts, butyl acrylate is 2 ~ 4 parts, poly(tributoxy titanium) is 2 ~ 3 parts, silester is 5 ~ 8 parts, calcium dodecyl benzene sulfonate is 6 ~ 9 parts, distilled water is 145 ~ 165 parts.
2. the preparation method of a kind of resisted shrinkage cotton curtain dressing liquid according to claim 1, is characterized in that preparation method comprises the following steps: (1) gets distilled water is 145 ~ 165 parts, is transferred in reactor, capping still after being heated to 50 DEG C ~ 55 DEG C; (2) open reactor, in reactor, add that silester is 5 ~ 8 parts, calcium dodecyl benzene sulfonate is 6 ~ 9 parts, carry out closing with dasher and stir, stir; (3) temperature of reaction kettle is risen to 80 DEG C, then open reactor, add that polyarylate is 3 ~ 5 parts, butyl acrylate is 2 ~ 4 parts, poly(tributoxy titanium) is 2 ~ 3 parts wherein again, reuse dasher and carry out closing and stir, stir; (4) after dressing liquid being incubated 2h ~ 3h at 80 DEG C, naturally cool to room temperature, be prepared into cotton curtain dressing liquid.
3. the preparation method of a kind of resisted shrinkage cotton curtain dressing liquid according to claim 2, is characterized in that the silester added is 8 parts.
4. the preparation method of a kind of resisted shrinkage cotton curtain dressing liquid according to claim 2, is characterized in that the poly(tributoxy titanium) added is 3 parts.
5. the preparation method of a kind of resisted shrinkage cotton curtain dressing liquid according to claim 2, is characterized in that the butyl acrylate added is 2 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310687560.4A CN103741478B (en) | 2013-12-17 | 2013-12-17 | A kind of resisted shrinkage curtain dressing liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310687560.4A CN103741478B (en) | 2013-12-17 | 2013-12-17 | A kind of resisted shrinkage curtain dressing liquid and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103741478A CN103741478A (en) | 2014-04-23 |
| CN103741478B true CN103741478B (en) | 2015-09-23 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310687560.4A Active CN103741478B (en) | 2013-12-17 | 2013-12-17 | A kind of resisted shrinkage curtain dressing liquid and preparation method thereof |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105401411A (en) * | 2015-12-25 | 2016-03-16 | 常熟市格林染整有限公司 | Velvet fabric dyeing and finishing technology |
| CN107893329A (en) * | 2017-11-30 | 2018-04-10 | 苏州绣艳天下刺绣工艺有限公司 | A kind of preparation method embroidered with anti-shrink finishing agent |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1070238A (en) * | 1991-07-18 | 1993-03-24 | 日本纯药株式会社 | The agent composition that is used for leather, fur and fibrous material |
| CN1751153A (en) * | 2003-02-19 | 2006-03-22 | 罗狄亚化学公司 | Use of a cross-linkable liquid silicon formulation as a textile coating base |
| CN101302276A (en) * | 2008-06-16 | 2008-11-12 | 宁波润禾化学工业有限公司 | Preparation technology of soft highly-elastic fabric anti-fluffing anti-pilling finishing agent |
-
2013
- 2013-12-17 CN CN201310687560.4A patent/CN103741478B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1070238A (en) * | 1991-07-18 | 1993-03-24 | 日本纯药株式会社 | The agent composition that is used for leather, fur and fibrous material |
| CN1751153A (en) * | 2003-02-19 | 2006-03-22 | 罗狄亚化学公司 | Use of a cross-linkable liquid silicon formulation as a textile coating base |
| CN101302276A (en) * | 2008-06-16 | 2008-11-12 | 宁波润禾化学工业有限公司 | Preparation technology of soft highly-elastic fabric anti-fluffing anti-pilling finishing agent |
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| CN103741478A (en) | 2014-04-23 |
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Owner name: GU XIANGMAO Free format text: FORMER OWNER: GOLDSUN HOLDING GROUP CO., LTD. Effective date: 20150828 |
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Effective date of registration: 20150828 Address after: 266000 Licang, Qingdao, No. nine East water road, No. 320, No. Applicant after: Gu Xiangmao Address before: 226300 Jiangsu city of Nantong province Tongzhou District Industrial Park building sun Zhihao Applicant before: Goldsun Holding Group Co., Ltd. |
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Address after: 225327 Jiangsu city of Taizhou province Yongan high port Zhou Zhen rain Road No. 26 Patentee after: Gu Xiangmao Address before: 266000 Licang, Qingdao, No. nine East water road, No. 320, No. Patentee before: Gu Xiangmao |
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Address after: Tian Zhen Qing Guan Lu Pingdu City 266700 Shandong city of Qingdao province No. 11 Patentee after: Gu Xiangmao Address before: 225327 Jiangsu city of Taizhou province Yongan high port Zhou Zhen rain Road No. 26 Patentee before: Gu Xiangmao |
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Address after: 210000 Longshi Center, No. 2 Guangzhou Road (221 Central Road), Gulou District, Nanjing City, Jiangsu Province Patentee after: Gu Xiangmao Address before: 266700 11 Tsing Guan Road, Tian Zhuang Town, Pingdu City, Qingdao, Shandong Patentee before: Gu Xiangmao |
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Effective date of registration: 20191012 Address after: 314000 Fengming Street Industrial Park, Tongxiang City, Jiaxing City, Zhejiang Province Patentee after: Zhejiang Jiaming dyeing and finishing Co., Ltd. Address before: 210000 Longshi center, No. 2, Guangzhou road, Gulou District, Nanjing City, Jiangsu Province Patentee before: Gu Xiang Mao |